Por Point Cloud Point Maunal

Operating Instructions
Automatic Pour Point- and

Cloud Point- Analyzer
HCP 852
Walter Herzog GmbH: Testing Equipment for Petroleum Products

Badstrae 3-5
D-97912 Lauda-Knigshofen, P.O.Box 1241
Germany
Telefax: (+49) (0)9343 / 640-101

Sales department: Telephone: (+49) (0)9343 / 640-0
E-Mail: Sales@Walter-Herzog.com
Service: Telephone: (+49) (0)9343 / 640-181
E-Mail: HSC@Walter-Herzog.com
Automatic Pour Point- and Cloud Point-analyzer HCP852 Combi
The Operations Instructions contain detailed requirements pertaining to the installation and
operation of the equipment described herein. The publishers have endeavored as much as
possible to maintain the manual current, yet errors may not have been entirely eliminated.
This manual may be revised occasionally without any obligation by the manufacturer to
provide advance notice.
We expressly point out that any warranty or liability claims shall be rendered null and
void, should the equipment be used in any other fashion than that described in the
operations instructions given below, or as shown in any subsequent revised documentation.
This manual may not, under any circumstances, be used or copied, partially or in full,
without prior written permission of WALTER HERZOG GmbH.
Operations Instructions: Pour Point as per ASTM D97/IP 15/ISO 3016

Cloud Point in conjunction with ASTM D2500/IP 219/
ISO 3015
Documentation No.: 820-089
Copyright 1994 / 95 WALTER HERZOG GmbH
2 Introduction V5.1D
Table of Contents
Chapter
1.0 Introduction................................................................................................................... 7
2.0 Technical details............................................................................................................ 9
3.0 Analyzer Unit HCP 852 .............................................................................................. 11
4.0 Ordering information and Accessories: .................................................................... 13

4.1 Ordering information ............................................................................... 13
4.2 Accessories: ............................................................................................. 14
5.0 Equipment Start Up ................................................................................................... 17

5.1 General .................................................................................................... 17
5.2 Connecting the HCP-852 to a printer ...................................................... 18
5.3 Connecting several HCP-852s to one printer .......................................... 18
5.4 Zero Adjustment of The Measuring Sensor ............................................ 20
6.0 Operation ..................................................................................................................... 21

6.1 General .................................................................................................... 21
6.2 Keyboard and display .............................................................................. 21
7.0 Start of a Pour Point Analysis ................................................................................... 23

7.1 General .................................................................................................... 23
7.2 Input Sample Number.............................................................................. 23
7.3 Program Selection ................................................................................... 24
7.4 Expected Pour Point ................................................................................ 24
7.5 Safety Query: Start Test ?........................................................................ 25
7.6 Starting the test ........................................................................................ 25
7.7 Terminating the test ................................................................................. 25
7.8 Pour Point Measuring Method................................................................. 26
7.9 Pour Point, LFP, Printing & Data Transfer ............................................. 27
7.9.1 Last Pour Point ......................................................................................... 27
7.9.2 Last Floating Point ................................................................................... 28
7.9.3 Test Status ................................................................................................ 28
7.9.4 Sample and bath temperature ................................................................... 29
7.9.5 Printing..................................................................................................... 29
7.9.6 Data Transfer ........................................................................................... 29
7.10 Overview Program Menu ........................................................................ 31
8.0 Start of a Cloud Point Analysis ................................................................................. 33

8.1 General .................................................................................................... 33
8.2 Input Sample Number.............................................................................. 33
8.3 Program Selection ................................................................................... 34
8.4 Expected Cloud Point .............................................................................. 34
8.5 Safety Query: Start Test ?........................................................................ 35
V5.1D Introduction 3
8.6 Starting the test ........................................................................................35

8.7 Terminating the test .................................................................................35
8.8 Cloud Point measuring method ................................................................36
8.9 Cloud Point, H-CP, Printing and Data Transfer ......................................37
8.9.1 Last Cloud Point .......................................................................................37
8.9.2 H-CP: Cloud Point with high accuracy ....................................................37
8.9.3 Test Status ................................................................................................38
8.9.4 Sample and bath temperature ...................................................................38
8.9.5 Printing .....................................................................................................38
8.9.6 Data Transfer ............................................................................................39
8.10 Overview Program Menu .........................................................................41
9.0 Parameter program.....................................................................................................43

9.1 General .....................................................................................................43
9.2 Password ..................................................................................................43
9.3 Program selection and standard/non-standard test procedure ..................44
9.4 Language selector: German / English ......................................................45
9.5 Temperature unit: C / F.........................................................................45
9.6 Calibration of the PT 100 sample thermometer .......................................45
9.7 Calibration of the bath thermometer ........................................................46
9.8 Preheat temperature .................................................................................46
9.9 Final Test Temperature ............................................................................46
9.10 Expected Pour Point and Cloud Point ......................................................46
9.11 Start temperature before the expected result ............................................47
9.12 Initial test temperature .............................................................................47
9.13 Test interval .............................................................................................48
9.14 Cooling program ......................................................................................48
9.14.1 Step bath .................................................................................................48
9.14.2 Differential bath .....................................................................................49
9.14.3 Linear Bath .............................................................................................49
9.14.4 Linear sample (not yet implemented) .....................................................50
9.15 Parameters for Pour Point detection ........................................................50
9.15.1 Detection level 1 .....................................................................................50
9.15.2 Detection level 2 .....................................................................................50
9.16 Parameters for Cloud Point Detection .....................................................51
9.16.1 Detection factor ......................................................................................51
9.16.2 Detection threshold.................................................................................51
9.17 Video amplification .................................................................................51
9.18 Printer selection .......................................................................................51
9.19 Result printing: standard or expanded ....................................................52
9.20 Result printing automatic or manual ........................................................52
9.21 Data transfer: automatic or manual ..........................................................52
9.22 Acoustic Signal ........................................................................................53
9.23 Changing the password ............................................................................53
9.24 Print parameters .......................................................................................54
9.25 Example of a parameter report:................................................................54
9.25.1 Pour Point parameter ..............................................................................54
9.25.2 Cloud Point parameter ............................................................................56
9.26 Overview parameter program ..................................................................57
10.0 Brief guideline for determination of analyses .......................................................... 61

10.1 Pour Point analysis .................................................................................. 61
10.2 Cloud Point Analysis ............................................................................... 62
11.0 Diagnostic menu .......................................................................................................... 63

11.1 General .................................................................................................... 63
11.2 R-min/R-max ........................................................................................... 64
11.3 Sample and bath temperature .................................................................. 64
11.4 Alcohol and circulation temperature ....................................................... 64
11.5 Temperature of an external thermometer ................................................ 64
11.6 Measuring values of the quadrants .......................................................... 65
11.7 Display of tilt angle and delay period...................................................... 65
11.8 Gray values of recorded picture .............................................................. 65
11.9 Calculation of curves ............................................................................... 66
11.10 Magnetic valve for cooling ...................................................................... 66
11.11 Magnetic valve for circulation................................................................. 67
11.12 Bath heating ............................................................................................. 67
11.13 Illumination of sample surface ................................................................ 67
11.14 Buzzer ...................................................................................................... 68
11.15 Lift-motor ................................................................................................ 68
11.16 Tilting motor............................................................................................ 69
11.17 Seeking the zero point of the measuring head ......................................... 69
11.18 Display of internal instrument data ......................................................... 70
11.19 Display of the clock mode ....................................................................... 70
11.20 Setting the date ........................................................................................ 71
11.21 Setting the clock ...................................................................................... 71
11.22 Herzog Token Ring (HTR) ...................................................................... 71
11.23 Software-Versions ................................................................................... 72
11.24 Overview diagnostic program ................................................................. 73
12.0 Messages ...................................................................................................................... 77
13.0 Survey of the design of the HCP-852 ........................................................................ 83

13.1 Thermometer positions ............................................................................ 83
13.2 Power supply and fuses ........................................................................... 83
13.3 Electronic components, top view ........................................................... 84
13.4 Electronic components, side view left ................................................ 85
13.5 Electronic components, side view right............................................... 86
14.0 Maintenance and calibration of the HCP 852 .......................................................... 87

14.1 General .................................................................................................... 87
14.2 Calibration of PT 100 .............................................................................. 88
14.3 Testing: Automatic Pour Point determination ........................................ 89
14.4 Testing: Automatic Cloud Point determination ...................................... 89
14.5 Testing: Video Unit ................................................................................. 89
14.5.1 Check of Image Change: ........................................................................ 89
14.5.2 Function Test: ........................................................................................ 90
15.0 Serial output of the HCP-852 .....................................................................................91
16.0 Spare parts for analyzer HCP 852 .............................................................................93

16.1 Recommended spare parts for appr. 2 years of operation ........................93
16.2 Other spare parts ......................................................................................95
16.3 Configuration of the Measurement Unit ................................................100
16.4 CPU with keyboard and display controller 607-252..............................101
16.4.1 Configuration Master/Slave .................................................................101
16.4.2 Configuration Display controller..........................................................101
17.0 Hardware documentation .........................................................................................103

17.1 Views of parts for the HCP 852 .............................................................103
1.0 Introduction
The measurement of the flow behavior of oil when subjected to different temperatures is
carried out using ASTM D 97. (Standard Test Method for Pour Point of Petroleum
Products).
When manually determining the pour point, an oil sample is poured into a test glass which
is heated to 45C and then cooled down in several successive steps in the cooling bath.
When the test temperature is 9K above the anticipated pour point, the test glass containing
the sample is taken from the cooling bath and any condensating moisture is wiped away
with a clean towel, while, at the same time, the glass is held at an angle. Should, at any
time, there be motion on the surface, the test glass is returned to the cooling bath for
continued cooling. This total process must be carried out with great care and should be
concluded within 3 seconds. After every successive cooling up to 3K this particular
procedure should be repeated until the test glass can be held for 5 seconds in a horizontal
position without setting the oil in motion. Consequently, the results of these manually
determined pour points are influenced by thermal antecedents, as well as prior mechanical
treatment and flow point reformers within the sample itself. Hence, the test results in many
cases may turn out to be extremely inaccurate.
With the Herzog Automatic Pour Point Analyzer Unit HCP 852, all test samples are treated
as if they were analyzed manually in accordance with the ASTM D97 standard method.
The HCP 852 features a robotic lever which handles the removal, tilting and replacing of
the sample back to the cooling bath. While doing so, the test sample surface is carefully
monitored by video camera in order to detect any motion. Should the camera recognize
motion, the lifting and tilting modes will be terminated and the standard test glass will be
returned into the cooling bath. In the process the surface of the sample is subjected to video
camera scrutiny for any detection of motion. In the event that the camera detects motion,
the lifting and tilting process is interrupted which will cause the standard test glass to be
returned into the cooling bath. At the moment the test glass is held five seconds at a 90
angle without causing the slightest motion to occur at the samples surface, the
corresponding temperature is recorded and that temperature helps to determine the pour
point (3K will be added to the temperature as measured so that the result can be listed as a
final pour point).
The motion detected on the surface of the sample is not uniform in every case. A manually
conducted pour point determination which the laboratory technician observes scans the
entire sample surface for possible motion to occur. A determination via automatic
Analyzer equipment, this observation is carried out with a video camera. In comparison to
other Analyzer equipment utilizing a single beam of light and a photoelectric cell detector,
this clearly provides for solid improvement throughout.
As there are temperature ranges that can be shortened, detection by the HCP 852 in which
the samples are tilted achieves a better solubility by far than the Standard Method (3K
Solubility) is able to deliver. Testing of this method has shown that even solubilities down
to 0.5K were made possible. Deviations from temperature ranges common with the
Standard Method (3K Solubility) are only possible where user-defined programs determine
them (see Chapter 8.3 and 8.10).
The method to determine a Cloud Point is likewise based upon visual examination of the
sample. As the HCP 852 is equipped with all electronic and mechanical requirements, it is
reasonable to suggest that this equipment could likewise be used to measure the Cloud
Point.
Pursuant to ASTM D 2500, the sample is brought to a temperature of 14K above the
anticipated Cloud Point and then its cooled down in several subsequent cycles within the
cooling bath. During the cool down process by graduations of 1K, the sample is hoisted
from the cooling bath, and after testing for cloudiness, is again lowered into the cooling
bath.
In case no cloudiness is detected at any of the respective fixed test steps, the sample is
subjected to switching to the next lower cooling stage (for instance: at a sample
temperature of 10C, the cooling bath is switched from 0C to -17C).
As the sample becomes cloudy, it will still be subject to cooling by about two to three
degrees Kelvin, based upon determinable technical reasons, until the result can be
confirmed. As the equipment enables the laboratory technician to view the sample during
hoisting, a visual screening of the result is made possible.
The result is shown with an accuracy of 1K. Complementary there is shown a second result
(H-CP). The H-CP shows the result with a higher accuracy.
2.0 Technical details
Standards Pour Point: ASTM D 97, D 5950, IP 15, ISO 3016 and JIS K2269
Cloud Point: ASTM D2500, D5771, IP219, IP444, ISO3015, JIS
K2269
Performance Measuring Range: -80 to +50C (-112 to 122F)
Sample Heating: ASTM or user-defined
Sample Cooling: ASTM or user-defined; temperature
steps, constant rate, or delta
temperature
Initial Test Temperature: ASTM or user-defined
Test Frequency: ASTM or user-defined
Optical Detection System CCD Video Camera. Video Composite Signal for black/white
Monitors (e.g. Herzog accessories: Monitor (629-029), Bracket for
monitor (629-030), Cable (627-104)
Configuration Several HCP852 may be connected to one circulation cooler and
one printer
Sample Temperature Temperature display C / F
Measurement Temperature display of sample resistance thermometer Pt 100,
(sample temperature)
C -110...+100, accuracy 0.1C
F -166...+212, accuracy 0.1F
Probe deviation can be corrected by on screen offset calibration of
resistance thermometer.
Auto calibrating thermometer amplifier circuit. Self calibration of the
electronic circuit with integrated, high precision calibration
resistors eliminates temperature and long term drift of the amplifier
components.
Cabinet/Chassis All steel, baked epoxy resin coated: electromagnetic isolation,
solvent resistant. Width only 24 cm (9.5)
Sample Cooling Bath Step Bath(as required by ASTM D97 and D2500):
(jacket) and Heating Sample cooling ramps in defined steps from a -34C base
System temperature to bath (jacket) temperatures of 51C and 67,
ultimately cooling to the final user-defined low temperature. As a
result, switching speed is completely independent of the users
external cooling systems chilling capacity and lowest bath (jacket)
temperature, thus permitting use of a variety of independent
cooling systems.
Differential Bath:
It is possible to program a constant difference between the sample
temperature and the bath (jacket) temperature.
Linear Bath:
The bath (jacket) is cooled at constant rate between 0.5 5 C/min
depending on the cooling capacity of the chiller.
When test is finished:
Automatic heating to the start temperature of the next test.
Display Bright, two lines alphanumeric display
Keyboard/ Pushbuttons Numeric keypad with cursor operation, Start Stop and Menu key.
Mains ON/OFF switch
V5.1D Technical details 9

