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Proceedings of National Symposium for Post Graduate Students (NSPGS 2010), 24 25 April, 2010: Vol 4 Civil, Materials &

p; Metallurgy

Squeeze casting of aluminium alloy and composites


P. Manikandan1*, K. Sukumaran and D. Jebakani1
1
Dept. of Mechanical Engg., Government College of Engineering, Tirunelveli
2
National Institute of Interdisciplinary Science and Technology, CSIR, Trivandrum
*Email: tuticorinmani@rediffmail.com

Abstract ceramic particles such as SiC , B4C and A2O3 to


Squeeze casting is an advanced metal the alloy is expected to increase the mechanical
forming process for manufacturing near net properties considerably [2]. Metal matrix
engineering components. The process of squeeze composites (MMCs) have an edge over polymer
casing is the combination of metal casting and
matrix composites owing to their high
forging. Enhanced mechanical properties can be
achieved because of fine grain structure caused by temperature withstanding ability, wear
rapid solidification. Very low shrinkage and gas resistance, lower coefficients of thermal
porosity can also be characterized. Squeeze casting expansion and no out gassing. In metal matrix
is suitable for high strength, high ductility, composites, the matrix is a metal or an alloy and
lightweight structural aluminum castings needed the reinforcements are mainly ceramics in
for advanced components. The present paper deals different morphologies viz. continuous fiber,
with to study the effect of squeeze casting on short fiber, whisker and particulates. Amongst
microstructural refinement leading the improved the MMCs developed, discontinuously
mechanical properties of aluminum alloy and metal
reinforced MMCs (DMMCs) have an edge over
matrix composites.
continuously reinforced MMCs in view of their
Keywords: Squeeze casting; Aluminium, Metal ease of synthesis and shaping and lower cost.
matrix composites The components are generally shaped by
conventional methods such as forging/rolling
1. INTRODUCTION which are high energy intensive processes. But
The use of light-metal components in squeeze casting is an economical, single-step
aerospace and automobile applications has near-net shaping process and have advantages of
increased during the last decade. One advantage manipulating the microstructure within the
is that light-metal components lead to an overall material thereby isotropic properties can be
reduced weight and, thus, to reduced energy achieved in the components. Squeeze casting is a
consumption. Another advantage, which may be relatively new and developing casting process. A
just as important from an environmental point of major market is the automotive market which is
view, is the fact that aluminium components may increasingly demanding lightweight components
be recycled with relative low energy demands [1- to improve fuel efficiency. Because squeeze
4]. casting is relatively new, much work needs to be
The most economical process of making done to better understand the fundamentals of the
metallic components is casting. In the casing process.
process is pouring molten metal into a mold to
produce an object of desired shape. 2. Squeeze Casting
The major drawback of casting such as gas
porosity, shrinkage defects, misruns, cold shuts, Squeeze casting (SC) for producing ultra
inclusions, hot tears and hot spots. In order to strong, metallic component from liquid metal.
compensate the drawback of casting several new Liquid alloy is injected inside the metallic die
casting techniques have been developed. One of and subjected to high pressures for a small time
the methods to minimize the casting defect is by in the cavity. Superior quality components are
solidifying the melt under pressure and the possible [6].
process is termed as squeeze casting. In the
squeeze casting has got great potential to
fabricate near-net shape components having high
integrity with very low defects level [1-2].
High strength wrought alloy are generally
used in aerospace industry for making structural
components. Addition of high wear-resistant

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Proceedings of National Symposium for Post Graduate Students (NSPGS 2010), 24 25 April, 2010: Vol 4 Civil, Materials & Metallurgy

investment casting, die casting and metal matrix


composite-making arts.
3.1. Processing techniques of squeeze casting
for metal matrix composites

There are two processing


method are available for metal matrix
composites by squeeze casting.

A. Squeeze Casting Infiltration.


B. Squeeze casting by stir casting method.

A. Squeeze Casting Infiltration

Squeeze Casting Infiltration is a forced


infiltration method of liquid phase fabrication of
Metal Matrix Composites, using a movable mold
part (ram) for applying pressure on the molten
metal and forcing it to penetrate into a performed
dispersed phase, placed into the lower fixed
mold part [8].

Fig. 1 : Process chart of Squeeze casting [6].

The process of squeeze casting consist of


following steps [1]:

1. A metered quantity of liquid metal is poured


into a preheated and well lubricated die cavity of
require size and shape kept on the bed of a
hydraulic press.

2. The liquid metal is then pressurised using a


suitable punch after a dwell time.
Fig. 2: Schematic of the Squeeze Casting Infiltration [8].
3. The pressure is maintain for a reasonable time
till the molten metal solidifies completely.
Squeeze Casting Infiltration process has the
4. The punch is then withdrawn and the casting following steps:
is ejected out.
1. A preform of dispersed phase (particles,
3. Squeeze casting of metal matrix composites fibers) is placed into the lower fixed mold
half.
A squeeze-casting method is taught for
manufacturing metal matrix composites which
require little or no finishing operations. This 2. A molten metal in a predetermined amount is
method utilizes a combination of techniques, poured into the lower mold half.
fundamentals of which are found in the

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Proceedings of National Symposium for Post Graduate Students (NSPGS 2010), 24 25 April, 2010: Vol 4 Civil, Materials & Metallurgy

3. The upper movable mold half (ram) moves


downwards and forces the liquid metal
to infiltrate the preform.

