Rheocalc Manual PDF

BROOKFIELD RHEOCALC
APPLICATION SOFTWARE
Programming and Operation Instructions
Manual No. M/99-222-D0106
SPECIALISTS IN THE
MEASUREMENT AND
CONTROL OF VISCOSITY
BROOKFIELD ENGINEERING LABORATORIES, INC.

11 COMMERCE BOULEVARD, MIDDLEBORO, MA 02346 USA
TEL 508-946-6200 or 800-628-8139 (USA excluding MA)

FAX 508-946-6262 INTERNET http://www.brookfieldengineering.com
The information in this document is believed to be accurate and reliable. However,
Brookfield Engineering Laboratories, Incorporated, cannot accept any financial or other
responsibilities that may result from the use of this information. No warranties are granted or ex-
tended by this document.
Brookfield Engineering Laboratories, Incorporated reserves the right to change any or all
information contained herein without prior written notice. Revisions may be issued at the time of
such changes and/or deletions.
Any duplication of this manual or any of its parts without expressed written permission from
Brookfield Engineering Laboratories, Incorporated is strictly prohibited.
Any correspondence regarding this document should be forwarded to:
Brookfield Engineering Laboratories, Incorporated

11 Commerce Boulevard
Middleboro, Massachusetts 02346
U.S.A.
Telephone: (508) 946-6200
FAX: (508) 946-6262
Internet: http://www.brookfieldengineering.com
The following Brookfield Engineering Laboratories, Incorporated trademarks and service marks may
appear in this document:
Brookfield
Rheocalc
Rheovision
Wingather
Thermosel
UL Adapter
All other trademarks or registered trademarks are the property of their respective holders.
Copyright 2000 Brookfield Engineering Laboratories, Incorporated Printed in U.S.A.

Rheocalc 32 Programming and Operation Manual
Table of Contents
Section 1 - Introduction
About Rheocalc ........................................................................................................................... 1-1
System Requirements .................................................................................................................. 1-2
Registering Rheocalc ................................................................................................................... 1-2
Contacting Brookfield Engineering Laboratories, Inc. ............................................................... 1-2
Section 2 - Getting Started

Rheocalc Software Installation .................................................................................................... 2-1
RS-232 Cable Installation ............................................................................................................ 2-1
Starting Rheocalc ......................................................................................................................... 2-2
Section 3 - Using Rheocalc

Introduction ................................................................................................................................. 3-1
Main Menu .................................................................................................................................. 3-1
Main Menu Operation ........................................................................................................... 3-1
Main Menu Description ......................................................................................................... 3-2
Dashboard Page ........................................................................................................................... 3-3
Dashboard Page Operation .................................................................................................... 3-3
Dashboard Page Description ................................................................................................. 3-4
Tests Page .................................................................................................................................... 3-8
Tests Page Operation ............................................................................................................. 3-8
Tests Page Description........................................................................................................... 3-9
Run/Data Page ........................................................................................................................... 3-12
Run/Data Page Operation .................................................................................................... 3-12
Run/Data Page Description ................................................................................................. 3-14
Test Data Grid ................................................................................................................ 3-15
Test Data Plot ................................................................................................................. 3-18
Analysis Page ............................................................................................................................ 3-20
Analysis Page Operation ..................................................................................................... 3-20
Analysis Page Description ................................................................................................... 3-21
Bingham ........................................................................................................................ 3-22
Casson ............................................................................................................................ 3-23
NCA/CMA Casson ........................................................................................................ 3-24
Power Law ..................................................................................................................... 3-25
IPC Paste ....................................................................................................................... 3-26
Herschel Bulkley ........................................................................................................... 3-27
Setup Page ................................................................................................................................. 2-29
Setup Page Operation .......................................................................................................... 3-29
Setup Page Description ........................................................................................................ 3-29
Custom Page .............................................................................................................................. 3-33
Custom Page Operation ....................................................................................................... 3-33
Manual No. M/99-222-D0106 iii
Rheocalc 32, Programming and Operation Manual
Section 4 - B.E.A.V.I.S. Programs

What is a B.E.A.V.I.S. Program? ................................................................................................. 4-1
B.E.A.V.I.S. Commands .............................................................................................................. 4-1
Command Groups .................................................................................................................. 4-1
Wait Command Group ..................................................................................................... 4-1
Setup Command Group ................................................................................................... 4-1
Data Command Group ..................................................................................................... 4-1
Loop Commands Group .................................................................................................. 4-1
Save Data Commands Group .......................................................................................... 4-1
Report Commands Group ................................................................................................ 4-1
Command Examples .............................................................................................................. 4-4
Geometric Speed Progression Command Example ......................................................... 4-4
Up/Down Geometric Speed Progression Example .......................................................... 4-5
A Geometric Speed Progression Run At Multiple Temperatures .................................... 4-6
Section 5 - Troubleshooting
Communication Errors ................................................................................................................ 5-1
Instrumentation Setup ............................................................................................................ 5-1
Windows NT .......................................................................................................................... 5-1
Windows 2000 / XP............................................................................................................... 5-2
Communication Port Settings ...................................................................................................... 5-3
Appendix A - Customer Support
Appendix B - Drawings
Appendix C - Spindle and Model Codes
Index
iv Manual No. M/99-222-D0106

Section 1 - Introduction
About Rheocalc
Rheocalc is designed for use with either the Brookfield Engineering Laboratories, Inc.
DV-III Ultra, DV-III+, DV-III Rheometer, or DV-II+ Pro Viscometer and MS-Windows
2000 and above computer operating systems. Its purpose is to control the instrument
from a PC, collect data from the instrument and allow it to be saved, viewed, printed,
plotted and analyzed. Its features include:
An easy to learn and use graphical user interface.
A scripting language to allow flexible data collection.
Test Wizard for setting up commonly used tests.
On-line plotting of data during a data gather.
Background printing of data, graphs and programs.
Mathematical analysis of collected data.
Optional control of a Brookfield Engineering Labs temperature controller for

use with the Thermosel or Brookfield Engineering Labs temperature bath.
Manual No. M/99-222-D0106 1-1

Introduction
System Requirements
The system requirements outlined in Table 1-1 must be met in order for Rheocalc soft-
ware to operate properly.
Table 1-1: System Requirements

System Parameter Requirement
Microprocessor Pentium II, min.

Memory 128 MB RAM minimum; at least 256 MB RAM recommended
Video VGA (800 x 600 resolution) minimum
Operating System MS-Windows NT, 2000, XP
Mouse Required
RS-232 Port One free COM port required; a second COM port is required
for use with a temperature controller if desired.
Registering Rheocalc
With your software registration on file at Brookfield, we will notify you when new
releases of Rheocalc are introduced. To register, locate the registration.pdf file on the
software application disk. Complete the form and return to us by either mail, fax or email
(sales@brookfieldengineering.com).
Contacting Brookfield Engineering Laboratories, Inc.

Refer to Appendix A for customer support information.
1-2 Manual No. M/99-222-D0106

Section 2 - Getting Started
Rheocalc Software Installation

NOTE: Make sure all other software applications on your computer have been closed
before proceeding with Rheocalc software installation.
NOTE: You must log in as an administrator to install Rheocalc succussfully on your

PC.
1. Insert the CD-ROM disk into the appropriate drive on your computer.
2. If AutoRun is enabled on your computer, the CD-ROM will go directly to the Main
Welcome Screen of the installation.
3. If the CD-ROM does not automatically run after being read by the CD drive, run the
setup.exe program manually by performing one of the following steps:
a. Using Windows Explorer, open the window of the appropriate drive then select
the setup.exe file from the route directory of the CD.
b. Choose START from the desktop, then select RUN. Select BROWSE and locate
the appropriate drive, then select the setup.exe file from the route directory of the
CD. Select the OK button.
Using either method causes the Main Welcome Screen to be displayed.
4. Once the Main Welcome Screen of the installation is displayed, select NEXT to view
the available software installations, choose Rheocalc off of this list, then select
NEXT to install Rheocalc.
5. The keycode for the Rheocalc installation is printed on the silver label tucked inside
the CD-ROM jacket. Enter this keycode when prompted, then select NEXT and
follow the on-screen prompts to complete the Rheocalc software installation.
6. After installation, the Rheocalc program icon will be placed on the START/PRO-
GRAMS bar.
RS-232 Cable Installation

1. Make sure the instrument and optional temperature accessory are properly connected
to the appropriate communication (RS-232) ports on the host computer.
Manual No. M/99-222-D0106 2-1

Getting Started
Starting Rheocalc
1. Locate and select the Rheocalc icon within the Rheocalc group window. The
Rheocalc software will be started.
2. Select the DASHBOARD tab.
NOTE: After each COM port is selected, Rheocalc must be restarted to intialize the the
selected port.
3. From the Instrument Status section, select the appropriate computer COM port to
which the Rheometer is connected.
4. From the Instrument Status section, select the appropriate computer COM port to
which the optional temperature accessory is connected.
5. Once the COM ports have been selected, restart Rheocalc to initialize the COM ports
you have selected.
6. Once Rhecoalc has been restarted, the data boxes on the Dashboard page will display
live rheometer data.
NOTE: If live data is not visible within the data boxes, refer to
Section 5 - Troubleshooting.
2-2 Manual No. M/99-222-D0106

