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(Polycon department)
PREPARED BY
SYED ASIM ALI SHAH
(03022700702)
Ameer Hamza
Tabish ali jamali
SUBMITTED TO
Hr department
DAWOOD UNIVERSITY OF
ENGINEERING AND TECHNOLOGY
INTERNSHIP REPORT (Novatex Limited)
ACKNOWLEDGEMENT
All praises belong to almighty ALLAH who is the supreme Authority Knowing the
ultimate relations underlying all sorts of phenomenon going on in this universe.
without His guidance, I am nothing. All our faith belongs to him and by his grace I
have completed our three-week internship program in NOVATEX limited.
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INDEX
S.NO CONTENTS
1 INTRODUCTION
3 POWER HOUSE
POWER HOUSE 1
POWER HOUSE 2
4 QUALITY CONTROL
5 MECHANICAL DEPARTMENT
6 UTILITY
COMPRESSOR UNIT
NITROGEN PLANT UNIT
DEMIN WATER UNIT
RAW WATER UNIT
7 PROCESS
POLYCON DEPARTMENT
SOLID STATE POLYMERIZATION (SSP)
8 POSITIVE SIDES
9 SUGGESTION
10 CONCLUSION
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INTRODUCTION
GATRON Ltd. and NOVATEX Limited belong to a group of companies, G&T GANI &
TAYUB. The group is in business since 1948. These five decades of operational
excellence, experience and expertise have all formed a combined strength to
empower the group as a leading name in fashion garments (BONANZA), Synthetic
Textiles, Polyester Filament Yarn, Polyester Chips and PET Resin in Pakistan. The
group employs more than 6,000 people in the country.
NOVATEX Limited (along with GATRON Limited) is the only PET Resin Bottle Grade
manufacturer in Pakistan, with the brand name of "GATRONOVA."
NOVATEX produces PET Resin for Domestic & Export sales.
GATRON produces PET Resin for in-house use in the manufacturing of PET
Preforms.
The Group is in Polymer production since 1988 and in PET Resin production since
1998.
The total PET resin production capacity is 235,000 mt/annum, out of which more
than 70% of the quantity is available for export.
Certified to meet FDA & EEC standards.
Suitable for all applications of PET, including sheet.
Widely approved by major CSD and Mineral water brands in the World.
Used by customers in more than 45 countries with major quantities going to
Western Europe.
Fast Reheat resin is also available.
With the advantage of regular in-house testing on both injection molding and blow
molding machines, GATRONOVA has the advantage of utilizing this complete loop
to continuously optimize it's quality.
Capacity to produce over 1.5 billion preforms per year. The PET Resin (raw
material) for these preforms is produced in-house by GATRON and NOVATEX and
therefore gives standardized & consistent preforms.
Sizes range from 13 gms to 55 gms, with neck sizes 28 mm PCO / BPF & 30/25, for
330ml to 2250 ml Water / CSD bottles.
Produced on Husky HYPET & G-Line Machines mainly installed after 2004.
Nearly half of the perform production is exported.
Preforms are tested not only in the laboratory but also by actual blowing into
bottles on regular basis. So, quality of preforms is also monitored in actual use.
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MECHANISM OF FIRE
There are three things to need for fire.
Fuel
Oxygen
Temperature
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TYPE OF FIRE
A class fire: fire on wood, paper, plastic etc.
B class fire: fire on liquid like oil and petrol etc.
C class fire: fire on flammable gas like CH4, CO, H2 etc.
D class fire: fire on metals Al, Mg, Ti etc.
E class fire: fire on electrical apparatus.
EXTINGUISHER
Extinguisher is the equipment which is used to put off the fire
PASS TECHNIQUE
Pass technique is use to operate the fire extinguisher.
TYPES OF EXTINGUISHER
The following types of extinguisher NOVATEX is using.
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QUALITY LAB
OBJECTIVE:
The control laboratory of NOVATEX is modern facility and equipped with state
of the art instrument for testing and examining the in process and out process
material quality. The purpose of having laboratory is to ensure quality and
standard production to meet the consumer requirement. The samples are tested
and the results are collected to evaluate and compare with standards. This samples
are raw material, in process amorphous and crystalline chips and final product.
They go through various chemical, thermal and physical tests in the lab and the
results are forward to the decision body. There is no recommendation given by lab,
its the upper authority that decides whether to reject or clear it to proceed further.
