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NDT2A/2B
Radiographic Interpretation
Preparation Course Radiographic Theory
NDT2A/2B
Contents
Section Subject
Preliminary pages
Standards and Associated Reading
COSHH, H&S, Cautions and Warnings
Introduction to NDT Methods
Certification Schemes
4 Ionising Radiation
5 X-rays or Bremsstrahlung
5.1 X-ray equipment
6 Gamma Rays
6.1 Alpha and beta emission
6.2 Sealed sources
6.3 Penetrating power of gamma radiation
6.4 Quantity of gamma radiation
6.5 Radioactive isotope containers for industrial radiography
6.6 Comparison of X- and gamma rays
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9 Sensitivity
9.1 Radiographic sensitivity
9.2 Controlling radiographic quality
9.3 BS EN 462-1 wire type IQIs
9.4 Other wire type IQIs
9.5 BS EN 462-2 step-hole type IQIs
9.6 ASTM E 1025 plaque type penetrameters
9.7 IQI sensitivity
11 Interpretation of Radiographs
11.1 Introduction
11.2 Viewing conditions
11.3 Reporting
11.4 Film quality
11.5 Interpretation of radiographic images
11.6 Artefacts
11.7 Interpretation of weld radiographs
11.8 Interpretation of casting radiographs
12 Localisation
12.1 90 method
12.2 Tube (source) shift method
12.3 Tube (source) shift method with lead markers
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15 Radiation Safety
15.1 Precautions
15.2 Exposure limits for radiation workers
15.3 Permitted levels
15.4 Safe working distances
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Prelims
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Associated Reading
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COSHH, H&S, Caution and Warnings Relevant to TWI Training & Examination
Services
Introduction
The use of chemicals in NDT is regulated by law under the Control of Substances
Hazardous to Health (COSHH) Regulations 2005. These regulations require the
School to assess and control the risk of health damage from every kind of substance
used in training. Students are also required by the law to co-operate with the
Schools risk management efforts and to comply with the control measures adopted.
What is exposure?
Exposure to a substance is uptake into the body. The exposure routes are by:
Many thousands of substances are used at work but only about 500 substances
have Workplace Exposure Limits (WELs). Until 2005 it had been normal for HSE to
publish a new edition of EH40, or at least an amendment, each year. However with
increasing use of the website facilities the HSE no longer always publishes a revised
hardcopy edition, or amendment.
The web based list which became applicable from 1st October 2007 can now be
found at http://www.hse.gov.uk/coshh/table1.pdf
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Other advantages of NDT over destructive testing are that every item can be
examined with no adverse consequences, materials can be examined for conditions
internally and at the surface and most importantly parts can be examined whilst in
service making a good balance between cost effectiveness and quality control1.
NDT is used in almost every industry with the majority of applications coming from
the aerospace, power generation, automotive, rail, petrochemical and pipeline
markets, safety being the main priority of these industries. When properly applied,
NDT saves money, time, materials and lives. NDT as it is known today has been
developing since around the 1920s with the methods used today taking shape later
with vast technological advancements being made during the Second World War.
The five principal methods, other than visual inspection, are:
Penetrant testing
Magnetic particle inspection
Eddy current testing
Ultrasonic testing
Radiography
In all NDT methods interpretation of results is critical. Much depends on the skill and
experience of the technician, although properly formulated test techniques and
procedures will improve accuracy and consistency.
Further enhancements to video technology include pan, tilt and zoom lenses,
mounting cameras to platforms and wheels, all allowing more parts to be tested and
better images for improved inspection. Video devices also allow recording of
inspections to be taken meaning permanent records can be kept. This has a number
of advantages such as enabling other inspectors to observe the test as it was
performed and allowing further review and evaluation.
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Penetrant Testing
Penetrant testing locates surface-breaking discontinuities by covering the item with a
penetrating liquid, which is drawn into the discontinuity by capillary action. After
removal of excess penetrant the indication is made visible by application of a
developer. Colour contrast or fluorescent systems may be used.
Advantages Disadvantages
Applicable to non-ferromagnetics Only detects defects open to the surface
Able to test large parts with a portable kit Careful surface preparation required
Batch testing Not applicable to porous materials
Applicable to small parts with complex Temperature dependant
geometry
Simple, cheap, easy to interpret Cannot retest indefinitely
Sensitivity Compatibility of chemicals
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liquid penetrant. These dyes would then fluoresce when exposed to ultraviolet light
(sometimes referred to as black light) rendering indications from cracks and other
surface flaws more readily visible to inspectors. UV lights have become increasingly
portable with hand held UV torches now readily available.
Advantages Disadvantages
Will detect some sub-surface defects Ferromagnetic materials only
Rapid and simple to understand Requirement to test in two directions
Pre-cleaning not as critical as with dye penetrant Demagnetisation may be required
inspection (DPI)
Will work through thin coatings Odd shaped parts difficult to test
Cheap rugged equipment Not suited to batch testing
Direct test method Can damage the component under test
This form of NDT became much more common post First World War, in the 1920s,
when William Hoke discovered that flaws in magnetised materials created distortions
in the magnetic field. When a fine ferromagnetic powder was applied to the parts, it
was observed that they built up around the defects providing a visible indication.
Magnetic particle inspection superseded the oil and chalk method in the 1930s as it
proved far more sensitive to surface breaking flaws. Today it is still preferred to the
penetrant method on ferromagnetic material and much of the equipment being used
then, is very similar to today, with the only advances coming in the form of
fluorescent coating to increase the visibility of indications and more portable devices
being used. In the early days battery packs and direct current were the norm and it
was some years before alternating current proved acceptable.
Magnetism
The phenomenon called magnetism is said to have been discovered in the ancient
Greek city of Magnesia, where naturally occurring magnets were found to attract
iron.
The use of magnets in navigation goes back to Viking times or maybe earlier, where
it was found that rods of magnetised material, when freely suspended, would always
point in a north-south direction. The end of the rod which pointed towards the North
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Pole star became known as the North Pole and consequently the other end became
the South Pole.
Advantages Disadvantages
Sensitive to surface defects Very susceptible to permeability changes
Can detect through several layers Only on conductive materials
Can detect through surface coatings Will not detect defects parallel to surface
Accurate conductivity measurements Not suitable for large areas and/or complex
geometries
Can be automated Signal interpretation required
Little pre-cleaning required No permanent record (unless automated)
Portability
It was left to Dr. Friedrich Frster in the late 1940s to develop the modern day eddy
current testing equipment and formulate the theories which govern their use.
Since then, eddy current methods have developed into a wide range of uses and are
recognised as being the forerunner of NDT techniques today. From the mid 1980s
the microprocessor based eddy current testing instruments were developed which
had many advantages for inspectors. Modern electronics have made instruments
more user friendly, providing reduced noise levels which made certain test
applications very difficult, but also improving methods of signal presentation and
recording capabilities.
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Ultrasonic Testing
Ultrasonic testing measures the time for high frequency (0.5 50MHz) pulses of
ultrasound to travel through the inspection material. If a discontinuity is present, the
ultrasound will return to the probe in a time period other than would be expected of a
fault free specimen.
Advantages Disadvantages
Sensitive to cracks at various orientations No permanent record (unless automated)
Portability Not easily applied to complex geometries and
rough surfaces.
Safety Unsuited to coarse grained materials
Able to penetrate thick sections Reliant upon defect orientation
Measures depth and through-wall extent
The origin of modern ultrasonic testing (UT) is the discovery by the Curie brothers in
1880 that quartz crystals cut in a certain way produce an electric potential when
subjected to pressure - the piezo-electric effect, from the Greek piedzein, to press or
strike. In 1881 Lippman theorised that the effect might work in reverse, and that
quartz crystals might change shape if an electric current was applied to them. He
found this was so and experimented further. Crystals of quartz vibrate when
alternating currents are applied to them. Crystal microphones in a modern stereo rely
on this principle.
When the Titanic sank in 1912, the Admiralty tried to find a way of locating icebergs
by sending out sound waves and listening for an echo. They experimented further
with sound to detect submarines during the First World War. Between the wars,
marine echo sounding was developed and in the Second World War ASDIC (Anti-
Submarine Detection Investigation Committee) was extensively used in the Battle of
the Atlantic against the U-boats.
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in the Second World War to fit small airborne radar sets into aircraft. It made the UT
set as we know it possible. Around 1931 Mulhauser obtained a patent for a system
using two probes to detect flaws in solids and following this Firestone (1940) and
Simons (1945) developed pulsed UT using a pulse-echo technique.
In the years after the Second World War researchers in Japan began to experiment
on the use of ultrasound for medical diagnostic purposes. Working largely in isolation
until the 1950s, the Japanese developed techniques for the detection of gallstones,
breast masses, and tumours. Japan was also the first country to apply Doppler
ultrasound, an application of ultrasound that detects internal moving objects such as
blood coursing through the heart for cardiovascular investigation.
The first flaw detector was made by Sproule in 1942 while he was working for the
Scottish firm Kelvin & Hughes. Similar work was carried out by Firestone in the USA
and by German physicists. Sproule went on to develop the shear-wave probe.
Initially UT was limited to testing aircraft, but in the 1950s it was extensively used in
the building of power stations in Britain for examining thick steel components safely
and cheaply. UT was found to have several advantages over radiography in heavy
industrial applications:
It did not have health hazard associated with radiography, and a UT technician
could work next to welders and other employees without endangering them of
holding up work.
It was efficient in detecting toe cracks in boilers a major cause of explosions
and lack of fusion in boiler tubes.
It could find planar defects, like laminations, which were sometimes missed by
radiography.
A UT check on a thick component took no more time than a similar check on a
thin component as opposed to long exposure times in radiography.
Over the next 20 years, improvements focused on accurate detection and sizing of
the flaws with limited success, until 1977 when Silk first discovered an accurate
measurement and display of the top and bottom edges of a discontinuity with the
Time of Flight technique (TOFD). Advances in computing technology have now
expanded the use of TOFD as real time analyses of results are now available.
It was also during the 1970s that industries focused on reducing the size and weight
of Ultrasonic flaw detectors and making them more portable. This was achieved by
using semi-conductor technology and during the 1990s microchips were introduced
into the devices to allow calibration parameters and signal traces to be stored. LCD
display panels and digital technology have also contributed to reducing the size and
weight of Ultrasonic flaw detectors. With the development of Ultrasonic Phased Array
and increased computing power, the future for Ultrasonic inspection is very exciting.
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Radiography
Radiography monitors the varying transmission of ionising radiation through a
material with the aid of photographic film or fluorescent screens to detect changes in
density and thickness. It will locate internal and surface-breaking defects.
