Вы находитесь на странице: 1из 5

170 ELECTRONICS & POWER FEBRUARY 1983

The constraints on the design


and use of silicon-diaphragm
pressure sensors
As with all devices, the silicon-diaphragm pressure
sensor has limitations to both its design and field of
application. This article highlights the types of
compromise the designer of such devices is forced
to make

by J.H. Greenwood

Silicon-diaphragm pressure sensors tensively in the aircraft, medical and must watch.
have been available for a decade. They process-control industries. Like all Physical design: A silicon pressure sen-
are a good example of how techniques devices, however, they have certain sor consists of a thin silicon diaphragm
developed for the manufacture of in- limitations, and the purpose of this arti- into which are diffused resistors (Fig. 1).
tegrated circuits have been adapted to cle is to introduce the user to the deci- Mechanically the resistors form part of
produce devices for measuring physical sions the designer of such sensors must the diaphragm, but electrically they
quantities. Their advantages include face. It is hoped that this will help to ex- function independently, being isolated
small size, low power consumption, com- plain some of the compromises in the from the rest of the diaphragm by the p-n
patibility with electronic circuits and manufacturers' specifications and to junction. These resistors function as
cheapness, and they have been used ex- demonstrate the points which the user strain gauges.
The simplest design would be to make
such a diaphragm and attach it to the
crystallographic end of a support tube, but a joint so close
orientations to the strain gauges will usually in-
troduce hysteresis. The diaphragm is
[on] therefore generally made by creating a
recess on the reverse side of the silicon
chip and leaving a solid 'frame' around
it. The material can be removed
-wire bonds mechanically, using ultrasonic or high-
speed diamond machining, but although
these methods are relatively fast they
leave a damaged layer which has to be
removed by chemical etching. If the
crystal orientation is (100), anisotropic
etching, using, for example, potassium
hydroxide, will produce a hole with a flat
bottom and pyramidal {111} sides along
<011> directions, resulting in a square
substrate diaphragm. A further method is to grow
an epitaxial layer with a different doping
level on the substrate and to use a
preferential etch which will remove the
substrate in the area of the recess and
1 Schematic representation of silicon pressure sensor stop when it reaches the epitaxial layer.
0013-5127/83/020170+ 05 $01-50/0 ^IEE: 1983
ELECTRONICS & POWER FEBRUARY 1983 171
The epitaxial layer then becomes the
diaphragm.
Limitatation due to strength: The
strength of silicon, like that of glass,
depends entirely on the state of the sur-
face. At room temperature there is effec-
tively no plastic flow, and when the first
flaw reaches its critical stress the silicon
breaks. Larger diaphragms should be
weaker because there is a greater
chance of a large flaw being present.
The diffused surface of the diaphragm
will be that of the original silicon wafer,
protected in general by a layer of silicon
dioxide, and the reverse will be a blank
surface formed by one of the processes
stated above. Although very high
strengths have been attained with
careful handling, a general production
value is 500 MPa. Allowing for a safety
factor of five, appropriate to brittle
materials with a wide scatter of
strengths, and including the overload
limit, the maximum stress at the edge of
a circular diaphragm would be
100 MPa. For most pressures this max-
imum stress dictates the output that can
be obtained from the sensor.

Electrical design maximum output:


The piezoresistivity of doped silicon is
such that there are two choices of 2 Example of the variation In nonllnearlty of a silicon pressure sensor as a function of
design: n-type resistors in a p-type thickness. As the pressure range Is Increased the nonllnearlty changes from positive,
through S-shaped, \o negative and back to positive. Circular diaphragm sensor, 5 V In-
substrate of (110) orientation or p-type put, 150 mV output
resistors in an n-iype substrate of (100)
orientation. The second orientation is 5000 fl (applied voltage 5 V), n44 = 1-15 these dimensional restrictions have a
more favoured because of better lineari- x 10~9 Pa" 1 , v = 0-07, omax = 100 large effect on the output. Long resistors
ty and because it enables one to use MPa, the maximum output is about 270 are often folded to the shape of an S or a
anisotropic etching. The gauges are sen- mV. U to keep them near the edge. A prac-
sitive to tension and compression along The values of the bridge current; and tical maximum output for the example
their length and also, to an equal and resistance R will be chosen to suit the ex- quoted above would be 150 mV, or 3%
opposite extent, to stresses perpen- ternal circuit, limited only by resistive of the applied voltage.
dicular to them. If pressure is applied to heating in the gauge. The commercially
the diffused side of the bridge illustrated available sensors all differ. The doping Diaphragm thickness upper pressure
in Fig. 1 the upper and lower gauges will level, on the other hands is fixed by limit: For a 100 kPa (1 bar) pressure
extend and thus increase in resistance, temperature considerations to be about 3 range typical diaphragm dimensions are
while the left and right hand gauges x 1018 atoms/cm3, giving the value of a radius of 1 mm and a thickness of
sense the transverse tensile stress and n44 quoted above. The surface resistivity, 27 jim. Higher pressure ranges are ob-
will decrease in resistance by an almost depending on the junction depth, is then tained by increasing the thickness:
equal amount. The four are used typically 120 fi/Q. The gauge resistance doubling it will increase the pressure
together as a complete bridge, whose will be defined by the shape of the range by a factor of four.
output for a circular diaphragm is given resistor, and for process control applica- The thickness can be increased until it
by the formula tions, subject to intrinsic safety re- approaches the size of the diaphragm,
quirements, typical limitations of 1mA which then ceases to function as a
Pr2 and 5V will define a resistance of
V = iR %n44 (1 - v) diaphragm at all. Silicon pressure
h2 5000 J2, with an aspect ratio of 5000:120 transducers are generally available up
or 42:1. to about 70 MPa (Druck), although
where / and R are bridge current and
gauge resistance, n44 is a piezoresistive In the example quoted above it is special designs will go up to 150 MPa.
coefficient for silicon, v is the Poisson's assumed that the whole strain gauge will At such levels the mounting and
ratio for <011> directions, P is the ap- see the maximum stress of 100 MPa. In pressure connections are likely to cause
plied pressure, h is the diaphragm reality the resistor will have a finite size. more problems than the chip itself.
thickness and r the radius of the Orienting the mask to generate the
diaphragm. recesses on one face of the silicon wafer Lower pressures the problem of
with respect to the diffusion on the op- nonlinearity: As the pressure range is
The maximum stress at the diaphragm posite face can easily result in alignment
edge is equal to lowered, so the diaphragm must be
errors, and for this reason the gauge will made progressively thinner. The
have to be spaced a certain distance ultimate limit would be when the diffu-
from the diaphragm edge. The final sion depth (1-2/um) approached the
max = W choice of dimensions depends on the neutral axis of the diaphragm, and
quality of the manufacturer's silicon diaphragms 7 ^m thick have
and the maximum output is therefore photolithography and the degree of been achieved for other purposes. For
theoretically equal to reproducibility he requires from sensor pressure sensors, however, the
to sensor. tolerances on thickness, or output, and
1/2
^ * 4 4 ( 1 - v)omax As the contribution of the gauge to on diaphragm taper set a practical limit
pressure sensitivity is proportional to the of about 20 jim, or thicker if mechanical
For a diaphragm with ;' = 1mA, R = square of its distance from the centre, machining is used. When this limit is
172 ELECTRONICS & POWER FEBRUARY 1983

15r

3=10
. /i 0.03
pressure sensitivity (negative)

resistance change,
resistance (positive)

en
o
/
/ 50 100

-5
y temperature, C
io 18 io 1 9 io 2 0 i o 2 1 .22
10'
dopant concentration, atoms/cm3

