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INDUSTRIAL
STANDARD
Translated and Published by
Japanese Standards Association
JIS G 0321
:2010
(JISF)
ICS 77.040.01;77.140.01
Reference number: JIS G 0321 : 2010 (E)
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7S
G 0321 : 2010
JSA 2011
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G 0321 : 2010
Contents
Scope ...................................................... 1
4
4.1
4.2
5
5.1
5.2
Analysis method 3
Chemical composition specified in each standard of wrought steel 3
Chemical composition not specified in each standard of wrought steel 3
(i)
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Page
G 0321 : 2010
Foreword
This translation has been made based on the original Japanese Industrial Standard
revised by the Minister of Economy, Trade and Industry, through deliberations at
the Japanese Industrial Standards Committee as the result of proposal of revision
of Japanese Industrial Standard submitted by The Japan Iron and Steel Federation
(JISF) with the draft being attached, based on the provision of Article 12 Clause 1
of the Industrial Standardization Law applicable to the case of revision by the provision
of Article 14.
Consequently JIS G 0321: 2005 has been replaced with this Standard.
This JIS document is protected by the Copyright Law.
(ii)
Copyright Japanese Standards Association
Provided by IHS under license with JSA
No reproduction or networking permitted without license from IHS
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Attention is drawn to the possibility that some parts of this Standard may conflict
with a patent right, application for a patent after opening to the public, utility model
right or application for registration of utility model after opening to the public which
have technical properties. The relevant Minister and the Japanese Industrial Standards
Committee are not responsible for identifying the patent right, application for a patent
after opening to the public, utility model right or application for registration of utility
model after opening to the public which have the said technical properties.
1 Scope
This Japanese Industrial Standard specifies the product analysis and its tolerance
for the killed steel products of rolled or forged carbon steel, alloy steel, stainless steel
and heat resisting steel (hereafter referred to as "wrought steel").
In addition, the application of this Standard shall be as stated in the individual product standards.
2
Norma ti ve references
The standards listed in table 1 contain provisions which, through reference in this
text, constitute provisions of this Standard. The most recent editions of the standards
(including amendments) indicated in the table shall be applied.
For the purpose of this Standard, the terms and definitions given in JIS G 0417
and JIS G 1201, and the following apply:
3.1
heat analysis
This analysis is generally carried out on analytical samples 1) taken during a series
of procedures in which the molten steel is poured into a mould from a ladle and then
solidified.
Note
3.2
1)
Where it is not feasible to obtain the analytical sample from the molten
steel, such as in vacuum arc remelting method (VAR), electro-slag remelting method (ESR), or other method, the analysis is carried out on analytical samples taken from steel ingot, steel slab, or steel material, and
the results are applied to the heat analysis.
product analysis
3.3
permissible deviation of the individual value of product analysis from the upper limit
value and/or the lower limit value of the heat analysis specified in a standard of wrought
steels
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G 0321: 2010
NOTE:
For example, when the upper limit value of heat analysis of carbon (C)
specified in a standard of wrought steel is 0.25 %, and the tolerance for
product analysis on the plus side designated in a standard of wrought
steel in accordance with this Standard is +0.03 %, the permissible upper
limit value of product analysis is 0.28 %.
b)
An analytical method prepared by altering a part 2) of the procedures of the relevant JIS standard method so as to have a broader range of application, and which
satisfies the critical limit from a certified value, repeatability limit and within laboratory reproducibility limit specified in 7.2 or 7.3 of JIS G 1201.
Note
2)
3.5
sample product
product sampled from the test unit for inspection and/or test
4.1
a)
The analytical sample for product analysis shall be taken from a position representing the average chemical composition of the cross-section of the original steel
billet.
If the method of sampling is not specified in the product standard or in the requirements given in the order of the product, the analytical sample may be directly
taken from the specimens or test pieces for the mechanical test, or a sample product.
b)
The analytical sample shall be free from scales, rust, paint, plating metal, decarburized layer and impurities. Further, the analytical sample shall not be used if
oxidized, rusted or soiled during storage.
When the sample is taken from chips produced in machining, the sampling procedure shall be in accordance with 4.4 of JIS G 0417.
c)
When the analytical sample is to be taken directly from a sample product, the
procedure in clause 10 of JIS G 0417 shall be applied. However, if this is impracticable, analytical samples shall be taken by a suitable method referring to 4.1 a)
and 4.1 b). In this case, the sampling method shall be subjected to the agreement
between the purchaser and the manufacturer.