Advantages Disadvantages
Gives a permanent record, the radiograph Radiation health hazard
Detects internal flaws Can be sensitive to defect orientation and so can
miss planar flaws
Detects volumetric flaws readily Limited ability to detect fine cracks
Can be used on most materials Access is required to both sides of the object
Can check for correct assembly Skilled radiographic interpretation is required
Gives a direct image of flaws Relatively slow method of inspection
Fluoroscopy can give real time imaging High capital cost
High running cost
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One of the minerals Becquerel worked with was a uranium compound. On a day
when it was too cloudy to expose his samples to direct sunlight, Becquerel stored
some of the compound in a drawer with photographic plates. Later when he
developed these plates, he discovered that they were fogged (exhibited exposure to
light). Becquerel questioned what would have caused this fogging. He knew he had
wrapped the plates tightly before using them, so the fogging was not due to stray
light, in addition, he noticed that only the plates that were in the drawer with the
uranium compound were fogged. Becquerel concluded that the uranium compound
gave off a type of radiation that could penetrate heavy paper and expose
photographic film. Becquerel continued to test samples of uranium compounds and
determined that the source of radiation was the element uranium. Becquerel did not
pursue his discovery of radioactivity, but others did.
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Since these discoveries, many other radioactive elements have been discovered or
produced. Radiography in the form of NDT took shape in the early 1920s when Dr.
H.H. Lester began testing on different materials. Radium became the initial industrial
gamma ray source. The material allowed castings up to 10 to 12 inches thick to be
radiographed. During the Second World War industrial radiography grew
tremendously as part of the Navy's shipbuilding programme. In 1946, man-made
gamma ray sources such as cobalt and iridium became available. These new
sources were far stronger than radium and much less expensive. The man-made
sources rapidly replaced radium, and use of gamma rays grew quickly in industrial
radiography.
Direct Radiography systems (DR) are also used based upon CMOS (complimentary
metal oxide sensor) technology and TFT (thin film transistors). These systems have
the ability to directly convert light into digital format, additionally they may be coupled
with a scintillator which coats CMOS and CCD (charged couple device) sensors, the
scintillator converts photon energy to light before the sensor and ADC converts to
digital format. Systems which use scintillators in this way are often referred to as
indirect systems.
Quality issues of any digital system are based upon the effective pixel size and the
SNR (signal to noise ratio).The benefits of using Digital systems is the speed of
inspection, the absence of chemical processing requirements and wet film, however,
the initial equipment costs will be high.
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Section 1
Penetration
The ability to pass through solid objects such as metals, woods, plastics,
bone etc. In fact these materials actually absorb some or even all of the
radiation depending upon their thickness, density and atomic number.
Rectilinear Propagation
This simply means that radiation used in radiography, like visible light, travel
in straight lines. If this were not the case, we would not be able to produce a
true image on the radiograph.
Ionisation
The ability of a the radiation energy to knock an electron out of its orbit,
leaving a charged atom and oppositely charged particle.
Fluorescence
At some wavelengths, radiation can cause some chemicals to fluoresce
when exposed to ultra-violet light. X-Rays lie within the same band of
electro-magnetic energy as UV light and therefore have the same effect on
these chemicals.
Chemical Effect
This is the effect that the radiation has on the emulsion used on
radiographic film. After processing, the affected emulsion turns black.
Physiological Effect
This is the harmful effect that radiation has on living tissue.
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Properties of Penetrating Radiation
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Film
Source
of radiation
Object
Figure 1.2 the radiograph that would result from the set-up above in figure 1.1.
Note: In film radiography thin sections appear darker while thicker sections
appear lighter. The opposite is true if a fluorescent screen rather than a
photographic film is used as a radiation detector.
1-2
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Properties of Penetrating Radiation
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Film
Object
Source of
radiation
Figure 1.3 Radiation passing through an object containing two voids at different
depths.
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Properties of Penetrating Radiation
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Set-up
Resultant
radiograph
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Properties of Penetrating Radiation
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2 The darkest area on a radiographic film is the part of the film that:
a It's cheaper.
b A permanent record is directly produced.
c Lack of fusion is easily detected.
d All of the above are significant advantages.
a Volumetric flaws.
b Planar flaws.
c Both volumetric and planar flaws.
d Laminations in rolled steel products.
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Section 2
A high density material is like a fine sieve due to the size of the atoms (the
nucleus and amount of orbiting electrons). In order for the photon energy to
pass through the material it will need to be small to pass through the gaps in
the fine sieve, hence, higher energy. The thickness of the material also
means that there are more possibilities that the individual photons will
collide with either a nucleus or orbiting electrons where scattering (explained
in section 8) will cause absorption of the photons.
The amount of energy therefore that is eventually emitted after the photon
energy passes through a material of a given density and thickness depends
upon the above factors.
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The Electromagnetic Spectrum
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Ideally selecting a wavelength (or energy level) that just passes through the
sieve will produce the best quality radiograph with high contrast on the
radiographic film. Using an energy level where the wavelength is much
smaller than the sieve will mean the photons pass easily through the sieve
but results in a lower contrast radiographic image. With this in mind the
radiographic standards highlight the maximum energy values that can be
used for a given material and thickness, to ensure the best quality is
achieved.
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The Electromagnetic Spectrum
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1 One thing that x-rays and gamma rays have in common with visible light
is that x-rays, gamma rays and light:
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Section 3
proton nucleus
neutron
electron
Each element has its own characteristic number of protons in the nucleus.
This number is the atomic number, usually abbreviated as Z. It is the atomic
number that determines the chemical properties of a given substance.
However, each element can exist as any one of a number of nuclides or
isotopes. Each isotope of a given element has the same atomic number,
number of protons and chemical properties, but each isotope has a different
atomic mass number.
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Simple Atomic Theory
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59
Co
27
where:
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Simple Atomic Theory
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1 An electron:
2 An ion is:
a A proton.
b A beta particle.
c An electron.
d A neutron.
a A.
b .
c Z.
d W.
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Section 4
Ionising Radiation
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Ionising Radiation
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4 Ionising Radiation
The two types of penetrating radiation most used in industrial radiography,
X- and gamma rays, are often referred to as ionising radiation. This is
because the nature of their interaction with matter is to cause ionisation.
Ionisation is caused by loss of an orbiting electron which leaves the
atom in a electrically positively charged state (+ ion). Alpha and beta
particles, which are products of radioactive fission also cause ionisation and
are therefore included within the term ionising radiation. Neutron radiation
is a hazard in the nuclear power industry, it can [indirectly] cause ionisation,
and it is therefore often included within this group of types of radiation
referred to as ionising. Alpha and beta particle radiation are covered in
greater detail in Sections 6 and 7.
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Ionising Radiation
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Ionising radiation
a Fusion.
b Fission.
c Friction.
d Ionisation.
3 Ionisation is:
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Section 5
X-rays or Bremsstrahlung
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X-rays or Bremsstrahlung
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5 X-rays or Bremsstrahlung
The term X-ray is applied to ionising radiation produced when a beam of
high velocity (ie high kinetic energy) electrons collides with the atoms of a
target material. The photon energy of the X-radiation thereby produced
depends on two factors:
X-ray photon
(low energy)
Deflected
electron
Atom in target
material
X-ray photon
(high energy)
High velocity
electrons Captured
electron
Characteristic
radiation peaks
Radiation intensity
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X-rays or Bremsstrahlung
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1 Source of electrons.
2 Target, constructed from a suitable high melting point material.
3 Means of accelerating electrons toward the target.
High velocity electrons cannot travel far in air, therefore the process of
acceleration must take place in a high vacuum.
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X-rays or Bremsstrahlung
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Tungsten filament
The target material is usually tungsten because this has a very high melting
point (3370C). This reduces the chances it will be vaporised by the large
amount of heat generated. Tungsten has a high atomic number and
therefore a large number of electrons, this makes it a relatively efficient
material for converting kinetic energy to X-ray energy which in turn helps to
reduce the amount of heat produced as a proportion of the total output of
energy. Sometimes the target is constructed from tantalum (melting point
2996C) and less frequently from other refractory metals.
Nearly all anodes are hooded (see Figures 5.3 and 5.4). The hood is a high
conductivity copper shroud which is designed to intercept stray electrons
and prevent them from hitting the tube walls. The hood has a window in the
form of a beryllium insert or a thinned section of copper which permits
X-rays to exit without unduly increasing inherent filtration. Inherent filtration
is the term used to describe removal of X-rays from the primary beam due to
absorption by the materials used in X-ray head construction. The reason
that a beryllium window is used in many X-ray heads is that beryllium has a
very low absorption factor and this minimises inherent filtration whilst still
affording the tube walls protection from stray electrons.
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X-rays or Bremsstrahlung
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High conductivity
copper
Hood
Electrons
Cooling fins
Beryllium
window
Tungsten target
Useful X-rays
Hood
Electrons
Cooling fins
Beryllium
window
Tungsten target
Useful X-rays
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X-rays or Bremsstrahlung
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70o
Aluminium shell
Ceramic
insulator
Cathode Anode
Electrons
X-rays
Evacuated
chamber Ceramic
insulator
The X-ray beam produced is filtered by the wall of the glass (or metal-
ceramic) envelope. This reduces the useful quantity of X-rays produced,
with the low energy components of the spectrum being particularly affected.
Therefore it is common in glass tubes that the tube wall is ground thinner in
the region of the useful beam in order to minimise the X-ray energy lost due
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X-rays or Bremsstrahlung
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X-ray tubes are invariably mounted inside some form of tank. This is usually
a metal cylinder that may be fitted with a beryllium or plastic window to
minimise self-filtration of the X-rays produced. The tank contains a coolant
which may be oil or some type of gas. It provides high voltage insulation and
mechanical protection. In portable equipment the high voltage transformer is
mounted inside the tank.
Applied
single phase
AC voltage
Resultant
tube current
flowing
Most older type portable X-ray sets were half-wave self-rectified. This
produced a considerable weight-saving compared with the earlier types of
constant potential unit. Most modern portable units are constant potential
and use lightweight solid state rectifiers to produce what is effectively DC
current.
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X-rays or Bremsstrahlung
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Older type constant potential industrial X-ray units were extremely heavy,
bulky and suitable for use only in fixed installations. Much of the weight and
bulk came from the rectification circuitry used, the so called Greinacher
Circuit and the large external oil-cooling system necessary to dissipate the
large amount of heat generated.
Single phase
AC voltage
Greinacher
circuit
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X-rays or Bremsstrahlung
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Self-rectified
Constant potential
Wavelength
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X-rays or Bremsstrahlung
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1 Voltage control: This alters the tube voltage (kV) by varying the low
voltage supply to the high voltage transformer. Note that high voltage is
not generated in the control panel, this minimises the hazard to
personnel.
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X-rays or Bremsstrahlung
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This is because the amount of radiation produced is the same in each case.
Obviously it would be desirable to use a high value of mA, in order to reduce
the exposure time, but as explained above the use of high tube currents can
severely damage the anode of the X-ray tube and thus reduce its service
life. Therefore it is usual to operate at a value of mA which is well within the
tubes specified capabilities.
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X-rays or Bremsstrahlung
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preferred to linear accelerators because they are more compact and less
expensive to manufacture.
Linear accelerators
Linear accelerators (often called linacs) accelerate electrons to very high
velocities along a straight path by means of an electromagnetic waveform
generated by a device called a magnetotron. The particle velocities are
similar to those achieved in betatrons but a much higher output of radiation
is achievable. For radiation energies above 10MeV linear accelerators are
generally the preferred solution.
