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ADIGRAT UNIVERSITY
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DANAYT MESELE
HAILEMARIAM ASEGEDOM
KINFE GIRMAY
MELES HAGOS
SEID ARAGAW
SELAMAWIT LEMMA
TEKESTE MULAW
TEKLAY GODEFAY
TEMESGEN ABREHALEY
TEMESGEN TEKLU
TESFAMARIAM HADUSH
TESFAYE BAYILE
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RET 0364 /06
RET 0748/06
RET 0934/06
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RET 1293/06
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RET 1477/06
RET 1499/06
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EXPERIMENT No #3
NETWORK 7&8
NETWORK 7&8
3. OBJECTIVES
3.1 General Objectives
To separate Potassium hydrogen carbonate (KHCO3) using distilled water was extracted
from aluminum oxide (Al2O3) or Potassium hydrogen carbonate solid mixture using solid
liquid extraction.
4. THEORY
Solid-liquid extraction (Leaching) is the dissolving of one or more constituents of a solid mixture
by contact with liquid solvent.
Solid-Liquid extraction (Leaching) is the preferential solution of one or more constituents of a
solid mixture by contact with a liquid solvent. This unit operation, one of the oldest in the
chemical industries, has been given many names, depending to some extent upon the technique
used for carrying it out. Leaching originally referred to percolation of the liquid through a fixed
bed of the solid, but is now used to describe the operation generally, by whatever means it may
be done.
NETWORK 7&8
Page 1
Selectivity
Solubility
Chemical reaction properties
Boiling properties
Electronic balance
Beaker
Dropper/Bottle for water
Container/bowel
Chemicals
Aluminum oxide (Al2O3)
Potassium hydrogen carbonates (KHCO3)
Distilled water
7. PROCEDURE
First, some gram weight of aluminum oxide (Al2O3) was weighed. Secondly, some gram of
potassium hydrogen carbonate (KHCO3) was weighed. After weighed these two compounds
were mixed in the material feeder. Thirdly, the mixtures were mixed with some liter of distilled
water or some liter of distilled water was added to the mixtures. Fourthly, left the solution for
around 24 hour. After 24 hours thermal heat was given to the solutions and the result were
recorded for respectively two minute differences with constant temperature or varying
temperature (T1,T2) and Constant flow rates or varying flow rate (C 1, C2). Finally, the excess
residual solution was shaken off. The aluminum oxide (Al2O3)/Potassium hydrogen carbonate
solid mixture (Extract material) prepared can be dried in the ambient air (for example on backing
tray) or in an oven if required.
RESULT AND DISCUSSION
NETWORK 7&8
Page 2
Solid mixture
Al2O3 + KHCO3
Extract
Recommendation
LAB REPORT ON SOLID- LIQUID EXTRACTION
NETWORK 7&8
Page 3
solid.
NETWORK 7&8
Page 4