3 Variation in resistance with temperature for boron-doped 4 Temperature coefficients of resistance and of pressure sensitivi-
silicon strain gauge ty as a function of dopant concentration for boron-doped silicon
reached it may be possible to increase pressures the sensor characteristic internal or external compensation, at
the radius instead, although the becomes S-shaped and both positive and least for zero.
manufacturer will want to avoid using negative nonlinearities are present.
too many different photolithographic Below about 20 kPa the nonlinearity Temperature zero shift: The resitivity of
masks. Increasing the ratio of dia- becomes positive and intolerably high. silicon doped with 3 x 1018 boron
phragm diameter to thickness will in- These figures only apply to a par- atoms/cm3 increases with temperature at
crease the sensitivity, but at the same ticular design of circular diaphragm, 0-2 to 0-3%/K. The increase is
time it will also increase the nonlineari- but it is notable that below 100 kPa some nonlinear, following a curve such as that
ty. manufacturers compromise their speci- in Fig. 3. If the bridge is perfectly
Nonlinearity in silicon diaphragms fication. They may prefer to quote a balanced then all four arms, or gauges,
arises from the mechanics of the lower output than a worse nonlinearity; will increase proportionally with
diaphragm and from the piezoresistive how far one reduces the output is temperature, and the bridge will remain
effect itself. The piezoresistivity of governed, apart from the limitations of balanced. In reality there will be an off-
transverse gauges is more linear than for the amplifier, by the extent to which one set at zero pressure which will change
radial ones, but for <01 l>p-type gauges trusts the stability of the zero. This is with temperature in the same way as the
the nonlinearity of the gauges in tension, discussed in more detail below. resistors. The less the offset, the less the
or transverse compression, approxi- Some manufacturers achieve better problem. That is the basic temperature
mately compensates for those in compres- linearities by using different proprietary zero dependence.
sion, or transverse tension, if two of each gauge configurations. ICT has a long Unfortunately, however, it is not the
are used to complete the bridge. The rectangular diaphragm with transverse sole factor. There are other effects that
piezoresistive contribution to the gauges which sense the barrel-like alter the temperature dependence of the
nonlinearity will depend on the level of distortion across the centre, taking ad- individual gauges, and once the sen-
strain, or the output of the chip. vantage of the more linear performance sitivities of the gauges differ, the effect
The mechanical nonlinearity has two of transverse gauges and the increased on the temperature zero dependence is
components. When a pressure P is ap- output of this form of diaphragm. En- dramatic. Consider, for example, a 5 K,
plied, the diaphragm deflects, and at devco uses a diaphragm with thick 1 mA bridge with an initial offset of
first the strain is linearly proportional to 'islands' and thin channels below the 20 mV at 20C that changes to 22 mV at
P. As the strain increases the tension in strain gauges, which again sense 70C. If the temperature sensitivity of
the diaphragm (the balloon effect) will transverse stress. Motorola uses a shear- one gauge is changed by only 1 % from
reduce the overall stress levels by a fac- gauge configuration. Using these 0-2 to 0-202% per degC, the zero at
tor dependent on P2. However, at the methods it is possible to go down to 70C is changed from 22 to 23-3 mV.
surface of the diaphragm this same ten- 25 kPa without compromising on The temperature dependence of the out-
sile stress will add to the tensile compo- nonlinearity or output signal. With the put now averages 0-33%/K, an increase
nent of the bending stress a factor 'islands' design the small area under of 65%.
dependent on P3. maximum stress can also result in a Such changes in the temperature
For circular diaphragms of the type strength advantage, and so enables such dependence of individual gauges can be
shown in Fig.l, designed for a pressure sensors to be used at higher maximum caused by:
range of about 200 kPa, these two factors pressures.
practically cancel out and, when the Large, thin diaphragms are also more differences in shape and diffusion
diaphragm is pressurised on the diffused sensitive to frequency, the resonant fre- depth
face, the output signal is almost linear. quency being proportional to h/r2. Most leakage currents