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X-rays or Bremsstrahlung
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X-rays
a Copper.
b Beryllium.
c Tungsten.
d Aluminium.
a tube voltage
b filament current
c tube current
d the square of the focus to film distance
a Tube current.
b Tube voltage.
c (tube current) x (tube voltage)
d Both (a) and (b).
a The diameter of the beryllium window and the diameter of the tungsten
target.
b The diameter of the electron beam and the diameter of the tungsten
target.
c Diameter of the beryllium window and the angle of the tungsten target
with respect to the window.
d Diameter of the electron beam and the angle of the tungsten target with
respect to the electron beam.
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X-rays or Bremsstrahlung
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a Compton radiation.
b Cosmic radiation.
c Bremsstrahlung.
d Black body radiation.
7 The body of the anode in an x-ray set is usually made from pure copper
why? Because pure copper:
a For a direct type film with lead screens the same film density will be
produced provided that the product of exposure (in this sense radiation
intensity) and time remains constant.
b Radiation intensity is inversely proportional to the distance from the
source squared.
c Film density is directly proportional to radiation intensity and time.
d None of the above.
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Section 6
Gamma Rays
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Gamma Rays
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6 Gamma Rays
Gamma () ray is the term applied to the electromagnetic radiation which is
sometimes produced when the atomic nuclei of a radioactive isotope
disintegrate in the process known as atomic fission. Alpha () and beta ()
particles may also be produced during the disintegration process; in fact
gamma emission is always a by-product of alpha or beta emission. Of the
three main types of radiation produced by fission alpha is by far the most
hazardous to health; alpha and beta radiation must be taken into
consideration when assessing safety. Except as a health hazard, alpha and
beta particle radiation have no significance for industrial radiography since
they are easily absorbed by very thin materials.
60 60
27 Co 28 Ni
031MeV 1.17MeV 1.33MeV
For example:
239 235 4
94 Pu 92 U+ 2 He
Thus in alpha emission there is a loss of 4amu from the nucleus and a
reduction in atomic number of 2 (see the example above). Alpha particle
radiation cannot penetrate more than a thin sheet of paper or a few
centimetres of air, it is, however, very strongly ionising. The great danger to
health with alpha emitters is that they may be ingested radioactive
contamination. Once within the human body they will in most cases cause
cancer.
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For example:
14 14
6 C 7 N E
Thus in beta emission there is no loss from the atomic mass number whilst
the atomic number increases by 1 (see the example above). Beta radiation
is more penetrating than alpha. It can penetrate the outer layers of the skin
and lead to fatal skin burns. The damage caused is very similar to sunburn,
but much more severe. Many of the early victims of the Chernobyl disaster
died as a result of skin burns caused by exposure to high intensities of beta
radiation. If beta emitters are ingested they will often lead to cancer.
All gamma sources in use today are man-made. They are manufactured by
neutron bombardment of non-radioactive raw materials in the core of a small
nuclear reactor. The sources in use are all beta emitters, gamma rays being
produced as a by-product of beta emission. In order to prevent beta
emission or contamination hazard the sources used in industrial radiography
are invariably sealed sources. The fissile material is encapsulated in a high
integrity titanium or stainless steel shell. Beta radiation is not capable of
penetrating the walls of the capsule, and the capsule further precludes any
possible contamination hazard so long as it remains intact.
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100
Note that the Iridium 192
spectrum includes several other
less significant gamma
emissions. The emissions shown
50
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Isotope
Glass fill material
Titanium capsule
Figure 6.3 shows the typical encapsulation arrangement for iridium 192 and
cobalt 60. Some isotopes such as caesium 137 are double encapsulated. In
the case of caesium 137 this is because it is in the form of caesium chloride
which is highly corrosive and highly water soluble (but this is still an
improvement on caesium metal which causes an explosion on contact with
water).
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Example:
All other factors being equal the exposure time would therefore be:
The half life of various commonly encountered isotopes are given in Table 2.
If the half life of an isotope is known then the source activity at a given time
can be calculated if the source activity had previously been measured.
Suppose that an isotope having a half life h, had an activity S0, at time t = 0.
Then at time t, the source strength or activity St, can be calculated using:
St = S0 2-(t/h)
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Gamma Rays
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Sealed
source Locking device
Connector
for delivery
tube Connector
for wind-out
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Projection tube
Isotope container
Wind-out
mechanism
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The output of radiation per unit time is variable for X-ray equipment up to the
maximum mA rating of the tube. The output of radiation from a radioactive
isotope is fixed by the source activity. The output of radiation produced by
X-ray equipment is generally much greater than that produced by
radioactive isotopes.
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Cobalt 60 50 8.9 10
Iridium 192 350 22.4 166
(1)
Caesium 137 25 3.5 2
(2)
Thulium 170 1,000 4 85
Note:
1 Density is for compressed caesium chloride (CsCl).
2 Density is for thulium oxide (Tm2O3).
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Note that the maximum activity of a gamma ray source is limited by its
physical size. The most useful isotopes are those which have a high value
of practically achievable specific activity. In an iridium 192 source at the
maximum achievable activity, about 2.5 atoms per 100 million are
radioactive. In a cobalt 60 source the figure is only about 1 atom in every
10,000 million.
The output of radiation from a typical X-ray machine is much greater than
from a typical gamma source. This means that in X-radiography the use of
long focal to film distances is more economically feasible than in gamma
radiography. Thus, even though the focus is similar in physical size when
compared with the average gamma source, it is generally the case that
geometric unsharpness is better for X-ray techniques than for gamma.
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A typical self-rectified 300kV rated X-ray set (which is useful for the
radiography of steel sections of up to 60mm thickness) is on the other hand
considerably less portable and less manoeuvrable. A typical 300kV SR tube
head could weigh 55kg and measure 300 x 300 x 750mm while the
associated control panel might weigh as much as 30 kg and measure 450 x
350 x 250mm. Low kilovoltage equipment offers improved portability and
manoeuvrability but this has to be offset against the reduced penetrating
power.
X-ray exposures tend to be shorter so there can be a cost saving with X-ray
equipment if the setting-up time between successive exposures is
minimised. Overall gamma radiography tends to be the most cost effective
solution for construction site work but X-radiography may provide the
cheapest option where are large number of similar radiographs are required
(such as may be the case in pipeline or mass production environments).
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Gamma rays
a Electron.
b Helium nucleus.
c Proton.
d Neutron.
3 The half life of Iridium 192 is 74 days. If an 80 curie source arrives today,
222 days from now the source activity will be:
a 5 Ci.
b 10 Ci.
c 20 Ci.
d 40 Ci.
a 3.7 x 108.
b 3.7 x 109.
c 3.7 x 1010.
d 3.7 x 1011.
a Minus 2.
b Zero.
c Minus 4.
d Plus 4.
a Source activity.
b Half life.
c Exposure time.
d The square of the source to film distance.
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a Naturally occurring.
b Produced by neutron bombardment.
c By products of nuclear fission.
d By products of nuclear fusion.
a X-rays.
b Gamma rays.
c Beta particles.
d Alpha particles.
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Section 7
Methods of Producing a
Radiographic Image
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Methods of Producing a Radiographic Image
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Coarse grained film requires a shorter exposure time than fine grain film
because each grain of silver halide needs only to receive as few a single
photon of radiation or single secondary electron in order to become
sensitised. When a sensitised grain contacts the developer solution the
entire grain, regardless of its size, is converted to image forming metallic
silver. Large grains of silver will block out more light than small grains so a
coarse grained film will appear darker after processing than will a fine
grained film even though the exposure conditions were exactly the same.
Table 5 lists the direct type radiographic films produced by various
manufacturers in order of their relative film speed.
For the most part, industrial radiography is carried out using fine grain film
such as Kodak CX, Agfa D7, Cronex NDT 70 or Fuji 100. Ultrafine grained
film is used where adequate sensitivity cannot be achieved using fine
grained film. Coarse grained film is rarely used where except very rapid
results have to be obtained.
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For most purposes lead foil screens 0.125mm thickness are used but thicker
screens are used for high energy radiography. Copper screens tend to be
used only for extremely high energy techniques (above 1MeV). The lead
screens found in pre-packed film are only a few microns thick, they produce
a strong intensifying effect but have a much reduced effect on the scattered
radiation as compared with standard re-useable lead screens. Pre-packed
film is available either in individual disposable cassettes or as rollpack
where a long narrow length of film is supplied complete with lead screens in
a protective light proof sheath. Rollpack film can be cut to any desired
length. The cut ends have to be light sealed with suitable adhesive tape.
Rollpack is commonly used on pipelines in conjunction with the panoramic
technique.
Salt screens
Salt screens consist of a layer of calcium tungstate (or other fluorescent
material), attached using a suitable binding material, to a sheet of
cardboard. While salt screens can produce a dramatic reduction in exposure
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time when used with screen type film they are seldom used in industrial
radiography because they produce an image of inferior quality, are
expensive and very easily damaged.
Fluorometallic screens
These screens, which attempt to combine the advantages of lead screens
with those of salt screens are occasionally used in industrial radiography
when there are strong financial pressures for a reduction in exposure time.
One such application is on offshore pipe laying barges. They are even more
expensive than salt screens at around 70 for a pair of 10x40cm screens
and they are just as easily damaged. They do not provide quite the same
reduction in exposure time as do salt screens but the image quality is
considerably improved (although still inferior to that produced using lead
screens). Fluorometallic screens consist of a cardboard backing material
with a layer of lead foil attached, then a layer of calcium tungstate or other
fluorescent crystalline material suspended in a suitable binding material.
Velcro fastening
Lead foil
Velcro fastening
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Development
The first stage in film processing is development. During this stage a
reducing agent such as hydroquinone or metol reduces the sensitised silver
halide grains in the film emulsion to metallic silver. Development, whether
manual or automatic, must be carried out within the temperature range
recommended by the developer manufacturer otherwise image quality will
be severely impaired.
Stop bath
The stop bath serves two purposes: (1) Curtail the action of the developer
and (2) Protects the fixer by reducing carry over of developer solution. It is
not essential to use a stop bath but it is desirable because it will
considerably extend the life of the fixer. It will also help to avoid possible film
artefacts, dichroic fogging in particular, damage to the fixer. It is normal to
allow a time of 2-3 minutes when using running water stop baths.
The process of removing excess silver halides is called fixing. The chemical
used to achieve this is sodium (or ammonium) thiosulphate (sometimes
called hypo).
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Washing
After fixing the film must be thoroughly washed so as to remove all traces of
the fixer chemicals from the emulsion. Insufficient washing will result in the
formation of brownish yellow stains while over-washing can cause water
marks or even frilling (see above). Adequate wash times in a running water
wash vary from 10 minutes at 30C to 30 minutes at 10C. Most film
manufacturers recommend that the wash temperature should not be more
than 25C. Film can be washed successfully in a still water bath provided
that the water is changed regularly.
Drying
The application of a wetting agent to the film prior to drying will help the film
to dry quickly/evenly without watermarks. If the films are to be dried using a
warm air draught then care must be taken to ensure that dust is not blown
onto the wet films. Warm air dryers with a downward draught dry the film
more quickly.
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1 In manual film processing agitation of the film in the developer should be:
a Is 0.125mm.
b Increases with increasing radiation energy.
c Decreases with increasing radiation energy.
d Is 0.05mm.
