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5. Fabrikasi sensor : Fabrication of GCE was carried out by the as-grown Ce2S3-CNT NCs
using 5% ethanolic Naon solution as the conducting binder. It was then heated in an oven
at 65 C for 2 h to obtain a dry lm on GCE. In the electrochemical cell, a working electrode
(WE) was made of the Ce2S3-CNT NC-coated GCE, whereas the counter electrode was made
by a platinum (Pt) wire and aqueous UA in the buffer solution was the electrolyte. To use as
target analytes, aqueous UA solution (0.1 M) was diluted to different concentrations (from
1.0 mM to 0.01 nM) using deionized water. All IV measurements were carried out in 5.0 mL
of phosphate buffer solution (PBS; 0.1 M; pH 7.0). From the slope of the current vs. voltage
plot, the sensitivity of the proposed UA sensor was estimated.37 Using an electrometer, IV
method was applied to UA solutions with Ce2S3-CNT NCs/GCE as the WE. Real samples were
obtained from the medical center (KAU medical center). Initially, the rabbit serum was
isolated from the blood. Aer dilution in PBS buffer, real serum and urine samples were
analyzed via the fabricated Ce2S3-CNT NCs/GCE sensor using the IV method under ambient
conditions.
7. Karakterisasi sensor :
8. Uji interfensi :