When pressure is applied to the reverse sensors have resonant frequencies of nonohmic contact resistance at the
face, however, the two factors add to 50 kHz and above, but this can also be aluminium-silicon interface
produce a highly nonlinear compromised for low pressure ranges. external stresses.
characteristic. At lower pressures the
difference in linearity between the two Changes in the overall shape of the
pressure directions becomes more ex- Temperature effects gauges, due to errors in photo-
treme. Compared with other types of strain lithography or variations in diffusion
The range of terminal-based gauge, boron-doped silicon is very sen- depth, will contribute in the first order to
nonlinearity measured on sensors with sitive to temperature. There are essen- the offset in output signal at zero
circular silicon diaphragms is shown in tially two effects: the temperature pressure. The position of the p-n junc-
Fig. 2. Terminal based nonlinearity is dependence of resistance, which affects tion will vary with temperature, and any
about twice the often quoted best- the zero; and the temperature inequality between gauges will con-
straight-line (BSL) fit. At high pressures dependence of the pressure sensitivity, tribute to the temperature zero shift. It is
the nonlinearity is positive, whereas at which affects the span. It would be im- quite common to find small differences
200-300 kPa it is close to zero. At possible to operate a silicon strain- in temperature sensitivity between the
100 kPa it is negative, and at lower gauge pressure sensor without providing pair of gauges in tension and those in
ELECTRONICS & POWER FEBRUARY 1983
compression, even when their geometric wrong way round for good linearity. The
shape is nominally identical. oxide is also a home for contaminating
Leakage currents in these devices can ions, notably sodium, whose electro-
increase by ten times if the temperature static fields cause local distortion and in-
rises by 25 K. A leakage current of stability of the p-n junction. Thermal
10 nA across one arm of a 5kft, 1 mA stresses in the mounting or simple elec-
bridge will produce an offset of 2 trical leakages under varying humidity
0-025 mV. Leakage currents of this conditions are further sources of error.
order can easily occur in manufacture. 'o Some of these problems can be avoid-
At 75C, however, this current could -2 ed in the design and manufacture of the
have risen to the order of 1 \iA and give chip. Thermal cycling and 'burning in'
an offset of 2-5 mV. Leakage currents 0 50 100 are standard methods in the semicon-
temperature, #C
are a main contributor to the ductor industry and would be expected
temperature zero shift at higher to reduce high temperature shifts.
temperatures and are the factor limiting Gauges 'buried' below the silicon sur-
the temperature at which silicon- face by ion implantation, leaving a p-n
diaphragm pressure sensors can be junction above as well as below the im-
used. 5 Typical temperature dependence oi planted gauge, ensure that there is no
Nonohmic contact resistances should sensor output under constant-current contact with the oxide at all. Contact is
have been detected at the manufactur- conditions made through wide lead-in areas off the
ing stage. They are, however, a common actual diaphragm, and so the metal-
fault in semiconductors, their occur- By slightly reducing the doping level the silicon interface is large and not under
rence will be unpredictable and their curve can be 'tilted' to the left and the stress.
temperature dependence may be highly output held constant over a lower For many general-purpose applica-
nonlinear. temperature range. Some manufacturers tions these levels of errors may be in-
therefore give a choice of compensated significant. They are, however, the fac-
External temperature-dependent temperature range. This method of com-
stresses on the diaphragm can be caused tor which limit the level of acceptable
pensation is subject, of course, to the output from low-pressure devices. They
by differential thermal expansion in the tolerance band within which the doping
mounting or by the silicon dioxide layer are particularly important in high-
level itself can be maintained. If the out- accuracy instruments, such as altimeters
directly over the gauge surface. put is to be kept constant over a wider
To avoid any transient effects it is or differential pressure devices for
temperature range, such as say - 2 0 to measuring flow.
essential that all four strain gauges on + 70C, external compensation will be
the chip are at the same temperature. required.
This is generally achieved by placing Limits on temperature range: The