3 With which type of intensifying screen is the main intensifying effect due
to the emission of secondary electrons?
a Salt screens.
b Fluorometallic screens.
c Lead screens.
d All of the above.
a Thicker emulsion.
b Lower contrast.
c Increased inherent unsharpness.
d Smaller grain size.
a A raw image.
b An underdeveloped image.
c An imaginary image.
d A latent image.
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a Kryptonite.
b Sodium thiosulphate.
c Silver bromide.
d Calcium tungstate.
8 The intensifying effect of lead screens occurs above what minimum x-ray
kilovoltage?
a 180 kV.
b 80 kV.
c 55 kV.
d 120 kV.
9 X-ray film differs from photographic film in that the film emulsion is
applied to both sides of the base. What advantage is gained by double
coating the film in this way?
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Section 8
Production of a Radiographic
(Film Radiography)
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Radiographic sensitivity
Contrast Definition
8.1.1 Contrast
Contrast can be defined as the ease with which it is possible to distinguish
between two adjacent areas of different film density. The chief factor which
determines whether or not the two areas will be clearly defined is the degree
of difference in film density.
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The factors affecting film and subject contrast are discussed below.
The logarithm to the base 10 of a number is just the power of 10 that will
produce the number itself.
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For example:
Figure 8.2 Film characteristic curves CX-D7-MX (direct type film/lead screens).
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8.0 10.0
MX
6.0 D7
CX
4.0
2.0
0.0
Figure 8.3 Gradient of the film characteristic curve versus film density for Kodak
MX, Agfa D7 and Kodak CX.
Figures 8.2 and 8.3 show how film density affects film contrast. Film density
does not affect subject contrast. The gradient of the film characteristic curve
is a good measure of film contrast. The gradient for all films increases with
increasing film density. If the gradient is steep then a small change in
radiation intensity or exposure time will produce a large change in film
density. The gradient of all of the film characteristic curves becomes shallow
at film densities of less than 1.5, indicating that film contrast will be poor at
low film densities. In view of this all relevant national standards stipulate a
minimum film density of about 2.0 for industrial radiography.
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Film density
(The dotted lines show the average gradient between film densities 1.5 and
2.5 for film having a base fog level of 0.1 and 0.5 respectively. The average
gradient with a base fog level of 0.1 is about 3.6 while that for a base fog
level of 0.5 is about 2.7. This decrease in average gradient is indicative of a
reduction in film contrast.) can, to some extent, be increased to compensate
for a lower developer temperature or reduced if the temperature is above
the optimum, but this will invariably be at the cost of reduced film contrast.
It is useful to talk about different radiation energy in terms of its half value
layer. The half value layer can be defined as the thickness of any particular
material which will reduce the intensity of the incident radiation by a factor of
2. The thickness of the half value layer for any material increases with
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8.1.2 Definition
Definition is a measure of the sharpness of the images on the radiograph. It
can be defined as the width of the boundary between two areas of different
density on a film. The opposite of definition is unsharpness.
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Increasing unsharpness
Figure 8.5 The unsharpness of the boundary between light and dark increases
from left to right.
Focus
Object
Image
Umbra
Penumbra
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The focal spot of an X-ray tube and a radioactive isotope always have finite
physical dimensions so a penumbra is always produced. Once the achieved
penumbra falls below about 0.2mm the unaided human eye ceases to
perceive any further improvement in definition. For very high quality
radiographic techniques geometric unsharpness is therefore generally kept
to a value of less than 0.2mm. To achieve this, the object to film distance is
kept short and the radiation source to film distance is made as long as
necessary depending upon the radiation source dimensions.
To determine the focal sport size of an X-ray tube, the pin-hole camera
method can be used.
f OFD
Ug
FOD
Figure 8.7 Geometric unsharpness.
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Source
Photoelectric effect
Takes place below 0.6MeV where all the energy of the incident X- or
gamma photon is transferred to an orbiting electron which is ejected from
the atom. When the atom re-captures an electron an x-ray is emitted.
Compton (incoherent)
Occurs between 0.6MeV and 6MeV where only part of the incident photon
energy is transferred to an orbiting electron. The remaining photon energy
continues as a lower energy X-ray although slightly deflected from its
original path.
Pair production
Generally occurs above 6MeV where the incident photon collides with the
nucleus or inner shell, converting to an electron-positron pair. The positron
is short lived and when meeting with an electron and annihilation takes
place, emitting 2 photons of 0.541MeV radiation. Note: pair production
cannot take place below a 1.02MeV threshold.
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Side scatter
Radiation may be scattered by parts of the object that are not within the
diagnostic area of the radiograph or by the walls of the exposure room. This
is termed side scatter.
This type of scatter can be reduced by collimating the beam such that only
the area to be examined is subjected to the primary beam and by the use of
lead masking, diaphragms or grids. In X-radiography the use of a filter may
help to reduce side scatter.
Back scatter
Back scatter is caused by the primary beam striking an object behind the
film and scattering back.
It can easily be reduced by shielding the back of the film cassette with a
sheet of lead; approximately 2mm thick is adequate for most applications. In
X-radiography the use of a filter may help to reduce back scatter.
Note: If a dark image of the letter B appears this is not excessive back
scatter. It merely indicates scatter caused by the letter B itself.
Should back scatter be detected then the thickness of the lead sheet
shielding the back of the film cassette must be increased.
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Self-scatter
Self-scatter is scattered radiation originating from within the test component.
The detrimental effect on film quality can be reduced by the use of lead
intensifying screens placed in contact with the film and in X-radiography, by
the use of filters.
If the radiation source is an X-ray tube then the use of a copper filter can
help to reduce the effects of this type of scatter. A copper filter significantly
reduces the proportion of low energy radiation within the primary beam.
Since it is the low energy radiation which is chiefly responsible for scatter
the use of such a filter can reduce the overall amount of scatter occurring
and in this way improve image quality. Filters made from lead, steel or other
metals may be used in a similar way.
Metallic foil intensifying screens made from lead or other metals reduce the
effects of self-scatter for both X and gamma ray radiography as they filter
out the low energy scattered radiation and prevent it from reaching the film.
The principle of collimation is simply that if there is less radiation then there
will be proportionally less scatter.
8.2.4 Diaphragms
Diaphragms take collimation a step further. They consist of a sheet of lead
which has a hole cut in it the same shape as the object which is being
radiographed. Using a diaphragm the radiographer is attempting to shield
out all unwanted radiation, the set up for radiography must however, be
extremely accurate if it is to be successful. Diaphragms are therefore more
likely to be seen where a fully automated technique is in use that allows for
a very high degree of repeatability in the set-up accuracy.
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Factors affecting the intensity of radiation reaching the film (Table 7 Part 2)
Factor Comments
Material type The amount of radiation absorbed by a material increases with
increasing density and atomic number.
Material thickness The amount of radiation absorbed by an object rises exponentially with
increasing material thickness.
I = I0e-t
E al D2
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Steel thickness/mm
Exposure/mAmins
Exposure/mAmins
Pantak 200kV
Kodax CX
FFD 914mm
Lead screens
Density 2.2
Steel thickness/mm
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Steel thickness, mm
Exposure/curie hours
Steel thickness.mm
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Example:
Figure 8.11 Butt weld in 15mm plate. Radiograph of a butt weld in 15mm thickness
steel plate (allows for a weld reinforcement of 3mm).
Taking the example given in Figure 8.11 above lets suppose that we wish to
achieve a geometric unsharpness of 0.25mm or better. This would be
sufficient to satisfy the requirements of most national codes or standards
including BS EN 1435 class A.
f (OFD)
Ug =
(FOD)
but the OFD can be taken as being equal to the material thickness, in this
case 18mm, and the FFD is equal to the FOD plus the material thickness
so:
f x 18
0.25 =
(FFD 18)
If we choose to use the Pantak 200 CP the effective focus size on the broad
focus setting is about 4mm, so:
4 x18
Minimum FFD = + 18 = 306mm
0.25
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f (d-OFD)+OFD
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110% of the nominal thickness. For Class A the requirement is that the
penetrated thickness shall not exceed 120% of the nominal thickness at the
end of the DFL. This translates to a DFL that is approximately 0.9 x FFD for
Class B and 1.3 x FFD for Class A. In this case lets apply the BS EN 1435
Class A requirement. If we want to achieve a DFL of 450mm the minimum
FFD based on this will be 450/1.3 = 346. For convenience we can round this
up to say 400mm.
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Note: that the film factors given in Table 8.8 are approximately correct for
radiation energy in the range 0.1-1.0MeV. Film factors can vary with
radiation energy.
New exposure =
Old exp osure x (Film factor B).
Film factor A
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Therefore using MX film, for a film density of 2.5 our exposures become
140mA-mins at 120kV or 37mA-mins at 140kV. The exposure at 120kV is
now rather long (14 minutes at 10mA) so an exposure using 140kV of
around 3 minutes at 12.1mA would be preferred.
From the table it can be seen that at 140kV the copper equivalence factor is
probably about 1.55, while that for steel is 1.0, so 18mm copper is
radiographically equivalent to (18 1.0) x 1.55 = 27.9mm steel.
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Suppose that we wish to radiograph our 18mm thickness steel weld using
the Pantak 200 at 140kV with a focus to film distance of 400mm. The
exposure required for a film density of 2.5 without a filter was calculated
above as 9.2mA-mins if using CX film. The equivalence factor for copper at
140kV is about 0.64. Therefore 1mm of copper will be radiographically
equivalent to 10.64 x 1 = 1.6mm of steel. To find the correct exposure (for
a copper filter thickness of 1mm) we simply need to add this amount to the
steel thickness which is being radiographed:
18 + 1.6 = 19.6mm
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Production of a radiograph
a D2.
b D.
c 1/D.
d 1/D2.
3 An exposure chart for iridium 192 that has been constructed for SFD =
500mm gives an exposure of 100 Ci-min for 25mm of steel. The
specification calls for a minimum SFD = 800mm. If all other factors
remain equal what exposure is needed at the specified minimum SFD?
a 160Ci-min.
b 62.5Ci-min.
c 39.1Ci-min.
d 256Ci-min.
4 At 160 kV the equivalence factor for copper is 1.6 while that for steel is
1.0. This means that:
5 The major cause of scatter up to a radiation energy of about 0.6 MeV is:
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a 0.25mm.
b 0.30mm.
c 0.24mm.
d 0.27mm.
a 100mAmins.
b 113mAmins.
c 53mAmins.
d 91mAmins.
9 If the effective focus size = 4mm, the object to film distance = 35mm and
the focus to film distance = 750mm what is value the geometric
unsharpness that has been obtained?
a 0.196mm.
b 0.200mm.
c 0.125mm.
d 0.187mm.
a Zero.
b 0.1.
c 0.2.
d 0.3.
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a Penumbra.
b Film unsharpness.
c Geometric unsharpness.
d Chromatic aberration.
a 414mm.
b 459mm.
c 503mm.
d 519mm.
a 42 curie minutes.
b 65 curie minutes.
c 155 curie minutes.
d 239 curie minutes.
a 33.33mAmin.
b 15.17mAmin.
c 40.00mAmin.
d 20.00mAmin.
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a 16mm.
b 18mm.
c 19mm.
d 17mm.