User Programs 4 total; unit ships with ASTM D97 and D2500 preprogrammed;
2 other programs may be defined by user
Result Documentation Test results are displayed on the display and can also be output
automatically or on demand to an optional companion printer or
computer system.
Normal report:
Includes the Instrument Name and ID, Sample ID and Name, Date
and Time, Pour Point and Last Floating Point Result or Cloud Point
and High-Resolution CP Result, Measurement Program,
Preheating Temperature and Test Start Temperature.
Extended test report:
prints a table with: Test Temp. in 1C steps, Time between Suction
Cycles, Suction Time, Max. Sample Temp. after Suction Cycle,
Time to reach the Max. Sample Temp., Sample flow out Time.
Data Memory The last test result is permanently stored in the analyzer
Communications Serial transmission of all data with selectable field delimiters. Local
area network (LAN) compatible, via RS232 serial link.
Printer Any printer with CENTRONICS interface and ASCII character set
may be used.
Calibration The temperature probes for sample and bath temperature can be
offset adjusted. The vacuum system can be calibrated in two
points. The position of the test head can be adjusted.
Password Security Protection against unauthorized change of parameters
Diagnostics All mechanical and electrical components are permanently
checked by the instrument. About 30 faulty conditions are
automatically detected such as: Broken thermometers, light
barriers defective, cooling or heating errors etc.
However all components can be manually enabled and disabled in
the Diagnostics mode of the HCP852.
Alarm Functions Automatic detection of method or safety violations.
Utility Requirements Electrical: Switch able 230/115 V 10%; 50/60Hz; 350W
External Cooling Unit: Circulating, low temperature chiller capable
of operating at a minimum of 20C below the lowest temperature
range. A single chiller may be cable of connection to multiple
Herzog instruments. Chillers and an isolated coolant distribution
system is available as accessories
Cabinet Dimensions 235 (W)x 420 (D)x 590 (H) mm;
9.5 x 196.5 x 23.2 inches
Weight 25 kg (55 pounds)
Attention: When the instrument is connected to the cooling system, do not close the shut
off valves of the supply pipe and the return pipe from the test unit to the main
cooling system. Otherwise, while warming up there might be an overpressure
that will damage the cooling bath in the instrument.
10 Technical details V5.1D

3.0 Analyzer Unit HCP 852
The ASTM D97 is an empirical standard method in order to properly determine the Pour
Point. Therefore, it is extremely important that the standard programs of the HCP 852
Analyzer Unit reflect as closely as possible any of the manually derived Standard Methods.
The standard programs shall cover the systems theory standpoint, as well as the ensuing
process itself.
The HCP 852 Pour Point Analyzer Unit is a totally closed-loop system. For cooling
materials to be sampled in a test flask, an independent cooling system is required.
Basic equipment for the Analyzer Unit includes a sample cooling bath, electronic
components, as well as an indicator unit.
The upper section of said system consists of a mechanical unit equipped to hoist, and
thereby remove, the test glass from the cooling bath and tilt it to a maximum of about 90
(measuring head), plus a stationary video camera. Furthermore, it includes two stepping
motors and the electronic circuitry required to function as a motor controlling device.
Immediately beneath the video camera mount a special clamping device is installed for
positioning the testing flask. To determine the sample temperature, a Resistance
Thermometer (PT-100) is placed within the test glass proper.
As a basis to determine the Cloud Point, ASTM D 2500 is applicable. It is extremely

important that the Standard Program of the HCP 852 to determine the Cloud Point of a
manually derived Standard Method should be well-rounded with regard to equipment
features, as well as the system processes per se. However, several compromises had to be
made because the equipment evolved into multi-purpose system units.
The details are highlighted as follows:
The thermometer must be placed at the bottom of the test glass when determining the
Cloud Point, which is in contrast to determination of the Pour Point, which calls for
thermometer positioning directly under the surface of the sample. The thermometer of the
HCP 852 is a rigid configuration mount which causes the Cloud Point determination to
take place in a shortened sample vessel. Consequently, the sample vessel is placed higher
inside the cooling bath than is usually stipulated by standard procedure. However, a series
of experiments have shown that this has practically no influence whatsoever upon the
result. To guarantee a better determination of the Cloud Point, said shortened sample
vessel is furnished with a reflector-lined bottom. Again, there is no influence detected on
the end result. The (inside) bottom of the test glass is covered with a layer of lacquer,
which proves to be inert against cleaning agents such as benzine. With solvents like
acetone, however, the lacquer is less resistant.
A spare parts listing for the HCP 852 and accessories are located in Chapter 0, which also
includes all corresponding parts numbers.
V5.1D Analyzer Unit HCP 852 11

12 Ordering information and Accessories: V5.1D

4.0 Ordering information and Accessories:
4.1 Ordering information
Order No. Description Picture

08521-000-00 HERZOG automatic Pour- and Cloud Point
tester model HCP 852acc. to ASTM D 97, ISO
3016, DIN 51 597, IP 15 - for Pour Point-
determinations from +20 to -60 degree C., and
in correlation to ASTM D 2500, ISO 3015 from
+35 to -60 C. f.Cloud Point determinations.
Complete and ready for use, however without
circulation cooler. For 230/115 V (switch able)
+/-10%, 50/60 Hz.
The unit is supplied complete with:
1 x 820-089 Instruction manual
1 x 101-052 Power cord with Continental
European IEC/DIN plug.
2 x 501-143 Test jar for CP determination
2 x 501-157 Test jar for PP determination
1 x 385-072 Verification gauge for video
signal
1 x 412-221 Set of hexagonal wrenches:
1.5; 2; 2.5; 3; 4; 5mm.
1 x 626-082 Connection cable for HTR
communication, instrument to
instrument, short, 0,8 m
V5.1D Ordering information and Accessories: 13

4.2 Accessories:

08284-000-00 Circulation cooler
Continuous cooling by working with max. cooling
capacity, depending on load, up to -80C.
With air-cooled compressors, floor-mounted unit
with grips and 4 castors.
Temp-adjustment/display: digital red LED
Display resolution: 1C
Flow rate: 22 l/min. max.
Max. feed pressure: 0,5 bar
Bath Volume: 11 ltr. appr.
Cooling capacity: 450 W at 20 C
90 W at -80 C
Cooling medium: R 404 a/TP5R3
-free of CFC-
Dimensions (WxDxH): 50x62x75 cm
Voltage: 230V, 50Hz,
Power: 1,1 kW max.
Power cord with Continental European IEC/DIN
plug.
301-047 Silicone connection hose in8x2mm with No Picture
out 32mm Armaflex isolation for connection of
cooler to viscometer (2 m)
346-037 Cooling liquid distribution system for 1 HCP
842/852 measuring place comprising of
mechanical filter with hose connector, pipe with
mechanical valve and exit with screw able
connector and reflux-pipe with screw - connector,
all insulated against loss of coolant. End of tubes
are equipped with removable stops (for extension
to other measuring places). Total length appr. 27
cm
346-036 Cooling liquid distribution system for additional
measuring positions or end tubes within the MP
842/MP 852 system comprising insulated flow- and
reflux pipe with screw connectors, stop and
mechanical valves for the exits. Total length appr.
27cm.


629-029 Video Monitor to watch the pour and cloud signal
of the video camers, (), ()
629-030 Turn-table for monitor
627-104 Video signal cable from HCP852 to monitor 629-

029
101-214 Matrix dot printer, 40 columns, using endless

paper roll of 76mm width, Centronics interface,
Dimensions: 156mm (W) x 248 mm (D) x 132
mm (H).110V to 230 VAC, 24W,
Power cord with Continental European IEC/DIN
plug.
Centronics Printer cable 626-029 not included
101-184 Ink ribbon for Matrix dot printer 101-175 and 101- No Picture
176
101-212 Ink ribbon for Matrix dot printer 101-214 No Picture
101-185 Paper rolls (10 pcs.) for Matrix dot printer
101-175, 101-176 and 101-214
76 mm x 60 x 12mm
101-137 Ink jet printer with English and German manual,

ASCII compatible, for 100 230VAC, Power cord
with Continental European IEC/DIN plug.
V5.1D Ordering information and Accessories: 15


626-029 Printer connection cable (Centronics) to HCP842.
This is a special wired cable for certain Herzog
instruments only.
626-082 Connection cable for HTR communication,

instrument to instrument, short 0,8 m
101-194 Pt100 probe simulator box 40 to +100C with 6

fixed temperatures. Including 4-wire connecting
cable 626-122 with Herzog Pt100 connector

5.0 Equipment Start Up
5.1 General
CAUTION:
SWITCH ON YOUR HCP 852 AFTER MAKING SURE THAT ALL RETAINING
CLIPS USED DURING TRANSPORTATION ARE REMOVED!
For the purpose of safe transportation, your HCP 852 Analyzer has two retaining angle
brackets. These devices must be removed prior to initiating the Start Up procedures for
this equipment.
IF THESE RETAINING CLIPS ARE NOT REMOVED, SEVERE DAMAGE TO

YOUR HCP 852 UNIT MAY RESULT.
1. Remove the two screws on the top of the protective cover of the vertical unit.
2. Take off the protective cover.
3. Remove the transport safety angles from the two carriages with an allen wrench.
4. Replace the protective cover.
Suggestion: Save the retaining clips and safety screws in case your HCP 852 has to
be moved again in the future.
Suitable Location:
Place the HCP 852 Analyzer on top of a heavy-duty lab table and keep out of the
sunlight; sunlight can severely hamper motion detection by the sensitive optics of the
video camera system.
Cooling:
Proper cooling of the test material requires an independently-dedicated refrigeration
system Hence, the refrigeration temperature must be responsive to a temperature setting
which needs to be at least 10C under the lowest required cooling bath range of the
HCP 852. If, for instance, a required cooling range of -51C is to be used, the cooling
system, in turn, would be adjusted to a minimum of -61C; lower than that would be
even better. A normal case requires the adjustment of the refrigeration system be at the
lowest temperature. The cooling system hoses will in all cases be connected to the
respective connectors, such as cooling in/out located on the back-side of the HCP 852
Unit.
Caution:
During initial start up procedure after connection to the cooling system, it is strongly
recommended that the coolant liquid level on the refrigerating machine is routinely
checked!
V5.1D Equipment Start Up 17

Insulation of Refrigeration Hoses:

