107207017 ‘Sirkand Float Separation Process
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ink and Float Separation Process
The Sink and Float Separation
Metallurgical Content
Process is an alternative to the staturgieat conten
progressive depletion, during the 0.1 Sink and Float PROCESS History and Development
last quarter century, of ores 0.2 QUIESCENT SEPARATION
which could be economically 0.3 SIZE OF ORE FEEDING A SINK & FLOAT SEPARATOR,
treated by the old methods of 0.4 Sink and Float Process DESCRIPTION
gravity concentration 0.4.1 OPERATING CIRCUITS
necessitated the development of 0.4.2 COMMERCIAL Sink and Float PLANTS:
0.5 Operating Cost of Sink & Float Plants
0.6 When is a Sink & Float Process Applicable or Appropriate
1 SINK FLOAT TEST PROCEDURE
more efficient methods of
concentration, the most
successful and widely used of
these methods being the
Flotation Process. But during the past few years millman have realized that there is still a place for
improved gravity concentration in a modern flowsheet, either in conjunction with flotation or alone.
This is the result of the commercial application of the more refined and accurately controlled
method of gravity concentration known as the Sink and Float Process.
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Sink and Float PROCESS History and Development
For many years there have been effected in laboratory work separations of ore particles of different
specific gravities through immersion of the mixed particles in a medium of a true heavy liquid with
a specific gravity intermediate between the specific gravities of the heavy and light particles to be
separated. The particles of Lower specific gravity float on the surface of the medium, while the
particles of higher specific gravity sink to the bottom. The two types of particles are removed
separately from the medium and a separation of particles achieved according to the individual
specific gravities. The principle hardly needs elaboration. Its application to ore dressing depends
upon the fact that the specific gravity of valuable minerals generally differs from the specific
gravity of the worthless gangue with which it is associated and from which substantial portions can
usually be freed by crushing
The earlier processes of this type employed suspension media which were of low kinetic stability;
that is to say, the solids of the media would rapidly settle out unless kept in suspension by some
form of agitation, In 1928 the deVooys Process was introduced for the separation of shale from
coal. This process employs as “medium” a practically stable suspension of barytes and clay in
water whose high kinetic stability makes it possible to dispense with stirring devices for
maintaining uniformity of suspension, Thus the separation takes place in a quiescent medium—a
most important point, since currents in the medium are bound to interfere to a greater or lesser
degree with the accuracy of the gravity separation taking place in the medium.
Since 1931, commercial deVooys plants have been installed capable of handling over millions
of tons annually. Utilizing the experience of their associated company with the deVooys plants for
coal, employing relatively low separating medium densities, Huntington, Heberlein & Company,
Ltd., Whitford, Holywell, North Wales, Great Britain, perfected the Sink and Float Process for higher
separating medium densities with the resultant broadening of the field to include other non-
metallic as well as metallic ores.
QUIESCENT SEPARATION
The speed at which the separation of the “sink” from the “float” particles takes place depends upon
the weight of individual particles and also on the difference in specific gravity between the
particles and the medium. Thus, the large or heavy particles sink fast, and separation of these from
float particles is easily achieved while the smaller particles, or those with a small gravity
differential from the medium, are not as readily separated. Comparatively large particles, viz., ¥-
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importance of quiescent conditions.
In practice the finer fractions of the ore are not subjected to Sink and Float treatment, as even
under the best conditions the rate of separation would be uneconomically slow. If there are
currents in the medium, this puts an even higher limit to the fine size of the ore which can be
5 4successfully separated.
The Sink and Float Process reduces medium currents to a minimum with the following benefits:
* Prevents interference with accuracy of separation by classifying effects.
* Reduces the fine size limit at which ore can be separated.
* Increases the recovery of particles of marginal density.
FIGURE I—H. H. SINK AND FLOAT SEPARATOR
DRAINAGE AND
WASHING SCREENS
Undue Medion
Te. Sepertor,
Die weston
"a Tochoner
SIZE OF ORE FEEDING A SINK & FLOAT SEPARATOR
In the case of the so-called “metallic” ores the density of the separating medium is adjusted so
that only those pieces of mineralized gangue float which carry a small particle of mineral. These
lightly mineralized gangue particles are mixed with a large proportion of barren gangue so that
the average assay of the float is not high. On the other hand, the heavily mineralized gangue pieces
are found in the sink product, which is not generally high enough grade to be a finished product
but is usually ground finer for further concentration. In operation the role of Sink and Float is to
reject a substantial proportion of the gangue as a worthless tailing of coarse size. These tailings
are usually of the same or of Lower grade than could be obtained by other processes, while the
costly operations of fine grinding and flotation are avoided for a large proportion of the ore. This
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the application to finer sizes is now being developed. The upper size limit depends upon the
degree of freedom of the mineral after crushing to various sizes; it is seldom above 1%-inch. Thus
ores are treated in the full size range from 1¥%-inch to 3/32-inch, without intermediate sizing
Heavy Media
Separation
Sink and Float Process DESCRIPTION
The separation achieved in the H. H. Sink and Float Process is obtained by using:
+ Apparatus which carries out its necessary function of removing separated products with a
minimum of disturbance of the medium.
