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Designation: D 178 – 01e1

Standard Specification for


Rubber Insulating Matting1
This standard is issued under the fixed designation D 178; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.

This standard has been approved for use by agencies of the Department of Defense.

e1 NOTE—A precision and bias statement was added editorially in May 2004.

1. Scope D 570 Test Method for Water Absorption of Plastics 4


1.1 This specification covers acceptance testing of rubber D 573 Test Method for Rubber Deterioration in an Air
insulating matting for use as a floor covering for protection of Oven 3
workers. D 1692 Test Method for Rate of Burning or Extent and
1.2 Two types of matting, differing in chemical and physical Time of Burning of Cellular Plastics Using a Specimen
characteristics, are provided and are designated as Type I and Supported by a Horizontal Screen 5
Type II matting. 2.2 American National Standard:6
1.3 The following safety hazards caveat applies only to the ANSI C84.1 Voltage Ratings for Electric Power Systems
test method portion, Sections 17 to 19, of this specification: and Equipment (60 Hz)
This standard does not purport to address all of the safety
3. Terminology
concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and 3.1 Definitions:
health practices and determine the applicability of regulatory 3.1.1 user, n—as used in 4.3.1, the entity employing the
limitations prior to use. actual worker(s) utilizing the equipment; if no separate em-
ployer, then the individual.
NOTE 1—Rubber insulating matting should remain flexible for use 3.1.2 voltage, maximum retest, n—voltage, either ac rms or
through normal temperature ranges.
dc avg, which is equal to the proof-test voltage for new
NOTE 2—Rubber as used in this specification is a generic term that
includes elastomers and elastomer compounds, regardless of origin. protective equipment.
3.1.3 voltage, retest, n—voltage, either ac rms or dc avg,
2. Referenced Documents that used protective equipment must be capable of withstand-
2.1 ASTM Standards: ing for a specified test period without breakdown.
D 149 Test Method for Dielectric Breakdown Voltage and 3.1.4 voltage, nominal design, n—a nominal value consis-
Dielectric Strength of Solid Electrical Insulating Materials tent with the latest revision of ANSI C84.1, assigned to the
at Commercial Power Frequencies 2 circuit or system for the purpose of conveniently designating
D 297 Test Methods for Rubber Products—Chemical its voltage class.
Analysis 3 3.1.5 voltage, maximum use, n—the ac voltage (rms) clas-
D 412 Test Methods for Vulcanized Rubber and Thermo- sification of the protective equipment that designates the
plastic Rubbers and Thermoplastic Elastomers—Tension 3 maximum nominal design voltage of the energized system that
D 471 Test Method for Rubber Property—Effect of Liq- may be safely worked. The nominal design voltage is equal to
uids 3 phase-to-phase voltage on multiphase circuits.
D 518 Test Method for Rubber Deterioration—Surface 3.1.5.1 If there is no multiphase exposure in a system area,
Cracking 3 and the voltage exposure is limited to phase (polarity on dc
systems) to ground potential, the phase (polarity on dc sys-
tems) to ground potential shall be considered to be the nominal
1
This specification is under the jurisdiction of ASTM Committee F18 on design voltage.
Electrical Protective Equipment for Workers and is the direct responsibility of
Subcommittee F18.25 on Insulating Cover-Up Equipment. This standard replaces
ANSI Standard J 6.7, which is no longer available. 4
Annual Book of ASTM Standards, Vol 08.01.
Current edition approved March 10, 2001. Published May 2001. Originally 5
Discontinued January 1978; see the 1977 Annual Book of ASTM Standards,
published as D178 – 23 T. Last previous edition D178 – 93 (1998). Part 36.
2
Annual Book of ASTM Standards, Vol 10.01. 6
Available from American National Standards Institute, 11 West 42nd Street,
3
Annual Book of ASTM Standards, Vol 09.01. 13th Floor, New York, NY 10036.

Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.