To assure proper insulation of the silicon-hoses attached to the HCP 852 Analyzer Unit,
we recommend a special layer of foam-insulation with a minimum of 2 cm, more
appropriate would be a total wall thickness of 4 cm. Several HCP 852 Units may be
connected to one single refrigeration system, where the connecting point for each unit to
the cooling system would be in parallel. As to how many units might be considered for
such attachments, this depends primarily upon the performance factors of your cooling
system, as well as the temperatures to be measured with regard to the Pour Point and
Cloud Point, respectively. When connecting several HCP 852s to one system, it is
essential to make the insulating hose connections as short as possible in order to avoid
cooling line losses.
If longer hoses are needed, that has to be taken into consideration in setting the
refrigerator temperature.
Power Supply:
Caution: Remove plug from receptacle prior to switching to the rated voltage!
The HCP-852 can run on 230 V or 115 V alternating current. The voltage required is
selected at the power box on the back of the instrument. Pry the box cover up with a
screwdriver and set the switch to 230 V or to 115 V. The fuses are behind the arrows
below the switch. Please insert the fuses to match the line voltage selected (see
Drawing PP 3). Then close the cover again and connect the HCP-852 to the power line.
5.2 Connecting the HCP-852 to a printer
A printer can be connected to the Pour Point system to print the measurements. A
standard printer with a parallel printer connection and the expanded IBM character set
can be used. Use Cable No. 626-029 to connect the printer to the parallel interface on
the back of the HCP-852. (The Centronics cables usually used for PC do not fit the
HCP-852 printer connection.)
5.3 Connecting several HCP-852s to one printer
If several test instruments (up to 16 HCP-852s) are to be connected to one printer, they
are connected using the supplied cable 626-082 to the HTR connector (on the back of
the test instrument).
18 Equipment Start Up V5.1D

Unit 1 Unit 2 Unit 3
Cable No. 626-082 Cable No. 626-082
Master Slave Slave
Cable No. 626-029
Printer
Be sure that the printer is connected to the master test instrument and that the other
instruments are set to be slaves.
Also, each instrument must have a different instrument number (instrument numbers
0-15).
Coding the instruments

When shipped, the instruments are coded as Instrument 1 and Master. To change the
coding, disconnect the HCP-852 from the power supply and open the right side of the
housing. The D.I.L switch (S1) and the wrap pegs (WP1 and WP2) are on board No.
607-063 or 607-252 beside the 9-pin connector (see the drawing in the hardware
documentation).
INSTRUMENT NUMBER
0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
S 1.1 on off on off on off on off on off on off on off on off
W 1.2 on on off off on on off off on on off off on on off off
I 1.3 on on on on off off off off on on on on off off off off
T 1.4 on on on on on on on on off off off off off off off off
C 1.5 on on on on on on on on on on on on on on on on
H 1.6 on on on on on on on on on on on on on on on on
1.7 on on on on on on on on on on on on on on on on
1.8 X X X X X X X X X X X X X X X X
Switch 1.8 X = off = Master

Switch 1.8 X = on = Slave
Comment:
If an instrument is to be changed from Master to Slave (or the reverse) the
jumper must also be changed appropriately. To work as a Master the 3 jumpers
must connect the WP1 pegs. To work as a Slave they must connect the WP2 pegs.
Make sure that only one of the networked instruments is coded as a Master.
V5.1D Equipment Start Up 19

5.4 Zero Adjustment of The Measuring Sensor
The motors used for the removal and tilting actions of the test glass are stepping motors.
Each of these motors is driven by a micro-controller. Zero adjustment of the sensor is
accomplished during manufacturing, and is to be repeated only in case of mechanical
changes involving the linear unit component (for instance: repair) or in the event of a
loss affecting all zero adjustments (i.e., checksum errors in Master. For details
pertaining to zero adjustment, refer to Chapter 11.15).
20 Equipment Start Up V5.1D

6.0 Operation
6.1 General
Before turning the HCP-852 on, the line voltage, frequency, and power consumption
must be compared with the values on the line connection and set there if necessary (see
also Chapter 5.1). Then the power cable is plugged in and the instrument is turned on
with the power switch on the front.
6.2 Keyboard and display
The front of the instrument has a two-line display, a numerical key field, various
function keys, and a display of the selected menus and programs with indicator lights.
Display Menu/Program Display
HERZOG MP 842
Version 1.00
Menu
Key
Start
Key
Stop
Key
On / Off Left Arrow
Numeric Keyboard
V5.1D Operation 21
When the switch is actuated, the monitor display will show the appliance type, the
applicable number, as well as the current software version used.
HERZOG M P-852 1
Version: 1.00
Shown below is the menu/program selection window located on the right side of the
main panel. The currently selected menu or program is displayed.
PROGRAM
DIAGNOSTIC
PARAM ETER
M ESSAGES
PROGRAM 1
PROGRAM 2
PROGRAM 3
PROGRAM 4
Program Menu item to start a Pour Point or Cloud Point Analysis

(see Chapters 6 or 7, below).
Diagnostics When selected, this menu enables the user to test various appliance
functions. During a Pour Point Analysis, this particular function cannot be
called up. (see Chapter 11.0).
Parameter Various parameters which control the program can be changed here
(see Section 7).
Messages In case of an error during an analysis (for instance: Cooling problems) the
test will be terminated and an appropriate error message will appear. This
menu will be of assistance in such cases (see Chapter 12.0).
The program change between menus will involve the M key

Program Program Program Program
M M M M
Diagnostic Diagnostic Diagnostic Diagnostic
Parameter Parameter Parameter Parameter
Messages Messages Messages Messages
Furthermore, the number of the program which is currently on test run and being carried
out will be displayed.
22 Operation V5.1D
7.0 Start of a Pour Point Analysis
7.1 General
For proper determination of a Pour Point Analysis, it is mandatory that the taller
test glasses without the reflective base be used ! Otherwise, the test material might
be poured down the measuring sensor as the vessel tilts!
As the HCP 852 is actuated, the display will show the model no. of the appliance and
the software version pertaining to the selected Master Program. Immediately following,
a status message Ready appears along with the last entered test number.
Ready 1
S. Nr.: SAMPLE 1520
Using the key, a particular submenu can be called up which enables the user to
obtain the previous (last) result, as well as have access to the Print and Data
Transfer functions (see Chapter 7.9 for the Pour Point and Chapter 8.9 for the Cloud
Point).
Using the START key, the next page will appear.
CAUTION: This causes the measuring sensor component to move to the uppermost
position.
7.2 Input Sample Number
It is now essential that the filled test glass, containing the test prepared in accordance
with the ASTM code, be fitted into the glassholder. After placing the test glass in its
holder, Do Not exert additional pressure upon the adjustment lever of the glassholder
because such action could easily break the vessel.
Input Sample Number
S. Nr.: SAMPLE 1520
At this point alphanumeric characters may be entered. Numbers are entered directly,
letters and special characters via the or keys while scrolling forward or backward
through the alphabet. Such possible characters are either 0..9, letters A..Z, or
special characters such as [,] and \.
V5.1D Start of a Pour Point Analysis 23

As numbers are entered, the cursor within the display window will move automatically;
other entries require the key be used for information movement. To change
characters, the cursor, in conjunction with the corresponding key, is guided to the
desired position, so as to overwrite with a new character. If a character needs to be
erased, just overwrite using a period [.].
Using the START key, advance to the next page.
7.3 Program Selection
Four programs with different parameters can be stored in the HCP-852. One of these
programs is selected by entering the program number (1, 2, 3, or 4) on this page of the
display. We recommend making the standard Pour Point program number 1, the
standard Cloud Point program number 3.
Program 0 specifies the parameters with which the last test was started.
Furthermore, there will be an indication whether the program had been utilized for
determination of measurements for Pour Point or Cloud Point. (see Chapter 9.3).
Program 1
Pour Point
However, this particular page also carries a submenu which can be accessed using the
key. This submenu allows for changes to be made for preheat and test-start up
temperatures (see Chapter 7.10).
Caution: When pressing the STOP key, all changes made within the submenu will
be lost permanently; all values will revert to parameters stored by the selected program.
When pressing the START key, the page will advance to Expected Pour Point.
7.4 Expected Pour Point
As an expected Pour Point is entered, the system automatically determines the correct
value of the parameter Start before expected result. This is added to the Pour Point
and thus reveals the test-start temperature. According to the standard Parameters, the
added value equals 9 K.
If no expected Pour Point is entered, the procedure will start with the hoisting and tilting
modes of the test sample in accordance with a pre-determined value parameter known
as the test-start temperature (see Chapter 9.11).
Expected Pour Point

C
24 Start of a Pour Point Analysis V5.1D

When pressing the START key, the page changes and displays Start Test?.
7.5 Safety Query: Start Test ?
Start Test?
Testing does not begin immediately. Press the STOP -key if you need to interrupt the
starting sequence. By pressing the STOP -key, the HCP 852 will return to the page that
signals Ready.
Caution: Pressing the STOP key will cause deletion of all changes made within the
submenu and return to the values of parameters entered in the selected
program. This will also delete all entered values pertaining to the expected
Pour Point.
With the START key, testing will be initiated.
7.6 Starting the test
After having started the test, the sample will be inserted into the cooling bath. Shortly
thereafter, a status message cooling or heating appears, depending primarily on the
preheat temperature previously entered into the respective parameters.
cooling 20.3 C
S. Nr: SAMPLE 1520
7.7 Terminating the test
The test can be terminated at any time with the STOP key. When this key is pressed
for the first time a question whether the test should really be stopped appears.
Stop Test ?

If the STOP key was pressed accidentally, then respond to the Stop Test ? question
with the START key. The test continues with display of the current status.
If the test is really to be terminated, the STOP key must be pressed once more. If the
final test temperature is above the current sample temperature, it is reheated before the
test is finally terminated.
stopped 19.1 C
S. Nr. SAM PLE 1520
7.8 Pour Point Measuring Method
Initially, the sample in the test glass is heated to the pre-determined temperature. When
it reaches it, the cooling phase is set in motion.
The sample temperature is measured during the cooling cycle. In conjunction with the
ASTM Standard Measuring Method, a total of 7 steps of pre-programmed temperature
regulations will take place within the cooling bath. The cooling bath temperature will be
gradually lowered. The HCP 852 also allows programming of customized temperature
parameters, such as:
Differential regulation: Cooling bath temperature to be regulated via

differential temperature to the actual sample temperature.
Degradation of cooling bath temperature to be linear (C/Time).
Degradation of sample temperature to be linear (C/Time).
Option currently not available.
Hoisting, as well as tilting of the sample, takes place based on pre-determined

temperatures and at pre-set temperature ranges. As motion is detected on the liquid
surface area by the video camera, prior to the sample being tilted to an angle of approx.
90, the test glass is returned to the cooling bath and the cooling process continues.
At a 90 -tilting angle the sensitivity factor for video detection increases. With no
surface motion detected within a 5 second period of time, Pour Point calculation is
based upon the sample temperature. The temperature range is added and the subsequent
total result is the established Pour Point.
After establishing the Pour Point, the sample is heated to a previously established final
temperature level (see Chapter 8.9). As this particular temperature is reached, the test
vessel is hoisted out of the cooling bath and a buzzer sounds. On pressing the STOP
key, the buzzer turns off.

In accordance with ASTM Standard Method D97, the sample material must be observed
at temperature ranges of 3K. This implies that the temperature solubility for Pour Point
determination lies at 3K. In order to achieve higher temperature solubility a series of
smaller temperature ranges may be programmed (see Chapter 8.12). This could result in
deviations to the values established by ASTM D97. Such deviations could be attributed
to intensified motions of the sample during hoisting and tilt which, subsequently,
appears to change the kinetics caused by crystallization of paraffins. This, in turn, could
lead to varying Pour Point results.
Unit HCP 852 was developed so as to obtain a refined temperature solubility state,
without deviating from ASTM D97-type testing. Herzog calls this value the Last
Floating Point (LFP). The HCP 852 calculates the LFP via numeric analysis based on a
previous motion occurrence on the test surface (i.e., size and velocity of the ripples
caused by the sample during hoisting and tilting of the sample). The LFP is delivered
automatically by the HCP 852, along with a solubility of 0.1K.
Upon completion of analysis with the HCP 852, the LFP is displayed by pressing the
-key.
7.9 Pour Point, LFP, Printing & Data Transfer
As the HCP 852 attains the status mode Ready, a submenu is visible which displays
the LFP and from where the printing, as well as data transfer, functions can be executed.
It is also possible to again display the results obtained from the last Pour Point analysis
again. Pressing the key changes into this submenu. If there is an error message, it
will be shown on the first display page of said submenu, along with the termination
temperature of the test. If there is still a test result to be determined, such result will then
be displayed within the submenu.
7.9.1 Last Pour Point

At this point, the last determined pour point result will be displayed. This result,
along with the test data contained therein, will be retained in memory, even after
the appliance is turned off.
Caution: When a new analysis is started, all data will be erased, even if the
newly started test is immediately interrupted.
POUR POINT -21 C

S. Nr.: Sample 1520
Data entries are not allowed at this point. When pressing the -key, the next
available page of the submenu appears.

