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f1 debinding degree C 120 140 r1

f2 debinding minutes min 40 60


percentage% %
XLSTAT 2014.1.01 - Surface response designs - on 20/03/2014 at 20:00:47
Short name: Workbook = demoDOET2.xls / Sheet = Sheet1 / Range = Sheet1!$B$1:$B$2 / 2 rows and 1 column
Long name: Workbook = demoDOET2.xls / Sheet = Sheet1 / Range = Sheet1!$C$1:$C$2 / 2 rows and 1 column
Unit: Workbook = demoDOET2.xls / Sheet = Sheet1 / Range = Sheet1!$D$1:$D$2 / 2 rows and 1 column
Unit (symbol): Workbook = demoDOET2.xls / Sheet = Sheet1 / Range = Sheet1!$E$1:$E$2 / 2 rows and 1 column
Minimum: Workbook = demoDOET2.xls / Sheet = Sheet1 / Range = Sheet1!$F$1:$F$2 / 2 rows and 1 column
Maximum: Workbook = demoDOET2.xls / Sheet = Sheet1 / Range = Sheet1!$G$1:$G$2 / 2 rows and 1 column
Short name: Workbook = demoDOET2.xls / Sheet = Sheet1 / Range = Sheet1!$B$1:$B$2 / 2 rows and 1 column
Long name: Workbook = demoDOET2.xls / Sheet = Sheet1 / Range = Sheet1!$K$1 / 1 row and 1 column
Unit: Workbook = demoDOET2.xls / Sheet = Sheet1 / Range = Sheet1!$L$1 / 1 row and 1 column
Unit (symbol): Workbook = demoDOET2.xls / Sheet = Sheet1 / Range = Sheet1!$M$1 / 1 row and 1 column

Variable information:

Short nameLong name Unit Unit (symbol)


f1 debinding degree C
f2 debinding minutes min

Model name: Ceram

Experimental design(Central composite design):

ObservationSort order Run order Repetition


debinding temperature
debinding
percentage
timeof extracted binder
Obs1 1 1 1 120 40 58.25
Obs2 2 2 1 140 40 64.75
Obs3 3 3 1 120 60 66.05
Obs4 4 4 1 140 60 69.35
Obs5 5 5 1 115.8579 50 59.55
Obs6 6 6 1 144.1421 50 68.05
Obs7 7 7 1 130 35.85786 60.15
Obs8 8 8 1 130 64.14214 69.85
Obs9 9 9 1 130 50 71.55
Obs10 10 10 1 130 50 71.85
Obs11 11 11 1 130 50 71.15
Obs12 12 12 1 130 50 71.55
Obs13 13 13 1 130 50 71.65
/ 2 rows and 1 column
2 rows and 1 column
s and 1 column
2 / 2 rows and 1 column
2 rows and 1 column
2 rows and 1 column
/ 2 rows and 1 column
w and 1 column

row and 1 column


XLSTAT 2014.1.01 - Analysis of a surface response design - on 20/03/2014 at 20:01:18
Model name: Workbook = demoDOET2.xls / Sheet = Ceram / Range = Ceram!$B$22 / 1 row and 1 column
Y / Results: Workbook = demoDOET2.xls / Sheet = Ceram / Range = Ceram!$H$26:$H$39 / 14 rows and 1 column

Summary statistics:

Variable Observations
Obs. withObs.
missing
without
data missing
Minimum
data Maximum Mean Std. deviation
percentage 13 0 13 58.250 71.850 67.212 5.024
debinding 13 0 13 115.858 144.142 130.000 8.165
debinding 13 0 13 35.858 64.142 50.000 8.165

Variable information:

Short nameLong name Unit Unit (symbol)


f1 debinding degree C
f2 debinding minutes min

Model name: Ceram

Experimental design(Central composite design):

ObservationSort order Run order Repetition


debinding temperature
debinding time
Response 1
Obs1 1 1 1 120 40 58.25
Obs2 2 2 1 140 40 64.75
Obs3 3 3 1 120 60 66.05
Obs4 4 4 1 140 60 69.35
Obs5 5 5 1 115.8579 50 59.55
Obs6 6 6 1 144.1421 50 68.05
Obs7 7 7 1 130 35.85786 60.15
Obs8 8 8 1 130 64.14214 69.85
Obs9 9 9 1 130 50 71.55
Obs10 10 10 1 130 50 71.85
Obs11 11 11 1 130 50 71.15
Obs12 12 12 1 130 50 71.55
Obs13 13 13 1 130 50 71.65