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G 0321: 2010
d)
When the analytical samples for the emission spectrometric analysis and fluorescent X-ray analysis of the product analysis are to be directly taken from a sample
product, the samples which comply with JIS G 1253 and JIS G 1256 shall be taken
in accordance with clause 10 of JIS G 0417. However, when the sample for instrumental analysis can not be taken in accordance with 4.1 a), the analysis shall
not be carried out.
4.2
5 Analysis method
Chemical composition specified in each standard of wrought steel
Analysis method shall be as follows. In the case of doubt arising as to the analytical value obtained by the instrumental analysis, a re-analysis may be performed by a
chemical analysis method.
5.1
JIS
JIS
JIS
JIS
JIS
JIS
JIS
G
G
G
G
G
G
G
1211, JIS G 1212, JIS G 1213, JIS G 1214, JIS G 1215-1, JIS G 1215-2,
1215-3, JIS G 1215-4, JIS G 1216, JIS G 1217, JIS G 1218, JIS G 1219,
1220, JIS G 1221, JIS G 1222, JIS G 1223, JIS G 1224, JIS G 1225,
1226, JIS G 1227, JIS G 1228, JIS G 1229, JIS G 1232, JIS G 1233,
1234, JIS G 1235, JIS G 1236, JIS G 1237, JIS G 1253, JIS G 1256,
1257, JIS G 1258-1, JIS G 1258-2, JIS G 1258-3, JIS G 1258-4,
1258-5, JIS G 1258-6, JIS G 1258-7, JIS G 1281
5.2
b)
The values obtained from the product analysis shall not exceed the prescribed
maximum value of chemical composition plus the upper limit value given in tables
2 to 5 or be lower than the prescribed minimum value minus the lower limit value
given in the said tables. However, the tolerance shall be obtained from the table
of tolerance based on the specified maximum value of chemical composition. If only
the minimum value is specified, the tolerance shall be obtained from the table of
tolerance based on the minimum value of the chemical composition.
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G 0321: 2010
c)
For the tolerance of one kind of wrought steel, all or a part of the tolerances in
one table shall be applied, and tolerances in 2 or more tables shall not be used in
mixture.
When the result of analysis does not conform to this Standard, a re-sampling and
re-analysis may be performed upon agreement between the purchaser and the manufacturer.
Normative references
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Table 1
5
G 0321: 2010
Table 1
JIS G 1256 Iron and steel-Method for X-ray
fluorescence spectrometric analysis
JIS G 1257 Iron and steel-Methods for
atomic absorption spectrometric analysis
JIS G 1258-1 Iron and steel-ICP atomic
emission spectrometric method-Part 1:
Determination of silicon, manganese,
phosphorus, nickel, chromium, molybdenum, copper, vanadium, cobalt, titanium
and aluminium contents-Dissolution in
acids and fusion with potassium disulfate
JIS G 1258-2 Iron and steel-ICP atomic
emission spectrometric method-Part 2:
Determination of manganese, nickel, chromium, molybdenum, copper, tungsten, vanadium, cobalt, titanium and niobium
contents-Dissolution in phosphoric and
sulfuric acids
JIS G 1258-3 Iron and steel-ICP atomic
emission spectrometric method-Part 3:
Determination of silicon, manganese,
phosphorus, nickel, chromium, molybdenum, copper, vanadium, cobalt, titanium
and aluminium contents-Dissolution in
acids and fusion with sodium carbonate
Table 2
(concl uded)
JIS G 1258-4 Iron and steel-ICP atomic
emission spectrometric method-Part 4:
Determination of niobium content-Dissolution in phosphoric and sulfuric acids or
dissolution in acids and fusion with potassium disulfate
JIS G 1258-5 Iron and steel-ICP atomic
emission spectrometric method-Part 5:
Determination of boron content-Dissolution in phosphoric and sulfuric acids
JIS G 1258-6 Iron and steel-ICP atomic
emission spectrometric method-Part 6:
Determination of boron content-Dissolution in acids and fusion with sodium carbonate
JIS G 1258-7 Iron and steel-ICP atomic
emission spectrometric method-Part 7:
Determination of boron content-Distillation as trimethyl borate
JIS G 1281 Methods for chemical analysis of
nickel-chromium-iron alloys
Elements
Si
Mn
Tolerance
Lower limit
Upper limit
0.15 or under
0.02
0.03
0.03
0.04
0.03
0.05
Over 0.80
0.03
0.06
0.30 or under
0.02
0.03
0.05
0.05
0.60 or under
0.03
0.03
0.04
0.04
0.05
0.05
0.060 or under
0.010
0.060 or under
0.010
0.02
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Cu
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G 0321: 2010
Table 3
Elements
Over
65000 mm 2
up to and incl.