7.9.2 Last Floating Point

On this page, the last determined LFP result will be displayed. This result, along
with the test data contained therein, will be retained in memory, even after the
appliance is turned off.
Caution : When a new analysis is started, all the data is erased, even if the newly
started test is immediately interrupted.
LFP -21,8 C
S. Nr.: Sample 1520
Data entries are not allowed at this page. When pressing the -key, the next
7.9.3 Test Status

Shown on this page are actual status messages, indicating precisely at what stage
of the analysis the appliance is located, either during or after completing an
analysis.
ready 22,8 C
S. Nr.: Sample 1520
Appliance Status Description:
Ready Appliance is ready for a new analysis cycle
Heating Test is complete or interrupted; the sample

is in the process of being heated to test-end
temperature.
Cooling Test in progress; sample is currently cooling
Finished Test completed; Test end temperature
accomplished. This status is equivalent to
the
ready status, however, the test has not been
acknowledged by pressing the START key.
Error Test interrupted by error (See Chapter 5.2
and Chapter 11.0)

7.9.4 Sample and bath temperature

The current sample and bath temperature are displayed on this page.
Sample Bath
+23.2 C +21.0 C
No inputs are possible here. The next page of the submenu is reached with the
key.
7.9.5 Printing
The result of the Pour Point test can be printed automatically at the end of the test,
or manually. Manual printing is started with the key. During data transfer to
the printer the message started is superimposed. Printing can be repeated as
often as desired.
Print ?
Analysis results to be printed in a standard print version only:
HERZOG HCP-852 Instrument Number 1
Sample No. SAMPLE 1520 Date 10.04.94 08:45
Pour Point -21C LFP -22.4C
Program 2
Preheating Temp. 45C Test Start Temp. 0C
Enhanced printer action (from parameter menu) will print all additional messages.
7.9.6 Data Transfer

If the result is to be stored on an external computer (PC), Data Transfer may be
activated from this page by pressing the -key. During Data Transfer the
message started will be briefly superimposed on the display screen.

Data Transfer
However, a terminal program must be started on the external computer system

which will display the characters received:
1ER;PP-852;SAMPLE.1520...;940208124719;-21.0 -22.4 -21.1

Explanation:
1ER: Result from Instrument 1
PP-852: Test Procedure (PP for Pour Point), Instrument type
SAMPLE.1520: Sample number
940208: Date: 8 February 1994
124719: Time test started: 12:47:19
-21.0: Pour Point -21C
-22.4: LFP
-21.1: Test-end Temperature
If a test has been terminated, the temperature at this terminating moment is shown
at the end of this string.
By pressing the -key, the next page of the submenu is available.

7.10 Overview Program Menu
ready 1 Error -8,8 C This Display post only in case of error

S-Nr. TANK 1250
Start Start
Pour Point -6,0 C

Start
LFP -6,9 C
Start
finished
Start Pr-Nr. TANK 1250
Sample Bath
Start -6,9 C 17.0 C
print ?
start printing
Input Sample Number Data Transfer

# num. input Start data transfer
S-Nr. TANK 1250
Start
Program 1
# Program number 0, 1, 2, 3 or 4
Pour Point
Start
Preheating Temp. # num. Input

+45,0 C
Start
Test Start Temp. # num. Input

+ 30,0 C
Start
Expected Pour P.
# num. Input
-12 C
Start
Start Test ? General: Stop will return nto "ready" status
Start
Test has started

32 Start of a Cloud Point Analysis V5.1D

8.0 Start of a Cloud Point Analysis
8.1 General
For proper determination of Cloud Point analysis, use the shortened sample glass
equipped with the reflecting base.
As the HCP 852 is actuated, the display will show the model no. of the appliance and
the software version pertaining to the selected Master Program. Immediately following,
a status message Ready appears along with the last entered test number.
Ready 1
S. Nr.: SAMPLE 1520
Using the key, a particular submenu can be called up which enables the user to
obtain the previous (last) result, as well as have access to the Print and Data
Transfer functions (see Chapter 8.9 for the Cloud Point).
Using the START key, the next page will appear.
CAUTION: This causes the measuring sensor component to move to the uppermost
position.
Description of the sample glasses used to determine the Cloud Point:

The bottom part of the test glass is covered with a layer of lacquer which is insensitive
to various cleansing agents, such as cleaning fluid. This layer of lacquer is less resistant,
however, to more aggressive solutions, such as acetone.
8.2 Input Sample Number
It is now essential that the filled test glass, containing the test prepared in accordance
with the ASTM code, be fitted into the glassholder. After placing the test glass in its
holder, Do Not exert additional pressure upon the adjustment lever of the glassholder
because such action could easily break the vessel.
Input Sample Number
S. Nr.: SAMPLE 1520
V5.1D Start of a Cloud Point Analysis 33

At this point alphanumeric characters may be entered. Numbers are entered directly,
letters and special characters via the or keys while scrolling forward or backward
through the alphabet. Such possible characters are either 0..9, letters A..Z, or
special characters such as [,] and \.
As numbers are entered, the cursor within the display window will move automatically;
other entries require the key be used for information movement. To change
characters, the cursor, in conjunction with the corresponding key, is guided to the
desired position, so as to overwrite with a new character. If a character needs to be
erased, just overwrite using a period [.].
Using the START key, advance to the next page.
8.3 Program Selection
Four programs with different parameters can be stored in the HCP-852. One of these
programs is selected by entering the program number (1, 2, 3, or 4) on this page of the
display. We recommend making the standard Pour Point program number 1, the
standard Cloud Point program number 3.
Program 0 specifies the parameters with which the last test was started.
Furthermore, there will be an indication whether the program had been utilized for
determination of measurements for Pour Point or Cloud Point. (see Chapter 9.3).
Program 3
Cloud Point
However, this particular page also carries a submenu which can be accessed using the
key. This submenu allows for changes to be made for preheat and test-start up
temperatures (see Chapter 7.10).
Caution: When pressing the STOP key, all changes made within the submenu will
be lost permanently; all values will revert to parameters stored by the selected program.
When pressing the START key, the page will advance to Expected Cloud Point.
8.4 Expected Cloud Point
As an expected Cloud Point is entered, the system automatically determines the correct
value of the parameter Start before expected result. This is added to the Cloud Point
and thus reveals the test-start temperature. According to the standard Parameters, the
added value equals 14 K.
If no expected Cloud Point is entered, the procedure will start with the hoisting modes
of the test sample in accordance with a pre-determined value parameter known as the
test-start temperature (see Chapter 9.11).

Expected Cloud Point

C
When pressing the START key, the page changes and displays Start Test?.
8.5 Safety Query: Start Test ?
Start Test?
Testing does not begin immediately. Press the STOP -key if you need to interrupt the
starting sequence. By pressing the STOP -key, the HCP 852 will return to the page that
signals Ready.
Caution: Pressing the STOP key will cause deletion of all changes made within the
submenu and return to the values of parameters entered in the selected program. This
will also delete all entered values pertaining to the expected Cloud Point.
With the START key, testing will be initiated.
8.6 Starting the test
After having started the test, the sample will be inserted into the cooling bath. Shortly
thereafter, a status message cooling or heating appears, depending primarily on the
preheat temperature previously entered into the respective parameters.
cooling 20.3 C
S. Nr: SAMPLE 1520
8.7 Terminating the test
The test can be terminated at any time with the STOP key. When this key is pressed
for the first time a question whether the test should really be stopped appears.

Stop Test ?
If the STOP key was pressed accidentally, then respond to the Stop Test ? question
with the START key. The test continues with display of the current status.
If the test is really to be terminated, the STOP key must be pressed once more. If the
final test temperature is above the current sample temperature, it is reheated before the
test is finally terminated.
stopped 19.1 C
S. Nr. SAM PLE 1520
8.8 Cloud Point measuring method
Initially, the sample in the test glass will be heated to the pre-determined temperature.
Upon reaching it the cooling phase is set in motion.
The sample temperature is measured during the cooling cycle. In conjunction with the
ASTM Standard Measuring Method, cooling is achieved via step-by-step cooling
module action within exact pre-determined temperatures. As an alternative version to
the above, however, these temperatures may be changed, the cooling module may be
linear, or cooling may take place adhering to a constant differential.
Hoisting of the sample takes place based on pre-determined temperatures and at pre-set
temperature ranges. If the video camera shows no definite sample turbidity, the test
glass returns to the cooling module and the cooling process continues.
If turbidity is detected, measurement continues for an additional 3K in order to

determine the exact turbidity point. The determined value will then be displayed as the
Cloud Point.
After establishing the Cloud Point the sample is heated to a previously established final
temperature level (see Chapter 9.9). When this particular temperature is reached, the test
vessel is hoisted out of the cooling module and a buzzer sounds. By pressing the STOP
-key the buzzer is turned off.
Pursuant with the ASTM Standard Method D 2500, the sample material must be
observed during temperature ranges of 1K. This implies that the temperature solubility
for a Cloud Point determination lies at 1K. Internal calculations obtained from
measuring data of the Cloud Point, however, will be determined more precisely to 0.2K.
In order to achieve a still higher temperature solubility, even smaller temperature ranges

can be programmed (see Chapter 9.12). This may lead to deviations from the values
determined per ASTM D 2500.
8.9 Cloud Point, H-CP, Printing and Data Transfer
When the HCP 852 attains the status mode, Ready, a submenu is accessible which
displays the last determined result and where printing and data transfer functions can be
executed. By pressing the -key, this particular submenu changes. If there is an
Error message, it will be shown on the first display page of said submenu, along with
the termination temperature of the test. If there is still a test result to be determined,
such result will then be displayed within the submenu.
8.9.1 Last Cloud Point

At this page, the last determined Cloud Point result is displayed. This result,
along with the test data contained therein, will be retained in memory, even
though the appliance is turned off.
Caution: As a new analysis is started, all of the previous data is erased, even if
the new test is immediately interrupted.
Cloud Point -21 C

S. NR.: Sample 1520
Data entries are not possible at this page. By pressing the -key the next
8.9.2 H-CP: Cloud Point with high accuracy

At this page, a result with a better accuracy is shown.
Caution: As a new analysis is started, all of the previous data is erased, even if
the new test is immediately interrupted.
H-CP -20,4 C
S. NR.: Sample 1520
Data entries are not possible at this page. By pressing the -key the next

8.9.3 Test Status

Shown on this page are the actual status messages, indicating precisely that the
appliance is at a particular stage of the test, either during or after completion of an
analysis:
Ready 22.5 C
S. Nr.: Sample 1520
Appliance status: Description:

Ready Appliance is ready for a new analysis cycle.
Heating Test is complete or interrupted; the sample is in process
of being heated to test-end temperature.
Cooling Test in progress and the sample is currently cooling.
Finished Test complete, Test end temperature accomplished. This
status is equivalent to the ready status, however, the test
has not been acknowledged by pressing the start key.
Error Test interrupted by error (see Chapter 5.2 and Chapter
11.0).
Data entries are not allowed at this time. By pressing the -key, the next
8.9.4 Sample and bath temperature

The current sample and bath temperature are displayed on this page.
Sample Bath
+23.2 C +21.0 C
No inputs are possible here. The next page of the submenu is reached with the
key.
8.9.5 Printing
The result of the Cloud Point test can be printed automatically at the end of the
test, or manually. Manual printing is started with the key. During data transfer
to the printer the message started is superimposed. Printing can be repeated as
often as desired.

Print ?
Analysis results to be printed in a standard print version only:
HERZOG HCP-852 Instrument Number 1
Sample No. SAMPLE 1520 Date 10.04.94 08:45
Cloud Point -21C H-CP -22.4C
Program 2
Preheating Temp. 20C Test Start Temp. 0C
Enhanced printer action (from parameter menu) will print all additional messages.
8.9.6 Data Transfer

If the result is to be stored on an external computer (PC), Data Transfer may be
activated from this page by pressing the -key. During Data Transfer the
message started will be briefly superimposed on the display screen.
Data Transfer
However, a terminal program must be started on the external computer system

which will display the characters received:
1ER;CP-852;SAMPLE.1520...;940208124719;-21.0 -20.4 -21.1
Explanation:
1ER: Result from Instrument 1
CP-852: Test Procedure (CP for Cloud Point), Instrument type
SAMPLE.1520: Sample number
940208: Date: 8 February 1994
124719: Time test started: 12:47:19
-21.0: Cloud Point -21C
-20.4: H-CP

If a test has been terminated, the temperature at this terminating moment is shown
at the end of this string.
By pressing the -key, the next page of the submenu is available.