1
D 178 – 01e1
3.1.5.2 If electrical equipment and devices are insulated, or 5.1.2.1 A—Ozone resistance
isolated, or both, such that the multiphase exposure on a 5.1.2.2 B—Flame resistance
grounded wye circuit is removed, then the nominal design 5.1.2.3 C—Oil resistance
voltage may be considered as the phase-to-ground voltage on 5.1.3 The class designation shall be based on the electrical
that circuit. properties as shown in Table 2.
4. Significance and Use
6. Ordering Information
4.1 This specification covers the minimum electrical,
chemical, and physical properties guaranteed by the manufac- 6.1 Orders for matting under this specification should in-
turer and the detailed procedures by which such properties are clude the following information:
to be determined. The purchaser may at his option perform or 6.1.1 Type,
have performed any of these tests in order to verify the 6.1.2 Class,
guarantee. Claims for failure to meet the specification are 6.1.3 Thickness,
subject to verification by the manufacturer. 6.1.4 Width,
4.2 Rubber insulating matting is used for personal protec- 6.1.5 Length, and
tion; therefore when authorizing its use a margin of safety 6.1.6 Color.
should be allowed between the maximum voltage at which it is 6.2 The listing of types, classes, thicknesses, widths,
used and the proof-test voltage at which it is tested. The lengths, and colors is not intended to mean that all shall
relationship between proof-test and the maximum voltage at necessarily be available from manufacturers; it signifies only
which matting shall be used is shown in Table 1. that, if made, they shall conform to the details of this
4.3 Work practices vary from user to user, depending upon specification.
many factors. These may include, but are not limited to,
operating system voltages, construction design, work proce- 7. Manufacture and Marking
dures and techniques, weather conditions etc. Therefore, ex-
7.1 The matting shall consist of a rubber compound with a
cept for the restrictions set forth in this specification because of
smooth, corrugated, or diamond design on one surface and may
design limitations, the use and maintenance of this equipment
be backed with fabric, or may have one or more fabric inserts.
is beyond the scope of this specification
The back of the matting may be finished with cloth imprint or
4.3.1 It is common practice and the responsibility of the user
other slip-resistant material. Any such fabric insert shall not
of this type of protective equipment to prepare complete
affect adversely the dielectric characteristics of the matting.
instructions and regulations to govern the correct and safe use
of such equipment. 7.2 Each piece of matting shall be marked clearly and
permanently at a maximum interval of 1 m (3 ft) with the name
5. Classification of the manufacturer or supplier, ASTM D178, type, and class.
5.1 Matting covered under this specification shall be desig-
nated as Type I or Type II; Class 0, Class 1, Class 2, Class 3, 8. Dimensions and Permissible Variations
or Class 4. 8.1 Width—Standard widths shall be 610 6 13 mm (24.0 6
5.1.1 Type I, made of any elastomer or combination of 0.5 in.), 760 6 13 mm (30.0 6 0.5 in.), 914 6 25 mm (36 6
elastomer compounds, properly vulcanized. 1 in.) and 12206 25 mm (48 6 1 in.).
5.1.2 Type II, made of any elastomer or combination of 8.2 Thickness—The thickness of the matting shall be as
elastomeric compounds with one or more of the following specified in Table 3. Measurements shall be made over the
special properties: corrugations or diamonds. The corrugations shall be not more
than 3.2 mm (0.125 in.) deep. The diamonds shall not be higher
TABLE 1 Proof Test/Use Voltage Relationship than 1.6 mm (0.062 in.).
NOTE 1—The ac voltage (rms) classification of the protective equip-
ment designates the maximum nominal design voltage of the energized 9. Workmanship and Finish
system that may be safely worked. The nominal design voltage is equal to: 9.1 The matting shall be free of harmful physical irregulari-
a. The phase to phase on multiphase circuits or ties, which can be detected by thorough test or inspection.
b. The phase to ground voltage on single phase grounded circuits.
9.1.1 Nonharmful Irregularities—Surface irregularities may
Nominal Maximum
Class of Insulat- Use Voltage A AC Proof-Test Volt- DC Proof-Test Volt-
be present on all rubber matting due to imperfections in molds
ing Matting Phase-Phase age, rms V age, avg, V and inherent difficulties in the manufacturing processes. These
ac rms, max irregularities may appear as indentations, protuberances, or
0 1 000 5 000 20 000 imbedded foreign material that are acceptable provided that:
1 7 500 10 000 40 000
2 17 000 20 000 50 000
9.1.1.1 The indentation or protuberance tends to blend into
3 26 500 30 000 60 000 a smooth slope upon stretching of the material.
4 36 000 40 000 70 000 9.1.1.2 The rubber thickness at any irregularity conforms to
A
Except for Class O equipment, the maximum use voltage is based on the the thickness requirements.
following formula:
Maximum use voltage (maximum nominal design voltage) 0.95 ac proof-test 9.1.1.3 Foreign material remains in place when the matting
voltage − 2000 is bent and stretches equally with the material surrounding it.