Section 3 - Using Rheocalc
Introduction
Section 3 describes the features and functions of each Rheocalc page and dialog box.
Main Menu
The Main Menu provides general commands and information which apply to all of
Rheocalcs pages.
Main Menu Operation
Viewing/Hiding Control Windows

1. Choose View from the Main Menu.
2. Click on a checked title to hide that Control Window.
3. Click on an unchecked title to show that Control Window.
4. Click on Tools/Default Toolbar Positions to return all control windows to their

default size and place.
NOTE: For more information about manipulating Control Windows, see the Custom
Page section.
Setting Up Instrumentation
1. Use Instrumentation/Rheometer COM Port to choose the port that the rheometer is
connected to.
2. Use Instrumentation/Accessory COM Port to choose the port (if any) that the op-
tional temperature controller is connected to.
3. Once communication is established with the rheometer, use Instrumentation/Auto

Zero to zero the rheometer.
Manual No. M/99-222-D0106 3-1

Using Rheocalc
Main Menu Description
View Menu
The View Menu is used to show/hide Control Windows.
Instrumentation Menu
The Instrumentation Menu is used to establish communications with the rheometer and
optional temperature controller.
Tools Menu
The Tools Menu is used to save the users settings or return to the default settings.
Help Menu
The Help Menu is used to access Rheocalcs online Help system.
Save Settings Button

The Save Settings button is used to save the current settings to an INI file.
Default Window Positions Button

The Default Window Positions button returns all control windows to their default size
and place.
About Button
The About button displays various system information including Rheocalc, Windows,
instrument and BDE versions.
Help Button
The Help button displays the Rheocalc online help file.
Exit Button
The Exit button exits the user from Rheocalc. Any open data files are closed as well as
any open COM (RS-232) ports.
Date/Time
The Date and Time boxes display the current date and time.
Test Status
The Test Status box indicates whether a test is currently running.
Test File Name

The Test File Name box displays the name of the test which is currently running.
3-2 Manual No. M/99-222-D0106

Dashboard Page
The Dashboard Page, shown in Figure 3-1, gives a live display of the current readings.
Figure 3-1: Dashboard Page
Dashboard Page Operation

The Dashboard Page can be used to establish communication with instrumentation and to
set single speeds and/or temperatures.
Establish Instrument Communication

Use the appropriate cables to connect the rheometer or temperature controller to the host
computer (part #DVP-80 for the DV-III, DV-III+ and DV-II+ Pro instruments and part
#HT-106 for Brookfield temperature controllers). The RS-232 cable for the TC-50x
series baths is supplied with the bath. Select the COM (RS-232) port for the rheometer
and attached temperature controller using the Rheometer/Accessory drop down list. If
the port selected is already in use (by Rheocalc or another application) or is unavailable
for any other reason, a message box is displayed. If communication is lost with any of
the connected instrumentation, a message box is displayed after approximately 10 sec-
onds. If this problem occurs, refer to Section 5 Troubleshooting for more information.
Manual No. M/99-222-D0106 3-3

Using Rheocalc
Set Single Speed

1. In the Set Speed/Temperature Control Window, choose the Speed tab.
2. Enter the desired speed in either the RPM or Shear Rate field.
3. Click the Run button.
Set Single Temperature

1. In the Set Speed/Temperature Control Window, choose the temperature tab.
2. Enter the desired temperature in the Temperature field.
3. Click the Run button.
Dashboard Page Description
Dashboard Control Window

The Dashboard Control Window displays the instrument status and the current readings.
Viscosity
The Viscosity display indicates the fluid viscosity in units of centipoise (cP) or
millipascal-seconds (mPas).
Speed
The Speed display indicates the current rotational speed of the spindle (in rpm).
Torque
The Torque display indicates the % of scale (the % of the rheometers full scale
torque range capability for the model in use) measured by the rheometer.
Shear Stress
The Shear Stress display indicates the force per unit area required to move the fluid in
units of dynes per square centimeter (D/cm2) or Newtons per square meter (N/m2).
Shear Rate
The Shear Rate display indicates the velocity gradient of fluid rotating with the
spindle in units of reciprocal seconds (1/sec).
Temperature
The Temperature display indicates the fluid sample temperature measured by the
temperature controller, accessory, or rheometer temperature probe in units of C or F.
NOTE: When a temperature controller is in use, the value displayed in the Temperature
display is read from the controller's probe and is shown in red. Otherwise, the
temperature is that sensed by the rheometer's probe is shown in yellow.
3-4 Manual No. M/99-222-D0106

Temperature Controller Setpoint

The Temperature Controller Setpoint display indicates the current temperature set
point if a temperature controller is connected in units of C or F.
NOTE: This Temperature Controller Setpoint display is blank if no controller is present.
Instrument Status
The Instrument Status display indicates the type of rheometer or temperature control-
ler connected to the computer. A green light is displayed along with the instrument
identification.
NOTE: A red light indicates that an instrument is not connected.
Advanced Button
The Advanced button displays the Communication Port Settings dialog box as shown
in Figure 3-2. This window is used to display the communication parameters for the
devices being used with Rheocalc and to adjust the communications timing if neces-
sary.
NOTE: Refer to Section 5 - Troubleshooting for more information on the Communi-

cations Port Setting window.
Figure 3-2: Communications Port Setting Window
Manual No. M/99-222-D0106 3-5

Using Rheocalc
Model
The Model display indicates the rheometer model type being used with Rheocalc.
NOTE: The Model Display information is automatically provided by the rheometer.
Spindle
The Spindle display indicates the spindle type currently installed on the rheometer.
NOTE: The Spindle selected must be updated when the actual spindle is changed to
ensure correct viscosity, shear stress and shear rate calculations.
Maximum Viscosity @ RPM

The Maximum Viscosity @ RPM display indicates the maximum measurable (math-
ematically) viscosity based on the model, spindle, and speed (rpm) in use. As differ-
ent spindles are selected using the spindle box on this page, this maximum value is
automatically updated.
Zero Button
The Zero button displays a message box that reminds the user to level the instrument
and remove the spindle in preparation for the auto zero process. Once the instrument
is leveled and the spindle is removed, the OK button in the message box can be
pressed to perform the auto zero function. This process takes approximately 10-12
seconds.
NOTE: The Auto Zero function must be performed before the instrument can be used
to collect data.
Set Speed/Temperature Control Window

The Speed/Temperature Control Window is used to set single speeds and/or tempera-
tures.
RPM (Speed tab)

The RPM field is used to enter the speed (in RPM) at which to run the rheometer.
Entering a value into this field will automatically update the Shear Rate field.
Shear Rate (Speed tab)

The Shear Rate field is used to enter the speed (in 1/sec) at which to run the rheom-
eter. Entering a value into this field will automatically update the RPM field.
Temperature (Temperature tab)

The Temperature field is used to enter the temperature (in the current units, C or F)
at which to run the optional temperature controller.
3-6 Manual No. M/99-222-D0106

Run Button
If the Speed tab is chosen, the Run button runs the rheometer at the speed specified.
If the Temperature tab is chosen, the Run button sets the controller to the temperature
specified.
Stop Button
If the Speed tab is chosen, the Stop button stops the rheometer. If the Temperature
tab is chosen, the Stop button sets the controller to the Standby Temperature (refer to
the Setup page section for more information).
Manual No. M/99-222-D0106 3-7

Using Rheocalc
Tests Page
The Tests page, shown in Figure 3-3, is used to create, save and print B.E.A.V.I.S
(Brookfield Engineering Advanced Viscometer Instruction Set) programs.
NOTE: Refer to Section 4 - B.E.A.V.I.S Programs for more information on B.E.A.V.I.S

Programs.
Figure 3-3: Tests Page
Tests Page Operation
Loading an Existing Program

1. Select the LOAD button.
2. Using the standard Load File dialog box, select and load the appropriate program file
(*.RCP).
Creating a New Program

1. Highlight the line in the Program Grid where you want to insert a command.
3-8 Manual No. M/99-222-D0106

2. Highlight the appropriate command in the Command List and either double-click the
command or select the INSERT button to place the command in the Program Grid.
3. Continue to build your program in this manner using the INSERT button to add
commands and the DELETE button to remove unwanted commands.
NOTE: A new command cannot be added until the appropriate command parameter has
been entered on the previous line if required.
Saving/Printing Programs
1. Select the SAVE button to save the program to disk using the standard Save File
dialog box.
2. Select the PRINT button to print the program using the standard Print dialog box.
Setting up a Manual Test

