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Designation: D2974 14
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D2974 14
where: 8.3 Organic Matter Determination:
AD = mass of the air-dried sample, g, and 8.3.1 Calculation:
B = mass of the oven-dried sample, g. 8.3.1.1 Determine the amount of organic matter to the
(1) This calculation gives moisture content of the air dried nearest 0.1 % by difference, as follows:
sample as a percentage of oven-dried mass. Organic matter, % 5 100.0 2 D (4)
8.2 Ash Content Determination: where:
8.2.1 Test Method C:
D = ash content, % (nearest 0.1 %).
8.2.1.1 Determine the mass of a covered high-silica or
porcelain dish to the nearest 0.01 g. 9. Report: Test Data Sheet(s)/Form(s)
8.2.1.2 Place a part or all of the oven-dried test specimen 9.1 The methodology used to specify how data are recorded
from a moisture determination in the dish and determine the on the test data sheet(s)/form(s), as follows, is covered in 1.4.
mass of the dish and specimen to the nearest 0.01 g.
9.2 Record as a minimum the following general information
8.2.1.3 Remove the cover and place the dish in a furnace.
(data):
Gradually bring the temperature in the furnace to 440 6 40C
9.2.1 Sample/specimen identifying information, such as
and hold until the specimen is completely ashed (no change of
Project No., Boring No., Sample No., Depth, and alike.
mass occurs after at least 1 hr period of heating).
9.2.2 Any special selection and preparation process, such as
8.2.1.4 Cool in a desiccator, and determine the mass to the
removal of gravel or other materials.
nearest 0.01 g keeping the exposure to the room atmosphere to
9.2.3 Technician name or initials, method used and date.
a minimum.
8.2.1.5 This test method should be used for general classi- 9.3 Record as a minimum the following test specimen data:
fication purposes, except the use of peat for fuel. 9.3.1 Results for organic matter and ash content, to the
8.2.2 Test Method D: nearest 0.1 %.
8.2.2.1 Determine the mass of a covered high-silica or 9.3.2 Furnace temperature used for ash content determina-
porcelain dish to the nearest 0.01 g. tions.
8.2.2.2 Place a part of the oven-dried test specimen from a 9.3.3 Express results for moisture content as a percentage of
moisture determination in the dish and determine the mass of oven-dried mass as follows:
the dish and specimen to the nearest 0.01 g. 9.3.3.1 Below 100 % to the nearest 1 %.
9.3.3.2 Between 100 % and 500 % to the nearest 5 %.
8.2.2.3 Remove the cover and place the dish in a furnace.
9.3.3.3 Between 500 % and 1000 % to the nearest 10 %.
Gradually bring the temperature in the furnace to 750 6 38C
9.3.3.4 Above 1000 % to the nearest 20 %.
and hold until the specimen is completely ashed (no change in
mass of the sample after further drying periods in excess of 1 10. Precision and Bias
h). 10.1 PrecisionTest data on precision is not presented due
8.2.2.4 Cool in a desiccator, and determine the mass to the to the nature of the soil materials tested by this test method. It
nearest 0.01 g keeping the exposure to the room atmosphere to is either not feasible or too costly at this time to have ten or
a minimum. more laboratories participate in a round-robin testing program.
8.2.2.5 This test method should be used when peats are 10.1.1 The Subcommittee D18.22 is seeking any data from
being evaluated for use as a fuel. the users of this test method that might be used to make a
8.2.3 Calculation for Test Methods C and D: limited statement on precision.
8.2.3.1 Calculate the ash content as follows:
10.2 BiasThere is no accepted reference value for this test
Ash Content, % 5 ~ C 3 100! /B (3) method, therefore, bias cannot be determined.
where: 11. Keywords
C = mass of ash, g, and 11.1 ash content; moisture content; organic soil; peat; per-
B = oven-dried test specimen, g.
cent organic matter
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D2974 14
SUMMARY OF CHANGES
Committee D18 has identified the location of selected changes to this standard since the last issue
(D2974 13) that may impact the use of this standard. (Approved November 1, 2014)
(1) Changes made throughout to clarify the uses of the different (2) Reference to D2944 was added for sampling methodology.
test methods contained in this standard.
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