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  • r5 Acril

    Загружено:

    james rodriguez
    10 просмотров6 страниц
    The document contains proton NMR spectral data from an experiment with the following parameters: - Solvent was CDCl3 - Temperature was 300.0 K - 8 scans were acquired - Chemical shifts are reported from 8.0 to -0.5 ppm - Peaks are observed between 7.3 to 2.1 ppm and 1.57 ppm

    Исходное описание:

    Nmr

    Оригинальное название

    r5_acril

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    © © All Rights Reserved

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    The document contains proton NMR spectral data from an experiment with the following parameters: - Solvent was CDCl3 - Temperature was 300.0 K - 8 scans were acquired - Chemical shifts are reported from 8.0 to -0.5 ppm - Peaks are observed between 7.3 to 2.1 ppm and 1.57 ppm

    Авторское право:

    © All Rights Reserved
    Скачайте в формате PDF, TXT или читайте онлайн в Scribd
    Отметить как неприемлемый контент
    10 просмотров6 страниц

    r5 Acril

    Загружено:

    james rodriguez
    The document contains proton NMR spectral data from an experiment with the following parameters: - Solvent was CDCl3 - Temperature was 300.0 K - 8 scans were acquired - Chemical shifts are reported from 8.0 to -0.5 ppm - Peaks are observed between 7.3 to 2.1 ppm and 1.57 ppm

    Авторское право:

    © All Rights Reserved
    Скачайте в формате PDF, TXT или читайте онлайн в Scribd
    Отметить как неприемлемый контент
    из 6

    7.

    31
    7.29
    7.23
    7.21
    7.19

    2.37
    2.36
    2.34
    2.34
    2.32
    2.31
    2.25
    2.19
    2.18
    2.17
    2.17
    2.16
    2.14
    2.13
    2.12
    2.11
    2.10
    2.10
    2.09
    2.08
    2.07
    1.57

    0.10
    Parameter Value

    1 Data File Name / / nmr400/ data/


    pasquale/ nmr/ AC R 5/ 1/
    fid
    2 Title AC R 5.1.fid
    AC R 5.1.fid
    3 Comment

    4 Origin UXNMR, Bruker


    Analytische Messtechnik
    GmbH
    5 Owner root
    6 Site

    7 Instrument spect
    8 Author

    9 Solvent CDCl3
    10 Temperature 300.0
    11 Pulse Sequence zg
    12 Experiment 1D
    13 Probe 5 mm Multinuclear inverse
    Z-grad Z8202/ 44

    14 Number of Scans 8
    15 Receiver Gain 90.5
    16 Relaxation Delay 10.0000
    17 Pulse Width 8.5000
    18 Presaturation
    Frequency
    19 Acquisition Time 3.6438
    20 Acquisition Date 2017-12-12T16:44:47
    21 Modification Date 2017-12-12T16:45:56
    22 Class

    23 Spectrometer 400.13
    Frequency
    24 Spectral Width 4496.4
    25 Lowest -415.3
    Frequency
    26 Nucleus 1H
    27 Acquired Size 16384
    28 Spectral Size 65536
    36.25

    3.00

    8.0 7.5 7.0 6.5 6.0 5.5 5.0 4.5 4.0 3.5 3.0 2.5 2.0 1.5 1.0 0.5 0.0 -0.5
    f1 (ppm)
    7.30
    7.29
    7.24
    7.24
    7.21
    7.21
    7.19

    2.43
    2.38
    2.35
    2.33
    2.27
    2.24
    2.23
    2.18
    2.17
    2.16
    2.15
    2.12
    2.11
    2.09
    2.08
    2.06
    1.57

    0.10
    Parameter Value

    1 Data File Name / / nmr400/ data/


    pasquale/ nmr/ AC R 5/ 3/
    fid
    2 Title AC R 5.3.fid
    AC R 5.3.fid
    1H Disaccoppiato dal 31P 3 Comment 1H Disaccoppiato dal 31P
    4 Origin UXNMR, Bruker
    Analytische Messtechnik
    GmbH
    5 Owner root
    6 Site

    7 Instrument spect
    8 Author

    9 Solvent CDCl3
    10 Temperature 300.0
    11 Pulse Sequence zgdc
    12 Experiment 1D
    13 Probe 5 mm Multinuclear inverse
    Z-grad Z8202/ 44

    14 Number of Scans 32
    15 Receiver Gain 256.0
    16 Relaxation Delay 1.0000
    17 Pulse Width 8.5000
    18 Presaturation
    Frequency
    19 Acquisition Time 3.4079
    20 Acquisition Date 2017-12-12T16:52:06
    21 Modification Date 2017-12-12T16:54:03
    22 Class

    23 Spectrometer 400.13
    Frequency
    24 Spectral Width 4807.7
    25 Lowest -403.2
    Frequency
    26 Nucleus 1H
    27 Acquired Size 16384
    28 Spectral Size 65536
    1.00

    0.09

    8.0 7.5 7.0 6.5 6.0 5.5 5.0 4.5 4.0 3.5 3.0 2.5 2.0 1.5 1.0 0.5 0.0
    f1 (ppm)
    AC R 5.3.fid
    1H Disaccoppiato dal 31P

    AC R 5.1.fid

    8.0 7.5 7.0 6.5 6.0 5.5 5.0 4.5 4.0 3.5 3.0 2.5 2.0 1.5 1.0 0.5 0.0 -0.5
    f1 (ppm)
    AC R 5.3.fid
    1H Disaccoppiato dal 31P

    AC R 5.1.fid

    7.95 7.90 7.85 7.80 7.75 7.70 7.65 7.60 7.55 7.50 7.45 7.40 7.35 7.30 7.25 7.20 7.15 7.10 7.05 7.00 6.95 6.90
    f1 (ppm)
    AC R 5.3.fid
    1H Disaccoppiato dal 31P

    AC R 5.1.fid

    2.55 2.50 2.45 2.40 2.35 2.30 2.25 2.20 2.15 2.10 2.05 2.00 1.95 1.90
    f1 (ppm)
    Parameter Value
    31P Disaccoppiato

    41.93
    41.71

    39.86
    39.64

    29.69
    29.45
    29.10
    28.88

    18.38
    18.16
    17.38
    17.16
    1 Data File Name / / nmr400/ data/
    pasquale/ nmr/ AC R 5/
    2/ fid
    2 Title AC R 5.2.fid
    3 Comment 31P
    4 Origin UXNMR, Bruker
    Analytische
    Messtechnik GmbH
    5 Owner root
    6 Site

    7 Instrument spect
    8 Author

    9 Solvent Acetone
    10 Temperature 300.0
    11 Pulse zgdc
    Sequence
    12 Experiment 1D
    13 Probe 5 mm Multinuclear
    inverse Z-grad Z8202/
    44

    14 Number of 193
    Scans
    15 Receiver Gain 5160.6
    16 Relaxation 1.0000
    Delay
    17 Pulse Width 20.5000
    18 Presaturation
    Frequency
    19 Acquisition 0.1688
    Time
    20 Acquisition 2017-12-12T16:47:17
    Date
    21 Modification 2017-12-12T16:51:11
    Date
    22 Class

    23 Spectrometer 161.98
    Frequency
    24 Spectral Width 48543.7
    25 Lowest -24271.8
    Frequency
    26 Nucleus 31P
    27 Acquired Size 8192
    46 44 42 40 38 36 34 32 30 28 26 24 22 20 18 16 14 12 28 Spectral Size 16384
    f1 (ppm)

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