1. Click on the Manual tab to display the Manual Page.
2. Enter the desired speed and click the Run button to start the rheometer.
3. If an optional temperature controller is connected, click on the Temperature tab, enter

the desired temperature and click the Run button to set the controller.
4. Once the desired speed and temperature have been reached, click the Start Program
button.
5. Click the Data button whenever a data point is desired.
6. Click the Stop Program button when data collection is complete.
Tests Page Description

The Tests page is shown in Figure 3-3 and described in the following paragraphs.
Program Grid
The Program Grid displays the current user program. Each line consists of a line number,
a three letter command, and a parameter if one is required.
Settings Dialog
The Settings Dialog is used to set options for the LWC and RMR commands (Refer to
Section 4 - B.E.A.V.I.S Programs for more information on these commands).
Manual Page
The Manual page is used to gather data at manually controlled speeds and tempera-
tures.
Manual No. M/99-222-D0106 3-9

Using Rheocalc
Test Wizard Button

This button displays the Test Wizard dialog which allows the user to easily setup
several common tests.
Insert Button
The Insert button inserts the command highlighted in the command list.
Delete Button
The Delete button removes the highlighted line in the program grid.
Clear Button
The Clear button clears the program grid.
Confirm Deletions
When checked, the Confirm Deletions check box causes a message box to be displayed
requesting confirmation whenever an attempt is made to delete a program line or to clear
the entire program.
Shear Rate Mode

When checked, the Shear Rate Mode check box causes all speed entries (i.e. for SSN and
SSI commands) to represent shear rates (units of 1/second) instead of rotational speed
(rpm).
Load Button
The Load button displays a standard File Load dialog box. This dialog box displays
Rheocalc program files that were previously saved and can now be loaded.
Save Button
The Save button displays a standard file save dialog box. This dialog box allows pro-
grams to be saved for later use. B.E.A.V.I.S. programs are saved as lines of ASCII text
consisting of a line number, command, and parameter.
Print Button
The Print button displays the standard Windows Print dialog box which allows a printer
to be selected, its properties changed and the data to be printed.
NOTE: Refer to the MS-Windows on-line help for more information regarding printing
and printer setup.
Start Button
The Start button starts the program displayed in the Program Grid.
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Stop Button
The Stop button stops the program displayed in the Program Grid. The rheometer will
stop and any attached temperature controller enters stand-by mode and sets the controls
to the default temperature of 25 C.
Next Button
The Next button causes the program to skip to the next program step before the wait
condition is reached.
NOTE: The Next Button is only enabled while a program is running and the current
step is a Wait command (i.e WTI, wait for time interval).
Manual No. M/99-222-D0106 3-11

Using Rheocalc
Run/Data Page
The Run/Data page shown in Figure 3-4 allows the execution of B.E.A.V.I.S. programs
and browsing and editing of any valid Rheocalc data file.
Figure 3-4: Run/Data Page
Run/Data Page Operation

The Run/Data page is used to execute programs and to view, edit, load, save, export,
import and print data.
Executing a Program
1. Ensure that a new or existing program is displayed in the program Grid (Tests Page).
2. Click the Start Program button in either the Test Status Control Window or the Test
Setup Control Window (Tests Page).
3. The program status (i.e. Step Time, Step Status, Loop Count, Reading Time) will be
displayed in the Test Status Control Window at the top of the page. Live data will be
displayed in the Test Data Grid Control Window in the middle of the page. As they
are collected, data points will be plotted on the graph in the Test Data Plot Control
Window at the bottom of the page.
3-12 Manual No. M/99-222-D0106

Viewing Saved Data

1. Either click the LOAD button OR
2. Double click on any line in the Plot List.
3. A standard file load dialog will appear. Using this dialog box, select and load the
appropriate data file (*.DB).
4. The data file will be listed in the Plot List: on the first line if the LOAD button is
used, or on the selected line if the Plot List is double clicked.
5. The data will appear in the Test Data Grid and the datas plot will be added to the
existing plots in the Test Data Plot. Up to five data files may be plotted at one time.
6. To remove a data sets plot from the graph, uncheck the box beside the data file name
in the Plot List.
7. To view a different data set in the Test Data Grid, click on the data files name in the
Plot List.
Loading Existing Data

1. Select the LOAD button.
2. Using the Load File dialog box, select and load the appropriate data file (*.DB).
Saving/Printing Data
1. Select the SAVE button to save the data to disk using the standard Save File dialog
box.
2. Select the PRINT button to print the data using the standard Print dialog box. The
data, sample name, and user notes are all printed.
Exporting Data
1. Select the EXPORT button. Use the standard Save File dialog box to save the data
in MS-Excel format (*.XLS) for use in other programs.
Importing Data
1. Select the IMPORT button. Use the standard Load File dialog box to load in
Rheocalc Text Data from previous versions of Rheocalc (DOS and Windows 3.x
versions). The data is displayed in the Data Grid and treated as unsaved data.
Analyzing Data
1. Select the ANALYZE button. The Analysis page is displayed showing the results
and graph for the selected equation using the data displayed on the View/Edit page.
Manual No. M/99-222-D0106 3-13

Using Rheocalc
Extracting Data from a Rheometer

1. Ensure a rheometer is connected to the PC and is communicating with Rheocalc.
2. Select the DV-III+ button. After a few seconds, data will appear in the Data Grid.
Data was taken with the rheometer in its stand-alone mode and is extracted from the
rheometers internal data buffer.
NOTE: This option only works with a DV-III, DV-III+ or DV-III Ultra connected.
Run/Data Page Description

The Run/Data page is shown in Figure 3-4 and described in the following paragraphs.
Test Status
Step Time
The Step Time box displays the amount of time the current step (as displayed in the
program grid) has been executing.
Loop Count
The Loop Count box displays the number of loop iterations remaining in the current
loop block (consisting of an LSC + LEC or LWC + LWE command).
Step Status
The first box within the Step Status area displays the current steps action (i.e. for a
WTI command, the box displays the message: COUNTING DOWN TIME INTER-
VAL. The second box displays the pertinent step parameter (i.e. for a WPT command,
the box displays the current % torque value so the user knows how far from the target
torque the step is).
Reading Time
The Reading Time box displays one of the following:
Time Since Last Reading

The elapsed time since a data point was last taken. If a data interval is not in
effect (i.e. the time of the next data point is not known), this is the time that is
displayed.
Time Until Next Reading

The time that must elapse until another data point is taken. This value is dis-
played when a fixed data interval is in effect (using the DCI command).
Start Program Button

The Start button starts the program displayed in the Program Grid.
3-14 Manual No. M/99-222-D0106

Stop Program Button

The Stop button stops the program displayed in the Program Grid. The rheometer
will stop and any attached temperature controller enters stand-by mode and sets the
controls to the default temperature of 25C.
Next Button
The Next button causes the program to skip to the next program step before the wait
condition is reached.
NOTE: The Next button is only enabled while a program is running and the current
step is a Wait command (i.e. WTI, wait for time interval).
Data Button
The Data button is used to collect a single data point during a Manual Test (refer to
the Tests Page section).
Test Data Grid

Model
The Model box displays the spring torque of the instrument from which the data was
taken. When in edit mode, this value can be changed by using the arrow to the right of
the box. Once a change is made, all data in the grid is re-calculated based upon the new
choice.
Spindle
The Spindle box displays the spindle used to take the data. When in edit mode, this value
can be changed by using the arrow to the right of the box. Once a change is made, all
data in the grid is re-calculated based upon the new choice.
File
The File box displays the file and path of the data file being used.
Data Display Grid

The Data Display grid displays the data (newly gathered or loaded from disk). Use the
mouse to select a field to be edited when in edit mode.
Manual No. M/99-222-D0106 3-15

Using Rheocalc
Data Base Navigation Bar

Refer to Figure 3-5 for a description of the button functions with in the Data Base Navi-
gation Bar.
1 2 3 4 5 6 7 8
BUTTON LEGEND
1. Moves the highlight to the first record in the data grid.
2. Moves the highlight to the previous line in the data grid.
3. Moves the highlight to the next line in the data grid.
4. Moves the highlight to the last record in the data grid.
5. Adds a blank record (data line) at the highlighted line in the data grid.
6. Deletes the highlighted data line in the data grid.
7. Turns edit mode ON.
8. Turns edit mode off and locks the database.
Figure 3-5: Data Base Navigation Bar Buttons
NOTE: When in Edit mode, only the Speed, % Torque, Temperature, and Time Interval
fields may be changed by the user. All other parameters are automatically
calculated by Rheocalc. The data will not change until the data field being
edited has been exited.
Record
The Record boxes indicate the total number of records in the data set and the number of
the record currently selected.
Load Button
The Load button displays a standard file load dialog box. This dialog box displays
Rheocalc data files that were previously saved and can now be loaded.
Save Button
The Save button displays a standard file save dialog box. This dialog box allows data to
be saved for later use. Data is saved in a Paradox database file along with an ASCII text
file of the same name which contains user sample name and notes.
Print Button
to be selected, its properties changed and data to be printed.
and printer setup.
3-16 Manual No. M/99-222-D0106