If a constant voltage supply is chosen highest temperature at which the sensor
them close together. On a 5 kfl, 1 mA can operate is dictated by leakage ef-
bridge an offset of 0 25 mV can be caus- the pressure sensitivity decreases with
temperature, as described above, and fects on the chip or to shifts in the mount-
ed by just one gauge being 0 1 K hotter ing. Sensors designed for higher
than the other three. For sensitive will always need external compensation.
temperatures must have fully insulating
calibration and compensation layers instead of the p-n junction. The
measurements it is essential to stabilise Thermal drifts and stability: Zero drift,
particularly after heating and cooling, is lowest operating temperature is also set
the temperature, and it can be helpful to by the materials in the mounting.
use the bridge resistance directly as a the Achilles heel of silicon pressure sen-
sors. It is difficult to quantify or to prove Within the overall temperature range
nonlinear temperature scale. or disprove; some manufacturers quote most manufacturers quote a compen-
Temperature span shift: The stability or reproducibility values and sated range within which the transducer
piezoresitive coefficients of silicon, and others quote for temperature hysteresis. performance is clearly specified. The
thus pressure sensitivity of the sensor, During pressure-sensor development we specification for span, in particular, will
decrease with temperature. Unlike the have observed: be governed by the curve in Fig. 5. A
resistance, the dependence is fairly typical compensated range would be 0 to
linear. The magnitude is - 0 - 2 to hysteresis between heating and cool- 50C within an operating range from
-0-3%/K and therefore requires com- ing curves of about 0'3 mV -40 to +150C.
pensation. instability on heating around 0C
This can be achieved by using a con- drifts at lower temperatures, Compensation
stant-current bridge supply and a con- recovered by heating to 100C Silicon-diaphragm pressure
trolled doping level. Fig. 4 shows the permanent shifts at 100C of several transducers all need additional compen-
dependence of the temperature coeffi- mV. sation. Some have discrete resistors,
cients of zero and span on doping level. some a hybrid circuit and some are
By choosing the doping level to equal These errors are shown schematically in available with the circuitry on the' chip
one of the crossover points the two Fig. 6. itself. Individual compensation will
temperature coefficients are equal and All those factors that were mentioned always be required for zero offset,
opposite. The lower crossover point is as contributing to the zero temperature temperature zero shift and variability in
generally used because the pressure characteristic, which is repeatable, can output, while compensation for
sensitivity, which also depends on dop- contribute to these drifts, which are not. nonlinearity and temperature span shift
ing level, is higher. Any reduction in the The surface oxide, which is in direct depends on the specification to be
output signal due to a fall in sensitivity is contact with the diffused strain gauges, achieved.
then accompanied with an increase in is a particular source of trouble. Its ther- The variability in output signal is due
bridge voltage due to the increase in mal expansion coefficient is higher than chiefly to variations in diaphragm
gauge resistance, and therefore main- that of silicon and can therefore in- thickness, with contributions from errors
tains the value of the signal. troduce stresses or slippage at the sur- in alignment and taper mentioned
In theory the output is now indepen- face. Some surface oxides are sensitive above. This variability may easily reach
dent of temperature. In practice, to humidity, which no doubt accounts for 30% for low pressure ranges. Each
because the characteristic in Fig. 3 is the instabilities at around 0C and the chip therefore requires individual
curved, the dependence of output on drifts that can be recovered by heating calibration or compensation. Nonlineari-
temperature is nonlinear, as shown in to 100C. An absolute pressure sensor ty will also vary with thickness, but ex-
Fig. 5. There the doping has been with the reference vacuum on the diffus- ternal compensation is more complex,
chosen so that the output is constant to ed side should be insensitive to humidity and is avoided if possible.
within 0-25% between 20 and 70C. but, as mentioned above, this is the Initial offset and temperature zero shift
174 ELECTRONICS & POWER FEBRUARY 1983
and its expansion with temperature will
complicate the performance.