NOVATEX ensures reliable and standard product to their clients and follows
strict no tolerance policy in terms of quality and barriers.
TEST:
The lab works non-stop 24/7 where series of around 40 different types of tests
are carried out in the lab. The types and choice of test depends upon the
required parameters, nature and characteristic of the material on which the
quality depends. The test can be done on daily and on monthly basis
depending on the needs. There are some important test, carried out multiples
times in the day. The list of such type of tests are:
Determination of Intrinsic viscosity of PET & PBT ( I.V test ).
Determination of ash content in EG & TPA.
Determination of acid number of EG & TPA.
Determination of H2O and aldehyde in EG & liquid samples from polyester
production
Determination of iron in Antimony Triacetate, EG, TPA & in PET.
Determination of color number in TPA, EG & polyester chips.
Determination of density and crystallinity of chips from PET.
Determination of EG, DEG & TEG in the distillation products obtained from
the respective recovery plant.
The chemist are being appointed to carry out all these tests by following the
proper procedures and methods. Each and every test are done on different
scales and parameters to collect essential information regarding all the
concerned materials to check there properties that matters the quality.
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MECHANICAL DEPARTMENT
OBJECTIVE:
MAINTENANCE:
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Along with maintenance and regular inspecting of all the units (Poly I, Poly II, SSP I,
SSP II, SSP III) the Mechanical engineers are also involved in the expansion and
modification of plant as per feasibility and requirements. However, requirements
and operating parameters are set by the Process department but the case study is
done by Mechanical Engineers. From the initial study of project till its completion,
the Mechanical department keeps the steers in their hands to manipulate the
directions of project. We can say ME plays a strong role to keep the growth of
NOVATEX forward.
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UTILITY
OBJECTIVE:
Utility department is responsible to handle all the operation and maintenance
of all areas and equipment under utility. It also supply soft water to the plant
and maintains firefighting equipment and cooling tower.
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SUPPLY LINES
Each supply lines are indicated by unique color
Raw water
Cooling water
Soft water
Compress air line
Fire fighting
Instrument air line
Technical nitrogen
Pure nitrogen
Drain line
Rain drain line
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NITROGEN PLANT
Nitrogen is separated from air by pressure swing Adsorption.
Carbon sieves are used in absorption and regeneration and desiccant dryer
unit.
Compressor is used to compress the gas and to build up the pressure to
utilize it for transporting purpose.
Deoxidation reactor purified the nitrogen by removing oxygen
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POLYCON DEPARTMENT
OBJECTIVE;
NOVATEX has two polymerization plants. The main function of chemical engineers is
to run Polycone and SSP department. They utilized the raw material and all the
accessories like electricity from power house, technical nitrogen, oxygen, raw water
and demine water from utility for the production polyethylene terephthalate (PET).
Two main raw material which are used in bulky for the production of PET are as
following.
1) Pure terephthalic acetate (PTA) is main reactant and added 84% to 86%. It brought
from Indonesia (KASIE BAKERI), Thailand (MITSUI), Pakistan (LOTTE), india
(RELIANCE).
2) Mono ethylene glycol (MEG) is limiting reactant and added in 14%. It is brought
from Saudi Arab (SABIC). NOVATEX store MEG in three tanks of volume of 3000m3,
3000m3, 1800m3.
ADDITIVE
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All these ingredients are prepared in separate vessels which are then store in their
separate vessel and then all the ingredient are transferred in the paste hopper. Paste
hopper fed the paste into the paste vessel where materials are mixed uniformly by
agitation. Nitrogen is introduced from bottom of Paste hopper which prevent to stick
the material with hopper.
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SCRAPPER CONDENSOR:
PP1, PP2 and DRR are connected with scrapper condenser where vapors of E.G and
water are entered in scrapper condenser. Scrapper condenser is a vessel having tom
like shape liquid EG is showered from top of the tom column which contain umbrella
type perforated baffles that allow the larger contact area to condense the EG vapor
but some amount of E.G vapors remain uncondensed which are condense in separate
condenser and collect in separate vessel. it is low velocity vapors therefore a
supersonic velocity vapors of E.G that coming from glycol evaporator take these slow
vapors to the jet through venture to maintain the pressure.