130000 mm2
Over
130000 mm 2
up to and incl.
260000 mm 2
Over
260000 mm 2
up to and incl.
520000 mm 2
Si
Mn
0.25 or under
0.02
0.02
0.03
0.03
0.04
0.04
0.05
0.05
0.03
0.03
0.04
0.04
0.05
0.05
0.06
0.06
Over 0.55
0.04
0.04
0.05
0.05
0.06
0.06
0.07
0.07
0.35 or under
0.02
0.02
0.02
0.02
0.03
0.03
0.04
0.04
0.05
0.05
0.90 or under
0.03
0.03
0.04
0.04
0.06
0.06
0.07
0.07
0.06
0.06
0.06
0.06
0.07
0.07
0.08
0.08
0.050 or under
0.008
0.010
0.010
0.015
0.060 or under
0.008
0.010
0.010
0.015
0.03
Cu
0.02
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Table 4
Elements
Over
65000 mm 2
up to and incl.
130000 mm 2
Over
130000 mm2
up to and incl.
260000 mm2
Over
260000 mm 2
up to and incl.
520000 mm 2
Si
Mn
0.30 or under
0.01
0.01
0.02
0.02
0.03
0.03
0.04
0.04
0.02
0.02
0.03
0.03
0.04
0.04
0.05
0.05
Over 0.75
0.03
0.03
0.04
0.04
0.05
0.05
0.06
0.06
0.35 or under
0.02
0.02
0.02
0.02
0.03
0.03
0.04
0.04
0.05
0.05
0.06
0.06
0.06
0.06
0.07
0.07
0.90 or under
0.03
0.03
0.04
0.04
0.05
0.05
0.06
0.06
0.04
0.04
0.05
0.05
0.06
0.06
0.07
0.07
0.050 or under
0.005
0.010
0.010
0.010
0.060 or under
0.005
0.010
0.010
0.010
Cu
1.00 or under
0.03
0.03
0.05
0.05
1.00 or under
0.03
0.03
0.03
0.03
0.03
0.03
0.03
0.03
Ni
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Cr
Mo
Al
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.07
0.07
0.07
0.07
0.07
0.07
0.07
0.07
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.90 or under
0.03
0.03
0.04
0.04
0.04
0.04
0.05
0.05
0.05
0.05
0.06
0.06
0.06
0.06
0.07
0.07
0.10
0.10
0.10
0.10
0.12
0.12
0.14
0.14
0.20 or under
0.01
0.01
0.01
0.01
0.02
0.02
0.03
0.03
0.02
0.02
0.03
0.03
0.03
0.03
0.04
0.04
0.03
0.03
0.04
0.04
0.05
0.05
0.06
0.06
0.10 or under
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.02
0.02
0.02
0.02
0.02
0.02
0.02
0.02
0.03
0.03
0.03
0.03
0.03
0.03
0.03
0.03
0.01
0.01
0.01
0.01
1.00 or under
0.04
0.04
0.05
0.05
0.05
0.05
0.06
0.06
0.08
0.08
0.09
0.09
0.10
0.10
0.12
0.12
1.50 or under
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
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G 0321: 2010
Table 5
0.01
Upper limit
0.005
0.01
0.02
0.02
0.03
0.03
0.05
0.10
0.10
1.00 or under
Over 1.00 up to and incl. 4.50
Mn
Lower limit
-
Si
Tolerance
1.00 or under
0.04
0.03
0.04
0.040 or under
0.005
0.040 or under
0.005
Ni
Cr
Mo
Cu
1.00 or under
0.03
0.07
0.07
0.10
0.10
0.15
0.15
0.20
0.20
0.25
0.25
0.30
0.30
0.10
0.10
0.15
0.15
0.20
0.20
0.25
0.25
0.03
0.03
0.05
0.05
0.10
0.10
0.50 or under
0.03
0.05
0.05
0.10
0.10
0.10
0.10
Ti
0.05
Nb+Ta
0.05
Al
0.05
0.05
0.02
0.02
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