8.10 Overview Program Menu
ready 1 Error -8,8 C This Display post only in case of error

S-Nr. TANK 1250
Start Start
Cloud Point -6,0 C

Start
H-CP -5,7 C
Start
finished
Start Pr-Nr. TANK 1250
Sample Bath
Start -6,9 C 17.0 C
print ?
start printing
Input Sample Number Data Transfer

# num. input Start data transfer
S-Nr. TANK 1250
Start
Program 1
# Program number 0, 1, 2, 3 or 4
Cloud Point
Start
Preheating Temp. # num. Input

+45,0 C
Start
Test Start Temp. # num. Input

+ 30,0 C
Start
Expected Cloud P.
# num. Input
-12 C
Start
Start Test ? General: Stop will return nto "ready" status
Start
Test has started


9.0 Parameter program
9.1 General
The HCP 852 also offers additional possibilities to the user, allowing Pour Point or
Cloud Point analyses to be carried out which deviate from Standard Procedures; for
example, using a different cooling bath, control cycle or changed test range. There are
four variable programs (Programs 1 through 4) from which to choose. It is completely
up to the user which program is used to determine either the Pour Point or Cloud Point
analysis. Program 0 contains all the parameters which started the last test cycle.
Program 0 cannot be changed.
Please note: When a test run is in progress, parameter input is blocked and only display
is allowed. The STOP -key to interrupt testing or to silence the buzzer is not active in
this particular menu.
In order to either view or change the currently active parameter, it is the Menu M -
key that switches into the parameter menu.
The following detail-listing introduces the assigned key-functions:
Next parameter, with subsequent input initiation

Previous parameter, with subsequent input initiation
Change non-numerical parameters (for instance: no yes)
Change non numerical parameters (for instance: yes no)
# Symbol for numerical entries
. Comma-key to use with numerical input
STOP Delete an entry
M Change-key from parameter menu to message-menu.
9.2 Password
To prevent any unauthorized parameter changes, the input of information is protected

by a password. The password may contain up to eight characters. Thus, the
manufacturer furnishes the "00000000"-address. The password and changes to it are
covered in chapter 8.22. Using the "00000000" -password simply means that there is no
password protection required which causes the password input page to be skipped
during selection of menus. Changes to parameters will be possible at any given time.
If password protection is required, the first page shown when changing into the
parameter menu is the password-input page. The characters entered will be displayed as
#.
V5.1D Parameter program 43

Parameter
Password ########
Then the key is used to switch to the first parameter. If an incorrect password is
entered, there is a sound signal and the entry is erased. If no entry is made, the display
also switches to the first parameter, but no parameters can be changed.
9.3 Program selection and standard/non-standard test

procedure
At this point in time, programs 0 through 4, whichever is viewed or selected for change,
may now be selected. Program 0 contains all the parameters which started the last test
cycle. These parameters cannot be changed and therefore can only be viewed. However,
in programs 1 through 4, all parameters can be changed as necessary.
For both the Pour Point and Cloud Point procedures all standard parameters are pre-
programmed. If no changes are made, the message Standard appears on the display
screen. When changes are made to a parameter, the message non-standard appears on
this page. To re-enter standard values, the -key is used. The display will then change
to indicate Standard.
The term Standard does not imply that the parameters are in compliance with various
standard industrial norms, but indicates whether or not the built-in parameters of the
manufacturer were used.
Changes between the Cloud Point and the Pour Point procedure must be done by
pressing the -key. In so doing, no changes occur to the parameters. If, for instance,
we switch from CP to PP, we will change the test procedure, however, the CP
parameters will still remain active. In other words, we would still run a Pour Point
analysis using previous Cloud Point parameters. Consequently, these parameters are
switched by pressing the -key to Standard, and if necessary, tailoring them to
individual testing requirements.
The respective procedure will be sequentially displayed by showing the abbreviations
PP (Pour Point) or CP (Cloud Point).
Program 1
Standard PP
44 Parameter program V5.1D

9.4 Language selector: German / English
Notifications in the display are in two languages: German or English. Select the desired
language by pressing either the or the -key.
Language
English
9.5 Temperature unit: C / F
The desired temperature unit is selected by pressing either the or the -key.
However, Pour Points, LFP and Cloud Points, as well as temperature input data, will
always be displayed in C Celsius. This is established by the ASTM-Standard
Provision.
Temperature Unit
Degree C
9.6 Calibration of the PT 100 sample thermometer
It can happen that the sample temperature displayed diverges slightly from the actual
temperature. This divergence can be corrected with an offset. The offset is entered on
this page. The sign for the value is selected with the and keys.
Example: The sample temperature is established in a bath at exactly 0C; but the
display shows +0.2C. An offset of -0.2 K must be entered to correct this
deviation.
Note: the offset applies only for the program selected.
Offset Sample temp.
-0.0 K

9.7 Calibration of the bath thermometer
The procedure here is like that in Section 7.7. In this case, though, the bath is filled
with alcohol and the calibration thermometer hangs in the bath (see also Section 12.4).
Note: the offset applies only for the program selected.
Offset Bathtemp.
+0.0 K
Note:
There is a drain for condensed water on the bottom of the cooling bath. This drain must
first be closed on the bottom of the instrument.
9.8 Preheat temperature
In order to properly elevate the selected starting temperature, a preheat temperature can
be entered.
Preheat temperature
+45.0 C
9.9 Final Test Temperature
At the end of testing, the sample will be heated to the test-end temperature. This will
prevent freezing of the cooling bath and enable the test vessel, as well as the
thermometer, to be easily cleaned.
Test End Temp.

+20.0 C
9.10 Expected Pour Point and Cloud Point
Expected Pour Point:
Pursuant to ASTM Method D 97, the sample must be hoisted and tilted for the first time
when its temperature is 9C above the expected Pour Point. If yes is the selected
option, the expected Pour Point may be entered as the start-up sequence is initiated (see

Chapter 6.4). If the selection points to option no the question for the expected Pour
Point will not be asked in the start sequence. Tilting begins with the sample temperature
determined during the test-start temperature cycle (see Chapter 9.11).
Expected Pour Point ?

Yes
Expected Cloud Point:

Pursuant to ASTM Method D 2500, the sample is heated to 14K above the expected
Cloud Point. If yes is the selected option, the expected Cloud Point may be entered at
the beginning of the starting sequence (see Chapter 8.4). If the selection is option no,
the question for the expected Cloud Point will not be asked in the start sequence.
Measuring begins at the sample temperature determined during the test-start
temperature cycle (see Chapter 9.11).
Expected Cloud Point ?

Yes
9.11 Start temperature before the expected result
Test-start up for the Pour Point procedure is determined at 9K prior to the expected
result, whereas, for the Cloud Point, it is 14K. The temperature clearance may be
changed at this time.
Start before expected result
+9.0 K
9.12 Initial test temperature
If at the start of a test no expected Pour Point or Cloud Point has been entered, then the
first testing cycle of the sample is entered when it reaches the sample temperature,
indicated below.
Test Start Temp.
+20.0 C

9.13 Test interval
Normally, during the Pour Point procedure, the sample is hoisted from the cooling bath
for testing at a temperature clearance of 3K; during the Cloud Point procedure it is at a
temperature clearance of 1K. The former clearances may be changed as necessary.
(Please note: For the Cloud Point it remains at 1K!)
Test interval
3.0 K
9.14 Cooling program
Apart from the graduated cooling bath the HCP 852 offers still other cooling methods,
such as: differential cooling, linear cooling, as well as linear sample (not implemented
to date).
With and you may select the desired cooling program.
Cooling Program Cooling Program

Step Bath Difference
Cooling Program Cooling Program

Sample linear Bath linear
9.14.1 Step bath

The step bath has a maximum of seven sample stages and seven bath stages. Each
time the sample stage is reached the bath is switched to the next lower
temperature.
That is: The system is switched to bath stage 1 when the preheat temperature is
reached. When sample stage 1 is reached, the system switches to bath
stage 2.
Cooling program
Step Bath

Subsequently, changes to these various cooling or sample stages will be achieved

by pressing the -key. It will pass first through cooling stages 1 7,
subsequently, through the seven sample stages.
Bath-step 1
+ 15 C
Sample-step 1
10 C
9.14.2 Differential bath
In this chilling, a constant difference is maintained between the sample

temperature and the bath temperature.
Cooling program
Difference
By using the -key to change the page, the desired sample cooling-bath
differential will be shown. The possible minimum differential is 5K, the
maximum is 60K.
Diff. Sample-Bath
5.0 K
9.14.3 Linear Bath

The chilling bath is cooled at a constant cooling rate.
Cooling program
Bath linear
The desired cooling velocity is entered in Kelvin-degrees per minute, whereby it

is possible to attain cooling velocities of 0.5 5K/minute. Also enter the
temperature at which the linear cooling is to begin. This involves switching the

cooling bath to the starting temperature, and from that temperature, continuing
with linear cool-down.
Linear bath start
+ 0.0 C
Cooling speed
2.0 K/min
9.14.4 Linear sample (not yet implemented)

The chilling bath is cooled so that the cooling rate of the sample is linear.
Cooling program
Sample linear
9.15 Parameters for Pour Point detection
9.15.1 Detection level 1

The control sensitivity of the video camera, as well as the electronic transmission,
is determined in two steps. Control level 1 is referenced on the sensitivity of the
camera before the sample is tilted to about 90 C. This particular value must
never be changed.
Detection level 1
600
9.15.2 Detection level 2

Control level 2 is referenced on the control sensitivity of the camera to recognize
motions on the top surface of the sample at the very moment the test vessel is
tilted to about 90 C . This particular value must never be changed.
Detection level 2
600

9.16 Parameters for Cloud Point Detection
9.16.1 Detection factor

Controlling the Cloud Point will be shown by distinct pictorial changes from a
very clear to a turbid sample. Thus, the control factor allows for measurement of
the slightest changes. This particular value is never to be changed.
Detection factor
25
9.16.2 Detection threshold

The detection threshold shows minimum changes used during the conducting of
continuous measurements, prior to any results being finalized, i.e., to eliminate
disturbances such as frozen condensate formation on the sample glass. This
particular value must never be changed.
Detection threshold
600
9.17 Video amplification
The power-amplification rate of the video camera control can be fine-tuned. This
particular value must never be changed.
Video gain
83
9.18 Printer selection
Two printer drivers are selectable in the HCP-852. The Epson driver uses the extended
IBM text format through the parallel printer connection. The Citizen driver uses a
special format used by the Printer (#101-175 for 230V or 101-076 for 115V).
Printer (Citicen):
Dot matrix printer (Epson 24-pin):

Printer
Epson
9.19 Result printing: standard or expanded
Here you select either the simple or expanded printout of the result. The selection is
made with or . See also Section 7.9.4
Print-out
standard
9.20 Result printing automatic or manual
Automatic result printing means that the result found is output immediately to the
printer connected at the end of the test. Printing can be done manually through the
submenu in the ready state (see Chapter 6.9.3 or Chapter 7.9.3). Selection is done
with or .
Print result
Not automatic
9.21 Data transfer: automatic or manual
If an external computer with a terminal program running is connected, the result can be
transferred immediately to that computer. Manual transfer can be done through the
submenu in the ready state (see Chapter 7.9.4 or Chapter 8.9.4). Selection is done
with or .
Data Transfer
not automatic

9.22 Acoustic Signal
If a signal should sound at the end of the test, this is set to yes with . Otherwise set
it to no with .
Note: If the buzzer is turned off and the test is terminated by a failure in the
instrument, no sound signal is produced.
Buzzer
Yes
9.23 Changing the password
In order to change the password, the new password is entered on this parameter page
and the entry is confirmed with the key.
Change Password
The password is repeated in the following page and likewise confirmed with the key.
Repeat password
If the repetition was correct, the new password is stored and the next parameter page
appears. If the repetition was incorrect, the page Change password appears again and
the previous entries are deleted.
Comment: If the password is no longer known, it is possible to reset the password to

the default value. To do that, disconnect the HCP-852 from the network
and open the right side of the housing. The DIP switch (S1) is on board
607-252 (or 607-063) beside the 9-pin connector. Set switch 6 to the off
position. Now reconnect the instrument to the net and turn it on for a few
seconds. After turning the instrument off and removing it from the net
again, return Switch 6 to the on position and replace the cover. Now the
password is 00000000.
Survey of Change password:

Change Password
# Enter password
yes
Password
entered?
no Repeat password
# Repeatition of the
new password
yes Repitition
correct?
Next Parameter
no
9.24 Print parameters
All the parameters of the selected program can be printed on this page. Printing is
started with the key. The message Started appears during the data transfer to the
printer.
Print parameter?
9.25 Example of a parameter report:
9.25.1 Pour Point parameter

HERZOG HCP-852
Unit Number 1
Parameter
Program PP 1
Date 15.02.94 13:23
Cooling program
Cooling bath steps
Sample step Bath step
1. +27.0C +15.0C
2. +9.0C +0.0C
3. -6.0C -18.0C

4. -24.0C -33.0C
5. -42.0C -51.0C
6. -60.0C -69.0C
7. -78.0C -87.0C
Preheat temp. +45.0C

Test-end temp. +20.0C
Test-start temp. +30.0C
Expected Pour P.?
yes
Start bef. exp. res 9K
Detection level 1 600
Detection level 2 600
Video gain 83
Test interval +3.0K
Offset Sampletemp. +0.0K
Offset Bathtemp. +0.0K
Print-out
standard
Print result
not automatic
Data transfer
not automatic
Buzzer yes

9.25.2 Cloud Point parameter

HERZOG HCP-852
Unit Number 1
Parameter
Program CP 3
Date 15.02.94 13:23
Cooling program
Cooling bath steps
Sample step Bath step
1. +10.0C 0.0C
2. -7.0C -17.0C
3. -24.0C -34.0C
4. -41.0C -51.0C
5. -58.0C -68.0C
6. -75.0C -85.0C
7. -75.0C -85.0C
Preheat temp. +10.0C

Test-end temp. +0.0C
Test-start temp. +20.0C
Expected Cloud P.?
yes
Start bef. exp. res 14K
Detection level 25
Detection threshold 90
Video gain 83
Test interval +1.0K
Offset Sampletemp. +0.0K
Offset Bathtemp. +0.0K
Print-out
standard
Print result
not automatic
Data transfer
not automatic
Buzzer yes

9.26 Overview parameter program

Parameter
Password # Numerical input (password)
For Cloud Point:

Program 1 Standardparam. # Progr.-Nr. 0-4 Program 1
standard PP standard CP
Test procedure
Language German
German
English
Temperature Unit deg. C

deg. C
deg. F
Offset Sampletemp. + # Num. input

+ 0,0 K
-
Offset Bathtemp. + # Num. input

+ 0,0 K
-
Preheating Temp. + # Num. input

+ 45,0 C
-
Test End Temp. + # Num. input

+ 20,0 C
-
Expected Pour P. yes

yes
no
Start bef. exp. res.