4. The infiltrated material solidifies under the


pressure.

5. The part is removed from the mold by means


of the ejector pin.

B. Squeeze casting by stir casting method

In the Squeeze casting by stir casting method


the metal matrix composites are fabricated by
two stage.

a. Synthesis of the composites by stir casting


method

b. Processing of composites to the required shape Fig. 3: Schematic diagram of the stir casting [9].
by squeeze casting.

a. Synthesis of the composites by stir casting b. Processing of composites to the required


method shape by squeeze casting.
There are different methods for the synthesis of
metal matrix composites, namely, powder Squeeze casting, also known as liquid metal
metallurgy, stir casting, compocasting and forging, is a combination of casting and forging
infiltration. Out of these, stir casting is the process.
simplest and the cheapest.In the stir casting
method, stirring is done by means of an impeller,
or electromagnetism.Out of these, impeller
stirring is the cheapest and simplest means [10] .
For the synthesis of Al DMMC by impeller
stirring, the reinforcement is added into the
vortex created by stirring the melt with a
mechanical device most often by a rotating
impeller which causes the dispersoids to move
along with the fluids resulting in mixing. A
schematic of the setup for the synthesis of Al
DMMCs by stir casting is shown in Fig.3.
Synthesis of Al DMMCs by liquid melt impeller
stirring has to incorporate and suspend ceramic
particles in liquid Al metal homogeneously.

Fig. 4: Schematic diagram of the Squeeze Casting [8].

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Proceedings of National Symposium for Post Graduate Students (NSPGS 2010), 24 25 April, 2010: Vol 4 Civil, Materials & Metallurgy

Sequence of operations in squeeze-casting:

1. Bring a ladle filled with liquid metal matrix


composite close to the dies

2. Pour liquid in the bottom die cavity

3. Close dies and apply pressure

4. Open dies and eject the solidified product

3.2. Characterized of Squeeze castings

1.Low shrinkage and gas porosity

In the squeeze casting process, the high


pressure applied during solidification can
eliminate porosity caused by both gas and
shrinkage.

Table 1: The Density measurements and porosity percent [4].


Squeeze pressure

As cast 70 MPa 100 160


MPa MPa
Total 2.783 0.698 0.659 0.490
pore
area sq-
m/g
Bulk 2.5846 2.6735 2.6753 2.6976
Density 2.6527* 2.6894* 2.6902* 2.6917*
g/ml
Porosity 2.27 0.71 0.63 0.48
%
* Archimedes measurements.

2.Fine grain structure caused by rapid


solidification
In the squeeze casting process the increased
cooling rate caused by improved thermal contact
between the casting and die results in the
formation of fine grained structures.Fig. 5 shows
the macrostructural characterization conducted
on the squeeze cast alloys at 70, 100 and 160
MPa, respectively. It revealed no evidence of Fig. 5: Macrostructure of squeeze cast alloys (a) 70 (b) 100
blowholes or macropores. The macrostructure is and (c) 160 MPa [4].
an equiaxised structure and the grain sizes
decrease with increase of squeeze pressure from
70 to 160 MPa.

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Proceedings of National Symposium for Post Graduate Students (NSPGS 2010), 24 25 April, 2010: Vol 4 Civil, Materials & Metallurgy

3. Increasing mechanical properties alloys are less while the values of nontreated
The improvement in the mechanical alloys are the lowest. The eutectic Si in as-cast
properties can be attributed to the refinement in alloy is present as coarse, acicular needles which
the microstructure obtained by the application of act as stress raisers, and consequently, the
pressure during solidification.The mechanical material is easy fractured. The heat treatment
properties such as ultimate tensile strength, yield modifies the morphology of the Si from acicular
strength , percentage of elongation, hardness and to spherodized shape, thereby improving the
wear. mechanicalproperties. The enhancement of
strength properties obtained during aging
a. Tensile properties treatment is primarily owing to the metastable
In the squeeze the pressure applied during phase from the supersaturated solution. When
solidification has to improve the tensile both the solution and aging treatment effects on
properties. Tensile test determine the strength of the tensile properties are considered, the
material when subjected to a simple stretching properties would show an increase in
operation strength and decrease in ductility. The increase
of strength with increasing squeeze pressure is
Table . 2: Mechanical properties (UTS, YS and El.%) of due to the increased solubility of Si and the
investigated alloys [4].
virtual elimination of shrinkage and/or gas voids
Effect of heat treatment could allcontribute towards the observed
Pressure MPa Non Solution Aging improvements in strength of the alloys. The
treated treatment elongation percent increases with increasing
UTS As 103 147 150 squeeze pressure, the values of solution-treated
MPa cast alloys are the largest ones. The improvements in
elongation values are most likely to be due to the
70 128 173 198 increased volume fraction of the primary a phase
and improved soundness of the alloys. The
100 131 185 200 eutectic Si morphology plays a vital role in
determining the mechanical properties. Particle
160 132 190 208 size, shape and spacing are factors that
characterize Si morphology. Under normal
YS As 64 114 82 cooling conditions, Si particles are present as
MPa cast coarse acicular needles. The needles act as crack
70 87 136 136 initiators and lower mechanical properties
appreciably. The Si particle characteristics can
100 103 139 165 be altered by subjecting the casting to a high
temperature heat treatment for long periods.
160 114 140 190 Therefore, for prolonged solution treatment, the
EI.% As 2.5 4 3.5 observed change in tensile properties are
cast attributed to change in Si particle characteristic
70 4 13 5 [4].