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Section 9
Sensitivity
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Sensitivity
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9 Sensitivity
9.1 Radiographic sensitivity
Radiographic sensitivity can be defined as the ability of a radiographic
system to reveal small changes in section thickness. It may also be defined
as the ability of a radiographic technique to reveal the smallest possible
flaw. True radiographic sensitivity is a difficult quantity to measure.
These days the type of IQI most commonly in use is the wire type but other
types exist, two examples being the plaque and the step hole types.
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Note: that it is fairly easy to remember the wire diameters: if you can
remember the diameters of the first three, 3.2 and 2.5 and 2mm you can
arrive at all other wire diameters by halving as shown below in Figure 57.
Figure 9.2 Remembering the EN 462-1 wire diameters. Looking along each row
the wire diameters are successively halved, eg 3.2, 1.6, 0.8.
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The DIN 54 109 series consists of 16 wires corresponding exactly to the first
16 wires in the BS EN 462-1 series. The ASTM E 747 series consists of 21
wires ranging from 0.08-8.1mm in diameter; there are four overlapping
groups of six wires, each designated by a letter (A-D), see Table 9.11
below, and a large number of material groupings each designated by a
number with ferrous being 1.
Figure 9.4 BS EN 462-2 step-hole IQIs. These IQIs are supplied encased in plastic
complete with lead number identification similar to that used in EN 462-1 wire type
IQIs.
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It used to be common good practice to place the IQI in the least favourable
position within the diagnostic area of the radiograph. This would usually
have meant placing the IQI on the source side of the specimen and towards
the extremities of the diagnostic area because this is where the contrast and
definition would tend to be at their least favourable (highest value of
geometric unsharpness and lowest film density).
In the past it was not uncommon for national codes or standards to specify
an overall requirement for a radiographic sensitivity of 2% or better. This
was easy to achieve on thicker sections but often impossible to achieve on
thinner sections of material. Modern radiographic standards take account of
the fact that the best achievable sensitivity for a given situation and
technique is not a fixed quantity but a variable which depends upon such
factors as the type of radiation source, the technique and the thickness of
the specimen. Such standards specify a minimum sensitivity which should
be achievable using a good quality radiographic technique. One such
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Sensitivity
a 5 wires.
b 6 wires.
c 7 wires.
d 8 wires.
a 2: Fe, Al.
b 4: Fe, Al, Cu, Ti.
c 4: Fe, Al, Cu, Ni.
d 6: Fe, Al, Cu, Ti, Ni, Zn.
a 10mm.
b 25mm.
c 30mm.
d 40mm.
5 Using an EN 462 10-FE-EN IQI four wires are visible in the radiograph of
a butt weld in 15 mm thick steel plate. The sensitivity achieved is:
a 0.83%.
b 1.66%.
c 1.33%.
d 1.07%.
a 0.40.
b 1.25.
c 0.32.
d 0.16.
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a A.
b B.
c C.
d Any of the above as long as IQI wires and ident numbers are visible on
radiograph.
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Section 10
Radiographic Techniques
(for welds in plate and pipe)
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As a general rule, wherever possible, the IQI should be placed source side.
As then they are affected both by radiographic contrast and geometric
unsharpness. Film side IQIs indicate radiographic contrast only, thus source
side IQIs give a more accurate measure of the overall radiographic quality.
It used to be standard good practice to place wire type IQIs towards the end
of the diagnostic area, with the thinner wires toward the outside of the DFL;
the wires were invariably placed across the weld and sensitivity was
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assessed on the weld allowing for any weld reinforcement present. This way
of working would still meet ASME V article 2 requirements, although this
document does not specify where within the DFL the IQI should be placed.
In Europe matters are different; when working in accordance with
BS EN 1435 sensitivity should generally be assessed at the centre of the
DFL on the parent material.
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Table 10.14 BS EN 1435 applicable thickness ranges for gamma ray sources and
high energy X-rays.
Radiation source Penetrated thickness , w
Test Class A Test Class B
Thulium 170 w5 w5
(1)
Ytterbium 169 1 w 15 2 w 12
(2)
Selenium 75 10 w 40 14 w 40
Iridium 192 20 w 100 20 w 90
Cobalt 60 40 w 200 60 w 150
X-ray equipment, 1-4MeV 30 w 200 50 w 180
X-ray equipment, 4-12MeV w 50 w 80
X-ray equipment, 12MeV and above w 80 w 100
(1) For aluminium and titanium, the penetrated thickness is 10 w 70 for Class A and
25 w 55 for Class B.
(2) For aluminium and titanium, the penetrated thickness is 35 w 120 for Class A.
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f = SOD.
d = Focus Size.
b= OFD - object to film distance.
k= constant (7.5 or 15).
Figure 10.2 shows a typical set-up for exposure of a butt weld in flat plate.
The annotations refer to BS EN 1435 requirements.
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The source should be positioned on the centre line of the weld, directly
above the centre of the diagnostic area.
This technique may also be used for examining girth welds in cylindrical
pressure vessels. Using thulium 170 isotopes boiler tube welds, which may
have an outside diameter of only 40mm, are occasionally examined by this
technique.
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Figure 10.4 SWSI source internal and offset technique (BS EN 1435). Required
number of exposures: see Figure 10.8 for BS EN 1435 requirements.
Figure 10.5 SWSI film inside, source outside (BS EN 1435). Required number of
exposures: see Figure 10.6.
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t/De
De/f
t/De
De/f
Figure 10.6 BS EN 1435: Exposures required for film inside source outside (FISO)
techniques.
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X-ray tubes are bulky and the minimum achievable FFD will usually be
about 125mm plus the outside diameter of the pipe. A minimum of four
exposures per weld is therefore required when using an X-ray source for
this technique.
Being able to place the source of radiation in close contact with the pipe
gives gamma ray another significant advantage over X-ray techniques
particularly on smaller pipe diameters. Less offset is needed with gamma
ray sources in order to ensure that the image of the source side portion of
the weld is not superimposed upon the film side part of the weld. This can
increase the chance of finding vertical defects such as lack of root fusion in
the weld being radiographed.
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Because there will in general be no access to the inside of the pipe when
this technique is employed the location markers and IQI are always placed
film side
Figure 10.7 Double wall single image technique (required number of exposures:
see Figure 10.8).
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Figure 10.8 BS EN 1435: Exposures required for DWSI and SWSI source inside
film outside (SIFO) techniques.
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For pipes with a wall thickness to OD ratio in excess of about 0.15 the DWDI
(superimposed) technique is preferred.
Long source to film distances are needed because the minimum value of
object to film distance is equal to the OD of the pipe. Exposure times for this
technique, therefore, tend to be rather long especially in the case of gamma
ray techniques.
BS EN 1435 requires wire type IQIs to be placed on the parent material with
their wires parallel to the weld axis, see Figure 10.9). Working in accordance
with ASME V article 2 standard wire type IQIs should be placed with their
wires across the weld at 90 to the weld axis.
In the DWSI technique the film is wrapped around the pipe to remain as
close as possible to the weld. Conversely, in the DWDI technique the film
should be kept as flat as possible, see Figure 10.9.
As the image of the source side part of the weld is superimposed on the
image of the film side part of the weld it is often not possible to accurately
locate a weld defect when using this technique. This is not usually much of a
handicap because small diameter welds tend to be cut out and re-welded
rather than being repaired locally.
A single location marker per exposure is usually sufficient when using this
technique and it may be placed either source or film side. IQIs should
always be placed source side.
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The DWDI superimposed technique may be more likely than the elliptical
technique to successfully detect lack of root fusion due to the more
favourable angle of incidence of the primary beam.
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a 75mm or less.
b 80mm or less.
c 85mm or less.
d 100mm or less.
a 1.8.
b 2.0.
c 2.3.
d 2.5.
a The image of the IQI must appear in an area of uniform film density.
b The image of the IQI must appear in the image of the weld.
c Wires in wire type IQIs must be placed parallel to the weld axis.
d An image of at least one IQI must appear in every production radiograph.
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9 Most national codes and standards require that the location markers
used in weld radiography must:
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Section 11
Interpretation of Radiographs
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Interpretation of Radiographs
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11 Interpretation of Radiographs
11.1 Introduction
Competent interpretation of radiographs is a skill only gained through long
experience. This section gives the reader a guide to radiographic
interpretation and should be regarded as a base upon which to build.
Radiographs are easily damaged, therefore the viewing room must be clean
and dry and the radiographs must be handled with care. The viewer should
be mounted on a table or bench large enough to allow the films to be spread
out without the danger of them falling to the floor. A well shielded reading
lamp will allow reports to be read or notes to be made, without unduly
increasing the overall ambient lighting.
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The viewing of radiographs is often undertaken in the dark room where the
film was processed. This is satisfactory provided that the viewing bench or
table is clean and well away from the processing tanks. Under normal
circumstances films should NEVER be viewed whilst wet. There are two
reasons for this:
1 The film emulsion is swollen with water and the images are not as clear
as when the film is dry.
2 Emulsion is very delicate and any attempt to mask the film will result in
scratches or marks on the film, effectively ruining it.
11.3 Reporting
The initial interpretation of a radiograph should always be undertaken by the
manufacturer or designated representative. Other interested parties should
be presented with a report which includes an interpretation of each film.
They check this and agree or disagree with it. The radiographic report
should contain the following as a minimum:
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Geometric details, particularly the FFD or SFD and the effective focus or
source dimension.
Details of the component being radiographed, including the type of
material and method of manufacture, the thickness, the heat treatment
condition and the repair status.
Method of film processing.
Film density achieved.
Radiographic sensitivity achieved.
Technicians name, signature and date.
Interpreters name, signature and date.
An interpretation of each film and a statement of the components
acceptability or not.
Code or standard applicable to the radiographic technique.
Acceptance code or standard.
Reference to a written procedure or technique sheet.
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procedure should be in force which describes the standard method used for
the placement of location markers.
ASME V article 2 requires that the film density within the area of interest
must not vary by more than minus 15 or plus 30% from the value measured
through the body of the IQI. If necessary additional IQIs can be used in
order to satisfy this requirement for exceptional areas.
Occasionally an upper limit is specified for film density. ASME V article 2, for
example, specifies an upper limit of 4.
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Artefacts.
Surface irregularities in the component.
Internal discontinuities in the component.
11.6 Artefacts
Pressure marks (crimp marks)
Produced by careless film handling, if the film is crimped or buckled either
before or after exposure crescent-shaped images in the processed
radiograph will result. Light marks indicate crimping before exposure, dark
marks crimping after exposure but before film processing.
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Developer splashes
Appear as dark spots on the film and indicate poor dark room practice and
are usually visible in reflected light.
Fixer splashes
Appear as light spots on the film and again indicate poor dark room practice.
Such marks are usually visible in reflected light.
Water splashes
Appear as either light or dark images on a radiograph. Water splashes
before exposure tend to cause light marks, after exposure tend to cause
dark marks. Such marks are usually visible in reflected light.
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Water marks
Easily seen on the radiograph in both transmitted and reflected light and are
due to uneven drying. They commonly occur where a dry or partially dry film
is wetted locally either by splashing or by excess water running down from a
film clip. The appearance of water marks can be reduced or eliminated by
using a squeegee to remove excess water or a final wash that contains a
small amount of detergent (ie a wetting agent).