2
D 178 – 01e1
TABLE 2 Electrical Test Requirements
AC DCA
Proof Test Proof Test Dielectric Test
Class Electrode Clearances, min B Dielectric Test Voltage Electrode Clearances, min B
Voltage Voltage Voltage
mm in. rms V rms V mm in. avg V avg V
0 76 3 5 000 6 000 76 3 20 000 35 000
1 76 3 10 000 20 000 76 3 40 000 60 000
2 127 5 20 000 30 000 152 6 50 000 70 000
3 178 7 30 000 40 000 203 8 60 000 80 000
4 178 10 40 000 50 000 305 12 70 000 90 000
A
DC proof-test, voltages were determined using negative polarity.
B
These nominal clearances are intended to avoid flashover and may be increased by no more than 2 in. (51 mm) when required by change in atmospheric conditions
from the standard of 100 kPa (1 atm) barometric pressure and average humidity conditions. These clearances may be decreased if atmospheric conditions permit.

TABLE 3 Thickness Measurements 12. Guarantee


Thickness Tolerance
Class 12.1 The manufacturer or supplier shall replace, without
mm in. mm in. charge to the purchaser, unused matting which, at any time
0 3.2 0.13 0.8 0.03 within a period of nine (9) months from date of initial delivery
1 4.8 0.19 0.8 0.03
2 6.4 0.25 0.8 0.03
of shipment to the purchaser or his designee, fail to pass the
3 9.5 0.38 1.2 0.05 tests in this specification. This guarantee will be binding on the
4 12.7 0.50 1.2 0.05 manufacturer or supplier only if the matting has been properly
stored and has not been subjected to more than an original
acceptance test and one retest.
12.2 Any acceptance test made by the purchaser, or the
10. Chemical and Physical Requirements purchaser’s designee, shall be performed within the first two
10.1 Insulating matting shall conform to the physical re- (2) months of the guarantee period unless otherwise specified.
quirements in Table 4. For Type II matting, flame or oil
NOTE 3—Proper storage means that the matting is stored without
resistance can be determined by conducting the tests in 19.2.5
distortion, and not stored directly above or in proximity to steam pipes,
or 19.2.6, respectively. radiators, or other sources of artificial heat, or exposed to direct sunlight
or sources of ozone. It is desirable that the ambient storage temperature
11. Electrical Requirements shall not exceed 35°C (95°F).
11.1 The entire length of each roll of matting when new
13. Sampling
(unused) shall withstand the 60-Hz ac proof-test voltage (rms
value) or the dc proof-test voltage (average value) specified in 13.1 Each roll of matting in a lot or shipment shall be
Table 2. The test voltage shall be applied continuously for 1 subject to inspection and test by the manufacturer including
min. electrical proof test to levels required in Table 2 of this
11.2 The matting material when tested between 50-mm specification.
(2-in.) disk electrodes with edges rounded to a radius of 6 mm 13.2 An original sample of sufficient material shall be cut
(0.25 in.), shall show a 60-Hz dielectric strength of not less from the end of a roll or rolls selected from the lot for the test
than the requirements shown in Table 2 for the thickness of requirements of Section 10, 11.2, and 11.3. A lot is defined as
each individual specimen. that quantity of material produced by a common manufacturing
11.3 The Type IIA matting material shall show no visible process during a consecutive time period not to exceed 24 h. If
effects from ozone when tested in accordance with 18.6.1, or failure occurs in the first sample, a second sample of the same
18.6.2. In case of dispute, Method A of the ozone resistance test quantity shall be selected and tested.
shall be the referee test.
14. Rejection
14.1 Individual rolls shall be rejected if they fail to meet the
TABLE 4 Physical Requirements manufacturing and marking requirements of Section 7, the
Type I Type II electrical requirements of 11.1, the width requirements of 8.1,
Tensile strength, min, MPa (psi) 4.83 (700) 4.83 (700) the minimum thickness requirements of 8.2, or the workman-
Tension set, max, at 150 % elongation, 12.7 (0.50) 12.7 (0.50)
51-mm (2-in.) bench mark, mm (in.)
ship requirements of Section 9.
Elongation, min, % 250 250 14.2 The entire lot or shipment of matting shall be rejected
Moisture absorption, max in-crease A, 11⁄2 3 under any of the following conditions:
%
Flame resistance, Type IIB not applicable 12.7 mm (0.5 in.) 14.2.1 If 5 % or more, but not less than two rolls of the
after 30 s matting, in a shipment fail to meet the requirements of 11.1.
Oil resistance, max, volume increase, not applicable 4
Type IIC B 14.2.2 If two dielectric breakdowns that do not meet the
A
Distilled water—23°C (75°F). dielectric strength value specified in 11.2 occur in five tests on
B
ASTM Oil No. 2 room temperature for 24 h. the specimen.