+ Medium of high kinetic stability.
Apparatus: The apparatus used for the separation is shown above in Figure I. The ore is fed by
chute (1) into the separating vessel (2) which is mainly an inverted truncated pyramid. The top sides
are vertical and it is in the zone enclosed by these vertical sides that separation takes place. On top
of these vertical sides are four paddles (3), having horizontal shafts and each extending completely
across the separating zone. The paddle on the right in the figure is of smaller diameter than the
others and revolves about twice as fast; its function being to insure that all the ore feed is
completely immersed in the medium. The two center paddles are transporting paddles; they dip
slightly into the medium at the bottom of each revolution and move the float slowly across the
bath, The paddle on the Left in the figure is the float discharge paddle; it receives the float and
pushes it, together with a certain amount of medium, over the edge of the separator.
The bottom of the separating vessel is connected to the boot of the bucket elevator (4). The ore
which sinks below the paddles gradually falls to the boot of the elevator and is dredged up by the
buckets. The buckets are perforated and lift the ore a few feet above the medium level so that the
medium in the buckets drains out before the sink product is discharged from the buckets. In the
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stability can be achieved by fine grinding, but such a suspension could not be sufficiently fluid for
the ore particles to move freely in their separation, On the other hand, an excess of coarse particles
yields a high fluidity of the medium, but such a medium is not stable without a stirring device to
prevent settling out. In the H. H. Sink and Float Process optimum fluidity and stability are achieved
through control of size distribution of the medium particles and without any stirring or agitation of
54the medium.
Although the medium has high kinetic stability, there is naturally a tendency to settle out, for which
due compensation is provided. To counteract this incipient settling, a small flow of medium is
drawn over the weir (5) in the elevator casing. This flow is controlled by adjusting the weir height
and is held so that itis just sufficient to withdraw the medium which is beginning to settle out at
the bottom of the separator.
FIGURE II— ORE CIRCUIT FIGURE III— MEDIUM CIRCUIT
am
MEDIUM
+
INK.
REJECT PRopuct
water
i [Cigar tensiry tan]
ro waste ena WEAN? GENS TaN
Thus, medium is flowing out of the separator at two points, namely at the elevator weir and at the
float discharge. Medium is fed into the separator at a controlled rate equal to the two discharges;
one with the float reject and the other over the weir. The medium which is fed into the separator
consists of a mixture of these two flows of medium emerging from the separator. The medium is
actually slowly circulating, first into the separator, then out at two points and then back into the
separator. The rate of circulation equals the replacement of the entire contents of the separator in
20 to 40 minutes.
The high kinetic stability of the medium, combined with the stow withdrawal of medium from the
bottom of the separator, yields a small difference in density (in practice only 0.2) between the feed
medium and the medium at the bottom of the separator. This is an important factor as it prevents
an increase in medium density downward from separating zone to bottom of separator to a degree
sufficient to cause a piece of sink product, once separated near the top, to be prevented from
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Heavy Media Separation Process: Rocks are Floating
54,
OPERATING CIRCUITS
The foregoing has described the principles underlying the design and operation of the Sink and
Float Separator. The manner in which the plant is operated in practice is shown above. The ore
Circuit and the medium circuit are shown separately for clarity, though actually they Link up
together.
Ore Circuit: Figure I! illustrates the ore circuit. The ore, crushed to all pass 1%-inch, is fed at a
regular rate to the washing and sizing screen, where 3/32-inch ore and slime are removed. From
there the coarse ore goes to a slow-moving, inclined drainage conveyor, which removes surplus
water and also acts as a feeder to the separator (2). The separated float and sink products are
removed from the separator, as described above, to drainage and washing screens (6). On the
drainage screens the free medium is first drained off for return to the separator. Then the medium
adhering to the float and the sink is washed off on the washing screens, leaving the float ready for
rejection and the sink for any further processing that may be necessary.