Overload: As mentioned above, the


silicon diaphragm will withstand an
overpressure of two to five times full
scale range, depending on the safety
factor used. The overpressure limit may
instead be that at which the materials in
the mounting shift or break. For dif-
ferential pressure transmitters the
mounting must be designed such that the
zero does not shift under a high line
pressure the pressure and
temperature sensitivities are reasonably
independent of line pressure and the
device must be protected from acciden-
tal exposure to the line pressure on one
side only. Because of the small deflec-
tion of the diaphragm of the order of
micrometres it is not possible to build
in a mechanical stop to prevent it mov-
ing beyond a certain point. Overload
protection must be provided separately,
and this will greatly complicate the
mounting. Specifications for freedom
6 Schematic diagram of zero errors during thermal cycling from radio-frequency interface or intrin-
sic safety will provide futher constraint.
can be easily compensated for by adding high line pressures and the general
individual shunt and series resistances to reliability. Other factors affecting reliability:
the arms of the bridge, achieved for ex- Silicon pressure sensors are subject to
ample by laser trimming of an external Size: Small size is one of the important other problems common to micro-
hybrid circuit. In this way there should advantages of silicon pressure sensors. electronic devices. Some should have
be little problem in reducing the Many chips are around 4 mm square, been detected at the wafer stage. Corro-
temperature zero shift to the order of and with improvements in photo- sion of the aluminium contact pads and
0-01% of full scale output per kelvin. lithography the size of the complete the detachment of wire bonds are,
Thanks to the uniformity of modern device is likely to be dictated by the chip however, noted as possible causes of
doping methods the temperature span mounting, the size of the compensating failure.
shift is generally very repeatable, and it circuitry and the pressure and electrical
does not drift like the zero. If a wide connections rather than by the chip. Conclusion
compensated temperature range is re- Very small devices can be made, for ex- Silicon-diaphragm pressure sensors
quired the curve in Fig. 5 can be cor- ample, for medical applications. are ideal for use
rected with a simple resistor in shunt
with the bridge, a positive-feedback Pressure hysteresis: A silicon at pressures of 100 kPa and above ap-
method or a thermistor circuit applied to diaphragm on its own should be entirely plied in one direction only
the constant-current supply. It may be free from pressure hysteresis. It is essen- for a temperature range not ex-
possible to use a standard circuit without tial, however, to isolate the diaphragm ceeding 50 K, say from 0 to 50C
individual testing. as far as possible from any mechanical with dry gases or nonconducting non-
joint or interface likely to exhibit corrosive fluids
Packaging hysteresis. If the diaphragm is mounted for accuracies down to 0-25%.
Outwardly, the package will have directly on to a silicon platelet or glass
been designed to suit the application in tube the joint must be entirely free of The chips need individual electrical
mind, with suitable pressure ports and hysteresis, which is why gold eutectic testing and conditioning and their full
electrical connections. There is no stan- and ion migration bonding are preferred scale output will not be more than 3% of
dardisation and all devices are different. to epoxy adhesive or glass frit. the voltage applied.
The package must protect the chip from Specifications for pressure hysteresis are Beyond these limits the user may have
mechanical shock and from thermally in- generally good. to accept
duced stresses, hysteresis and light Chemical, compatibility:. The diffused
(some sensors are excellent photo- face of a silicon transducer consists of lower output
meters). A common method is to attach exposed silicon, silicon dioxide, degraded specification on linearity or
the chip to a silicon backplate using gold aluminium and gold. The undiffused temperature
eutectic bonding. If this is done under face is pure silicon. Any fluid contacting more complex electrical compen-
vacuum, the chamber formed between the transducer directly must be noncon- sating circuitry
the backplate and the original chip acts ducting and compatible with those overload protection
as a reference vacuum for absolute materials as well as any within the separator diaphragm
pressure measurements. The silicon can mounting. If it is only possible to apply higher price.
also be attached to the end of a boro- the fluid to the undiffused face, the
silicate CPyrex') glass tube, which has a nonlinearity will be worse. If neither face Users must be particularly cautious of
similar coefficient of linear expansion, is possible, the transducer must be pro- the zero stability, notably after large
using electrostatic or ion-migration bon- tected by a gel or by a flexible separator changes in temperature.
ding. Other bonding methods include diaphragm with the volume between fill-
the use of tin-gold and glass frit. The ed with an inert fluid, such as silicone
mounting and packaging design will The author is grateful to Brown Boveri Kent Ltd.
oil. Silicone oil must be filled under and to ERA Technology Ltd. for permission to
determine the size of the overall device, vacuum because of the solubility of air, publish this article.
the likelihood of pressure hysteresis, the
compatibility of different fluids, the Dr. Greenwood was formerly with Kent Process Control Ltd., Luton, Beds., and is now with
ability of differential sensors to withstand ERA Technology Ltd., Cleeve Road, Leatherhead, Surrey KT22 7SA, England

Вам также может понравиться