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At a glance:
Welcome (5 minutes)
Introduce yourself:
Your Name
Position/Job/Organisation
Your role in the workshop
Relevant experience to the workshop (University, projects, work etc.)
The purpose of the workshop is for participants to gain a greater understanding of the
importance of bio diesel and the way it can help with the increasing demand for oil in
transport . This is done via the presentation in the introduction session
With that complete the participants will have the chance to make their own biofuel
With fossil fuel reserves decreasing there is an increasing demand for alternative fuel
sources to power our vehicles. Some of the current suggestions are liquid gas, electric cars
and hydrogen fuel cells. Biodiesel is another alternative to the standard petroleum based
fuel.
In short, biodiesel refers to vegetable oil. It is made by reacting an oil with an alcohol. The
reason why standard vegetable oil isnt used on its own is because it is too thick. It wont run
in a standard diesel engine. The process of making biodiesel is to thin it out so it will work in
a standard engine. This is the much simpler option compared to re-designing an engine.
Biodiesel can be mixed with traditional diesel or used just on its own.
Biodiesel will generally work in any standard diesel engine. Some engines may struggle with
100% biodiesel. There are websites available to check this information (See further
information). Generally it is a very clean fuel to use and will often lubricate and extend the
life of an engine. Biodiesel offers a fantastic opportunity for the transport industry as it has
no carbon emissions and uses a waste product. Roughly 30 million gallons of waste
vegetable oil is thrown away from fast food restaurants in the USA each year.
Making biodiesel is very cost effective. Biodiesel can be made at home for about $1 a gallon
(Material cost, no start-up cost included). The industry is beginning to grow and more fuel
stations across America are beginning to sell biodiesel. Restaurants also becoming aware of
the situation and are willing to give their used cooking oil to people to make biodiesel
instead of throwing it away
There are however some problems with making biodiesel. To make it at home requires a
proper processor. It can be made in jugs, pans and buckets but to make enough to use a
processor is required. This will take time and effort to set up. It also will bring a fairly large
cost with it. Making biodiesel is often a messy process so requires a large area to do it
Before letting participants make their own it is a good idea to show them some samples of
biodiesel at different stages of the process. This way the participants know what they are
aiming for. It is especially worth showing them the stage at the end where the biodiesel
separates from the red glycerol at the bottom.
Once the samples have been shown the participants should be divided into groups according
to the numbers attending as well as the amount of equipment available.
For a more technical audience the chemistry behind the process of making biodiesel can be
presented in the introduction (See additional resources for a short clip on the chemistry of
biodiesel)
Practical (25 Minutes)
The step by step instructions for making the biofuel
Measurements dont need to be very accurate. When dealing with the potassium hydroxide
it is advised to wear protective gloves and protective eye wear if available. Make sure
participants are aware of the hazards of working with the sodium hydroxide.
1. Pass around the unfiltered cooking oil to each group. Each group should measure
out 500ml of the oil in a measuring jug.
2. The oil should be passed through a pair of nylon tights to filter it
3. Measure 100ml of methanol in a measuring jug
4. Measure 4g of Potassium Hydroxide (KOH) on the scales
NOTE: Wear protective gloves and eye wear if available. Potassium hydroxide can be a
dangerous chemical and should not be in contact with skin. Participants should be warned
of the dangers of potassium hydroxide before they begin using it
5. Add the KOH into the meth and keep stirring until it all dissolves (Can take about 5-8
minutes)
6. Heat the oil in the saucepan to about 60oC
7. Once the oil has reached the right temperature turn off the heat and add the
solution of methanol and KOH
8. Keep stirring the new solution for about 10 minutes
9. The new mixture will change colour quite a lot. It will go from a yellow oil colour to a
dark reddy brown.
10. Let the solution settle for 10 minutes. 2 layers should develop, a lighter colour fluid
on top and a darker fluid on the bottom (To see this happen it is best to transfer it
back to a clear measuring jug)
NOTE: Any stirring spoon used should be thrown away after (or only kept to be used in this
workshop again)
- The exact amount of KOH required to make bio diesel should be calculated by doing a
titration however for the purpose of a workshop the ratios above will produce suitable
results. The amount of methanol used is generally 20-22% of the amount of oil used.
- Once the two layers have developed the process is complete. The lighter fluid on top is the
biodiesel whilst the darker fluid on the bottom is the glycerol left over. By swirling the jug
with the mixture you should notice that the biodiesel is a lot thinner and moves about
quicker than the heavier glycerol.
- The biodiesel can be left to settle for a few more days to ensure all of the glycerol and
biodiesel has separated.
- Once the bio diesel has been separate from the glycerol it can be put into any diesel
operated vehicle like normal diesel oil.
- If you were making a significant amount of bio diesel at home you could drain the glycerol
from the bottom of the processing tank. When the colour changes from dark to light you
know you have removed all the glycerol from the remaining mixture.
- More often than not the bio diesel needs to be washed. The washing process removes any
remaining impurities or chemicals that havent reacted properly. A quick way to measure the
quality of the bio diesel is to have a glass jar filled with half bio diesel and half water. The jar
should be shaken quickly and then let to settle for 5 minutes. Between the layers of water
and oil there should be a middle layer called emulsion. The smaller this layer the easier the
wash process will be.
- Mist Wash: Adding water to the bio diesel from the top using a fine misting head. Water
droplets will form and fall through the bio diesel to the bottom of the tank collecting any
impurities on the way. Draining off the water and repeating will clean the bio diesel
affectively. Once the drained off water is clear the bio diesel is ready to use.
Closing (5 minutes)
Final few words:
http://www.youtube.com/watch?v=QbBp6x660e8&feature=mfu_in_order&list=UL A short
but effective video explaining the chemistry behind making biodiesel. There are further
videos explaining other aspects of biodiesel e.g. performance
Grater
Pestle & Mortar
Strainer
Beaker/Jars
Measuring cylinder/jug
Weighing scales
Indicator Paper
Portable hob
12.Organiser Checklist see relevant generic checklists Comment [M13]: List of things to
remember to take to the course. Could be
used with a generic course
checklist/timeline in the TIP?