Medium Circuit: The medium circuit is shown above in Figure ||. The medium of near operating
density, which drains from the first of the screens, is returned by an elevator to the separator. The
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to the medium elevator at the rate required to maintain the correct medium density in the operating
circuit.
There are two other operations necessary to maintain the medium in good condition. The medium
becomes contaminated with ore in a granular and ina slime condition, owing to the impossibility
540f completely freeing the original ore feed from these materials. The accumulation of these
S%**mnaterials in the medium causes deterioration of both stability and fluidity and they must be
removed. The granular portion is removed by means of a fine screen in the medium circuit. The finer
contaminant is removed by “bleeding off” a portion of the medium, cleaning it by flotation, and
returning the cleaned material to the circuit. The manner in which the medium is bled off and
returned to the circuit depends on what is most convenient for the particular operation—the
necessity is simply to maintain the operating medium ina sufficiently uncontaminated condition.
Often the washings are used as feed for a cleaning operation and the cleaned material is brought
to the necessary density either independently in a small filter or in the thickener.
The second operation is the provision of new make-up medium. This is required to compensate for
the small loss of medium left adhering to the products after final washing and for the need of
replacing worn medium. The loss on the products depends upon the nature of the ore, but is small.
A oss of only 0.1 lb. of medium per ton of product has been attained. The replacement of worn
medium is necessary periodically, but is not a loss. The necessary portion is extracted from the
Circuit in a high grade condition and is ready for sale at the full market price; an equivalent quantity
of newly prepared medium takes its place in the circuit.
The preparation of new medium consists of normal grinding and classification processes. The
grinding and classifying are carried out in such a manner that the necessary size distribution is
obtained in the material sent to the medium circuit.
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ro waste ‘eoua penne i i
WASHING. WATER cone 4
= oe come
conor
an
y
3A > a eno
1
0
WATER t
as
He
\ TARE AT
See.
‘a ' f
Ki | umes ib
T : = A macner.
ees
or BLOCKS,
\ rl '
eae, i
seas |
nae veavveon omar =
is hoisted into cone containing heavy liquid. Concentrate.
in suspension is recovered! by magnetism. Below left, ore
fed to the conveyor belt as tunnel grows
In American Cyanomid’s Heavy-Media process,
floats off top, waste sinks, or vie
and waste move across par
COMMERCIAL Sink and Float PLANTS
At least 4 commercial H. H. Sink and Float plants, had a capacity to treat more than 1,000,000
tons annually, have been constructed:
1. Halkyn United District Mines, Ltd., North Wales, Great Britain
2. Miniere Cave di Predil, Raibl, Italy
3. Central European Mines, Mezica, Jugo-Slavia
4, Bunker Hill and Sullivan Mining and Concentrating Company, Kellogg, Idaho
Today, the Nystar East Tennessee plant runs at 2,000,000 or so TPY.
Two more plants are under construction in the United States with a combined capacity of a further
1,500,000 tons annually.
As for example, the H. H. Sink and Float unit installed by Bunker Hill was designed to handle 1,700
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testing, of which the following is a typical result:
Weight Assay Distribution
% Pb % Pb
Float 573 0.4 06 3.3
Sink 42.7 15.8 6.0 96.7
Feed 100.0 7.0 2.9 100.0
Recent results for a month's operation of the commercial plant show:
Weight Assay Distribution
%Pb%Zn Ph Zn
Float 51.2 0.42 0.62 3.41 9.07
Sink 488 1245 652 96.59 90.93
Feed 100.0 6.29 3.50 100.00 100.00
The Sink and Float separator at Bunker Hill receives about 70 percent of the mine ore of sizes
ranging from 1%-inch to 1/8-inch. It rejects as unneconomic coarse waste about 50 percent of the
separator feed, or in other words, about 35 percent of the whole mine output. The remaining 65
percent of the mine ore, made up of 30 percent fines and 35 percent sink product, is further
crushed, ground and concentrated in the mill proper.
On the basis of a mill handling 1,000 tons daily before the installation of Sink and Float, it is
possible to handle 1,500 tons of mine ore with Sink and Float. After rejection of 500 tons as float
the unit returns 1,000 tons to the mill. In other words, the mill output is substantially increased
through the elimination of a sizeable portion of gangue from the mine ore before milling
The feed may contain some disseminated values. By raising or lowering the density of the
separating medium, more or less of these disseminated values appear in the float product. Thus
within limits the tailing assay from the Sink and Float operation can be raised or Lowered ina
controlled manner with, of course, an increase or decrease respectively in the proportion of such
tailings produced, The alteration in the proportion of Sink and Float tailings affects the subsequent
milling capacity and costs. Its therefore possible to control the medium density in the Sink and
Float operation to give the best economic balance between tailing assay and total milling costs
Operating Cost of Sink & Float Plants
Labor: For operating the separator, together with the medium circuit, two operators per shift are
usually required for either a large or small plant.