View Notes Button

The View Notes button displays the Notes dialog, shown in Figure 3-6. A sample name
and notes can be entered and saved here. These notes will be stored in a file with the
same name as the data file, but with an RCH extension.
Figure 3-6: View Notes
Analyze Button
The Analyze button switches to the Analysis page and displays the results and a graph of
the selected math model for the currently displayed data. See the Analysis Page section
for more information on math model analysis.
Export Button
The Export button opens a dialog (similar to a Save dialog) that allows the displayed data
to be exported to an MS-Excel spreadsheet.
Import Button
The Import button imports data from previous versions of Rheocalc (DOS and Windows
3.1 versions).
NOTE: Data from previous Rheocalc software versions was in an ASCII text format as
opposed to the Paradox database format currently used.
DV-III Button
When a DV-III or DV-III+ rheometer is connected, the DV-III button extracts the last data
set that was taken with the instrument in its stand-alone mode. The data will appear in
Manual No. M/99-222-D0106 3-17

Using Rheocalc
the data grid unsaved.
Test Data Plot

Time Scale Drop Down List
When Time Interval is selected for any axis, this drop down list allows the units of said
axis to be seconds, minutes, or hours.
X, Y and Y2 Axis Drop Down Lists

These drop down lists allow selection of the values to be plotted for their corresponding
axis (X, Y or Y2).
Y2 Checkbox
This checkbox determines whether the second Y axis is plotted.
Replot Button
Clicking this button causes all selected data sets to be replotted on the graph using the
current plot options.
Default Graph Settings Button

Clicking this button returns the graph to its default settings.
Color Prints Button

When the Color Prints button is selected, graph printouts are in color (if the selected
printer supports color).
Plot List
This box lists all data files which are currently loaded, and indicates which files are
plotted.
Plot Options Panel

The Plot Options panel, as shown below, provides control of how data is plotted. The
following lines describe each element of the Plot Options panel.
3-18 Manual No. M/99-222-D0106

1 Turns on tracking. As data is gathered, axes will scroll to keep the newest data in view.
2 Turns off tracking.
3 Axis will scroll when the user drags it.
4 Axis will zoom when the user drags it.
5 Zooms both axes out.
6 Zooms both axes in.
7 Allows a data point to be selected.
8 Allows the user to draw a box which the graph will zoom to.
9 Places crosshairs with coordinates on the graph.
10 Opens a dialog box with many graph display options.
11 Copies the graph to the clipboard.
12 Saves the graph as a bitmap.
13 Prints the graph.
Analysis Page
The Analysis page, shown in Figure 3-7, is used to mathematically analyze selected data
using various models associated with viscosity measurement and rheology. The results
Manual No. M/99-222-D0106 3-19

Using Rheocalc
are displayed both numerically and graphically, and they can also be printed to hard copy.
Figure 3-7 Analysis Page
Analysis Page Operation

1. Select the LOAD button to select and load a data file.
2. Choose the analysis model from the Model drop down list. As each model is high-
lighted, the equation for that model is displayed in the equation box.
3. Once a model is selected, the calculations are performed and the numeric and graphi-
cal results are displayed. The graph displays the data and the best fit straight line
using the selected equation.
4. Select the PRINT button to print the data, numeric results, and corresponding graph.
Analysis Page Description

The Analysis page is shown in Figure 3-7 and described in the following paragraphs.
3-20 Manual No. M/99-222-D0106

Model
Thix Index
Thix Index uses two viscosity measurements taken at different speeds to give an
indication of shear sensitivity.
NOTE: Data sets to be analyzed with this model should have two data points only.
The Thix Index equation is n = L/H where

n = Thix Index
L = Viscosity at low speed
H = Viscosity at high speed
The calculated parameters for this model are:

Thix Index(no units)
A plot of viscosity versus speed is displayed for this model.
Manual No. M/99-222-D0106 3-21

Using Rheocalc
Bingham
The Bingham equation is used to calculate the viscosity of materials that only flow
after the application of a sufficiently large yield stress. These materials are referred to
as Bingham plastic fluids and are described by the equation in Figure 3-8.
= o + D
SHEAR RATE
PLASTIC VISCOSITY
YIELD STRESS
SHEAR STRESS
Figure 3-8: Bingham Equation
Plastic Viscosity (cP or mPas)
Yield Stress (Dynes/cm2 or Newtons/m2)
Confidence of fit (%) or CoF
NOTE: In all cases, confidence of fit is a measure of how well the data fits the best
fit curve for this equation with 100% being the best fit.
A plot of shear stress versus shear rate is displayed for this model.
3-22 Manual No. M/99-222-D0106

Casson
The Standard Casson method is a direct implementation of the original Casson equa-
tion. A plot of the square root of shear stress versus the square root of shear rate is
displayed for this model. The Standard Casson equation is shown in Figure 3-9.
= o + D
SHEAR RATE
PLASTIC VISCOSITY
YIELD STRESS
SHEAR STRESS
Figure 3-9: Casson Equation
A plot of the square root of shear stress versus the square root of shear rate is dis-
played for this model.
Manual No. M/99-222-D0106 3-23

Using Rheocalc
NCA/CMA Casson
This Casson method is derived from the standard set forth by the National Confec-
tioners Association (NCA) and the Chocolate Manufacturers Association (CMA).
Although based on the original Casson equation, this implementation has been tai-
lored by the NCA and CMA specifically to applications involving chocolate. The
Chocolate Casson equation is shown in Figure 3-10.
( 1 + a) = 2 o + ( 1 + a ) D
SHEAR RATE
PLASTIC VISCOSITY
YIELD STRESS cone (BOB) RADIUS/INNER
SHEAR STRESS CUP RADIUS (GAP RATIO)
Figure 3-10: Chocolate Casson Equation
A plot of (1 + a ) times the square root of shear stress versus (1 + a ) times the square
root of shear rate is displayed for this model.
3-24 Manual No. M/99-222-D0106

Power Law
The Power Law equation is shown in Figure 3-18.
=k Dn
FLOW INDEX
SHEAR RATE
CONSISTENTCY INDEX
SHEAR STRESS
Figure 3-11: Power Law Equation
Flow Index (no units)
Consistency Index (cP or mPas)
A plot of the LOG of shear stress versus the LOG of shear rate is displayed for this
model.
Manual No. M/99-222-D0106 3-25

Using Rheocalc
IPC Paste
The IPC Paste Analysis method is based on the power law equation and is intended to
calculate the Shear Sensitivity Factor (pseudoplasticity) of pastes. A prime example
of its use is in the solder paste industry, thus the name IPC (Institute for Interconnect-
ing and Packaging Electronic Circuits). The Paste equation is shown in Figure 3-12.
=kRn
SHEAR SENSITIVITY FACTOR
ROTATIONAL SPEED (rpm)
CONSISTENCY MULTIPLIER
VISCOSITY
Figure 3-12: IPC Paste Analysis Calculation
Shear Sensitivity Factor (slope of line; no units)
Viscosity (cP or mPas)
A plot of the LOG of viscosity versus the LOG of speed (rpm) is displayed for this
model.
3-26 Manual No. M/99-222-D0106

Herschel Bulkley
= o + kDn
FLOW INDEX
SHEAR RATE
CONSISTENCY INDEX (cP)
YIELD STRESS
SHEAR STRESS
Figure 3-13: Herschel Bulkley Calculation

Flow Index (no units)
Consistency Index (cP or mPas)
Yield Stress (Dynes/cm2 or N/m2)
Confidence of fit (%)
A plot of the LOG of (shear stress - yield stress) versus the LOG of shear rate is displayed
for this model.
Manual No. M/99-222-D0106 3-27

Using Rheocalc
Calculate
The Calculate button updates the results box and the graph using the data and model type
selected.
Equation
The Equation box displays the equation for the model selected.
Results
The Results box displays the appropriate results, yield stress and confidence of fit results
of the analysis using the data and model type selected.
File
The File box displays the file and path of the data file being analyzed.
Data Graph
The Data Graph presents a plot of the raw data and the best fit line using the model
selected.
Load Button
The Load button displays the Load Files dialog box which can be used to load a saved
file for analysis.
Print Button
to be selected, its properties changed and data analysis results and graph to be printed.
and printer setup.
3-28 Manual No. M/99-222-D0106

Setup Page
The Setup page, shown in Figure 3-14, allows the user to set preferences which effect the
way Rheocalc operates.
Figure 3-14: Setup Page
Setup Page Operation

Adding a Special Spindle
1. In the Name box, enter a description for the special spindle.
2. Enter the Spindle Multiplier Constant in the SMC box and the Shear Rate Constant in
the SRC box.
3. Select the ADD button. The spindle will now appear at the bottom of the spindle list.
Modifying a Special Spindle

