Академический Документы
Профессиональный Документы
Культура Документы
Basic components:
- IR Source - Monochromator
- Sample cells - Detectors
- Readout devices
IR Sources
Low intensity radiation, 2-15 m.
Use bigger slit but it will effect resolution of wavelength.
Nernst glower : consist of rare-earth oxides.
Globar : made of silicon carbide but less intense,
satisfactorily for wavelength longer than 15m.
Globar
Nernst glower
1
10/4/2017
Instrumentation
Samples Cells Detector & Readout Devices
Various cells used for IR. Must be able to transduce heat to electrical signal.
Fixed cell such as NaCl is commonly used & must be Commonly used : Thermocouple and Balometers.
protected from moisture. Other detector : Photon detectors - highly sensitive
Silver chloride used for aqueous samples. & rapid measurements.
The shorter the path length, the more difficult for IR to Readout devices similar applications as other
be produced. equipments.
Repolished windows are not advisable for quantitative
analysis.
2
10/4/2017
Fingerprint Region
3
10/4/2017
4
10/4/2017
Ketones
5
10/4/2017
Applications of FTIR
Primary Use of IR methods