# Num. input
9K
Test Start Temp. + # Num. input

+ 30.0 C
-

Test Intervall
# Num. input
3.0 K
Cooling Program Cooling program selection

Step Bath
Cooling program selection
Depending upon selected cooling program

appropriate parameters are as follows
At Cloud Point:
Detection level 1 Detection level

600 # Num. input
30
Detection level 2 Detection threshold

# Num. input
600 75
Video Gain
83 # Num. input
Printer Epson
Epson
Data Mega
Print-out standard
standard extended
Print result automatic

not automatic
not automatic

Data Transfer automatic

not automatic not automatic
Buzzer yes
yes
no
Change Password
# Num. Input (new password)
Print parameters ? start print-out

10.0 Brief guideline for determination of analyses
10.1 Pour Point analysis
1. Switch on both the appliance and the cooling system. Please wait until the
refrigeration equipment needed for the cooling bath mode has reached the
required temperature.
2. If necessary, change parameters within the parameter program (see Chapter 8.0).
3. Enter sample number and the desired program on the keyboard.
4. Test sample, prepared in conjunction with industry norm, is poured into the test
vessel until it reaches the fill position marker.
5. Push the lever of the glassholder and insert the test glass into the glassholder in
such a manner so that the test glass settles to rest firmly on the holders plane
surface.. Now, slowly release the lever of the glassholder.
Caution: Do not exert pressure on the lever of the glassholder with the test glass
inside because the test glass might break.
6. Start the test. Testing will proceed automatically. As soon as the Pour Point is
detected, the sample will be heated to its final test-end temperature.
7. When testing is finished the buzzer, which lasts for one minute, will sound, but
can be interrupted by pressing the STOP -key.
8. Simply press the START -key in order to prepare the HCP 852 for another
analysis cycle.
V5.1D Brief guideline for determination of analyses 61

10.2 Cloud Point Analysis
1. Switch on both the appliance and the cooling system. Please wait until the
refrigeration equipment, needed for the cooling bath mode, has reached the
required temperature.
2. If need be, change parameters within the parameter program (see Chapter 8.0).
3. Enter test identification and the desired program on the keyboard.
4. Test sample, prepared in conjunction with industry norms, is poured into a

special testing vessel with a reflective base until it reaches the fill position marker.
5. Push the lever of the glassholder and insert the test glass into the glassholder in
such a manner that the test glass settles to rest firmly on the holders plane
surface. Now, slowly release the lever of the glassholder.
Caution: Do not exert pressure on the lever of the glassholder with the test glass
inside, as this could cause the test glass to break.
6. Start the test. Testing will proceed automatically. As soon as the Cloud Point is
detected, the sample will be heated to its final test-end temperature.
7. When testing is finished, the buzzer, which lasts for one minute, will sound, but it
can be interrupted by pressing the STOP -key.
8. Simply press the START -key in order to prepare the HCP 852 for another
analysis cycle.
62 Brief guideline for determination of analyses V5.1D

11.0 Diagnostic menu
11.1 General
All information to this point has primarily enabled the user of the HCP 852 to execute
the desired analysis. In this chapter we will look at checking the various appliance
functions which, in the event of problems, will help facilitate localization, as well as
assist in their remedy.
Please note: When a test is already in progress, all diagnostic functions are locked-out
and, thus can only be displayed in the interim period. The STOP -key,
intended to be used for interrupting tests or to silence the buzzer, cannot be
activated within the framework of this menu.
The menu key M is used to switch to the diagnostic menu.
Diagnostic-test
not locked
The keys listed below have the functions indicated:
next diagnostic function

previous diagnostic function
switch a component (e. g., valve open)
switch a component (e. g., valve closed)
# symbol for numeric entries
, decimal key for numeric entries
STOP delete an entry
M change from the diagnostic menu to the Parameter menu
V5.1D Diagnostic menu 63

11.2 R-min/R-max
The reference resistances are needed for analog measurements such as temperature and
vacuum in order to equalize them.
Range of values: R min: from 1600.0 to 2100.0
R max: from -100.0 to -500.0
Rmin Rmax
+1750.0 -250.0
No entries are possible here.
11.3 Sample and bath temperature
Sample Bath
+21,3 C +19,7 C
11.4 Alcohol and circulation temperature
This shows the alcohol temperature around the bath wall, and the temperature of the
coolant circulating in the HCP-852.
Alcohol Circulation
+15.0 C + 5.0 C
11.5 Temperature of an external thermometer
Ext. thermometer
+15.0 C
64 Diagnostic menu V5.1D

Entries are not possible here. If no external thermometer is connected, a random value
appears.
11.6 Measuring values of the quadrants
A picture captured via video camera will be equally sub-divided into four quadrants
through electronic switching. The total reflected light from each quadrant is measured.
The resulting deviations for each respective quadrant as they were previously captured
are displayed. Conversely, these values are relative and therefore are only intended for
internal use by the manufacturer.
Q0= 0 Q1= 0
Q2= 0 Q3= 0
No entries will be possible at this juncture.
11.7 Display of tilt angle and delay period
During the testing cycle the test vessel is subject to hoisting and tilting at regular
intervals. When the video camera starts to recognize motion on the samples top-
surface, the procedure is interrupted, and the test vessel is again returned into the
cooling module. The tilt angle of the test vessel will be shown in degrees. At a tilt angle
of 90 the duration is also shown which clearly defines the position assumed by the test
vessel. When controlling the Pour Point the test vessel is expected to be held as long as
5 seconds in the same position (tilted at about 90).
Tilting Angle 0
deg.
Waiting Time 0.0 s
No entries will be possible at this juncture.
11.8 Gray values of recorded picture
During Pour Point determination the sample is subjected to illumination by 12 small

light sources. Values thus indicated refer specifically to an observed refraction of light
at the surface of the sample. Conversely, it is again a question of relative values which
are EXCLUSIVELY for internal use by the manufacturer.

G0 = 32 G1 = 129 G4 = 109 G5 = 1555
G2 = 19 G3 = 98 G6 = 99 G7 = 659
G8 = 51 G9 = 108 G12 = 94 G13 = 568
G10 = 51 G11 = 156 G14 = 56 G15 = 312
No entries will be possible at this page.
11.9 Calculation of curves
Intermediate values calculated with the data from video-image changes and detection
parameters are displayed here. Conversely, these values are only intended for internal
use by the manufacturer.
K1 -1 K2 -1
K3 -1 K4 -1
No entries will be possible at this time.
11.10 Magnetic valve for cooling
M V Cooling
Closed +23.9 C
Display of the status of the magnetic valve for chilling, and display of the alcohol
temperature.
Possible entries are:

Open the valve, display open
Open the valve, display closed

11.11 Magnetic valve for circulation
M V Circulation
closed +23.9 C
Displays the state of the magnetic valve for circulation, and the circulation temperature.

Opens the valve, displays open"
Closes the valve, displays closed"
11.12 Bath heating
The bath heating can be switched here. In the on state, though, it is not heated
permanently but only for short intervals. Thus the display indicates both states
alternately. The bath temperature should not exceed 70C.
Note: The bath temperature is not tested in the diagnostic tests. That means that the
over-temperature protector will trip. If that happens the instrument must be
disconnected from the power line. Open the left side of the housing. The over-
temperature cut-off switch is about 15 cm from the front panel. This must be
reset by pressing the reset button. A distinct click is heard when it is reset. Then
replace the housing panel.
Heater
off +23.9 C

Turn the heater on, display on
Turn the heater off, display off
11.13 Illumination of sample surface
The HCP 852 illuminates the sample surface using 12 infra-red light sources which will
stay activated during the entire tilt process of the sample.

Illumination
On
It is possible to enter as follows:

Activate lighting system, display will read ON
De-activate lighting system, display will read OFF
11.14 Buzzer
For checking the sound signal.
Buzzer
off

Turn the buzzer on, display on"
Turn the buzzer off, display off
11.15 Lift-motor
Caution: The measuring head is to remain in the vertical position for this test.
Lift-motor
On +60
Information status display of the light barrier attached to the hoisting unit which is used
to properly control the measuring head position.
Status changes will only be recognized by pressing either the , or the -key.
Indicator for the hoisting motor steps during zero determination (see Chapter 10.16).
It is possible to enter the following:
START Measuring head moves up close to light barrier

Movement of measuring head upward, self test of light barrier status
Movement of measuring head downward, self test of light barrier status

11.16 Tilting motor
Please note: In order to carry out this test, the measuring sensor should be positioned
in the uppermost position; the unit is to be without a loaded sample.
Tilting motor
Off -30
Information status display of the light barrier attached to the vertical unit used to
properly control the measuring head position.
Status changes will only be recognized by pressing, either the , or the -key.
Indicator for the tilting motor steps during zero error determination (see Chapter 10.16).
It is possible to enter the following:

START Measuring head drives up close to light barrier
Movement of measuring sensor into horizontal position,
self test of light barrier status
Movement of measuring sensor into vertical position,
self test of light barrier status
11.17 Seeking the zero point of the measuring head
Attention please: Measuring head must remain at the base line !
If the measuring head is not positioned at its base position, the test appliance must be
switched off.. Once this is done, turn the measuring head at the upper end carefully in a
vertical position. Then move it down into the cooling bath until the measuring head lies
flat upon the bath itself. The measuring head is now resting in a truly perpendicular
position to the cooling bath. Starting from this base line position, the zero point location
can be determined.
Switch on the instrument . Do not press the START -key. Change with the M -key
to the diagnostic menu and scroll with to this page.
Search zero point
Measuring head down ?
Start to locate the zero point position.

Upon completion of the zero point determination, or if the program menu has
received the START -key signal, the following message is shown:

Search zero point
Locked
Upon completion of the zero point determination the corresponding amount of motor
steps carried out can be controlled using the diagnostic pages pertaining to the hoisting
motor and tilting motor.
Number of steps-tilting motor: - 25 ... -35

Number of steps-hoisting motor: +40 ... +70
Please note: If it becomes necessary to repeat a similar zero point determination, the
test appliance must be switched off again.
11.18 Display of internal instrument data
This display contains data on the course of the program. They are intended only for the
service technician.
1 +1500 +30 +200
+650 +533 +173 0
11.19 Display of the clock mode
Two different modes are available for the time:

- 12- hour display
- 24- hour display
24 / 12- hours
24- hours

Switch to 24-hour display
Switch to 12-hour display

11.20 Setting the date
The date display depends on the clock mode. The format is Day/Month/Year for the
24-hour display and Month/Day/Year for the 12-hour display.
Date
10/02/94

# Date entry
The date change is accepted only when the diagnostic test pages are changed with or
. If you leave this page with M the change is not accepted.
11.21 Setting the clock
The time can be corrected here if necessary.
Time
15:42:53

# Time entry
The time change is accepted only when the diagnostic test pages are changed with or
. If you leave this page with M the change is not accepted.
11.22 Herzog Token Ring (HTR)
Two instruments are needed to test the HTR interface. One must be coded as
Instrument 1, Master, and the other as Instrument 2, Slave. The two instruments must
be connected to the HTR interface with the cable 626-082 (see Section 4.3).
HTR-Test as M aster
Possible entries in the master instrument are:

Switch the buzzer in the slave instrument on

Switch the buzzer in the slave instrument off
For the slave instrument:
HTR-Test as Slave
Possible entries into the slave instrument are:

Switch the buzzer in the master instrument on
Switch the buzzer in the master instrument off
11.23 Software-Versions
The software versions in use are displayed on this last diagnostic page.
M a= X.XX S0= X.XX
S2= X.XX
No inputs are possible here.
Ma = Master Master software on the board 607-252 or 607-063

EPROM identification: 852M
S0 = Slave 0 Software to control the displays on board 607-081 or 607-059
EPROM identification: 852S0
S1 = Slave 1 Software for controlling the hoisting motors on the left-side card
number 607-068
EPROM designation: 852S1
S2 = Slave 2 Software for analog measurements on board 607-048
EPROM identification: 852S2
S3 = Slave 3 Software for a picture analysis on card number 607-079
S4 = Slave 4 Software for controlling the tilting motors on the left-side card-
number 607-068
Please note: The EPROMs used at Slave 1 and Slave 4 are identically marked as item
no. 852S1. The locations of all cards distributed within an appliance are
referred to in Chapter 11.0. Sometimes ****** appears instead of the
common software version, which indicates an error has crept in and as a
result no communication link exists on route to the Slave unit.