3
D 178 – 01e1
14.2.3 If one dielectric breakdown of five tests on the 17.1.3 Electrical proof test in accordance with the appropri-
original and one or more dielectric breakdowns of five tests on ate paragraphs of Section 18.
an additional specimen fail to meet the dielectric strength value 17.1.4 Breakdown voltage test in accordance with the ap-
specified in 11.2. propriate paragraphs of Section 18.
14.2.4 If the sample specimens of Type IIA matting, using 17.1.5 Ozone resistance tests in accordance with the appro-
the sampling methods and criteria specified in 18.6.1 or 18.6.2, priate paragraphs of Section 18.
fail to meet the ozone resistance requirements of 11.3. 17.1.6 Chemical and physical property tests in accordance
14.2.5 If the sample specimens of Type IIB matting using with Section 19.
the sampling methods and criteria specified in 19.2.5, fail to
meet the flame-resistant requirements of 10.1. 18. Electrical Tests
14.2.6 If the sample specimens of Type IIC matting using
18.1 Conditioning—Prior to testing, the matting shall be
the sampling methods and criteria specified in 19.2.6 fail to
made in a flat position.
meet the oil resistance requirements of 10.1.
14.3 The testing shall be terminated and the manufacturer or NOTE 4—Both ac and dc proof-test methods are included in this section.
supplier notified if, during the course of testing, 5 % or more, It is intended that one method be selected for the electrical acceptance
but not less than two rolls, of the matting in a lot or shipment, tests. The method selected shall be at the option of the purchaser, and the
supplier should be so notified of the selection.
fail to meet the requirements of 11.1, 11.2, or 11.3 as
determined by the rejection criteria of 14.1, 14.2, 14.2.1, 18.2 Warning: It is recommended that the test apparatus be
14.2.2, 14.2.3, 14.2.4, 14.2.5, or 14.2.6. The manufacturer or designed to afford the operator full protection in the perfor-
supplier may in such a case require the purchaser to submit mance of his duties. Reliable means of de-energizing and
proof that the test procedure and equipment conform to the grounding the high-voltage circuit should be provided. It is
appropriate paragraphs of Section 18. When such proof has particularly important to incorporate a positive means of
been furnished, the manufacturer or supplier may request that grounding the high-voltage section of dc test apparatus due to
his representative witness the testing of additional rolls from the likely presence of high-voltage capacitance charges at the
the shipment. conclusion of the test.
14.4 The entire lot or shipment of matting may be rejected 18.3 AC Proof Test:
at the option of the purchaser if two of the five specimens 18.3.1 Electrodes—Where electrodes are to be employed as
tested fail any of the separate requirements outlined in Section part of the test apparatus, they shall be of such design so as to
10. apply the electrical stress uniformly over the test area without
14.5 The entire lot or shipment of matting may be rejected producing corona at any point, or mechanical strain in the
at the option of the purchaser if 25 % of the matting in the lot material. The electrodes used in proof tests shall be of such
or shipment fail to meet the requirements of Section 8 or 9. dimensions that the flashover clearances specified in Table 2
14.6 All rejected material shall be returned unaltered except are not exceeded. A satisfactory procedure for ac proof testing
as required for sampling, as directed by the manufacturer at his utilizes electrodes that will provide intimate contact without
or the supplier’s request. However, those mats punctured when undue pressure.
tested in accordance with 11.1 or 11.2 shall be stamped,
punched, or cut prior to being returned to the supplier to NOTE 5—Rectangular metal sheets approximately 3 mm (0.06 in.)
thick, having smoothly rounded edges and corners, have been found to be
indicate that they are unfit for electrical use. satisfactory for this purpose. Also satisfactory are wet felt or sponge-top
electrodes.
15. Packaging
15.1 Matting shall be packaged either flat or in rolls and 18.3.2 Voltage Supply and Regulation:
shall not be distorted mechanically. 18.3.2.1 The test equipment used in both the proof-test
voltage and dielectric breakdown voltage tests shall be capable
16. Thickness Measurements of supplying an essentially stepless and continuously variable
16.1 Thickness measurements should be made on complete voltage to the test specimen. Motor-driven regulating equip-
matting samples with a caliper graduated to within 0.03 mm ment is convenient and tends to provide uniform rate-of-rise to
(0.001 in.). At least five thickness measurements shall be made the test voltage. The test apparatus should be protected by an
at selected points uniformly distributed over the test area of the automatic circuit-breaking device designed to open promptly
matting. on the current produced by breakdown of a specimen under
test. This circuit breaking device should be designed to protect
TEST METHODS the test equipment under any conditions of short circuit.
18.3.2.2 The desired test voltage may be obtained most
17. Sequence of Testing readily from a step-up transformer energized from a variable
17.1 The following order of procedure is suggested for low-voltage source. The transformer and its control equipment
testing rubber insulating matting. shall be of such size and design that, with the test specimen in
17.1.1 Inspection of the surfaces in accordance with Section the circuit, the crest factor (ratio of maximum to mean
9. effective) of the test voltage shall differ by not more than 5 %
17.1.2 The dimensions in accordance with Sections 8 and from that of a sinusoidal wave over the upper half of the range
16. of test voltage.