Air bells
Light marks caused by air bubbles adhering to the film in the early stages of
development and will not occur if the film is properly agitated.
Diffraction mottling
Can be a problem when X-rays are used to radiograph large grained
material, for example being austenitic steels. Diffraction is an apparent
bending of a beam of radiation due to interference. It occurs when radiation
passes through a grating that has a spacing approximately equal to one
wavelength. The spacing of atoms in a metallic crystal is about
0.1nanometres. This corresponds to X-ray radiation with a photon energy in
the region of 10keV. If low energy components are removed from the X-ray
beam by filtration the problem with diffraction mottling will disappear.
Diffraction mottling does not occur in gamma radiography because of the
absence of low energy beam components.
Diffraction can be used to advantage and it is the basis for the study of
metal crystals by X-ray crystallography.
Static marks
Penetrating radiation is by definition ionising. It always causes the build-up
of an electric charge on the film during exposure but under normal
circumstances this is not a problem because the charge quickly flows to
earth. In dry climates, however, a static charge may remain on the film until
it is unloaded in the darkroom, whereupon it flows to earth suddenly in a
manner which could be painful for the radiographer. Such a sudden
dissipation of electrical energy leads to the emission of a sudden burst of
light which produces dark tree-like marks on the finished radiograph. Static
marks can be avoided by careful film handling.
Dichroic fogging
Radiographs affected by dichroic fog will appear reddish when viewed using
transmitted light and greenish in reflected light. Dichroic means two-
coloured. It is caused when the development process continues during the
fixing process, when the fixer solution has become insufficiently acidic to
stop the development process. The use of an acidic stop bath between the
development and fixing processes will generally prevent the occurrence of
this seldom seen artefact.
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Reticulation
Appears on the radiograph as an orange peel-like mottling effect. It is
caused when the film emulsion is subjected to a temperature shock at any
stage during the film processing as the sudden change in temperature
causes the film emulsion to wrinkle. It will not generally occur as long as the
sudden change in temperature is less than 10C.
Light fogging
Exposure to light other than from darkroom safe lamps (and even prolonged
exposure to safe lamps) will cause fogging at any stage prior to fixing the
film. Such fogging may be localised or general - localised is not a problem
unless it encroaches onto the diagnostic film area but general light has the
same effect as fogging due to exposure to ionising radiation.
Solarisation
Image reversal due to extreme over exposure to X or gamma rays or
caused by exposure to light during film development.
Frilling
When the film emulsion becomes detached from the base, most commonly
due to over-fixing.
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there is doubt if a visual examination of the weld will often help. It is felt that
an indication resulting from surface geometry could mask a significant
defect indication, or where visual examination proves inconclusive, it may be
necessary to dress the weld to a smooth contour and reshoot the
radiograph.
Listed below are some of the common surface conditions that can produce
radiographic images.
Root concavity
A shallow groove which may occur in the root of a single sided weld, it
appears in the radiograph as a series of dark areas along the centre of the
weld varying in density according to the depth of imperfection and it is often
seen in welds made with the use of a backing gas. The pressure of the
backing gas can cause the weld root to collapse during welding of the first
subsequent weld run (hot-pass). Other possible causes are no root face;
travel speed too slow, amperage too high, incorrect polarity on the hot pass;
excessive pre-heat and root gap too narrow.
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Lack of reinforcement
This is a concave area of the weld cap where the weld is locally thinner,
sometimes thinner than the parent material. In the radiograph it appears as
a dark area towards the centre of the weld which has diffuse edges and is
caused by poor welding practice.
Undercut
An irregular groove at the toe the weld in the parent material due to burning
away during welding. It appears in the radiograph as a dark/irregular/
intermittent band in a position adjacent to either the cap or root weld toe or
between adjacent capping runs. It may therefore appear inside or outside
the weld image on the radiograph. The major causes are excessive
amperage and poor welding technique. Welds in the vertical or horizontal
vertical position tend to be prone to undercutting.
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Spatter
Spatter consists of globules of molten filler metal expelled during arc
welding on to the surface of the parent material or weld. It appears in the
radiograph as small light spots and the major causes of spatter are incorrect
polarity and welding current too high. Spatter particularly affects MIG, MAG,
MMA and FCAW, and is highly unlikely to be seen in association with welds
made by TIG or SAW. In pipe welding spatter is possible on both external
and internal surfaces.
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Torn surface
A surface irregularity due to breaking off of temporary attachments. The
radiographic indication produced has a shape corresponding to that of the
affected area which may be either light or dark depending on whether part of
the attachment has remained or parent material has been torn away,
caused by poor fabrication practice, often seen in association with storage
tank or ship hull welds.
Surface pitting
Surface imperfection, usually of the parent material but also the weld metal
where a component has been in service. It usually takes the form of small
depressions resulting from localised corrosion. Pitting appears in a
radiograph as small dark rounded images and it is possible to mistake this
for a welding defect, as its appearance can be identical to that of porosity.
Internal defects
Cracks
In weld radiography four basic types of crack are sometimes detected by
radiography.
1 Centreline (shrinkage).
2 Transverse (including chevron).
3 Heat affected zone or toe.
4 Crater.
Cracks are often invisible on radiographs but if detected appear as dark, fine
often branching lines, usually diffuse or discontinuous. The ability of the
radiographic technique to detect a crack is dependent on the cracks
orientation relative to the direction of the radiation. Figure 11.8 shows how
even a slight deviation from the optimum orientation will greatly reduce the
change in section thickness which the radiation experiences due to a planar
defect such as a crack. In the case shown a variation from optimum
incidence of just 1 will reduce the change in penetrated thickness from 10
to 1mm for a planar defect measuring 10mm by 17m.
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The second type is a chevron crack, which occurs at about 45 to the weld
axis, usually after the completion of welding. Chevron cracks are a special
type of hydrogen induced crack; the stress that causes the crack being due
to an excessive amount of dissolved hydrogen in the weld metal. They are
sometimes detected by radiography, but where there is a known problem,
other NDT methods with a higher probability of detection should be used.
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HAZ. It is this susceptible grain structure that makes the HAZ a prime site
for cracking. HAZ cracks are usually caused by one of two mechanisms.
The first involves dissolved hydrogen. Molten iron has a very high solubility
for hydrogen while solid iron has a very low solubility. Thus as the metal
freezes hydrogen will attempt to leave solution and escape from the weld
pool but this process is slow compared with freezing, therefore most of the
hydrogen becomes trapped in the solidified metal. The trapped hydrogen
then diffuses through the metal crystals and begins to build up an internal
pressure at points of weakness, usually the grain boundaries. In some
cases the internal pressure exceeds the strength of the material and
hydrogen cracking occurs. Hydrogen induced cracking may occur up to 48
hours after welding. Where ferrous materials operate in a hydrogen rich
environment, for example in sour gas service, hydrogen cracking can occur
as an in-service defect. High strength, high carbon equivalent steels are
most prone to hydrogen cracking. The presence of trace elements,
especially sulphur and phosphorus can make hydrogen cracking much more
likely to occur. Hydrogen induced cracks are not likely to be detected by
radiography and other methods such as ultrasonic testing should be used in
any situation where there is a high probability of occurrence.
A second type of cracking that can occur in the HAZ of a weld is sometimes
called weld decay. This can affect stainless steels and is caused by the
precipitation of brittle material (chromium carbide) at the grain boundaries.
All stainless steels contain a small proportion of carbon which is generally
held in solution within the austenitic grains, but the heat from welding can
cause it to combine with the chromium which is present forming chromium
carbide which is an extremely brittle material. Weld decay can be avoided
by reducing the carbon content of the parent material and filler wire.
Cracking caused by weld decay is unlikely to be detected by radiography.
Crater cracks
Occurs when the heat source is removed too suddenly at the end of a weld
run. The cracking mechanism is the same as that for centreline cracking.
The major dimension of a crater crack is usually less than 5mm, are often
star shaped in a radiograph and relatively easy to detect. Many welding
standards will permit this type of cracking provided that it does not exceed a
specified maximum dimension.
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Lack of fusion
Can occur either between the weld deposit and the parent material or
between successive layers of weld material, also due to lack of fill or
penetration.
Lack of fusion is where the solid material immediately adjacent to the molten
weld pool failed to become molten during the welding process leading to a
lack of union between the molten weld material and the adjacent solid
material. The ability of radiographic techniques to successfully detect lack of
fusion is strongly dependent on the orientation of the defect with respect to
the incident beam of radiation, (see Figure 11.10). Given favourable
orientation lack of fusion with the parent material will appear in the
radiograph as a fine dark straight line which may be continuous or
intermittent. Unfavourably orientated lack of fusion with the parent material
may sometimes still be detected due to the presence of associated slag
inclusions or porosity. A slag inclusion with a straight edge normally
indicates lack of fusion and gas escaping from an area lack of fusion during
the deposition of a subsequent welding run may lead to a line of linear
porosity.
Lack of fusion between subsequent layers of weld material will generally not
be detected by radiography unless it is associated with another type of
defect such as slag.
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Where welds are deposited without a root gap, lack of penetration may
appear as a single continuous or intermittent dark line. It should be noted
that root gaps frequently close during welding so even where there should
have been a root gap lack of penetration may appear in the radiograph as a
single dark line.
Non-metallic inclusions
Usually formed by slag, but occasionally other foreign matter such as wind
blown sand may become entrapped within the molten weld material. Slag
inclusions are irregularly shaped and may be either rounded/isolated or
linear/elongated. Linear slag inclusions with a straight edge often indicate
lack of fusion. Sometimes linear slag will appear on the radiograph as two
parallel lines, often referred to as tram lines or wagon tracks.
Although very rarely used, some types of covered welding electrode have a
high barium content in the flux coating and produce a slag radiographically
denser than steel so slag inclusion may appear as a light image.
Metallic inclusions
Dependent upon the nature of the welding process it is possible for foreign
metallic material to become entrapped within the molten weld material.
Associated with the gas tungsten arc welding process, tungsten inclusions
are probably the most commonly encountered form of metallic inclusion.
They are caused by the break-up of the non-consumable tungsten electrode
during welding and since tungsten has a melting point well in excess of
3000C particles of tungsten falling into the weld pool do not become
molten. Tungsten is radiographically extremely dense; therefore tungsten
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Metallic inclusions are quite common in aluminium welds, where such welds
are not properly segregated from their steel counterparts. Aluminium melts
at around 660C, steel at about 1400oC so particles of steel or iron oxide
falling into the weld pool will not become molten. Contamination can easily
occur if tools such as grinding disks which have been used for steel are
used on aluminium. Steel inclusions in aluminium appear as very bright
angular shapes with sharp edges.
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indicates that the electrode was faulty and group porosity usually occurs at
restarts and is due to poor welding technique.
Hollow bead can be caused by holding the arc at too shallow an angle with
respect to the work piece or by a strong draught of air along the inside of the
pipe during welding. On the radiograph it looks very similar to slag - the
radiographic indication usually has rounded ends and it is always situated
along the centre of the root bead.