11.24 Overview diagnostic program

Diagnostic -test
not locked
Rmin Rmax
+17500 -2500
Sample Bath
+24,0 C +40,3 C
Alcohol Circulation
+15,1 C +5,7 C
Ext. Thermometer
+15,1 C
Q0= 0 Q1= 0
Q2= 0 Q3= 0
Tilt Angle 0 deg.

Waiting Time 5 s
G0= 32 G1= 129

G2= 19 G3= 98
G4= 109 G5= 1555

G6= 99 G7= 659
G8= 51 G9= 108

G10= 51 G11= 156
G12= 94 G13= 568

G14= 56 G15= 312
K1 -1 K2 -1
K3 -1 K4 -1

MV Cooling open
closed +30,2 C
close
MV Circulation open
closed + 15,3 C
close
Heater on
off
off
Illuination on
on
off
Buzzer on
off
off
Movement upward
Lift-motor
off +60 Movement downward
Tilt horizontally
Tilt-motor
off -30 Tilt vertically
Search Zero Point Start seeking zero point

Measuring Head dn?
+0 +0 +0
+0 +0 +0 +0
24/12 - hours 24 hours

24 - hours 12 hours

Date
01/11/93 # Num. Input
Time
09:12:55 # Num. Input
HTR Test a^s Master Activate slave buzzer

De-Activate slave buzzer
Ma=#.## S0=#.##
S1=#.## S2=#.##
S3=#.## S4=#.##
Note: After the diagnostic run switch the analyser off, because other wise the
changed motor speeds will be taken over as standard parameters.

12.0 Messages
This menu lists the failure messages. When a test is started all the previous messages are
deleted.
We distinguish basically among four types of messages.
Messages with no effect on the course of the test
Messages with which the test is terminated
Messages with which the test cannot be restarted unless the instrument is first
turned off.
Messages regarding checksum errors. Any such error messages automatically use
standard parameters within the appropriate program. Furthermore, appropriate program
parameters must be reviewed and the zero point of the measuring sensor should be
checked.
Comment: If failure messages occur, first make sure there is no operator error.
Communications errors between master and slave can occur in the instrument
due to external disturbances, which crash the program. If this failure has
occurred due to such a disturbance it can be eliminated by RESET (turn the
instrument off and on again).
Note: Before trying to eliminate a failure by replacing a unit, such as a circuit

board, make sure that the supply voltages are applied to all the units.
Also check the corresponding cable connections.
The messages are presented in the following form:

No. Brief message Failure criterion
Cause of the failure and measures to be taken if it appears
1 R-min! Termination
The reference resistance is outside the range allowed.
Failure sources: Check the setting of the reference voltage on the instrument.
Unit 607-048 defective.
2. R-max ! Termination
The reference resistance is outside the range allowed.
Failure sources: Check the setting of the reference voltage on the instrument.
Unit 607-048 defective.
3. Pt100 Alcohol ! Termination

The alcohol thermometer is not in the measurement range.
Failure sources: Unit 607-048 defective.
alcohol PT100 defective.
V5.1D Messages 77
4 PT100 Circulation! Termination

The circulation thermometer is not in the measurement range.
Circulation PT100 defective.
5. PT 100 Bath ! Termination

The bath wall thermometer is not in the measurement range.
Bath wall PT100 defective.
6. PT 100 Sample ! Termination

The sample thermometer is not in the measurement range.
Sample Pt100 defective.
Note: If the first six failure messages occur together, no communication with the
slave temperature measurement (S2) is possible.
10. Centronics! None

Printing is not possible.
Failure sources: Automatic printing is selected in the parameter menu,
but no printer is connected.
The printer is turned off.
Wrong printer cable.
11. RS232! Termination

Data transfer disabled.
Failure sources: No file server connected.
File server not ready.
12. Video transfer ! Termination

Taking longer than 5 seconds, no communications with the Video - Slave (S3)
Failure sources: Video card no. 607-079 defective
Connection (6-pin ribbon-like cable) between CPU
and Video card defective
CPU 607-063 and 607-252 defective, respectively
13 Lift-motor transfer! Termination
Taking longer than 5 seconds, no communications with the hoisting motor-Slave (1)
Failure sources: Left-side stepping motor controls 607-068 defective
Connection (6-pin ribbon-like cable) between CPU and stepping
motor control defective
CPU 607-063 or 607-252 defective
14. Tilt-motor transfer! Termination

Taking longer than 5 seconds, no communications with the tilting motor-Slave (1)
Failure sources: Right-side stepping motor controls 607-068 defective
78 Messages V5.1D
CPU 607-063 or 607-252 defective
15. Lift-motor transfer! Termination

Taking longer than 5 seconds, no communications with the hoisting motor-Slave (1)
Failure sources: Left-side stepping motor controls 607-068 defective
16. Tilt-motor transfer! Termination

Taking longer than 5 seconds, no communications with the tilting motor-Slave (1)
Failure sources: Right-side stepping motor controls 607-068 defective
20 Hoisting motor zero point ! Appliance off

Motor unable to reach zero point setting within maximum allowable amount of steps
Failure sources: Wrong zero point
Torn tooth-belt
Defective motor
Left-side stepping motor control 607-068 defective
Defective light barrier at the hoisting unit
21 Tilting motor zero point ! Appliance off

Motor unable to reach zero point setting within maximum allowable amount of steps
Torn tooth-belt
Defective motor
Right-side stepping motor control 607-068 defective
Defective light barrier at the vertical unit
22 Hoisting motor motion ! Appliance off

Measurement sensor does not reach upper limit during tilt test process
Torn tooth-belt
Defective motor
Left-side stepping motor control 607-068 defective
Defective light barrier at the hoisting unit
23 Tilting motor motion ! Appliance off

Measurement sensor not in vertical mode prior to being submerged into cooling bath
Error sources: Wrong zero point
Torn tooth-belt
Defective motor
Right-side stepping motor control 607-068, defective
Defective light barrier at the vertical unit
V5.1D Messages 79
30. Heater! Instrument off

The bath wall temperature has a deviation of more than 2 K for more than 120
seconds during heating and the temperature change toward the set point is less
than 2 K/minute.
Failure sources: Overtemperature protector has tripped.
Refrigerator with a duplex pump has been used.
Defective fuse on board 607-077
CPU 607.084 defective.
Solid state relay defective.
Heater defective.
31. Cooling! None

On cooling the bath wall temperature had a deviation of more than 3 Kelvin for
more than 240 seconds and the temperature change is less than 0.5 K/min toward
the set point.
If the Cooling failure occurs on cooling, then if the temperature difference
between the bath and the sample is large enough, there is still a possibility of
producing a result. But in each case the technician must decide whether the result
is reasonable.
Failure sources: Refrigerator capacity inadequate.
Coolant too viscous.
Cooling magnetic valve defective.
Ribbon cable connection between CPU and power driver board
defective.
Board 607-077 defective.
CPU 607-252 defective.
32 Pour Point ?? None

Pour Point controlled within the initial tilting action
Failure sources: Adjustment of test-start temperature, too low
Entered wrong expected Pour Point
Changed control level within parameter menu
Defective annular illumination 607-076
Defective camera
Defective video card no. 607-079
33 No sample cooling Termination

Failure 31 has occurred and the Bath/Sample temperature difference is so low that
the sample temperature is decreasing by less than 1 K/h.
Failure sources: See failure 31.
34 Measuring values voided ! Termination

Values measured via camera are void
Error sources: Appliance exposed to utter vibrations during measurement recording
Reference picture void
35 Measuring values voided ! Termination
CP-detection not possible abnormal termination
Cause: Major change of picture without CP-Signal
80 Messages V5.1D
Error sources:
Camera problems
Analyzer is not set on an stable table
Test glass has not been fixed appropriately
Problems with video PCB
90. Checksum! Set standard
Wrong checksum in Program 0.
Failure sources: Program crashed.





Wrong checksum for common parameters.
Attention: Verify zero point setting
V5.1D Messages 81
82 Survey of the design of the HCP-852 V5.1D

13.0 Survey of the design of the HCP-852
The instrument must be turned off and disconnected from the power line before
servicing or maintenance work.
13.1 Thermometer positions
Sample thermometer: inserted in the measuring head. Unit accessible when lateral
measuring head cover is being removed
Bath thermometer: glass thermometer with thermally conductive paste installed in

the bath wall. Accessible from the bottom of the instrument.
Unscrew the perforated plate and remove the layer of
insulation.
Alcohol thermometer: metal thermometer installed in the bath. Accessible from the
bottom of the instrument. Unscrew the perforated plate and
remove the layer of insulation.
Circulation thermo.: Screwed into the magnetic valve block. Accessible by

unscrewing the back panel.
13.2 Power supply and fuses
Fuses: Power fuses are 4A at 230 V and 6.3 A at 115 V. The power
fuses are installed in the line filter.
The heater fuse (10 A) is on the power driver board 607-077.
The 6.3A fuse for 24V (magnetic valves, vacuum pump) and
for 32V (stepping motors) is on the power driver board 607-
077.
Line voltage: Switchable for 230 V or 115 V line at the power voltage switch
on the back of the instrument.
Low voltages: The +5, +15, and -15 volt supplies are provided from the
power supply. The 24 VAC is provided by a transformer,
which, like the power supply, is accessible by unscrewing the
back panel. The +12 and +24 voltages are derived from the 24
VAC on the driver board 607-077.
V5.1D Survey of the design of the HCP-852 83

13.3 Electronic components, top view

13.4 Electronic components, side view left
V5.1D Survey of the design of the HCP-852 85

13.5 Electronic components, side view right

14.0 Maintenance and calibration of the HCP 852
Please note: The HCP 852 is a very complex measuring unit. In case you encounter
major technical problems, especially those that are hard to solve,
please contact your local customer service engineer.
14.1 General
Sample glasses:
The bottom portion of the shortened sample glass required for the Cloud Point
determination is covered with a layer of lacquer which is insensitive against various
detergents such as cleaning fluid. Not used, however, should be very aggressive
solvents, as for example acetone which will positively dissolve the layer of lacquer in
no time at all.
Analysis appliance:
Testing of the HCP 852 regarding its orderly functions can easily be achieved through
regular comparison with results obtained by this appliance with equal laboratory results,
or by regular analysis of test samples whose particular Pour Point is well known. For
repairs and general maintenance purposes appropriate materials may be ordered from
Herzog company. In case of any disorderly functioning of the unit the diagnostics and
error message programs can be of great assistance as well.
Instruments available for this purpose are recommended as follows:
A) A stop watch equipped with a graduation of scale of 0.1 s and a degree of accuracy
equal to +/- 0,07 %.
B) Calibration of thermometers with a temperature range from -80 C through +50 C.
C) Resistance bridge and a decade box (accuracy of +/- 0.05 Ohm); those items may
be ordered from Walter Herzog GmbH.
D) Table offering comparison data of resistance / temperature ratio measurements

obtained by using a resistance thermometer from DIN EN 60751.
V5.1D Maintenance and calibration of the HCP 852 87

14.2 Calibration of PT 100
Temperature measurements may be checked out with the help of a decade box in
conjunction with the Resistance / Temperature table from DIN EN 60751. The decade
box is to be connected with the input-connectors of the thermometer, and thus the
temperature values of the instrument are to be compared with the appropriate resistance
values shown in the table. The required accuracy limit to be adhered to must be 0.02
C or 0.05 Ohm, respectively.
The cooling bath as well as sample temperature readings are obtainable from the
diagnostics test.
Sample thermometer calibration shall be carried out by using a separate external

calibration bath. The resulting offset must be entered into the parameter menu.
Attention: The cooling bath and sample temperature offset is only effective within
the program to which it had been entered. Whereas, the diagnostics test
the sample and cooling bath temperature will be duly corrected by the
offset, whose retained value is being stored in the program, when last
started.
For calibrating the resistance thermometer PT 100 attached to the cooling bath wall you
may proceed as follows:
1. Opening of a small hose (white/transparent plastic), which is located at the under

side of unit HCP 852, needs to be plugged and is later to be removed again without
any problem.
2. Alcohol to be poured into the cooling bath until a level of 70 mm high is reached.
3. You are ready to switch on the HCP 852. Inside of the parameter menu the following
parameters need to be changed (youll select a program that contains the standard
parameters, because these will easily be returned to the original status condition Set
standard-function. If you are relying on a self-defined program, you must make
written notes to yourself regarding the changed parameter values):
Preheat temperature -30 C
Cooling bath step 1: -20 C
Sample step 1: -30 C
Sample start temperature: -30 C
4. Do start testing without using a test glass. Wait approximately 20 to 30 minutes, to
allow the alcohol temperature ample adjustment, within the bath, to the particular
pre-set cooling bath temperature.
5. Read the cooling bath and sample temperatures (see Chapter 10.3). The differential
between cooling bath desired value plus sample temperature, equals the cooling bath
offset attained.
For example: Sample temperature = -19.5 C; Cooling bath temperature = -20.0 C
Hence it follows the resulting offset: -20.0 C - (-19.5 C) = -0.5 C
6. Youll now enter the cooling bath offset within that of the parameter menu cooling
bath offset (see Chapter 8.7).
88 Maintenance and calibration of the HCP 852 V5.1D

