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This test method is under the jurisdiction of ASTM Committee C01 on Cement
and is the direct responsibility of Subcommittee C01.31 on Volume Change.
Current edition approved Dec. 1, 2009. Published January 2010. Originally
approved in 1967. Last previous edition approved in 2007 as C596 07. DOI:
10.1520/C0596-091.
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Section on Safety, Manual of Cement Testing, Annual Book of Standards,Vol
04.01.
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For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Standards volume information, refer to the standards Document Summary page on
the ASTM website.
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C596 091
example of the method is given in Fig. 1 where a logarithmic scale is used suspect unless it exceeds 70 millionths. Where a test result is
for the drying shrinkage values and a reciprocal scale for the total time in the average of twelve specimens, four specimens being tested
weeks.
from each of three batches, the difference between duplicate
13. Precision and Bias results by the same operator should not be considered suspect
13.1 Precision: unless it exceeds 40 millionths.
13.1.1 The single-laboratory-operator multibatch-day preci- 13.1.3 ReproducibilityThe average result of four or
sion has been found to be 0.0223 (1S %) and the single- twelve specimens reported by one laboratory should not be
operator multilaboratory-batch-day precision has been found to considered suspect unless it differs from that of another
be 6.6 (R1S %) as defined in Practice E177, therefore 95 % laboratory by more than 25 % of their mean.
percent of the time two test results (each the average of four
13.2 BiasNo justifiable statement can be made on the bias
determinations of properly conducted tests) obtained by the
same operator on different days should not differ by more than of this test method since no reference samples are available.
70 millionths, and the test results (each the average of four
determinations of properly conducted tests) obtained by two 14. Keywords
laboratories should not differ by more than 25 % of their mean. 14.1 drying shrinkage; hydraulic cement; method; mortar
13.1.2 RepeatabilityWhere a test result is the average of
four specimens from a single batch, the difference between
duplicate results by the same operator should not be considered
SUMMARY OF CHANGES
Committee C01 has identified the location of selected changes to this test method since the last issue,
C59607, that may impact the use of this test method. (Approved December 1, 2009)
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C596 091
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