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Anis HAIDER
President of ITECA
PROCESS CONTROL
IN A
CEMENT PLANT
1
PROCESS CONTROL
PROCESS CONTROL
2
PROCESS CONTROL
LOW FREQUENCY
HUMAN ERRORS
PROCESS CONTROL
CENTRALIZED AUTOMATIC
LABORATORIES
3
Centralised Automatic Laboratory
Automatic Laboratory
Raw meal 1 Raw meal 2 Kiln Feed Hot Meal Clinker Cement 1 Cement 2
Field network
Transport
fan
FreeLimeAnalyser CarbonSulphurAnalyser
Toplantsystem
Gas Dust (LIMS,PLC,etc.)
(XRF/XRD) extraction
PSD
Technical room system
Workstation
Mill&
Instructionsto Press
rawmillweight Central
feeders control Vision
cabinet Software
Bridge
PSDAnalyser Workstation
XRF/XRD
Workstation Composite
samples Movable
RawMix XRF control
Control XRD Laboratory network console
Software
4
On line Process Control
Precalciner
Cement
Additives Silo
Additives Blending Silos
Quarry
Raw Mill Clinker Cement
Preblending
Silo Mill
Cooler
Crusher Kiln
o Simpler to operate
o Independent systems
no risk of having no analysis at all in the whole
plant
5
RAW MIX CONTROL
6
Raw Mix Control
WHY CONTROL THE RAW MIX ?
Check the LSF (Lime saturation factor)
7
Raw Mix Control
WHY CONTROL THE RAW MIX ?
8
Raw Mix Control
What are the major drawbacks with the traditional
method ?
Human error
LSF
1 HOUR
1 HOUR
9
Raw Mix Control
Best location to take a sample
Precalciner
Blending Silos
Kiln Dust
Additives
Quarry
Crusher Kiln
10
Raw Mix Control
Typical layout Major oxides quantification
+ raw mix control software
Automatic control of the weight
Sampling in a chute Sampling in an airslide feeders
Slot Sampler
Screw
Sampler
Mixing
Piston
Sampler
Mechanical
Transport
On site EDXRF
analyser
Up to 7 analysis
per hour To plant PLC or Raw
Mix Control
Up to 2 sampling Software:
points controlled Ca, Si, Al, Fe, etc.
with 1 single
analyser
Analyser Sampling
Sample Transport
11
Raw Mix Control Case Study
Results 10:29:00
10:49:00
13,32
13,54
3,12
3,23
2,96
3,04
42,68
42,72
0,993
0,976
2,19 1,05
2,16 1,06
11:09:00 13,50 3,27 2,98 42,69 0,978 2,16 1,10
Raw mix Analyser(FX-3500)
Time 11:29:00 13,69 3,31 3,06 42,59 0,962 2,15 1,08
SiO2 Al2O3 Fe2O3 CaO LSF SM AM 12:16:00 13,36 3,06 2,96 42,77 0,995 2,22 1,03
12:30:00 13,85 3,34 3,09 42,54 0,950 2,15 1,08
00:17:00 13,82 3,25 2,91 42,99 0,966 2,24 1,12
12:50:00 13,56 3,18 3,05 42,59 0,973 2,18 1,04
00:37:00 13,60 3,08 2,82 43,05 0,987 2,31 1,09
13:10:00 13,70 3,26 3,03 42,64 0,964 2,18 1,08
00:57:00 13,71 3,21 2,83 43,16 0,979 2,27 1,13
13:30:00 13,76 3,34 3,06 42,48 0,954 2,15 1,09
01:17:00 13,61 3,11 2,81 43,01 0,985 2,30 1,11
13:50:00 14,03 3,34 3,11 42,46 0,937 2,18 1,07
02:05:00 13,94 3,25 2,86 42,94 0,959 2,28 1,14
14:10:00 13,72 3,31 3,11 42,47 0,956 2,14 1,06
02:25:00 13,69 3,24 2,86 42,77 0,970 2,24 1,13
14:30:00 13,74 3,13 3,09 42,43 0,959 2,21 1,01
02:45:00 13,44 3,06 2,80 42,28 0,980 2,29 1,09
14:50:00 13,75 3,34 3,03 42,45 0,954 2,16 1,10
03:05:00 13,67 3,19 2,77 42,99 0,979 2,29 1,15
15:10:00 13,61 3,23 2,90 42,72 0,974 2,22 1,11
03:25:00 13,42 3,20 2,76 42,79 0,990 2,25 1,16
16:06:00 13,45 3,18 2,83 42,76 0,987 2,24 1,12
03:45:00 13,86 3,27 2,77 42,79 0,961 2,29 1,18
16:26:00 13,61 3,28 2,81 42,81 0,976 2,23 1,17