Wormholes
These are gas pores which have become frozen in the weld pool while
attempting to migrate to the surface of the weld pool. In addition to occurring
due to an excess of dissolved gas in the weld pool, they sometimes occur
due to laminations in the parent material which extend to the weld face.
Lack of fusion contains a small amount of entrapped air and this can cause
wormholes in a similar way.
A crater pipe will appear in the radiograph with an image very similar to that
of a wormhole. It can only be distinguished from a wormhole by its position
in the weld. Crater cracks are shrinkage cracks so have a relatively greater
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volume than most other cracks. They often have a star like appearance in a
radiograph and their radiographic image rarely measures more than 3 or
4mm.
Voids.
Cracks.
Cold shuts.
Segregation.
Inclusions.
Voids
Voids in castings are formed by gases dissolved in the molten material
precipitating from solution during the solidification process or by shrinkage
caused by inadequate feeding.
Macroshrinkage (piping)
Large cavity formed during the solidification process which occurs due to
lack of sufficient feed material. With good mould design macro-shrinkage
should be confined to the feeder heads.
Microporosity/microshrinkage
Very fine form of filamentary shrinkage due to lack of sufficient feed metal,
gas or both, in which a number of cavities occur either round the grain
boundaries or between the dendrite arms (a dendrite is a material crystal
which in the initial stages of growth is tree-like). These cavities tend to link
up in a three dimensional network throughout the material.
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Pinhole porosity
Cavities less than 1.5mm diameter formed due to the evolution of gas from
the molten material. The defect may be evenly distributed throughout the
casting or localised in a particular area. When it is local to the surface of the
casting, due to gas evolved at the mould face, it is known as subcutaneous
pinhole porosity.
Gas holes
Discrete cavity greater than about 1.5mm diameter caused by gas evolved
from the material as it freezes. It may also arise from gas evolved from the
core or mould, in which case it is called blowhole.
In pressure die casting where air may be injected with the material the
defect is usually more severe in the runners and may assume an angular
form. In pressure and gravity die castings this defect may occur in clusters
or as strings of small voids, whereas, in investment casting it may appear as
small rounded voids.
Cracks
Cracks are discontinuities caused by fracture of the material at the point of
solidification or some time thereafter. They appear on the radiograph as one
or more dark lines. The width and form of the indication depends on the type
of crack and radiographic technique used.
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Hot tears
Discontinuities of a decidedly ragged form resulting from stress developed
near the solidification temperature when a material has low mechanical
strength. They usually arise when the natural contraction of the casting is
restrained by the mould or core and occur mainly at or near a change of
section.
The defects are not necessarily continuous, they may exist in groups and
will often terminate at the surface and are sometimes referred to as pulls.
Radiographically hot tears are wavy, ragged dark lines, often discontinuous,
with areas appearing as approximately parallel dark lines which may
possibly be overlapping. Generally, the ends of the indication taper to
become fine.
Stress cracks
Well defined and approximately straight cracks formed after the material has
become completely solid, quite large stresses being required to cause
fracture. Distinctions are sometimes drawn between types depending on the
time at which fracture occurred.
In the radiograph stress cracks are often revealed as clearly defined smooth
dark lines - thus differing from the ragged appearance of hot tears.
Cold shuts
Discontinuities caused by the failure of a stream of molten material to unite
with either a confluent stream, or solid material, such as a chaplet, internal
chill or pouring splash.
In the radiograph these defects usually appear as dark lines and may be
difficult to distinguish from hot tears except by the typical involute
appearance of the end of the defects. The shape of an unfused chaplet or
chill in a radiograph is dependent upon orientation of the beam. A cold shut
resulting from a splash may appear as a dark crescent or circle.
Inclusions
Foreign matter (sand, slag, flux, dross, etc) entrapped in the casting. As an
inclusion may be of greater or lesser opacity then the surrounding material it
may appear radiographically as a light or dark area (eg a sand inclusion will
appear dark in steel and light in aluminium). Slag usually gives a rounded
image whereas material included in the casting as a solid (eg dross and
sand), will give an irregular shape. If dross is trapped as an oxide film it will
often produce a characteristic folded appearance in the radiograph.
Inclusions may in many respects resemble voids in radiographic
appearance but they will generally exhibit a greater variation in density.
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Segregations
Result from local concentrations of any of the constituents of an alloy and
may be classified as general, localised or banded.
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Interpretation of radiographs
a Porosity.
b Lack of inter-run fusion.
c Lack of root fusion.
d Heat affected zone crack.
a Insufficient pre-heat.
b Welding with damp electrodes.
c High carbon equivalent parent material.
d All of the above.
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a A volume of the parent material each side of the weld, which, although it
does not melt, is metallurgically changed by the heat of welding.
b Everything that becomes molten during the fusion welding process.
c Both (a) and (b) are included in the heat affected zone.
d In welding of carbon steel the HAZ is the entire volume that reaches a
temperature of 100C or more during welding.
a Densitometer.
b Photometer.
c Radiometer.
d Proportional counter.
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Section 12
Localisation
Rev 1 January 2010
Localisation
Copyright TWI Ltd 2013
12 Localisation
A radiograph is a two dimensional image of a three dimensional object.
When a flaw is detected using a standard technique there is no certain way
of telling how far below the surface the flaw is. In some cases it might be
desirable to have three dimensional information about the position of a flaw.
A technique called localisation can be used to estimate the through wall
position of a volumetric flaw such as a slag inclusion. It is important to note
that localisation of planar flaws such as cracks or lack of fusion is generally
not possible by radiographic methods.
12.1 90 method
Is the simplest method of localisation, but rather limited in its field of
application. A typical test object, where this method might be useful would
be a small to medium sized casting that has a fairly simple cross section.
Figure 12.1 shows how this method would work on a small cylindrical
casting. Two radiographs are taken with primary beam mutually at 90 to
each other. In an ideal situation the component would be placed on some
kind of turntable so that it could be moved accurately keeping the two
exposures in the same plane relative to the axis of the component. The
apparent defect position in each radiograph can be measured relative to
convenient datum point, the results plotted on a sketch and the defect
position then deduced by triangulation.
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Flaw
t
X
S
m
m = apparent movement
of flaw image
Radiograph
Figure 12.2 Tube shift method. Note: Source shift distance exaggerated for clarity.
( A d) ( x s)
Using similar triangles: =
B m
But x = t - d
( A d) t d s)
so: =
B m
Am + dm = tB - dB + sB
dB + dm = tB + sB - Am
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d(B + m) = B(t + s) - Am
B( t s) Am
d=
(B m)
Refer to Figure 12.3. The three triangles in the enlarged view will be very
similar as long as the source or focus to film distance is long in relation to
with the thickness.
a b c
= =
x y z
CX cy
So it follows that: a = and : b =
Z z
CX cy
Therefore we can write: c - t = and:c - d =
Z z
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CX cy
We have already established that: c - t = and c - d =
Z Z
cy
From this we can see that: d = C -
Z
CX
And: t = c -
Z
Y
So: d = c 1 [1]
Z
X
And: t = c 1 [2]
Z
Y
1
d Z
=
t X
1
Z
t, the thickness of the plate is known and x, y and z can be measured on the
radiograph. Therefore d can be calculated.
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Localisation
2 What does the tube shift method with lead markers rely on?
3 The tube shift method required two shots from differing tube positions.
What adjustment to each exposure time must be carried out to facilitate
this?
a Half.
b Double.
c Equal.
d Quarter.
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Section 13
The SI unit of ionising effect is the coulomb per kilogram, the quantity of
ionising radiation that produces a total electric charge of 1 coulomb per
kilogram (Ckg-1) of air at STP.
or
1 Ckg-1 = 3876 R
The CGS unit of absorbed dose is the roentgen absorbed dose (rad). The
rad is defined as the quantity of ionising radiation which releases 100 ergs
of energy per gram of absorber.
1 Gy = 100 rad
1R = 0.88 rad
The conversions above are approximate since the relationship between the
roentgen and the rad or the coulomb per kilogram and the gray varies to
some extent with radiation energy.
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In the CGS system multiplying the dose in rad by the appropriate quality
factor gives the dose in roentgen equivalent man (Rem) where 1Rem is the
amount of ionising radiation which has the same biological effect as 1rad of
X-rays.
Thus:
1Sv = 100Rem
or
1Rem = 0.01Sv
In the cgs system dose rate is generally measured in millirem per hour
(mRem/h) but may be measured in Rem per hour (Rem/h).
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1 mRem/h = 10 Sv/h
or
The CGS unit of source strength or activity is the curie (Ci). One curie is
equal to 3.7 x 1010 disintegrations per second.
1Ci = 37GBq
or
1GBq = 0.027Ci
13.7 Output
The output of a source of ionising radiation is the dose rate per hour at
some fixed distance, usually 1m from the source. For radioactive isotopes it
is useful to state output in grays, sieverts, rads or Rems per hour per curie
at 1m. Table 13.17 gives some examples.
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a Becquerel.
b Sievert.
c Gray.
d Roentgen.
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Section 14
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as to the direction from which the detected radiation is coming. They may
give a reading in counts per second, but usually the average current flowing
across the tube is measured with the ammeter scale being calibrated to
read microsieverts or millisieverts per hour. As radiation intensity increases
to high levels a geiger counter will become increasingly inaccurate, because
it suffers from a short dead time after a pulsing event has occurred, if
another photon of radiation arrives during the dead time it will not be
detected. Some instruments will cease to function if exposed to a very high
dose rate.
Phosphors have been used as radiation detectors since the very early days
of the discovery of ionising radiation; both Roentgen and Becquerel used
them. The amount of light produced can be quite small so phosphors are
always used in conjunction with a light amplification system such as the
photomultiplier tube. Modern instruments use charge coupled devices
(CCDs) in conjunction with a radiation sensitive phosphor. A CCD is at the
heart of any modern digital camera. Those used for radiation detection
measure the intensity of light emitted from the phosphorescent layer under
the influence of ionising radiation. Whichever system is used, scintillation
counters relate the intensity of light produced by the phosphor to the
intensity of the ionising radiation received. Generally they give a reading in
counts per second but occasionally they will be calibrated to read directly in
microsieverts or millisieverts per hour.
Scintillation counters are extremely sensitive and can detect very low levels
of ionising radiation. They are direction sensitive and very useful when
searching for radioactive contamination. They are used in industrial
radiography to check for leakage of fissile material from a sealed source.
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Monitoring film
Plastic filter
Copper filters
Open window
Aluminium filters
Plastic filter
The film badge of the type shown in Figure 14.3 contains a section of
carefully manufactured radiographic film having two emulsions, one fast and
one slow. The use of two emulsions extends the measurement range of the
badge. The badge holder is equipped with various filters which extend the
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The film badge has, in large part, been replaced by the thermoluminescent
dosimeter (TLD) (see below). Table 14.19 gives a comparison of typical film
badge and TLD specifications.
TLD badges are worn in specially designed plastic holders similar to those
used for film badges. The addition of plastic or aluminium filters extends the
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The quartz fibre electrometer (QFE) is a gaseous detector like the ionisation
chamber, proportional counter and Geiger counter described above. When
raised to the light a scale like on the right of Figure 14.4 can be seen
through the lens of the instrument. The vertical line is the quartz fibre. When
a static electrical charge is applied to the instrument the quartz fibre moves
to the zero point of the scale. As the gas inside the QFE becomes ionised
the static charge is gradually dissipated and the fibre begins to move to the
right. The corresponding total dose received can be read on the upper
scale.
