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TESTING OF LPG RESIDUE

DOC. NO.: PPL-HGPP-LAB/SOP/016


REV: ORIGINAL

PAKISTAN PETROLEUM LIMITED


PROCEDURE

Pakistan Petroleum Limited

STANDARD PROCEDURE FOR


TESTING OF LPG RESIDUE
OPERATING

Document No. :PPL-HGPP-LAB/SOP/016


Original Issue Date : 26-03-2016
Revision : 0riginal
Last Date of Revision : XX-YY-ZZZZ
STANDARD

Prepared by Reviewed by Approved by

Abdul Qadir Syed Aslam Shah M.Ali Khan


Lab Chemist Plant Manager PEIC, HGPP

Standard Operating Procedure Page 0 of 8


TESTING OF LPG RESIDUE
DOC. NO.: PPL-HGPP-LAB/SOP/016
REV: ORIGINAL

PAKISTAN PETROLEUM LIMITED

Copyright: © Pakistan Petroleum Limited


All rights reserved except as permitted by Pakistan Petroleum Limited. No
DOCUMENT CHANGE RECORD
Part of this document may be reproduced or distributed in any form and by
any means or stored in a database or retrieval system without the prior
written permission from Top Management
REV. DATE OF PAGES BRIEF DESCRIPTION OF CHANGES
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Standard Operating Procedure Page 1 of 8


TESTING OF LPG RESIDUE
DOC. NO.: PPL-HGPP-LAB/SOP/016
REV: ORIGINAL

PAKISTAN PETROLEUM LIMITED

TABLE OF CONTENTS

S. NO. CONTENTS PAGE NO.

Distribution List 3

List of Abbreviations 4

Terms & Definitions 5

1. Purpose 6

2. Scope 6

3. Responsibilities and Authorities 6

4. Potential Hazards 6

5. General Safety 6

5.1 Pre Job Safety Meeting 6

5.2 Permit to Work Requirements 7

5.3 Isolation Required 7


Special Precautions and Equipment Required For
6. 7
Procedure
7. Procedure 7

8. Procedure Close-OUT 7

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TESTING OF LPG RESIDUE
DOC. NO.: PPL-HGPP-LAB/SOP/016
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PAKISTAN PETROLEUM LIMITED

9. Training and Evaluation 7

10. Related Documents and Records 8

DISTRIBUTION LIST

Plant Manager
Laboratory

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TESTING OF LPG RESIDUE
DOC. NO.: PPL-HGPP-LAB/SOP/016
REV: ORIGINAL

PAKISTAN PETROLEUM LIMITED

LIST OF ABBREVIATIONS

°F Degree Fahrenheit
ASTM American Society for Testing & Materials
CCR Central Control Room
HGPP Hala Gas Processing Plant
LAB Laboratory
LPG Liquified Petroleum Gas
ml Milliliter
MSDS Material Safety Data Sheet
PEIC Production Engineer In-charge
PJSM Pre Job Safety Meeting
PM Plant Manager
PPE Personal Protective Equipment
PPL Pakistan Petroleum Limited
QHSE Quality, Health, Safety & Environment

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TESTING OF LPG RESIDUE
DOC. NO.: PPL-HGPP-LAB/SOP/016
REV: ORIGINAL

PAKISTAN PETROLEUM LIMITED

TERMS AND DEFINITIONS

TERMS DEFINITION

Ignition The action of setting something on fire or starting to burn.

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TESTING OF LPG RESIDUE
DOC. NO.: PPL-HGPP-LAB/SOP/016
REV: ORIGINAL

PAKISTAN PETROLEUM LIMITED

1. PURPOSE:

To provide necessary guidelines for safe Testing of LPG Residue - ASTM XX as


such should be used for the reference all the time.

2. SCOPE:

This control procedure outlines equipment detailed summaries along with testing
guidelines for Testing of LPG. Also the hazards involved and, tools required in
performing this task safely.

3. RESPONSIBILITIES AND AUTHORITIES:

Plant Manager and Deputy Plant Manager shall responsible for:

 To ensure that concerned Lab Chemist/ Operation Engineer comply with


the procedures as described herein.

Operation Engineer shall be responsible for:

 To ensure that all the concerned Lab Chemist comply with the
procedures as described herein.

Lab Chemist shall be responsible for:

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TESTING OF LPG RESIDUE
DOC. NO.: PPL-HGPP-LAB/SOP/016
REV: ORIGINAL

PAKISTAN PETROLEUM LIMITED

 To ensure that they have all the knowledge for Testing of LPG Residue -
ASTM XX as described herein.

4. POTENTIAL HAZARDS:

 Ignition source
 Inhalation

5. GENERAL SAFETY:

5.1 Pre Job Safety Meeting:

To ensure safe Testing of LPG Residue - ASTM XX, PJSM should be held to
identify any potential hazards that may occur during the charging procedure.

5.2 Permit to Work Requirements:

No any work permit is required before starting the procedure.

5.3 Isolation Required:

No any isolation is required.

6. SPECIAL PRECAUTIONS AND EQUIPMENT REQUIRED FOR PROCEDURE:

 Hand gloves
 Mandatory PPEs
 Radio for communication with CCR
 Refer to MSDS sheet
 Safety goggles

7. PROCEDURE:

 Rinse the weathering tube with the LPG to be sampled.


 Fill it with 100ml of LPG sample.
 Insert a thermometer in the tube and clamp the assembly with iron stand.
 Bring it at constant required temp of 40°F.

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TESTING OF LPG RESIDUE
DOC. NO.: PPL-HGPP-LAB/SOP/016
REV: ORIGINAL

PAKISTAN PETROLEUM LIMITED

 Read the remaining volume of LPG, as % of residue at 40°F.


 Refer ASTM - XX for this procedure.

8. PROCEDURE CLOSE-OUT:

 Note the reading.


 Contact CCR to let them know job is completed.

9. TRAINING & EVALUATION:

For effective implementation of this procedure:

 Plant Manager/ Deputy Plant Manager are responsible to arrange trainings on


the basis of training needs.

 Plant Manager/ Deputy Plant Manager will evaluate the overall effectiveness
of this program in Hala Gas Processing Plant on annual basis.

10. RELATED DOCUMENTS AND RECORDS:

ASTM Tests for Petroleum, Fuels, and Petrochemicals

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