Regression of variable percentage of extracted binder:

Goodness of fit statistics:


Observatio 13.000
Sum of wei 13.000
DF 7.000
R 0.996
Adjusted R 0.993
MSE 43.270
RMSE 6.578
MAPE 0.376
DW 2.286
Cp 6.000
AIC 52.929
SBC 56.319
PC 0.011
Press RMS 0.993
Press 6.903
Q 0.977

Analysis of variance:

Source DF Sum of squares


Mean squares F Pr > F
Model 5 301.717 60.343 359.921 < 0,0001
Error 7 1.174 0.168
Lack of fit 3 0.914 0.305 4.685 0.085
Pure error 4 0.260 0.065
Corrected T 12 302.891
Computed against model Y=0

Model parameters:

Source Value Standard error t Pr > |t|


Lower bound
Upper
(95%)
bound (95%)
Intercept 71.550 0.183 390.736 < 0,0001 71.117 71.983
debinding 2.728 0.145 18.841 < 0,0001 2.385 3.070
debinding 3.265 0.145 22.552 < 0,0001 2.922 3.607
debinding -3.825 0.155 -24.639 < 0,0001 -4.192 -3.458
debinding -3.225 0.155 -20.774 < 0,0001 -3.592 -2.858
debinding -0.800 0.205 -3.908 0.006 -1.284 -0.316

Equation of the model:

Response 1 = 71,55+2,72760191002141*debinding temperature+3,26473394437738*debinding time-3,825*debinding


Standardized coefficients:

Source Value Standard error t Pr > |t|


Lower bound
Upper
(95%)
bound (95%)
debinding 0.443 0.024 18.841 < 0,0001 0.388 0.499
debinding 0.531 0.024 22.552 < 0,0001 0.475 0.586
debinding -0.585 0.024 -24.639 < 0,0001 -0.641 -0.529
debinding -0.493 0.024 -20.774 < 0,0001 -0.549 -0.437
debinding -0.092 0.024 -3.908 0.006 -0.148 -0.036
Standardized coefficients

Response 1 / Standardized coefficients


(95% conf. interval)
0.600

0.400

0.200

0.000

-0.200

-0.400

-0.600

Variable
-0.800

Predictions and residuals:

Observation Weight Response


Pred(Response
1 1)
Residual Std.
Studentized
residual Studentized
residuals(Internal)
residuals(External)
Std. dev. on pred. (Mean)
1 1 58.250 57.708 0.542 0.082 0.135 0.135 0.324
2 1 64.750 64.763 -0.013 -0.002 -0.003 -0.003 0.324
3 1 66.050 65.837 0.213 0.032 0.053 0.053 0.324
4 1 69.350 69.692 -0.342 -0.052 -0.085 -0.085 0.324
5 1 59.550 60.043 -0.493 -0.075 -0.122 -0.122 0.324
6 1 68.050 67.757 0.293 0.044 0.073 0.073 0.324
7 1 60.150 60.483 -0.333 -0.051 -0.083 -0.083 0.324
8 1 69.850 69.717 0.133 0.020 0.033 0.033 0.324
9 1 71.550 71.550 0.000 0.000 0.000 0.000 0.183
10 1 71.850 71.550 0.300 0.046 0.051 0.051 0.183
11 1 71.150 71.550 -0.400 -0.061 -0.068 -0.068 0.183
12 1 71.550 71.550 0.000 0.000 0.000 0.000 0.183
13 1 71.650 71.550 0.100 0.015 0.017 0.017 0.183
Response 1[%] / Standardized residuals Pred(Response 1[%]) / Standardized residuals
Standardized residuals

Standardized residuals
0.100 0.100

0.050 0.050

0.000 0.000
55.000 57.000 59.000 61.000 63.000 65.000 67.000 69.000 71.000 73.000 75.000 55.000 57.000 59.000 61.000 63.000 65.000 67.000 69.000