4
D 178 – 01e1
18.3.2.3 The accuracy of the voltage-measuring circuit shall 18.6.1 Method A—The ozone resistance test shall be made
be within 6 2 % of full scale. The correct rms value of the in accordance with Procedure A of Test Method D 518. Cut the
actual sinusoidal voltage wave-form applied to the matting specimen to a 10 by 100-mm (0.5 by 4-in.) rectangular size. A
may be measured by one of the following methods: (1) a temperature of 40°C (104°F) shall be maintained. Procedure A
voltmeter used in conjunction with a calibrated instrument shall be followed using a 20 % extension. The ozone concen-
transformer connected directly across the high-voltage circuit, tration shall be maintained at 500 6 50 mm3/m3(50 6 5 pphm)
(2) a calibrated electrostatic voltmeter connected directly by volume for a 3-h test period. Type II matting shall show no
across the high-voltage circuit, or (3) an ac meter connected in effect from ozone exposure during this test period.
series with appropriate high-voltage type resistors directly 18.6.2 Method B—The ozone resistance test shall be made
across the high-voltage circuit. on a 100 by 150-mm (4 by 6-in.) specimen of the matting
18.3.2.4 The crest factor may be checked by the use of a material prepared from a sample suitably conditioned by lying
peak-reading voltmeter connected directly across the high- flat for 24 h. The specimen should be draped over a 25-mm
voltage circuit. If an electrostatic voltmeter or an rms voltmeter (1-in.) diameter metal tube of sufficient length to completely
in conjunction with an instrument potential transformer is underlie the specimen, while possessing additional length for
connected across the high-voltage circuit, a standard sphere the required mounting support. The metal tubing is electrically
gap may be sparked over and the corresponding voltage grounded. The free ends of the specimen shall be clamped
compared with the reading of the rms voltmeter. beneath the tubing electrode so that an intimate contact is
18.3.3 Test—The proof-test voltage shall be initially applied established between the specimen and the tubing along the
at a low value and then gradually increased at a constant upper half of the cylindrically-shaped electrode surface. A
rate-of-rise of approximately 1000 V/s ac until the prescribed piece of flat aluminum sheet foil, approximately 50 by 100 mm
test voltage level is reached, or failure occurs. The test period (2 by 4 in.), shall be placed over the draped specimen so as to
starts at the instant that the prescribed testing voltage is provide adequate separation distance to prevent flashover
reached. Reduce the applied voltage to at least half value, between the foil and the metal tubing. An electrode wire shall
unless an electrical puncture has already occurred, at the end of be connected to the aluminum foil.
the test period before opening the test circuit. 18.6.2.1 The outer electrode (metal foil) shall be energized
18.4 DC Proof Test: to approximately 15 kV ac (rms) from a stable 60-Hz source.
18.4.1 Electrodes—The dc proof-test may be made with dry The 15 kV potential may be derived from a suitably rated
electrodes that consist of two flat metallic plates, at least one of potential transformer energized from its low-voltage winding
which is sized so that the flashover distances recommended in through a continuously variable autotransformer. An overcur-
Table 2 are not exceeded. The edges of these plates should be rent protective device should be incorporated into the low-
rounded so as to eliminate sharp nicks and protuberances. voltage control circuit in case of an electrical breakdown.
18.4.2 Voltage Supply and Regulation: 18.6.2.2 The ozone resistance of the specimen should be
determined qualitatively, by inspection, after a 1-h exposure
18.4.2.1 The dc proof-test voltage shall be obtained from a
period in the test apparatus at the 15 kV potential. Any visible
dc source capable of supplying the required voltage. The
signs of ozone deterioration of the matting material such as
peak-to-peak ac ripple component of the dc proof-test voltage
checking, cracking, breaks, pitting, etc., shall be considered as
shall not exceed 2 % of the average voltage value under
evidence of failure to meet the requirements of Type IIA
no-load conditions.
matting. At least two specimens from each sample of matting
18.4.2.2 The dc proof-test voltage shall be measured by a selected in accordance with 12.2 shall be tested. Two speci-
method that provides the average value of the voltage applied mens should not be taken from the same section of the sample
to the matting. It is recommended that the voltage be measured matting.
by the use of a dc meter connected in series with appropriate
high-voltage type resistors across the high-voltage circuit. An NOTE 6—The rate of ozone degradation by use of Method B is
electrostatic voltmeter of proper range may be used in place of inversely proportional to the relative humidity of the surrounding air.
Empirical data indicate, however, that visible ozone effects will be evident
the dc meter-resistor combination. The accuracy of the voltage
over a broad range of ambient humidities under these test conditions.
measuring circuit shall be within 62 % of full scale.
18.4.3 Procedure—The procedure shall be the same as the 19. Chemical and Physical Tests
ac proof test, except that the rate-of-rise shall be approximately 19.1 Chemical Tests—The composition of the rubber hydro-
3000 V/s dc. carbon portion of Type I matting may be determined using the
18.5 Dielectric Breakdown Test—The dielectric breakdown test methods in Test Methods D 297, or the manufacturer’s
test shall be performed in accordance with Test Method D 149. formulation processes may be certified by appropriate person-
The voltage should be applied at the rate of 3000 V/s under the nel.
short-time procedure. The specimen shall be representative of 19.2 Physical Tests:
the matting material to be tested. Sufficient material shall be 19.2.1 Physical tests should be performed to determine the
available to permit making five tests. physical requirements specified in Section 8. The matting
18.6 Ozone Resistance Test—The ozone resistance test shall samples should be conditioned by storing in a flat position for
be made in accordance with one of the following methods to 24 h at room temperature.
ensure conformance of Type IIA matting with the requirements 19.2.2 The tensile strength, elongation, and tension set tests
of 11.3: shall be performed in accordance with Test Methods D 412.