1. Highlight the special spindle (only user-defined spindles can be modified) at the
bottom of the spindle list.
2. Make the appropriate changes in the Name, SMC and SRC boxes.
3. Select the UPDATE button to confirm these changes. The spindle list will show the
modifications.
Manual No. M/99-222-D0106 3-29
Using Rheocalc
Displaying the Viscosity Measurement Range for a Spindle

1. Select the appropriate spindle in the spindle list (standard or special).
2. Select the button with the green arrow to display the viscosity measurement range for
that spindle and to update the corresponding range graph.
Changing the Measurement Units
NOTE: Changing the Measurement or Temperature Units settings will cause Rheocalc
to restart in order to initialize the new settings.
1. Select the appropriate Measurement Units from the drop-down list.
2. Select the appropriate Temperature Units from the drop-down list.
3. Select the appropriate Data Format from the drop-down list.
Setting the Torque Alarm

1. Enter the appropriate Torque Alarm values. Select the ACCEPT button to enter the
values.
2. Select the ENABLE checkbox to enable the alarms.
Setting the Standby Temperature

1. Enter the appropriate Standby Temperature.
2. Select the Standby @ Program Completion checkbox to have Rheocalc return to

the Standby Temperature between test runs.
3. Click the APPLY button to apply the Standby Temperature settings.
Setup Page Description

The Setup page is shown in Figure 3-13 and described in the following paragraphs.
Spindle, SMC and SRC List

The Spindle, SMC, and SRC list displays a list of spindles from which to choose and
view measurement range information. Special (user) spindles are displayed at the bottom
of the list.
Name
The Name field is used to enter a name for a special (user created) spindle.
SMC
The SMC field is used to enter an SMC (Shear Multiplier Constant) for a special spindle.
Refer to Appendix C to learn more information on this constant.
3-30 Manual No. M/99-222-D0106

SRC
The SRC field is used to enter an SRC (Shear Rate Constant) for a special spindle. Refer
to Appendix C to learn more information on this constant.
Add Button
The Add button adds a special spindle to the bottom of the spindle list using the user
entered parameters.
Update Button
The Update button updates the selected special spindle within the spindle list with the
parameters entered at the left.
Delete Button
The Delete button removes the special spindle highlighted in the spindle list.
Viscosity Range
The Viscosity Range display present numeric representation of the measurement range
for the selected spindle. The range is calculated using a low torque of 10% and a high of
100%. The speed range for these calculations corresponds to the minimum and maxi-
mum speeds of the instrument (0.01 to 250 rpm).
Measurement Units
The Measurement drop-down list allows the user to select the CGS or SI units to be used
during Rheocalc operation.
NOTE: Rheocalc must be restarted after changing the Measurements Units setting.
Temperature Units
The Temperature drop-down list allows the user to select the temperature scale units
Fahrenheit (F) or Celsius (C) to be used during Rheocalc operation.
NOTE: Rheocalc must be restarted after changing the Temperature Units setting.
Date Format
The Date Format drop-down list allows the user to select the date format (U.S. : mm/dd/
yyyy) or (International: dd/mm/yyyy) to be used during Rheocalc operation.
Torque Alarms
The Torque Alarm warns the user that the % torque value has either fallen below (Low
Alarm) a preset value or risen above (High Alarm) a preset value.
Alarms can only be tripped (i.e. the % torque value falls outside the alarm values) if the
rheometer speed is greater than zero rpm, and the alarms are enabled (click the check box
next to the word Enabled to Enable/Disable alarms). Once alarm values are changed,
click the Accept button to use the new values.
Manual No. M/99-222-D0106 3-31

Using Rheocalc
When an alarm is tripped, a beep will be heard, and a picture of an alarm clock appears
next to the % Torque field on the Dashboard page.
NOTE: If the Motor Off alarm is tripped, in addition to the indications stated above, the
rheometer speed is set to 0 rpm. If a program is running at the time, the rheom-
eter remains at 0 rpm until it is commanded to another speed by any succeeding
program steps.
Standby Temperature
The Standby Temperature is used as the default temperature of the optional temperature
controller. This is the temperature which the controller will go to at startup.
If Standby @ Program Completion is checked, the controller will return to the Standby
Temperature after running a test. If it is unchecked, the controller will remain at the last
specified temperature when the test ends.
After changing the Standby Temperature options, click Apply to use the new settings.
3-32 Manual No. M/99-222-D0106

Custom Page
The Custom page is a blank page where the user can move groups of controls (called
Control Windows) from other pages. An example of a Custom page setup is shown in
Figure 3-15.
Figure 3-15: Custom Page
Custom Page Operation

Most of the applications controls are grouped together on Control Windows which can
be moved, resized, or hidden by the user.
Manipulating Control Windows

1. Moving the window: Click and drag the bar on the left of the window.
2. Undocking the window: Doubleclick the bar on the left of the window in order to
float it above the application.
3. Resizing the window: While the window is undocked, drag on the edges of the
window to resize it.
4. Hiding the window: Click on the x in the corner of the window.
Placing Control Windows on the Custom Page

Either undock the Control Window and drag it to the Custom Page, OR
Right-click on the Custom Page and choosing the Control Window from the popup list.
Manual No. M/99-222-D0106 3-33
Using Rheocalc
Removing Control Windows from the Custom Page

Either undock the Control Window and drag it to another page, OR
Right-click on the Custom Page and deselect the Control Window from the popup list.
3-34 Manual No. M/99-222-D0106

Section 4 - B.E.A.V.I.S. Programs
What is a B.E.A.V.I.S. Program?

B.E.A.V.I.S. Brookfield Engineering Advanced Viscometer Instruction Set is a command
language developed at Brookfield Engineering Labs that allows control of Brookfield
viscometers/rheometers and associated accessories (i.e. temperature controllers). The
commands allow the creation of both simple and complex test programs that provide
maximum flexibility in completely unattended data gathering.
B.E.A.V.I.S. Commands
Command Groups
Commands are grouped into functional groups which are identified by the graphic to the
left of the command. Icons for each group are shown in Figure 4-1.
WAIT SETUP DATA LOOP SAVE REPORT

COMMAND COMMAND COMMAND COMMAND COMMAND COMMAND
GROUP GROUP GROUP GROUP GROUP GROUP
Figure 4-1: Command Group Icons
Wait Command Group

Wait Commands wait for a certain condition to be reached. The time to reach the condi-
tion is displayed as Step Time on the Program page.
Setup Command Group

Setup Commands set program parameters (i.e. speed or temperature).
Data Command Group

Data Commands dictate the manner in which data is collected.
Loop Commands Group

Loop Commands mark the beginning and end of a loop (i.e. commands between the loop
start and end are repeated).
Save Data Commands Group

Save Data Commands save or append data to a disk file.
Report Command Group

Report Commands set the reporting options.
Manual No. M/99-222-D0106 4-1
B.E.A.V.I.S. Programs
Table 4-1: B.E.A.V.I.S. Commands used in Rheocalc
Command Function Description

WTI Wait for time Remains at the step until the specified time
interval (MM:SS) has elapsed.
WPT Wait for % torque Remains at the step until the specified % torque
value is reached.
WTP Wait for Remains at the step until the specified
temperature temperature value is reached.
WTS Wait for set point Remains at the step until the temperature reaches
temperature the set point value in the associated temperature
controller the specified value.
WDP Wait for data Remains at the step until the specified number of
points data points are collected from the time this
command is issued.
SSN Set speed Run the rheometer at the specified speed.
SSP Set spindle Set the spindle to use with the rheometer. The
user will be prompted to attach this spindle to the
rheometer, and this spindle's SMC and SRC will
be used for all calculations.
STM Set temperature Set the temperature controller set point to the
specified value and control to this temperature.
SSI Increase/Decrease Increment or decrement the current speed by the
Speed value specified.
STI Increase/Decrease Increment or decrement the current temperature
Temperature set point by the value specified.
DCI Data collection Begin collecting data at the specified time
interval interval (MM:SS).
DAI Data averaging Immediately begin averaging data. Averages the

specified number of points over each specified
time interval. Terminates any DCI already in
progress.
4-2 Manual No. M/99-222-D0106

Table 4-1: B.E.A.V.I.S. Commands used in Rheocalc
Command Function Description

DSP Collect a single Immediately collect a single data point.
data point
DSD Stop data Terminate any DCI already in progress.
collection
LSC Start count loop Marks the start of a loop. Perform all commands
starting after this one up to the next LEC (loop
end) the number of times specified.
LEC End count loop Marks the end of a loop. Perform all commands
before this one back to the most recent LSC the
number of times stated in the LSC.
LWC Start conditional Marks the start of a conditional loop. Performs
loop all commands starting after this one up to the
next LWE (conditional loop end) until one of the
specified conditions is met.
LWE End conditional Marks the end of a conditional loop. Performs
loop all commands before this one back to the most
recent LWC until one of the conditions stated in
the LWC is met.
FSA Append to Data Append any data in the capture buffer to the end
File of the specified file. If a full path name is not
specified, the file is saved in the initial program
directory. If the file does not exist, it is created.
FSO Save data to disk Save any data in the capture buffer to the file
file specified. If a full path name is not specified,
the file is saved in the initial program directory.
If a file of the same name already exists in the
path, it is overwritten. If the file does not exist,
it is created.
RMR Report results Reports the test results using the options
specified.
Manual No. M/99-222-D0106 4-3