The QFE has quite a narrow measuring range, typically 0-50mSv or less.
The example shown above has a measurement range of 0-200mRem,
equivalent to 0-2mSv. The QFE is sensitive to X- and gamma radiation in
the photon energy range 45keV-3.5MeV and is a very convenient means for
checking how radiation doses are accumulating during a working day but it
suffers from fragility and is very easily damaged.
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a Beryllium.
b Aluminium.
c Mica.
d Glass.
a An ionisation chamber.
b A Geiger counter.
c A Thermoluminescent doseimeter.
d A Scintillation counter.
3 How many basic types of survey meter are available for use in industrial
radiography?
a 3.
b 4.
c 5.
d 6.
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Section 15
Radiation Safety
Rev 1 January 2010
Radiation Safety
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15 Radiation Safety
All personnel working with ionising radiation should be aware that it is
injurious to the human body, or any other biological tissue. Anyone working
where radiography is carried out should make themselves fully aware of the
safety procedures and regulations in force and take care to observe all
warning barriers. Ionising radiation cannot be detected by the five human
senses and has cumulative effects upon the human metabolism and causes
genetic damage to the human body, the full effects of which may not be
apparent until 15-35 years after the initial exposure. Regardless of any
nominal safe limits it is always prudent to avoid exposure to radiation
whenever possible.
15.1 Precautions
15.1.1 Exposure booths
At locations where a large volume of industrial radiography is carried out
exposure booths of various shapes and sizes will generally be available,
which usually consist of enclosures having lead lined walls. Some exposure
booths have walls filled with spent casting sand or other radiation absorbing
material.
Safety switches are usually fitted to doors of exposure booths to prevent the
operation of X-ray sets or gamma ray equipment whilst the door is open.
Where overhead cranes might have to pass over an open topped exposure
booth similar safety switches are normally installed o trip out the X-ray set,
or wind back the gamma ray source, should the crane encroach upon the
irradiated area during exposure.
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Areas which will be irradiated at greater than the legal limit must be cleared
of all non-classified personnel prior to any exposure. Audible and visible
warnings must be given before any exposure takes place.
15.1.3 Scatter
Personnel should be aware that radiation can be scattered by structures,
apparently safe locations may be subject to stray scattered radiation.
15.2.1 Dosimeters
For work in radioactive environments (ie nuclear reactors) personnel must
be equipped with direct reading dosimeters which will display immediately
the accumulated dose received. Personnel working in these locations must
take particular care to avoid ingesting radioactive particles. Tightly fitting
breathing masks are required and protective clothing should be worn.
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Supervised area
Defined as an area where the annual dose is expected to equal or exceed
1mSv. Such areas should be clearly signed; unclassified persons are
permitted to pass through such areas but must not remain in them for
extended periods. Where possible verbal warnings should be given by the
radiographer.
Dose rate =
Dose rate at one metre
Dis tan ce in metres 2
If the source of ionising radiation is X-ray then it will not be possible to
calculate the dose rate at 1m although the dose rate will be proportional to
the tube current. Halving the tube current at a given tube voltage will halve
the radiation dose rate. If the source is gamma ray then the dose rate at 1m
can be calculated if the source strength (curies or gigabecquerels) and
output of the source are known. Output for any given isotope is the dose
rate per curie or gigabecquerel at 1m from the source.
Thus:
If we take 7.5Sv/hr to be the safe dose rate then we can calculate the safe
distance using the formula below:
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C is a constant for each isotope, for thulium 170 C = 1.86, ytterbium 169 C =
12.91, selenium 75 C = 15.49, iridium 192 C = 25.30 and for cobalt 60 C =
41.63.
15.4.1 Shielding
If shielding is introduced then the reduction in the minimum safe working
distance can be calculated if the magnitude of the half or tenth value layer of
the shielding material is known. The half value layer for any material is the
thickness of material that will reduce the radiation dose rate, for a given
radiation energy, by a factor of two. The tenth value layer is similarly the
thickness of material that will reduce the dose rate by a factor of ten. For
example the half value layer of lead for cobalt 60 is about 12.5mm while for
iridium 192 it is about 4.8mm. The tenth value layer of lead for cobalt 60 is
about 41.5mm while for iridium 192 it is about 16mm. If the shielding
thickness is an exact multiple of the half or tenth value layer then the dose
rate after shielding can be found simply by dividing the unshielded rate by
two for each half value layer or by ten for each tenth value layer. Where this
is not the case the formulae given below can be used.
RU RU
RS = or RS =
2 t / hvl 10 t / tvl
Where:
Ru = unshielded dose rate.
Rs = shielded dose rate.
t = thickness of shielding material.
hvl = half value layer.
tvl = tenth value layer.
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Self-Assessment Questions
Radiation Safety
1 Calculate the safe distance from an unshielded 50Ci Iridium 192 source:
(given that: (i) the "safe" dose rate = 7.5Sv/h; (ii) the output of Iridium
192 is 4.8mSv/h/Ci at 1 metre).
a 167m.
b 136m.
c 77.4m.
d 179m.
2 The output of Iridium 192 is 4.8mSv/h/Ci at 1 metre, thus the dose rate at
1 centimetre from a 1Ci source will be:
a 48 mSv/h.
b 48 Sv/h.
c 48000 Sv/h.
d 480 Sv/h.
a Exponential.
b Parabolic.
c Linear.
d Sinusoidal.
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End Assessment
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Instructions
Try and carry out this End Assessment under your own exam conditions
putting your answers on the sheet at the end of this section. When you are
finished, compare your answers to the correct ones (in the back of book)
and re-read the relevant sections in the notes if required.
a Ionisation of a gas.
b Nuclear disintegration.
c Nuclear fusion.
d Alpha emission.
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6 The part of a conventional x-ray tube that is usually made from tungsten
where deceleration of high velocity electrons takes place is called the:
a Anode.
b Cathode.
c Target.
d Filament.
a Softer.
b Essentially the same.
c Exactly double the intensity.
d Harder.
10 The property of a gamma ray source that is measured in curies per gram
is its:
a Self-absorption coefficient.
b Specific activity.
c Strength or activity.
d Penetrating power.
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a 1.
b 2.
c 3.
d 4.
a Plus 1.
b Minus 1.
c Zero.
d Minus 2.
a Plus 2.
b Zero.
c Minus 4.
d Minus 2.
a 74 days.
b 5.3 years.
c 74 weeks.
d 128 days.
a Alpha radiation.
b Beta radiation.
c Gamma radiation.
d All of the above.
a Alpha particles.
b Beta particles.
c Neutrons.
d Hand grenades.
18 The isotopes Ir 189, Ir 190, Ir 191 & Ir 192 all have the same:
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a Zero.
b Plus 1.
c Minus 1.
d Minus 2.
21 The shielding material in most modern gamma ray source containers is:
a Lead.
b Tungsten.
c Ferro-concrete.
d Uranium.
a 4 minutes.
b Twice the clearing time.
c 2 minutes.
d Equal to development time.
a Acetic acid.
b Potassium ferrocyanide.
c Silver bromide.
d Sodium or ammonium thiosulphate.
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e 100m.
f 10m.
g 1m.
h 0.1m.
a An oxidising agent.
b A reducing agent.
c An acid.
d None of the above.
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End Assessment
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31 The pinhole camera method, which involves the use of a sheet of lead
containing a small hole, is a technique used in industrial radiography to:
a 30cd/m2.
b 9cd/m2.
c 0.9cd/m2.
d 60cd/m2.
a Geometric unsharpness.
b Inherent unsharpness.
c Film unsharpness.
d Undercut.
a Subject contrast.
b Radiographic contrast.
c Film speed.
d Film contrast.
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a 6.0mA.
b 7.5mA.
c 9.0mA.
d 10.66mA.
a Fastest film.
b Slowest film.
c Film with the finest grain size.
d Film with the shortest development time.
a The type of film, the film density, the type of developer, the development
time and the development temperature.
b The x-ray kilovoltage.
c The material which is being radiographed.
d All of the above.
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a X-ray kilovoltage.
b The type of material.
c Scatter.
d The type of film.
a Definition.
b Contrast.
c Both a and b.
d Exposure time.
a 1.0.
b 2.0.
c 3.0.
d 4.0.
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End Assessment
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a 21 wires.
b 20 wires.
c 19 wires.
d 18 wires.
a 2.00%.
b 1.66%.
c 2.66%.
d 1.90%.
51 In x-ray radiography which of the following factors does not affect half
value thickness?
a 2.
b 3.
c 4.
d 5.
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a Oxidised developer.
b Lack of agitation during development.
c Exposure to light during development.
d Fixing film for too long at too high a temperature.
a Porosity.
b Slag inclusion.
c Lack of penetration.
d Heat affected zone crack.
58 One way to control root penetration in a single sided butt weld is to:
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End Assessment
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1 31
2 32
3 33
4 34
5 35
6 36
7 37
8 38
9 39
10 40
11 41
12 42
13 43
14 44
15 45
16 46
17 47
18 48
19 49
20 50
21 51
22 52
23 53
24 54
25 55
26 56
27 57
28 58
29 59
30 60
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Answers to Self Assessment Questions
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1 2 3 4 5 6 7 8 9 10
C B B A
1 2 3 4 5 6 7 8 9 10
D A C B
1 2 3 4 5 6 7 8 9 10
A D A C B C
1 2 3 4 5 6 7 8 9 10
D B C
1 2 3 4 5 6 7 8 9 10
C C B D B C B A D A
1 2 3 4 5 6 7 8 9 10
A C B C C A D B A B
11 12 13 14 15 16 17 18 19 20
B D
1 2 3 4 5 6 7 8 9 10
A B C D D D C D D D
1 2 3 4 5 6 7 8 9 10
D B D C A C D B A D
11 12 13 14 15 16 17 18 19 20
D B B A C C B
Section 9 Sensitivity
1 2 3 4 5 6 7 8 9 10
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Answers to Self Assessment Questions
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C D B A C C A
Section 10 Radiographic techniques (for welds in plate and pipe)
1 2 3 4 5 6 7 8 9 10
D C A B B A D D A C
1 2 3 4 5 6 7 8 9 10
B A B D D A D A A A
Section 12 Localisation
1 2 3 4 5 6 7 8 9 10
B C A
1 2 3 4 5 6 7 8 9 10
C B D
1 2 3 4 5 6 7 8 9 10
D D C
1 2 3 4 5 6 7 8 9 10
D B A
1 2 3 4 5 6 7 8 9 10
A C B C D C C D D B
11 12 13 14 15 16 17 18 19 20
B B AA D A C C A A A
21 22 23 24 25 26 27 28 29 30
D B B D D C A D C B
31 32 33 34 35 36 37 38 39 40
C B A D D D B A C D
41 42 43 44 45 46 47 48 49 50
A A D A A D B D C B
51 52 53 54 55 56 57 58 59 60
C B C B D B D D C B
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Section 9 Sensitivity
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Record Sheet
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Section 12 Localisation
End Assessment
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