5
D 178 – 01e1
The tensile strength and elongation specimens shall conform in maximum limits conforming to the requirements of classifica-
dimensions to Die C. The tensile set specimens shall conform tion SE (Self-Extinguishing).
to Die B. The elongation in the tensile set shall be as specified 19.2.6 The oil resistance tests called for in Type IIC shall be
in Table 4. performed in accordance with Test Method D 471.
19.2.3 The moisture absorption tests shall be performed in
accordance with Test Method D 570, using the 24-h immersion 20. Precision and Bias
procedure at a temperature of 23°C (75°F).
19.2.4 The accelerated aging tests shall be performed in 20.1 No statement is made about either the precision or the
accordance with Test Method D 573. After being subjected to bias of the test methods in this standard for measuring the
a temperature of 70 6 1°C (158 6 2°F) in circulating air for 7 dielectric strength since the results merely state whether there
days, the tensile strength of the specimen shall not be less than is conformance to the criteria for success specified in the
50 % of the original. procedure.
19.2.5 The flame resistance tests called for in Type IIB shall
be performed in accordance with Test Method D 1692, with the

APPENDIX

(Nonmandatory Information)

X1. TEST METHOD FOR RATE, EXTENT, OR TIME, OR A COMBINATION THEREOF, OF BURNING OF CELLULAR
PLASTICS USING A SPECIMEN SUPPORTED BY A HORIZONTAL SCREEN

X1.1 Scope D 2406 Methods of Testing Flexible Cellular Materials


X1.1.1 This test method covers a small-scale horizontal Molded Urethane Foam9
laboratory screening procedure for measuring the rate, extent, D 3014 Test Method for Flame Height, Time of Burning,
or time, or a combination thereof, of burning of rigid or flexible and Loss of Mass of Rigid Thermoset Cellular Plastics in
cellular plastics in accordance with this test procedure. a Vertical Position10
X1.1.2 Materials that exhibit pronounced shrinking, curling,
X1.3 Significance and Use
or melting away upon heating cannot be evaluated by this test
method. X1.3.1 Tests made on a cellular plastic under conditions
X1.1.3 This test method is not applicable to materials that herein prescribed can be of considerable value in comparing
cannot be ignited under the conditions of this test, or to the rate of burning and/or extent and time of burning of
materials that exhibit progressive combustion without flame different materials, in controlling manufacturing processes, or
(continued glowing or charring). as a measure of deterioration or change in burning character-
istics prior to or during use.
NOTE X1.1—The rate of burning or extent of burning of rigid cellular X1.3.2 This test method is not intended to be a criterion for
plastics also may be determined by Test Method D 3014 where the
fire hazard. The fire hazard created by materials depends upon
specimen is supported vertically.
NOTE X1.2—Caution: During the course of combustion, gases or the form and end use of the material. Assessment of fire hazard
vapors, are evolved that may be hazardous to personnel. Adequate includes, but is not limited to, many factors, such as, ease of
precautions should be taken to protect the operator. ignition, burning rate, flame spread, fuel contribution, intensity
X1.1.4 This standard does not purport to address all of the of burning, and products of combustion.
safety concerns, if any, associated with its use. It is the X1.4 Apparatus
responsibility of the user of this standard to establish appro-
priate safety and health practices and determine the applica- X1.4.1 Test Chamber—Any enclosure is satisfactory that is
bility of regulatory limitations prior to use. large enough to provide quiet, draft-free air surrounding the
specimen during the test, yet will permit normal thermal
X1.2 Referenced Documents circulation of air past the specimen during burning. A hood is
recommended in order to remove the sometimes noxious
X1.2.1 ASTM Standards:
products of combustion. If a test chamber is used. It should be
D 1564 Testing Flexible Cellular Materials—Slab Urethane
of such a design that it can be used in a hood. For referee
Insulating Oils7
purposes, test results with the chamber should be the same
D 1565 Specification for Flexible Cellular Materials—
whether or not the hood exhaust is on. In cases of discrepancy,
Vinyl Chloride Polymers and Copolymers (Open-Cell
values obtained with the damper closed or the hood fan off, or
Foam)8
both, will be considered valid.