B.E.A.V.I.S. Program Examples
Geometric Speed Progression Command Example

The program outlined in Table 4-2 starts at 10 rpm after which it waits for 30 seconds
before taking a data point. Speed is increased by 5 rpm at the bottom of the loop after
which program execution moves back to the LSC line and decreases the loop count (5) by
one. The program again waits 30 seconds before taking a data point, this time at 15 rpm.
This is repeated four more times for a total loop count of 5. The resulting data consists of
data points taken at 10, 15, 20, 25, and 30 rpm.
Table 4-2: A Geometric Speed Progression Command Example

Command Parameter Function
SSN 10 Sets speed at 10 rpm
LSC 5 Start loop; execute 5 times
WTI 00:30 Wait for 30 seconds
DSP - Take a data point
SSI 5 Increase speed by 5 rpm
LEC - Return to the corresponding LSC

command
Up/Down Geometric Speed Progression Example

The program outlined in Table 4-3 takes one data point after waiting for 30 seconds at
each speed with speeds progressing from 10 to 30 rpm in 5 rpm increments. This time,
however, after taking a data point at 30 rpm, speed is decremented back down to 10 rpm
in 5 rpm decrements with a data point being taken after 30 seconds at each speed.
4-4 Manual No. M/99-222-D0106

Table 4-3: Up/Down Geometric Speed Progression Command Example
SSN 10 Set speed at 10 rpm
LSC 5 Start loop; execute 5 times
SSI 5 Increase speed by 5 rpm

command
LSC 4 Start loop - execute 4 times
SSI -5 Decrease speed by 5 rpm

command
A Geometric Speed Progression Run At Multiple Temperatures

The program outlined in Table 4-4 runs the following geometric speed ramp at 25C,
50C, and 75C. The interior loop starts at 10 rpm after which it waits for 30 seconds
before taking a data point. Speed is then increased by 5 rpm when at the bottom of the
loop after which program execution moves back to the LSC line and decreases the loop
count (5) by one.
Manual No. M/99-222-D0106 4-5

At this point the program again waits 30 seconds before taking a data point, this time at
15 rpm. This is repeated four more times for a total loop count of 5. The resulting data
consists of data points taken at 10, 15, 20, 25, and 30 rpm.
Table 4-4: Geometric Speed Progression at Multiple Temperature Example
STM 25 Set the attached temperature

controller to 25 .
LSC 3 Run the temperature loop three
times
WTS 0.5 Wait until the process temperature
reaches the set point temperature
WTI 01:00 Wait for one minute for temperature
to stabilize
SSN 10 Set speed at 10 rpm
LSC 5 Start loop: execute five times
SSI 5 Increase by five rpm
LEC - Return to speed loop LSC command
STI 25 Increment the temperature set point

by 25
LEC - Return to speed loop LSC command
4-6 Manual No. M/99-222-D0106

Section 5 - Troubleshooting
Communication Errors
If the warning shown in Figure 5-1 is displayed for either the rheometer or the tempera-
ture controller, use the troubleshooting procedures in this section to resolve the problem.
Figure 5-1: Communications Warning Pop-up Window
Instrumentation Setup
1. Ensure that the rheometer or controller (or both) have the appropriate communica-
tions cable (Communications) connected to them and that the opposite end of the
cable is connected to a valid COM (serial) port on the host PC.
2. Ensure the rheometer, temperature controller, or both are powered ON. The rheom-
eter will display External Control on the front panel and the Remote LED on the
front panel of the HT-10X Series temperature controllers will be lit.
NOTE: For the TC-50X Series Baths, check the baths operation manual for RS-232
communication information
3. If communication problems still exist, perform one of the following procedures based
the computer operating system being used.
Windows NT
1. Select the START button.
2. Select SETTINGS then CONTROL PANEL.
3. Select the SYSTEM icon.
4. Select the PORTS icon. Either right-click the COM port in use and select PROPER-
TIES from the popup menu or double-click the COM port in use.
Manual No. M/99-222-D0106 5-1

Troubleshooting
5. Select SETTINGS then ADVANCED. NOTE: You must have Administrator

privleges to use the ADVANCED port features.
6. Make sure the check box labeled FIFO Enabled is checked.
7. Select the OK buttons to accept the changes and get back to the desktop.
8. If there is still a communication problem, follow the above procedure, but this time,
remove the check from the box labeled labeled FIFO Enabled.
10. If communication problems still exist, adjust the communications port settings using
the procedure described in the following section.
Windows 2000 / XP
1. Select the START button.
2. Select SETTINGS then CONTROL PANEL.
3. Select the SYSTEM icon.
4. Select the HARDWARE tab then click the DEVICE MANAGER button.
5. Select the PORTS icon. Either right-click the COM port in use and select PROPER-
TIES from the popup menu or double-click the COM port in use.
6. Select PORT SETTINGS then ADVANCED. NOTE: You must have Administrator
privleges to use the ADVANCED port features.
7. Make sure the check box labeled USE FIFO BUFFERS (requires 16550 compatible
UART) is checked. Make sure the sliderrs for the RECEIVE BUFFER and the
TRANSMIT BUFFER are both set all the way to the left (Low).
9. If there is still a communication problem, follow the above procedure, but this time,
remove the check from the box labeled labeled USE FIFO BUFFERS (requires
16550 compatible UART).
11. If communication problems still exist, adjust the communications port settings using
the procedure in the following section.
5-2 Manual No. M/99-222-D0106

Communication Port Settings

Perform the following procedure to establish the communication port settings for the
viscometer/rheometer being used and accessory device.
1. Select the DASHBOARD tab.
2. Select the ADVANCED button within the Instrument Status area of the Dashboard
window. The Communication Port Settings pop-up window appears as shown in
Figure 5-2.
Figure 5-2: Communication Port Settings Pop-up Window

3. The baud rate, data bits, stop bits and parity settings for the rhemoeter and accessory
are for viewing only.
4. Drag the slider up or down to set the correct TX Delay (data transmission delay) for
the rheometer and accessory being used.
5. Select the OK button. The Communication Port Settings have been established.
Manual No. M/99-222-D0106 5-3

Introduction
Use the information in Appendix A to Contact Brookfield Engineering
Laboratories, Inc. for technical assistance or service. Please have the following informa-
tion available when calling so that we may assist you:
Software Name
Software Version Number
Viscometer Model
Viscometer Firmware Version
Product Application
Specific Problem Area
Hours of Operation
Equipment Type
Computer Information: operrating system, microprocessor, amount of RAM,

hard drive size, number of RS-232 ports, modem, network card, or other
equipment being used with the computer.
North America
Brookfield Engineering Laboratories, Inc.
11 Commerce Boulevard
Middleboro, Massachusetts 02346 U.S.A.
TEL: 508-946-6200
800-628-8139 (USA only - excluding MA)
FAX: 508-946-6262
E-MAIL: sales@brookfieldengineering.com
Manual No. M/99-222-D0106 A-1

U.K.
Brookfield Viscometers Limited
1 Whitehall Estate
Flex Meadow
Pinnacles West
Harlow, Essex CM19 5TJ, United Kingdom
TEL: (44) 27/945 1774

FAX: (44) 27/945 1775
E-MAIL: sales@brookfield.co.uk
Germany:
Brookfield Engineering Labs. Vertriebs
Hauptstrasse 18
D-73547 Lorch, Germany
TEL: 7172/927100
FAX: 7172/927105
E-MAIL: info@brookfield-gmbh.de
A-2 Manual No. M/99-222-D0106

RS-232 Cables
Use the appropriate information in Figures B-1 and B-2 if you wish to make your own
RS-232 communication cable.
NOTE: Your computer may use either a standard 9-pin or 25-pin (male or female) D-
type connector.
Connected to Rheometer
9-pin male D Type
Connector
9
Note: jumper between pins 4 and
9 is required to place rheometer
in external control mode
2 3 45
Use shielded cable
7 3 2 5 3 2
Connected to Host Computer Connected to Host Computer

25-pin female D Type OR 9-pin female D Type
Connector Connector
Figure B-1: PC Interface Cable Drawing
Manual No. M/99-222-D0106 B-1

Connected to HT-10x
Temperature Controller 25-pin
male D Type Connector
25
Note: jumper between pins 13

and 25 is required to place the
controller in external control mode
2 3 7 13
7 5 3 2
3 2
Connected to Host Computer Connected to Host Computer