04:05:00 13,49 3,23 2,85 42,42 0,975 2,22 1,13
16:46:00 13,74 3,10 2,79 42,87 0,974 2,33 1,11
04:25:00 13,76 3,35 2,91 42,78 0,963 2,20 1,15
17:06:00 13,73 3,33 2,80 42,80 0,967 2,24 1,19
04:45:00 13,31 3,30 2,92 42,58 0,987 2,14 1,13
17:26:00 13,43 3,15 2,75 43,11 0,999 2,28 1,15
05:05:00 13,80 3,26 3,14 42,36 0,950 2,16 1,04
17:46:00 13,66 3,21 2,77 42,79 0,975 2,28 1,16
05:25:00 13,25 3,35 3,07 42,17 0,978 2,06 1,09
18:06:00 13,54 3,17 2,73 43,08 0,991 2,29 1,16
05:45:00 13,69 3,39 3,11 42,62 0,959 2,11 1,09
18:26:00 13,62 3,10 2,81 42,82 0,980 2,30 1,10
06:05:00 13,46 3,13 3,11 42,62 0,981 2,16 1,01
18:46:00 13,62 3,18 2,87 42,85 0,978 2,25 1,11
06:25:00 13,73 3,41 3,17 42,68 0,957 2,09 1,08
19:06:00 13,56 3,27 2,89 42,63 0,974 2,20 1,13
06:45:00 13,62 3,35 3,15 42,54 0,962 2,10 1,06
23:03:00 13,45 3,18 2,85 42,98 0,992 2,23 1,12
07:05:00 13,76 3,45 3,10 42,81 0,958 2,10 1,11
23:23:00 13,62 3,24 2,92 42,84 0,975 2,21 1,11
07:25:00 13,70 3,30 2,97 42,64 0,964 2,19 1,11
23:43:00 13,63 3,09 2,89 42,98 0,982 2,28 1,07
07:45:00 13,75 3,27 2,92 42,88 0,967 2,22 1,12
Min 13,25 3,06 2,73 42,17 0,94 2,06 1,01
08:22:00 13,71 3,27 2,93 42,80 0,968 2,21 1,12
Max 14,03 3,45 3,17 43,16 1,00 2,33 1,19
08:42:00 13,59 3,09 2,85 42,78 0,981 2,29 1,08
Ave 13,63 3,23 2,93 42,72 0,97 2,21 1,10
09:26:00 13,52 3,22 2,81 42,96 0,987 2,24 1,15
Std dev 0,16 0,09 0,13 0,22 0,01 0,06 0,04
10:09:00 13,59 3,21 2,94 42,34 0,966 2,21 1,09
12
Raw Mix Control Case Study
Results
Raw mix Analyser(FX-3500) Raw mill Lab XRF (Bruker-S4) Kiln feed Lab XRF (Bruker-S4) CLINKER ANALYSIS in Lab XRF (Bruker-S4)
Ave 0,97 2,21 1,10 0,97 2,24 1,12 0,97 2,18 1,08 0,92 1,22 2,13
Std dev 0,01 0,06 0,04 0,01 0,07 0,04 0,01 0,02 0,02 0,00 0,01 0,03
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Hot Meal Control
WHY CONTROL THE HOT MEAL ?
To either :
14
Hot Meal Control
TRADITIONAL CONTROL
Human error
15
Hot Meal Control
Quenching
system
Sample short
distance Transport
To plant PLC :
Calcination value
Up to 2 analysis
per hour
Loss on ignition
analysis
16
Hot Meal Control
Typical layout
Piston Sampler
PC303
Quenching
system
Sample short
distance Transport
To plant PLC :
Calcination value
Sulphur Content
Up to 4 analysis
per hour
Carbon Sulphur
Determination
LOI Analyser
Hot meal
Sampler
+ Quencher
17
Hot Meal Control Case Study
Automatic hot meal control system as
installed in a cement plant in India
Results
Date Time LOIAnalyserResult LabResult Variance
23.01.2013 15.26PM 97,32 97,51 0,19
15.56PM 97,90 97,89 0,01
16.26PM 98,28 97,98 0,30
16.56PM 97,74 97,72 0,02
Average 97,81 97,77 0,04
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CLINKER CONTROL
Clinker Control
WHY CONTROL CLINKER ?
Check the Free Lime Value (FCaO%)
-High free lime will have a negative impact on 28 day strengths.
Small hard burned free lime particles hydrate very slowly. They will
hydrate many days after being in contact with water, and double in
size, causing cracks in the concrete
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Clinker Control
WHY CONTROL CLINKER ?
Check clinker mineralogy
Clinker Control
WHY CONTROL CLINKER ?