7 9
Discontinued 1979; Replaced by D 3574. Discontinued 1980; Replaced by D 3574.
8 10
Discontinued 1998; See Annual Book of ASTM Standards, Vol 08.01. Annual Book of ASTM Standards, Vol 08.02.

6
D 178 – 01e1
X1.4.1.1 The recommended test chamber should be con-
structed of sheet metal or other fire-resistant material, having
inside dimensions 300 mm wide, 600 mm long, and 760 mm
high, open at the top, with a ventilating opening approximately
25 mm high around the bottom. A viewing window of
heat-resistant glass should be of sufficient size and in such a
position that the entire length of the specimen under test may
be observed. The chamber should be opened readily and closed
to facilitate mounting and ignition of the test specimen.
X1.4.2 Burner—A standard 9.5 6 0.5-mm outside diameter
barrel bunsen or Tirrill burner fitted with a 48 6 1-mm width
wing top.
NOTE X1.3—The wing top may have to be opened to approximately 3
6 0.1 mm to provide the flame required in X1.6.4.
X1.4.3 Fuel Supply—Propane gas of at least 85 % purity.
X1.4.4 Specimen Support—Wire cloth (wire screen)11
6.5-mm mesh using 0.8-mm diameter steel wire. The wire
cloth specimen support 75 by 215 mm shall have a 15 6 1 mm
of length bent to form a right angle. This will form the
specimen support as shown in Fig. X1.1 and Fig. X1.2.
X1.4.5 Specimen Support Holders—Any holding device
that will clamp the wire cloth specimen support horizontally so
that the bottom of the bent-up portion is 13 6 1-mm above the
FIG. X1.2 Relative Position of Burner Wing Top, Flame,
top of the burner wing top, as shown in Fig. X1.1. A typical Specimen, and Specimen Support
arrangement consists of two laboratory ring stands with two
adjustable flat-surface clamps, which may be locked in place
by set screw and lock nut. See Fig. X1.2 and Fig. X1.3. X1.5 Test Specimen
X1.4.6 Sheet of Asbestos Board, 250 by 250 by 6.5 mm shall
be placed on the bottom of the test chamber. X1.5.1 Five specimens 50 6 0.25 mm wide by 1506 1 mm
X1.4.7 Aluminum Foil. long are needed.
X1.4.8 Timing Device, accurate to 6 1 s. X1.5.1.1 Specimens shall be cut from representative mate-
X1.4.9 Measuring Scale, graduated in at least 2.0-mm rial. Materials supplied in thicknesses over 13 mm shall be cut
intervals. to 13 mm thickness. Materials formed in thicknesses of 13 mm
X1.4.10 A device to ensure correct relative positioning of or less shall be tested at the thickness supplied.
burner and specimen. X1.5.1.2 Materials with directional effects such as skin or
inserts shall be oriented so as to provide the most adverse
results.
X1.5.1.3 Sheet samples shall be cut from a thickness of
sheet normally supplied or molded to a desired thickness.
11
Stainless-steel wire cloth can be obtained from Cleveland Wire Cloth and Mfg. X1.5.1.4 Molded expanded or sponge materials not con-
Co., 3573 E. 78th Street, Cleveland, OH 44105. forming to the width requirements in X1.4.1 shall be tested as
agreed upon between manufacturer and purchaser.
X1.5.1.5 Each test specimen shall be marked across its
width by one line 125 mm from one end.