100 5.5 14 6 b. Hardness


The application of pressure during
160 6.5 15 8 solidification in squeeze casting minimizes
porosity and makes the metal more dense,
making the matrix to resist surfacial plastic
deformation, rendering higher hardness to the
Table 2 shows the values of ultimate tensile matrix[3].
strength (UTS), yield strength (YS) and
elongation percent (El%) of the non-heat-treated, c. Wear
solution-treated and aged alloys at different Ceramic particles such as SiC , B4C and
squeeze pressures. From the table UTS and YS A2O3 may be attributed to hardness of the
show an increasing trend with increasing of material a dominating factor affecting the wear
squeeze pressure from 70 to 160 MPa for all resistance. The decrease in wear weight loss may
alloys. Aged alloys have the largest value of also be attributed to higher load bearing capacity
UTS and YS, the values of solution-treated of hard reinforcing material[3].

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Proceedings of National Symposium for Post Graduate Students (NSPGS 2010), 24 25 April, 2010: Vol 4 Civil, Materials & Metallurgy

coefficient of friction compared to that of


aluminium alloy.

References

1. K. Sukumaran, R.M. Pillai, S.G.K. Pillai and


B.C. Pai , Squeeze Casting : A Novel Metal
Processing Technique INDIAN FOUNDRY
JOURNAL, Vol.50, No.2/February, 2004.

2. K. Sukumaran , K.K. Ravikumar, S.G.K. Pillai,


T.P.D. Rajan, M. Ravi, R.M. Pillai, B.C. Pai
Studies on squeeze casting of Al 2124 alloy and
2124-10% SiCp metal matrix composite
Materials Science and Engineering A 490 (2008)
235241.

3. K.R. Suresh , H.B. Niranjan , P. Martin Jebaraj ,


M.P. Chowdiah Tensile and wear properties of
aluminum composites Wear 255 (2003) 638
642.

4. M.T. Abou El-khair Microstructure


characterization and tensile properties of squeeze-
cast AlSiMg alloys Materials Letters 59 (2005)
894 900.

5. R. Ehsani and S.M. Seyed Reihani Aging


Fig. 6: Comparison of wear characteristics of squeeze cast Behavior and Tensile Properties of Squeeze Cast
alloy and composite [2] AL 6061/SIC Metal Matrix Composites Scientia
Iranica, Vol. 11, No. 4, pp 392-397.
The wear properties of the composite are much 6. Gopal P. Sinha1 and Ashis K. Choudhury
better than that of the monolithic alloy. The ADVANCES IN NET SHAPE
increased wear resistance in the composites is MANUFACTURING Proceedings of the
due to the presence of hard SiC particles which International Conference on Aerospace Science
and Technology 26-28 June2008, Bangalore,
act as protrusion over the matrix and protect the India
composite surface from severe wear. The
coefficient of friction in the composite is also 7. Kalakkath prakasan, Sambasivam seshan
observed to be very low compared to the base Microstructure and properties of squeeze cast
Cu-carbon fibre metal matrix composite
alloy (Fig. 6b). Here the particles help in JOURNAL OF MATERIALS SCIENCE 34
reduction of contact area between the composite (1999) 5045 5049
surface and counter surface during sliding wear.
This leads to lower temperature rise and 8. Dmitri Kopeliovich Liquid state fabrication of
Metal Matrix Composites
coefficient of friction of composite over base
alloy during wear [2]. 9. Ranjit Bauri, M.K. Surappa Processing and
properties of AlLiSiCp composites Science
and Technology of Advanced Materials 8 (2007)
4. Conclusions 494502

1. The Aluminium alloy and composite can be


squeeze cast to get the macrostructure and 10. K.G. Satyanarayana, R.M. Pillai, B.C. Pai, An
analysis of impeller parameters for aluminium
mechanical properties. metal matrixccomposites synthesis Materials
2. In the case of composite, the squeeze casting and Design 23 (2002) 553556.
is found to be very effective not only in
minimizing the defect level thereby increasing 11. Qiang Zhang, Gaohui Wu, Guoqin Chen,
Longtao Jiang, Bofeng Luan The thermal
the mechanical properties but in improving expansion and mechanical properties of high
the overall distribution of the second phase reinforcement content SiCp/Al composites
particles. fabricated by squeeze casting technology
3. The squeeze cast metal matrix composite Composites: Part A 34 (2003) 10231027
shows improved wear resistance and lower

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