Use the data to optimize the kiln burner operation
HOURS
20
Clinker Control
Free Lime and Kiln Data
Free Lime / Burning Zone T/ Kiln Amps and NOx are closely
correlated over the short term
Over the long term the relation between Free Lime / BZT/ Kiln Amps and
NOx changes
Clinker Control
Free Lime and Kiln Data
o Free Lime results are used to update the set points for each of the control
factors
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Clinker Control
TRADITIONAL CONTROL
TRADITIONALLY A SPOT SAMPLE IS COLLECTED
MANUALLY FROM THE COOLER DISCHARGE OR
FROM THE PAN CONVEYOR AND BROUGHT BACK
TO THE PLANT LABORATORY TO BE ANALYSED
ONCE AN HOUR
Clinker Control
Human error
22
Clinker Control
Best location to take a sample
Precalciner
Clinker
Silo
Cooler
Kiln
Clinker Control
Clinker sampling systems
Cooler
Kiln
Under
grate
Sampler
Cooler
Cooler
discharge
Kiln discharge Sampler
23
Clinker Control
Sample Transport system
Bend
Receiving cyclone
Sending station
Diverter (several lines)
Clinker Control
Sample Transport system
24
Clinker Control
Analyser using glycol extraction and conductivity
Analysis cell
Heating
Preparation Mixing of clinker + glycol
cell Conductivity measurement
Clinker Control
At Line XRD Analyser
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Clinker Control
At Line XRD Analyser
Typical installation
26
Clinker Control Case Study
Results
1
0,9
0,8
% Free lime
0,7
0,6
0,5
K-1
0,4
0,3
K-2
0,2
0,1
0
1 2 3
Date
27
Clinker Control
Savings
Direct Savings
A 0,5 % increase in free lime results in :
Indirect Savings
Manual analysis labour cost
CEMENT CONTROL
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Cement Control
WHY CONTROL CEMENT ?
Check the Gypsum Content (CaSO42H2O)
Gypsum is the set retarder for Ordinary Portland Cement (OPC).
Without gypsum, ground clinker exhibits flash setting in a few
minutes, due to the rapid hydration of calcium aluminates
SO3 Settingtime,min Compressivestrength,Mpa Heatofhydration,Kcal/kg
percent Initial Final 1day 3day 7day 28day 12hour 1day 3day 7day 28day
1.80 115 150 17.7 37.4 53.8 61.6 22.5 33.2 45.4 59.3 67.2
2.10 130 165 20.9 40.2 59.0 65.4 28.2 33.2 44.5 63.0 65.7
2.40 135 180 20.9 32.1 47.8 62.0 46.0 54.2 63.2 80.3 88.5
Cement Control
WHY CONTROL CEMENT ?
Check the Limestone Content (CaCO3)
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Cement Control
WHY CONTROL CEMENT ?
Check Cement Fineness
Cement Control
WHY CONTROL CEMENT ?
Check Cement Fineness
- Electrical energy used in the grinding process accounts for 1% of the
worlds energy supply
- Milling is very inefficient: < 5% of energy goes into size reduction, the
rest is wasted as heat
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Cement Control
TRADITIONAL CONTROL
TRADITIONALLY A COMPOSITE SAMPLE IS COLLECTED
MANUALLY FROM FEED TO THE TRANSPORT SYSTEM
TO THE CEMENT SILOS AND BROUGHT BACK
TO THE PLANT LABORATORY TO BE ANALYSED
ONCE AN HOUR
Cement Control
Human error
31
Cement Control
Blaine Values
2 samples each with same area but a different particle size distribution
Cement Control
Blaine Values
32
Cement Control
PSD Values
Zero contribution to
strengths > 32 microns
Cement Control
Best location to take a sample
33
Cement Control
C/S Analyser
Sampling in a chute Sampling in an airslide
Slot Sampler
Screw Sampler
Piston
Sampler P11
Screw sampler
Mechanical
Transport To plant PLC :
Limestone &
gypsum rates
Analyser CO2/SO3
Cement Control
C/S Analyser
34
Cement Control
C/S Analyser
Cement Control
PSD Analyser
Laser diffraction
35
Cement Control
PSD Analyser
Vertical
chute at
classifier
outlet
Sampling in a
Sampling
vertical chute
system
On line PSD
Cement Control
PSD Analyser
Scheme Vertical
chute at
separator
outlet
On Line PSD
Sampling
system
36
Cement Control
PSD Analyser
Continuous measurement:
results on a real time basis: %>X m, Dv(X), Blaine number, particle size distribution
15 kg/h of cement are analyzed: representative sample
Cement Control
PSD Analyser
37
Cement Control Case Study
PSD Analyser
Cement plant in the UK
Product specification change with off line analysis
PSD data not available to the operator during the change from OPC (Ordinary
Portland Cement) to RHPC (Rapid Hardening Portland Cement)
Blaine manual analysis
3 hours required to reach the required specifications
Loss of 100 T of cement!!
PSD data available to the operator during the change from OPC (Ordinary
Portland Cement) to RHPC (Rapid Hardening Portland Cement)
Less than 30 min required to reach the required specifications
Savings on purging time
38
Cement Control Case Study
PSD Analyser
Cement Plant in USA
Summary of the impact of automated control and real time particle size
measurement on production parameters
Before high level After high level With high level
control control, without control and on
on line PSD line PSD
PROCESS CONTROL
Conclusions
39
THANK YOU FOR YOUR
ATTENTION
40