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Conc. Sulphuric Acid Conc. Nitric Acid Conc.

Hydrochloric Acid
cold BP cold BP cold BP
Wool - + -F + - (+)Z
Silk + + Z + +2 +
Natural Cellulose + + - Z - Z
Regenerated Cellulose Fibres + + - + - +
Secondary Cellulose acetate + + + + + +
Cellulose Triacetate + + + + (+) +
Celon, Enkalon (Nylon 6) +* + +* +* +* +*
Nylon6-6 +* + +* +* +* +*
Terylene +* + - Z* - -
Polyacrylanitrile eg. Acrilan +* + - X* - -
Dynel Modacrylic (+-) + (-) K - -
Polyvinylchloride - + -Q - - -
Polypropylene + - - - - -
Modacrylic

2 Only fibroin dissolves; sercin insoluble


3 Melts in high boiling solvent and thus appears to dissolve. Separates as a film o
BP At boiling point of the solvent
- fibres undergo no visible change
(-) slight change occurs, eg. Fibres aggregate
+ fibres dissolve completely within 15 min.
(+) fibres dissolve slowly, or dissolution is incomplete
(+-) result not clear cut, either because fibres from different manufacturers show dif
(*) On cooling or diluting the solution, flocculation may follow the initial turbidity.
* On cooling or diluting the solution ( With water if miscible, otherwise methanol)
Z fibres disintegrate into fragments
K fibres clump together, the fibrous structure may remain visible, or a molten mas
S A smear forms on the wall of the tube
Q fibres are visibly swollen
(Q) slight swelling occurs, noticeable only under microscope
F fibres or solution discolour during the test
Formic Acid (98-100%) Glacial Acetic Acid 10% Na2CO3 40% KOH Solution Acetone
cold BP cold BP BP BP cold BP
- - - - K + - -
(+-) + - - - (+) - -
- - - - - - - -
- - - - - - - -
+ + + + Saponified Saponified + -
+ + + + Saponified Saponified + +
+* +* - +* - - - -
+* +* - +* - - - -
- - - +* -Q - - -
- - - - - (+-) - -
- Z - - - - (+) +
- - - - - -Z (+-)Z (+*)
- - - - - - - -

solve. Separates as a film on cooling

ent manufacturers show different behaviour or dissolution is difficult to detect under the conditions of the test eg. Because the fibre melts
follow the initial turbidity.
scible, otherwise methanol) a definate precipitate appears

ain visible, or a molten mass may be formed


Benzene Phenol Nitrobenzene
cold BP cold BP cold BP
- - - - - -
- - - - - -
- - - - - -
+ + - - - -
- + + - +
- - - +
- - + + - (+-)
- - (*) (*) (*) (*)
- - (-) +*
- - - K - -
- - - + - +
(Q) Q - +(*) (+) +*
- - - K +3 -

st eg. Because the fibre melts

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