FILTER (18-F01)
The material from DRR is enter into filter 18F01 where the further impurities is
removed. The size filter 18F01 is 40 micron and having 74 candles. The material from
DRR is highly viscous and due to its smaller micron size as compared to 16F01, 18F01
filter is blocked easily and then sent to the filter cleaning area.
CUTTER
The material from filter is then divided into 2 sections. One goes to three cutters and
other goes to another three cutters by passing through die head having 78 laces, 39 in
front and 39 at the back. Die head has 19 sensors that alarm at any dangerous and
unhealthy conditions, in this situation cutter goes at the waste. It uses three types of
water:
1) CONVEYING WATER: It is used in the cutter to prevent from high temperature.
2) OVER FLOW WATER: It is used to convey the laces or spaghetti.
3) SPRAY WATER: It is used to maintain the temperature during conveying.
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DRYER
After cutting, the chips are fed into the dryer where the water content is removed
from them by air sucked with the help of blower.
VIBROS CREENING
Over size and under size chips is separated in this section and then remaining sent to
the amorphous silos by the help of conveying air.
EVAPORATOR
The evaporators (12V01, 14V01, 15V01 and 17V01) are used to heat up the
condensate of HTM vapors by using HTM liquid. HTM vapors are responsible for
jacketed heating.
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SOLID STATE
POLYMERIZATION (SSP)
OBJECTIVE
The main objectives of solid state polymerization SSP are
SURGE SILOS
Amorphous chips are stored in three silos of having 300 m3 ,300 m3, 80 m3. The level
of these silo are monitored by laser sensor in order to maintain the level of chips
nitrogen is continuously blow from bottom of silo
PRE CRYSTILLIZER
Hot nitrogen gas fed from bottom of pre-crystallizer at 200 C and fluidize the chips.
Fluidization prevent the lambs formation, remove the aldehydes and dust particles
and transfer certain amount of heat for crystallization and chips achieve glass
transition temperature i,e about 78 to 80 C
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CRYSTILLIZER
Chips move down to crystallizer # 01 then to crystallizer # 02 where it achieve
temperature 160 to 180 while having pressure of 155mbar to 125mbar and 55 to 57%
crystallization occur respectively. Crystallizer contain two hollow screw in order to
transfer heat from HTM (heat transfer medium). These screws continuously agitate
the chips
1) HOT NITROGEN FILTER: Two giant blower suck the nitrogen and pass discharge into
hot nitrogen filter where remaining dust particles are removed.
2) ECONOMIZER: Nitrogen enters in gas to gas economizer where its temperature
rises to 250 C by coming exhaust nitrogen of 330 C form NPU reactor.
3) NPU REACTOR: Nitrogen is mixed with oxygen and heated into electrical nitrogen
heater and then mixture of oxygen and hot nitrogen enters in NPU (nitrogen
purification unit) reactor where combustion reaction take place in the presence of
1% platinum catalyst which remove Aldehydes and hydrocarbon present in
nitrogen. The exhaust nitrogen temperature riches to 330C which utilize
temperature in economizer.
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VIBRO SCREENING
Material goes to VIBRO screen. Screen
separates the oversized and under sized
chips which separately collected in two
silo and then used for molding purpose.
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POSITIVE SIDES
1) NOVATEX is ISO and HACCP certified and having other certification.
2) NOVATEX follows all the standard and SOPs.
3) Cooperative and discipline staff.
4) First rate safety and security.
5) Planed and schedule maintenances.
6) Neat and clean environment.
7) Experienced and skillful engineers.
8) Regular training session of health and safety.
SUGGESTION
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CONCLUSION
The 3 weeks in NOVATEX is proved a worthwhile experience for all three of us. The
time in the industry shows us a picture that realizes us to rethink and reconstruct our
learning style in different manner. The complex and large scale operations provided
us with a great value of information to broad and expand our educational sphere. We
assure with complete confidence that we had completed the given tasks and objectives
within the time and our purpose of doing internship is being fulfilled.
In last, concluding the 3 weeks of internship, that we had not only learned about
technical and engineering aspect of industry but we had been taught how the industry
runs, how the system works, how to expose the professionalism and technical skills
with discipline and dedication, and how an engineer can contribute to the industry.
Signing off and stepping out from the industry (NOVATEX) by saying we spent a
beneficial time.
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