14.3 Testing: Automatic Pour Point determination
During a continuous test cycle youll want to check out, with a stop watch in-hand, the
optical cooling as well as tilting procedures.
14.4 Testing: Automatic Cloud Point determination
During continuous testing it is possible to check out the sample, with extended
measuring sensor, optically for turbidities, and thus determines the Cloud Point
manually. Cooling itself can be checked out (i.e., temperature, and change over into
cooling bath temperatures) within a diagnostic test mode and using a stop watch.
14.5 Testing: Video Unit
The field of vision of the video camera is divided into four quadrants. The position of the
quadrants when the test head is dipped into the cooling bath is
Q0 -> rear left side

Q0 Q1
Q1 -> rear right side
Q2 -> front left side
Q2 Q3
Q3 -> front right side
14.5.1 Check of Image Change:

1. Clamp the test disk (385-031) in the glass holder instead of a sample glass in
order that the black circle
segment is in the quadrant Q2 (front left side).
2. Select the indication of the quadrants in the menu Diagnostic of the MP 852.
Q0 = Q1 =
Q2 = Q3 =
3. Delete the image saved with the STOP -key.
4. Take up the image with the START -key and save it.
5. Compare the image existing with the -key with the saved image. The quadrant
values Q0-Q3 must be
less than 250 points, but >0.
6. Turn the inserted test disk a quarter turn clockwise (looked at from above from
camera vision). Circle
segment in quadrant Q0.
V5.1D Maintenance and calibration of the HCP 852 89

7. Compare existing image with the -key with the saved image. The quadrant
values Q0 and Q2 must be
more than 2000 points.
9. Compare existing image wit the -key with the saved image. The quadrant
11. Compare existing image with the -key with the saved image. The quadrant
14.5.2 Function Test:
1. Change parameters.
a) Set parameters to standard.
b) Set pre-heating temperature to 0C.
2. Start a pour point test without sample glass with the changes program.
3. Read the tilting angle and the waiting time in the menu Diagnostic after the first
tilting cycle and write
them down.
4. The tilting angle may not be more than 35C.
If the values of the quadrants or of the tilting angle are not as described above, please write
down the values of all measurings and inform us.
90 Maintenance and calibration of the HCP 852 V5.1D

15.0 Serial output of the HCP-852
The HCP-852 Pour Point/Cloud Point tester has a serial RS 232 interface.
There are two 9-pin connectors on the back of the instrument. Use the one marked
RS 232 (serial input/output).
The parameters for the communication protocol are:

2400 Baud, No Parity, 8 Data bit, 1 Stop bit
The result is transferred either on command from a host computer or by starting a

transfer from the test instrument.
If the data are to be requested by a host computer, the following command must be
entered into the test instrument:
1TR0 Note: 0 = the character zero
1Instrument number (coded on the CPU board with a DIP switch; see Section 4.3).
TR0 Command to request the result
Note: The comment must be terminated with a <CR>.
Immediately following the request for data by the host computer, the HCP-842 responds
with the following character string:
1ER;MP-852;xxxxxxxxxxxxxx;YYMMDDHHMMSSam -21.0,-22.4,-21.1
1ER Result string from Instrument 1

MP-852 Instrument type
xxxxxxxxxxxxx: Sample number
YY: Year
MM: Month
DD: Day
HH: Hours
MM: Minutes
SS: Seconds
am: before noon
pm: after noon
-21.0: Pour Point -21C
-22.4: LFP
All the transmissions must be based on the ASCII character format. The semicolons are
part of the transmission. If the 24-hour clock is selected in the test instrument, two
semicolons are transmitted in place of am/pm.
V5.1D Serial output of the HCP-852 91

92 Serial output of the HCP-852 V5.1D

16.0 Spare parts for analyzer HCP 852
16.1 Recommended spare parts for appr. 2 years of operation
Order No. Description Qty Picture

122-029 Toothed belt for tilt motion 1
122-034 Toothed belt for lift for lift motion 1
285-061 Spring band coated with Elastosil for test jar holder 1
385-061 Glass holder cpl. / HCP 852 1
501-143 Test jar with reflecting bottom and ring mark for 20
CP/HCP 852
501-157 Test glass with opaque bottom and 45ml ring mark 20
for PP/HCP 852
V5.1D Spare parts for analyzer HCP 852 93

Order No. Description Qty Picture

613-050 Solid state relay 25A 1
615-027 Light barriers OPD-960 / MP 626 for tilt position 1
108-092 Solenoid coolant valve unit / MP 842 / 852 1

101-119 Plunger for108-092 (2 required) 2
628-007 Fuse 10 A - T 10
628-021 Fuse 2 A - T 10
628-025 Fuse 4 A - T 10
628-023 Fuse 6,3 A - T 10
645-025 Heating cartridge 80W/24V/ HCP842, MC 840 2
94 Spare parts for analyzer HCP 852 V5.1D

16.2 Other spare parts

108-182 Camera adjusted / MP-852
413-021 Bandfilter for 108-182 no Picture

385-029 Distance bolt, PVC no Picture
385-072 Verification gauge for video signal
403-017 Hose coupling 11*60mm
603-025 Power supply +5V, +/-15V

(up to 09.2012)
103615 Power supply +5V, +/-15V, with basic load

(since 09.2012)


607-048 Bath control P.C.B. for MP 842 / 852, without
EPROM
650-112 EPROM with latest software for 607-048

650-551 Bath control P.C.B. since 01.2005
Substitutes board 607-048.
Attention! The board is configured for use in the
HCP852 by setting the code switch!
see chapter: 16.3
607-068 Motor control PCB / MP 852, without EPROM
650-111 EPROM with latest software for607-068
607-075 Print key control / MP 842 / 852
607-076 Lighting ring PCB / HCP 852
607-077 Power pack PCB for cooling bath / MP 842/852


607-080 Position detection PCB / MP 852, without EPROM
607-081 Keyboard-control PCB
650-109 EPROM with latest HCP852 software for 607-081
607-082 Display P.C.B. green
607-084 CPU P.C.B. , without EPROM
607-252 CPU board with keyboard and display controller

without EPROM
Since Ser.-No. 058520695
Attention! The CPU board is only confabulated for

use in HCP852 after having programmed the code
switches! See chapter: 16.4
617-053 Main switch
618-107 Lift motor / MP 852


618-108 Tilt motor / MP 852
619-013 Varistor metallic oxide S20 K300
625-068 Transformer Mz90MM 300 VA
629-018 Over temperature protection (Capillary tube limiter)
636-039 Resistance thermometer for bath-wall-temperature
636-056 Pt100 Resistance thermometer/bath/MC 840, HCP

860
MP842/852 w.o. certificate
636-089 Resistance thermometer circulation / HCP 842/ 852


638-030 Support with Pt 100 cpl. (thermometer sample)

16.3 Configuration of the Measurement Unit
This board contains the software for all instruments using PT100-temperature sensors for measurement. The
measuring program for the particular instrument is set at the 4-pins code switch on the board.
Schalter-Kodierung/Switch code
Gert/Unit S1 S2 S3 S4
Beispiel: Einstellung fr/

MP 626 Pt 100 off on off on Example : Setting for:
HDA627/628/MP626
HDV 632 on on off on
HCP 852 off off on on
HCP 842 off off on on
HRB 754 on off on on
HFP 36X off on on on
HDA 627/628/626 on on on on

16.4 CPU with keyboard and display controller 607-252
16.4.1 Configuration Master/Slave

Photo1
- Encoding as
master
- Encoding as
slave see
photo 2
Encoding
switches S1.1
to S1.8 (see
manual)
Master-
EPROM
Photo 2
Switch S1.8 ON
16.4.2 Configuration Display controller

On the printed circuit board 607-252 there is a display controller integrated additionally to the CPU, which can
replace the external display controller board 607-092.
When do you have a new unit (without Display-Controller 607-092), then realize the settings as follows:
Photo 3

- Standard encoding
Slave 0 not assembled

when using an external
display controller board or
-092
- Standard encoding
- Master-EPROM =
27C512
- Standard encoding

17.0 Hardware documentation
Without express written permission of Walter Herzog GmbH, no circuit diagrams or

drawings of any kind, full copies even if only partially revealed, are to be made available
to third party individuals or competitors in general.
Hardware improvements will make it mandatory to change circuit diagrams as well.

Equipment deemed obsolete will no longer be offered. If you should receive spare parts
deliveries from us and it becomes apparent that the enclosed circuit diagrams do not
correspond with the parts delivered; simply request the correct wiring/circuit diagrams
from us.
Existing part numbers, in some cases, indicate several other versions (for instance: 607-061
and 607-061A). Added letters, such as A, B, C and so forth, also describe hardware
versions.
Hardware versions with like numbers might be used to offer other Herzog Appliances in
the market place.
In this case the hardware documentation for the HCP 852 consists of the following
drawings and circuit diagrams:
General circuit diagram (230 V) 841-003

General circuit diagram (low-tension voltage) 841-004
17.1 Views of parts for the HCP 852
PP1 Front view HCP 852
PP2 Indication device and keyboard for the HCP 852
PP3 Rear view of the HCP 852
V5.1D Hardware documentation 103

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Operating Instructions

Automatic Pour Point- and

Walter Herzog GmbH: Testing Equipment for Petroleum Products

Telefax: (+49) (0)9343 / 640-101

Operations Instructions: Pour Point as per ASTM D97/IP 15/ISO 3016

Documentation No.: 820-089

Copyright 1994 / 95 WALTER HERZOG GmbH

2.0 Technical details............................................................................................................ 9

3.0 Analyzer Unit HCP 852 .............................................................................................. 11

4.0 Ordering information and Accessories: .................................................................... 13

5.0 Equipment Start Up ................................................................................................... 17

6.0 Operation ..................................................................................................................... 21

7.0 Start of a Pour Point Analysis ................................................................................... 23

8.0 Start of a Cloud Point Analysis ................................................................................. 33

8.6 Starting the test ........................................................................................35

9.0 Parameter program.....................................................................................................43

10.0 Brief guideline for determination of analyses .......................................................... 61

11.0 Diagnostic menu .......................................................................................................... 63

12.0 Messages ...................................................................................................................... 77

13.0 Survey of the design of the HCP-852 ........................................................................ 83

14.0 Maintenance and calibration of the HCP 852 .......................................................... 87

15.0 Serial output of the HCP-852 .....................................................................................91

16.0 Spare parts for analyzer HCP 852 .............................................................................93

17.0 Hardware documentation .........................................................................................103

2.0 Technical details

V5.1D Technical details 9

10 Technical details V5.1D

3.0 Analyzer Unit HCP 852

As a basis to determine the Cloud Point, ASTM D 2500 is applicable. It is extremely

V5.1D Analyzer Unit HCP 852 11

12 Ordering information and Accessories: V5.1D

4.0 Ordering information and Accessories:

4.1 Ordering information

Order No. Description Picture

V5.1D Ordering information and Accessories: 13

Order No. Description Picture

14 Ordering information and Accessories: V5.1D

Order No. Description Picture

629-030 Turn-table for monitor

627-104 Video signal cable from HCP852 to monitor 629-

101-214 Matrix dot printer, 40 columns, using endless

Centronics Printer cable 626-029 not included

101-137 Ink jet printer with English and German manual,

V5.1D Ordering information and Accessories: 15

Order No. Description Picture

626-082 Connection cable for HTR communication,

101-194 Pt100 probe simulator box 40 to +100C with 6

16 Ordering information and Accessories: V5.1D

5.0 Equipment Start Up

IF THESE RETAINING CLIPS ARE NOT REMOVED, SEVERE DAMAGE TO

V5.1D Equipment Start Up 17

Insulation of Refrigeration Hoses:

5.2 Connecting the HCP-852 to a printer

5.3 Connecting several HCP-852s to one printer

18 Equipment Start Up V5.1D

Unit 1 Unit 2 Unit 3

Cable No. 626-082 Cable No. 626-082

Master Slave Slave

Cable No. 626-029

Coding the instruments

Switch 1.8 X = off = Master

V5.1D Equipment Start Up 19

5.4 Zero Adjustment of The Measuring Sensor

20 Equipment Start Up V5.1D