25-pin female D Type 9-pin female D Type
Connector Connector
Figure B-2: Temperature Control Interface Cable Drawing
B-2 Manual No. M/99-222-D0106

Introduction
Each spindle has two constants which are used to calculate viscosity, shear stress, and
shear rate. The Spindle Multiplier Constant (SMC) is used in viscosity and shear stress
calculations. The Shear Rate Constant (SRC) is used in shear stress and shear rate calcu-
lations.
NOTE: Where SRC = 0, no shear stress/shear rate calculations are performed and the
data displayed is zero (0) for these functions.
NOTE: Refer to Appendix A and contact Brookfield Engineering Laboratories, Inc. for
a copy of More Solutions to Sticky Problems for additional information.
Spindle Codes
Table C-1: Spindle Codes
Spindle Code SMC SRC

ULA 00 0.64 1.223
RV1 01 1 0
RV2 02 4 0
RV3 03 10 0
RV4 04 20 0
RV5 05 40 0
RV6 06 100 0
RV7 07 400 0
HA1 01 1 0
HA2 02 4 0
HA3 03 10 0
HA4 04 20 0
HA5 05 40 0
Manual No. M/99-222-D0106 C-1

Table C-1: Spindle Codes (continued)

HA6 06 100 0
HA7 07 400 0
HB1 01 1 0
HB2 02 4 0
HB3 03 10 0
HB4 04 20 0
HB5 05 40 0
HB6 06 100 0
HB7 07 400 0
SC4-14 14 125 0.4
SC4-15 15 50 0.48
SC4-16 16 128 0.29
SC4-18 18 3.2 1.32
SC4-21 21 5 0.93
SC4-25 25 512 0.22
SC4-27 27 25 0.34
SC4-28 28 50 0.28
SC4-29 29 100 0.25
SC4-31 31 32 0.34
SC4-34 34 64 0.28
CP40 40 0.327 7.5
CP41 41 1.228 2
CP42 42 0.64 3.8
CP51 51 5.178 3.84
CP52 52 9.922 2
C-2 Manual No. M/99-222-D0106

Table C-1: Spindle Codes (continued)

LV1 61 6.4 0
LV2 62 32 0
LV3 63 128 0
LV4 64 640 0
LV5 65 1280 0
LV-2C 66 32.0 0.212
LV-3C 67 128.0 0.210
SP-Y3 70 105 0.677
Vane-71 71 2.62 0.0
Vane-72 72 11.1 0.0
Vane-73 73 53.5 0.0
Vane-74 74 543.0 0.0
DIN-81 81 3.7 1.29
DIN-82 82 3.75 1.29
DIN-83 83 12.09 1.29
DIN-85 85 1.22 1.29
DIN-86 86 3.65 1.29
DIN-87 87 12.13 1.29
T-A 91 20 0
T-B 92 40 0
T-C 93 100 0
T-D 94 200 0
T-E 95 500 0
T-F 96 1000 0
Manual No. M/99-222-D0106 C-3

Model Codes
Table C-2 lists the model codes (spring torque) constants for each rheometer model.
Table C-2: Model Codes
Model
TK
TK Rheometer Screen
(Spring Torque)
LVDV-III 0.09373 LV
2.5xLVDV-III 0.2343 4L
5XLVDV-III 0.4686 5L
1/4 RVDV-III 0.25 1R
1/2 RVDV-III 0.5 2R
RVDV-III 1 RV
HADV-III 2 HA
2XHADV-III 4 3A
2.5xHADV 5 4A
HBDV-III 8 HB
2xHBDV-III 16 3B
2.5xHBDV-III 20 4B
5xHBDV-III 40 5B
Full Scale Viscosity Range Calculation

The full scale viscosity range for any rheometer model and spindle may be calculated
using the equation:
Full Scale Viscosity Range [cP] = TK * SMC * 10,000/rpm
Where:
C-4 Manual No. M/99-222-D0106

TK = Spring Torque Constant from model table

SMC = Spindle Multiplier Constant from spindle table
Shear Rate Calculation

The Shear Rate calculations is:
Shear Rate (1/sec) = SRC * rpm
Where:
SRC = Shear Rate Constant from spindle table
Using Non-Standard (Special) Spindle with a DV-III or DV-III+

Rheocalc allows the entry of spindle constants (Spindle Page) which the software uses to
calculate viscosity, shear stress, and shear rate for spindles in boundary conditions other
than the 600ml beaker or specified chamber. The spindles must conform to geometries
that allow for mathematical calculations of shear stress and shear rate (i.e. coaxial cylin-
der, cylindrical).
Two constants are required:
SMC (Spindle Multiplier Constant) which is used to calculate the viscosity

(cP) value.
SRC (Shear Rate Constant) which is used to calculate shear rate (1/sec) and
shear stress (Dyne/cm2) value.
If SRC = 0 (Ex. LV #1-4, RV, HA, HB #1-7 spindles), shear rate and shear stress values
are not calculated and cannot be displayed.
The SMC value for a spindle may be calculated as follows:
1. For new spindle conditions you calculate the SMC using a Newtonian fluid of known
viscosity (Brookfield Viscosity Standard). This is done in the container with the new
dimensions at the controlled temperature specified for the viscosity standard fluid.
2. The new full scale viscosity range is calculated for a selected rpm:
Manual No. M/99-222-D0106 C-5

R1 = 100n/Y
where:
R1 = The new full scale viscosity range

n = The viscosity (cP) of the Newtonian fluid
Y = The torque % reading at the selected rpm
3. The SMC value is then calculated:
SMC = [Full Scale Viscosity Range (cP) * [Selected rpm]

TK * 10,000
where:
TK = DV-III Torque Constant from Table C-2
The SRC value may be calculated for cylindrical spindle geometry using the following
equation:
Shear Rate (1/sec)=(2 * Rc2 Rb2)/(2 * [Rc2 - Rb2])
The SRC value may be calculated by first calculating the shear rate of the geometry at a
given rpm then solving the shear rate equation on page C-5 for SRC. For example; for a
cylindrical geometry, use the following equation:
Shear Rate (sec-1) = 2m Rc2 Rb2

X2 (Rc2 Rb2)
where:
m = (2/60)N = angular velocity of the spindle (rad/sec)

Rc = radius of the container (cm)
Rb = radius of the spindle (cm)
X = radius at which shear rate is being calculated (cm)
N = RPM
To calculate shear rate, refer to Brookfield Engineering Laboratories, Inc., More Solu-
tions to Sticky Problems publication for more information on calculations for various
geometries.
C-6 Manual No. M/99-222-D0106

INDEX
A COM (RS-232) ports 3-11, 3-16, 3-24, 3-38

A Geometric Speed Progression 4-6 COM (serial) port 5-1
a legend 3-29 COM port 2-1, 2-2, 5-2
About 3-8 Command Groups 4-1
Advanced 3-4 Command List 3-13
alarms 3-5 communication (RS-232) ports 2-1
Analysis 3-23, 3-32 communication port 3-2
Analysis page 3-33 Communication Port Settings 3-4, 5-2
ANALYZE 3-18 communications cable 5-1
Analyze 3-23 Communications Port Setting 3-4
ASCII text file 3-21 Confidence of fit 3-33, 3-34, 3-35, 3-36, 3-37
Auto Division 3-27 Confidence of fit 3-34, 3-35, 3-36, 3-37
Auto Zero 3-6 Confirm Deletions 3-15
Auto/Manual Scale 3-29 Consistency Index 3-36
axis limits 3-16 Customer Support A-1
B D
B.E.A.V.I.S 3-12 D/cm2 3-3
B.E.A.V.I.S. Commands 4-1 DASHBOARD 2-1, 3-2
B.E.A.V.I.S. Program 4-1 Dashboard 2-2, 3-5
B.E.A.V.I.S. program 3-16, 3-25, 3-31 Dashboard Page 3-1
B.E.A.V.I.S. Program Examples 4-4 Dashboard page 3-2
B.E.A.V.I.S. Programs 3-15 Data Base Navigation Bar 3-19
best fit curve 3-33, 3-34, 3-35, 3-36, 3-37 Data Display grid 3-19
Bingham plastic 3-33 Data Grid 3-13, 3-15
Brookfield Viscosity Standard C-6 data grid 3-19
data interval 3-14
C data point 3-14
cables 3-3 Data Point Marker 3-29
CALCULATE 3-32 Date Format 3-2, 3-5
Calculate 3-38 Date/Time 3-19
Casson 3-34 DCI 3-14
Celsius 3-5 DV-III 1-1, 3-3, 3-24, B-1, C-6
centipoise 3-2 DV-III Rheometer 1-1
CGS 3-4 DV-III+ 1-1, 3-4, 3-18, B-1
Chocolate Casson 3-35
CMA 3-35
Color Prints 3-30
COM (RS-232) port 3-3
Manual No. M/99-222-D0106 Index-1