-0.050 -0.050

Response 1[%] Pred(Response 1[%])


-0.100 -0.100

Cook's distances
0.006
Cook's distance

0.005

0.004

0.003

0.002

0.001

0.000
1 2 3 4 5 6 7 8 9 10 11 12 13
Observations

Contour plot (Response 1[%])


debinding time[min]

60.000
59.000
58.000
57.000
40.000 56.000
41.000 55.000
42.000 54.000
43.000 53.000
44.000 52.000
45.000 51.000
46.000 50.000
47.000 49.000
48.000 48.000
debinding time[m
60.000
59.000
58.000
57.000
40.000 56.000
41.000 55.000
42.000 54.000
43.000 53.000
44.000 52.000
45.000 51.000
46.000 50.000
47.000 49.000
48.000 48.000
49.000 47.000
46.000
50.000
45.000
51.000 44.000
52.000 43.000
53.000 42.000
54.000 41.000
55.000 40.000
56.000
120.000
121.000
122.000
123.000
124.000
125.000
126.000
127.000
128.000
129.000
130.000
131.000
132.000
133.000
134.000
135.000
136.000
137.000
138.000
139.000
140.000
57.000

debinding temperature[C]

40.000
Contour plot (3D view) 41.000
42.000
43.000
44.000
45.000
46.000
82.000 47.000
48.000
78.800
Response 1[%]

49.000
75.600 50.000
72.400 51.000
52.000
69.200 53.000
66.000 54.000
62.800 55.000
59.600 56.000
57.000
56.400
53.200
debinding time[min]
50.000
120.000
122.000
124.000
126.000
128.000
130.000
132.000
134.000

debinding temperature[C]
136.000
138.000
140.000

Trace debinding temperature


85
Response 1[%]

80

75

70

65

60

55

50
120 122 124 126 128 130 132 134 136 138 140
debinding temperature[C]
65

60

55

50
120 122 124 126 128 130 132 134 136 138 140
debinding temperature[C]

Trace debinding time

95
Response 1[%]

85

75

65

55

45
40 42 44 46 48 50 52 54 56 58 60
debinding time[min]
ow and 1 column
/ 14 rows and 1 column
ebinding time-3,825*debinding temperature^2-3,225*debinding time^2-0,800000000000001*debinding temperature*debinding time
Lower bound
Upper
95%bound
(Mean)
Std. dev.
95%on(Mean)
Lower
pred. bound
(Observation)
Upper
95%bound
(Observation)
95% (Observation)
Adjusted Pred.Cook's D
56.942 58.474 0.522 56.473 58.943 56.261 0.005
63.997 65.529 0.522 63.528 65.998 64.797 0.000
65.071 66.603 0.522 64.602 67.072 65.269 0.001
68.926 70.458 0.522 68.457 70.927 70.605 0.002
59.277 60.809 0.522 58.808 61.278 61.356 0.004
66.991 68.523 0.522 66.522 68.992 66.977 0.001
59.717 61.249 0.522 59.248 61.718 61.371 0.002
68.951 70.483 0.522 68.482 70.952 69.362 0.000
71.117 71.983 0.449 70.489 72.611 71.550 0.000
71.117 71.983 0.449 70.489 72.611 71.175 0.000
71.117 71.983 0.449 70.489 72.611 72.050 0.000
71.117 71.983 0.449 70.489 72.611 71.550 0.000
71.117 71.983 0.449 70.489 72.611 71.425 0.000
esponse 1[%]) / Standardized residuals Pred(Response 1[%]) / Response 1[%] Sta
75.000

Response 1[%]

Observations
70.000

65.000

59.000 61.000 63.000 65.000 67.000 69.000 71.000 73.000 75.000

60.000

55.000
Pred(Response 1[%])
55.000 60.000 65.000 70.000 75.000 -0.500 -0.400 -0.30
Pred(Response 1[%])
rature*debinding time
Standardized residuals / Response 1[%]

13

12
Observations

11

10

5
Standardized
4 residuals

-0.500 -0.400 -0.300 -0.200 -0.100 0.000 0.100 0.200 0.300 0.400 0.500

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