X1.6 Conditioning
X1.6.1 Specimens shall be conditioned prior to test for a
minimum of 24 h in an atmosphere having a temperature of 23
6 2°C and a relative humidity of 50 6 5 %. Tests shall be
made in this atmosphere or immediately after removal there-
from.

X1.7 Procedure
X1.7.1 Determine the density according to the proper test
method for the type of material being evaluated. The test can be
made in accordance with Test Methods D 1564, D 1565,
FIG. X1.1 Relative Position of Burner Wing Top, Specimen, and D 2406, or a test method agreed upon between the purchaser
Specimen Support and the seller.

7
D 178 – 01e1

FIG. X1.3 Apparatus for Support of Specimen

X1.7.2 Clamp the wire cloth specimen support horizontally seconds when the flame front reaches the gage mark; if this
so that the bottom of the wire cloth is 13 6 1 mm above the top does not occur, record the time in seconds for the flame to go
of the burner wing top as shown in Fig. X1.1. Cover the sheet out. If the flame goes out before reaching the gage mark, the
of asbestos board with a layer of aluminum foil and place it on extent of burning is equal to 125 mm minus the distance from
the bottom of the test chamber to catch any dripping or flaming the gage mark to the nearest evidence of the flame front, such
particles. The distance between the wire cloth and the foil shall as charring, along the upper surface of the specimen measured
be between 150 to 200 mm. Change the foil after each test, if to the nearest 2 mm. Note burning characteristics, such as
there is any debris on the surface from the previous determi- intumescence, melting, dripping, or smothering. Also record if
nation. Burn off any material remaining on the wire cloth from the dripping on the foil burns. In some cases, the burning may
the previous tests, or use a new wire cloth for each test. If a cease in the first 60 s. This is evident by the disappearance of
new wire cloth is not used for each test, the wire cloth should the yellow or characteristic flame.
be cool to the touch before being used. If dripping or melting
material fall into the wing top clean it before testing the next X1.8 Calculation
specimen. X1.8.1 If the flame front passes the gage mark in any one of
X1.7.3 Place the specimen on the support with one end the five specimens, the sample shall be judged as burning. The
touching the 15 mm bent-up portion of the support. The end of burning rate is calculated by the following equation:
the specimen nearest the gage mark should be away from the
A 5 B/C (X1.1)
bent-up end of the specimen support, so that the gage mark is
125 mm away from the bent-up end. See Fig. X1.1. where:
X1.7.4 Adjust the burner with the wing top to provide a blue A = burning rate, mm/s,
flame whose visible portion is 38 6 2 mm high with a clearly B = distance to gage mark 125 mm, and
defined inner cone 6.5 6 1.0 mm high. Place the burner under C = time for flame to reach gage mark, s.
the upturned end of the specimen support so that one edge of If only one specimen burns past the gage mark, its burning
the flame is in line with the upturned end of the wire cloth and rate shall be reported, otherwise the average of the specimens
the other edge of the flame extends into the front end of the that burn past the gage mark shall be reported.
specimen. See Fig. X1.2. X1.8.2 If the flame front does not reach the gage mark for
X1.7.5 Start the timing device when the flame is first all five specimens, average the burning time in seconds and
applied to the specimen. After 60 s, remove the burner at least average the distance burned in millimetres as measured on the
150 mm away from the test specimen. Record the time in top surface.

8
D 178 – 01e1
X1.9 Report X1.9.4 A description of burning characteristics, such as
X1.9.1 The report shall include the following information: melting, dripping, or intumescence and whether the dripping or
X1.9.1.1 A description of the material including the density, melting materials continued to burn on the aluminum foil.
the width and thickness, and any prior treatment or condition- X1.9.5 The caveat contained in X1.1.4 herein shall be
ing and the presence or absence of skin. If the specimen had incorporated in its entirety in the test report issued.
skins, the report shall include whether the skin surface was up
or down. X1.10 Precision and Bias
X1.9.2 Sample that burned to the gage mark, the burning X1.10.1 Interlaboratory round-robin testing12 has estab-
rate in millimetres/second. lished the precision for each part of the test as follows:
X1.9.3 For samples that did not burn to the gage mark, X1.10.2 Reproducibility—The standard deviation for inter-
report the average time of burning and the average extent of laboratory reproducibility is:
burning. For burning rates 60.08 mm/s
For ATB 68.5 s
Example: For AEB 69.9 mm
ATBXXa AEBXXmes
where:
ATB = average time of burning, and 12
Supporting data giving results of cooperative tests have been filed at ASTM
AEB = average extent of burning. Headquarters. Request RR-D20-1036.

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