Index
E L
Edit mode 3-20 LEC 3-14
Equation 3-38 Linear Scale 3-27
Exit 3-8, 3-11, 3-16, 3-24, 3-31, 3-38 Live data 3-13
EXPORT 3-18 Load File dialog box 3-7, 3-12, 3-17, 3-18,
Export 3-23 3-26
Exporting Data 3-18 Load Files dialog box 3-38
Extracting Data from a Rheometer 3-18 Logarithmic Scale 3-27
Loop Count 3-13, 3-14
F LSC 3-14
Fahrenheit 3-5
file load dialog 3-21 M
File Load dialog box 3-30 Major Grid 3-29
file save dialog 3-21 Manual Divisions 3-28
file save dialog box 3-15 Manual Scale 3-28, 3-29
Flow Index 3-36 math model 3-23
FSA 3-15 Maximum Viscosity 3-6
FSO 3-15 Measurement 3-2
full scale torque 3-2 measurement range 3-11
full scale viscosity C-5, C-6 Measurement Units 3-2, 3-4, 3-5
minimum and maximum speeds 3-11
G Minor Grid 3-29
Geometric Speed Progression 4-4 Model 3-5, 3-19, C-1
Geometry 3-2, 3-5 model 3-6, C-5
Go 3-6 model codes C-4
GRAPH 3-18 MS-Excel 3-18
Graph 3-22 MS-Excel spreadsheet 3-23
H N
Help 3-8, 3-11, 3-16, 3-24, 3-31, 3-38 N/m2 3-3
HT-10X (104,105,106,107) RS-232 Cable NCA 3-35
Drawing B-2 NCA/CMA Casson 3-35
Next 3-16
I Notes 3-20
IMPORT 3-18
Import 3-23 O
Importing 3-18 ON-LINE 3-13, 3-16, 3-31
Importing Data 3-18 On-Line 3-15, 3-31
Info button 3-31 On-Line Plotting 3-25
Instrument Status 2-1, 3-2, 3-3 On-Line plotting 3-13
IPC Paste Analysis 3-37 on-line plotting 3-13, 3-31
Open 3-7
Index-2 Manual No. M/99-222-D0106

P Save File dialog box 3-7, 3-13, 3-18

Paradox database 3-19, 3-20, 3-23 Saving data 3-18
Paradox database file 3-21 Shear Multiplier Constant 3-10
Plastic Viscosity 3-33, 3-34, 3-35 Shear Rate 3-3, C-5
Plot 3-10, 3-13, 3-15, 3-16, 3-18, 3-22, 3-25, shear rate 3-6, 3-33, 3-34, C-1, C-5
3-26, 3-30, 3-31 Shear Rate Constant 3-9, 3-10, C-1, C-5
Plot Limit dialog box 3-13 Shear Rate Mode 3-15
Plot Options 3-25, 3-26 shear rates 3-15
plot options 3-16 Shear Sensitivity Factor 3-37
plot parameters 3-13 Shear Stress 3-3
Power Law 3-36 shear stress 3-6, 3-33, 3-34, C-1, C-5
power law 3-37 Show X/Y 3-30
PRINT 3-18 SI 3-4
Print 3-15, 3-21, 3-30, 3-38 SMC 3-10, C-1, C-6
print 3-32 Software Installation 2-1
Print dialog box 3-13, 3-15, 3-21, 3-30, 3-38 special (non-standard) 3-9
Printing Data 3-18 special (non-standard) spindles 3-9
Program Grid 3-12, 3-13, 3-16 special (user created) spindle 3-10
program grid 3-14 Special (user) spindles 3-10
program status 3-13 special spindle 3-9, 3-10, 3-11
Programs 3-12, 3-13, 3-16, 3-25, 3-31 special spindles 3-9
pseudoplasticity 3-37 Speed 3-2, 3-20
speed 3-5, 3-6, 3-15
R speed plot 3-16, 3-25
Reading Time 3-13, 3-14 Spindle 3-6, 3-19, C-1, C-5
Record 3-20 spindle 3-2, 3-6, 3-9, 3-10, 3-11, C-5, C-6
records 3-20 Spindle Codes C-1
REPLOT 3-28 Spindle Multiplier Constant 3-9, C-1, C-5
Replot 3-30 Spindles 3-9, 3-10
Rheocalc Text Data 3-18 spindles C-5
rheometer 1-1 Spring Torque C-5
RPM 3-6 SRC 3-10, C-1, C-6
rpm 3-2, 3-15 SSI 3-15
RS-232 Cable 2-1 SSN 3-15
RS-232 cable 3-4 START 3-13
RS-232 Cables B-1 Start 3-16
RS-232 communication 5-1 step parameter 3-14
RS-232 communication cable B-1 Step Status 3-13, 3-14
Step Time 3-13, 3-14
Stop 3-6, 3-16
S
support 1-2
Sample box 3-19
Symbol Legend 3-29
sample name 3-19
System Requirements 1-2
Save 3-7
Save dialog 3-23
Manual No. M/99-222-D0106 Index-3

Index
T W
TC-501 Bath 5-1 WTI 3-16
TC-501 bath 3-4
Temperature 3-2, 3-3, 3-20 Y
temperature 3-6 Yield Stress 3-33, 3-34, 3-35
temperature accessory 2-2
temperature bath 1-1 Z
temperature controller 3-3, 3-8, 5-1 Zero 3-6
Temperature Controller Setpoint 3-3
temperature controllers 4-1
Symbols
Temperature Units 3-2, 3-5
% torque 3-16
Thermosel 1-1
*.DB 3-17
Time Interval 3-20
*.XLS 3-18
Torque 3-2, 3-5, 3-20
.RCH 3-19, 3-20
torque 3-5, 3-11, 3-14, 3-25, C-6
Torque Alarm 3-2, 3-5
Troubleshooting 3-3, 3-4, 5-1
U
Up/Down Geometric Speed Progression 4-5
user-defined spindles 3-10
V
View/Edit 3-17, 3-18, 3-19, 3-20
Viscosity 3-2, 3-37
viscosity 3-6, 3-32, 3-33, C-1, C-5, C-6
Viscosity Measurement Range 3-10
Viscosity Range 3-11
Index-4 Manual No. M/99-222-D0106

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BROOKFIELD RHEOCALC

Programming and Operation Instructions

Manual No. M/99-222-D0106

BROOKFIELD ENGINEERING LABORATORIES, INC.

TEL 508-946-6200 or 800-628-8139 (USA excluding MA)

Any correspondence regarding this document should be forwarded to:

Brookfield Engineering Laboratories, Incorporated

Copyright 2000 Brookfield Engineering Laboratories, Incorporated Printed in U.S.A.

Section 2 - Getting Started

Section 3 - Using Rheocalc

Section 4 - B.E.A.V.I.S. Programs

Appendix A - Customer Support

Appendix C - Spindle and Model Codes

iv Manual No. M/99-222-D0106

An easy to learn and use graphical user interface.

A scripting language to allow flexible data collection.

Test Wizard for setting up commonly used tests.

On-line plotting of data during a data gather.

Background printing of data, graphs and programs.

Mathematical analysis of collected data.

Optional control of a Brookfield Engineering Labs temperature controller for

Manual No. M/99-222-D0106 1-1

Table 1-1: System Requirements

Microprocessor Pentium II, min.

Contacting Brookfield Engineering Laboratories, Inc.

1-2 Manual No. M/99-222-D0106

Section 2 - Getting Started

Rheocalc Software Installation

NOTE: You must log in as an administrator to install Rheocalc succussfully on your

Using either method causes the Main Welcome Screen to be displayed.

RS-232 Cable Installation

Manual No. M/99-222-D0106 2-1

2. Select the DASHBOARD tab.

2-2 Manual No. M/99-222-D0106

Section 3 - Using Rheocalc

Main Menu Operation

Viewing/Hiding Control Windows

2. Click on a checked title to hide that Control Window.

3. Click on an unchecked title to show that Control Window.

4. Click on Tools/Default Toolbar Positions to return all control windows to their

3. Once communication is established with the rheometer, use Instrumentation/Auto

Manual No. M/99-222-D0106 3-1

Main Menu Description

Save Settings Button

Default Window Positions Button

Test File Name

3-2 Manual No. M/99-222-D0106

Figure 3-1: Dashboard Page

Dashboard Page Operation

Establish Instrument Communication

Manual No. M/99-222-D0106 3-3

Set Single Speed

3. Click the Run button.

Set Single Temperature

2. Enter the desired temperature in the Temperature field.

3. Click the Run button.

Dashboard Page Description

Dashboard Control Window

3-4 Manual No. M/99-222-D0106

Temperature Controller Setpoint

NOTE: This Temperature Controller Setpoint display is blank if no controller is present.

NOTE: A red light indicates that an instrument is not connected.

NOTE: Refer to Section 5 - Troubleshooting for more information on the Communi-