Power: Power consumption varies with the size of the plant. For a 1,500 to 2,000 tons per day
plant the consumption is 0.7 kwh per ton of mine ore.
Water: Consumption of water is extremely low. The only loss of water, aside from climatic
evaporation, is the water carried away as moisture adhering to the products leaving the plant-This
can be reduced to less than 10 gallons per ton of ore treated.
The water used in washing medium off the sink and float products is recovered as thickener
overflow. This is sufficient in amount for the primary washing of the ore. Where the products of the
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percent solids, so that the introduction of the Sink and Float treatment does not lead to any
additional water consumption.
Maintenance: No heavy maintenance costs are incurred. The main items requiring replacement are
screen plates and sink elevator parts.
54
S%*'Capital Cost: The cost of an installation depends materially on its size and location, Under normal
conditions the cost of equipment, exclusive of installation and housing, would be from $15 to $35,
per ton of daily capacity depending on the size of the plant.
When is a Sink & Float Process Applicable or Appropriate
The process may be used for pre-treatment of certain ores, both metallic and non-metallic, with
the object of reducing over-all treatment costs, reducing over-all installation costs and increasing
ultimate mill capacity without large capital expenditures.
It may be used to permit cheaper, non-selective methods of mining, since wall rock and low grade
ore can be cheaply handled with good recoveries. It may be used for preliminary reclamation of
values in tailing dumps.
It may be used to make a salable product, in the case of some non-metallic ores, and where
necessary excessive treatment of refractory or friable metallic ores leads to heavy losses.
Sink and Float treatment is not confined to lead and zinc ores or to those ores suitable only for
jigging or tabling. Provided a substantial proportion of uneconomic gangue is freed at a coarse
size, it may be removed from the ore by Sink and Float treatment regardless of the subsequent
treatment necessary to free and recover the values.
SINK FLOAT TEST PROCEDURE
Sink float tests aid in the evaluation of products, identification of minerals and give approximate
separation of gangue minerals. Sink Float Concentration is used in mineral dressing laboratories
for:
1. Separation of samples into different specific gravities to aid in the identification of minerals.
2. Determining the separation which can be made between the heavier minerals and lighter gangue
minerals.
3. Evaluation of products by separating into sink and float fractions.
Sink-Float Tests are classed as bulk or selective separations. A bulk test gives two products, first,
the lighter minerals with a gravity less than 2.8 to 3.3 and, second, minerals having a gravity
heavier than 2.8 to 3.3. The separation depends on the gravity of the media used.
The heavy media generally used are as follows:
1. Acetylene Tetrabromide having a specific gravity of 2.964 at 20°C
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‘decanting ott the neavy Liquid.
Tests on fine sized products are made by using a separatory funnel. The sink product is the drawof,
A selective sink float separation can be made by removing the heaviest minerals as a sink product
and adding a sufficient amount of diluting media, such as carbon tetrachloride to acetylene
4tetrabromide, to give the desired lower gravity. This will allow the next heavier minerals to
slieseparate as a sink product. Recovery of the media for reuse may be by virtue of different boiling
points or miscibility in other liquids.
WEIGHED SAMPLE
WEIGHED SAMPLE ~I0 MESH MATERIAL
+10 MESH MATERIAL i
STIR
C7 Frost
LADLED OFF}
STIR
DECANT
SUPE RNATENT
LiguiD
REGOVER SINK PRODUCT
RECOVER SINK PRODUGT
Here below from the Popular Mechanics.
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54
“we I conveyor belt drops ore in Diesel trectortraier
ied wht oye fot meling exinest sowpebnece
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Oz YOU CANT operate Diesel trucks
underground,” the visiting engineer
argued. “Phe carbon monoxide fumes will
Keil every man in the mine.”
The visitor was deep in an Eagle-Picher
lead-zine mine in Oklahoma and had just
watched a big Dicacl tractor rumble by,
towing a 10-ton load of ore.
The mine's superintendent grinned,
“Usually that’s true,” he admitted, “only
those trucks don't give off carbon monox-
ide. There’s a constant chemical change in
the exhaust pipe, transforming the monox-
ide to carbon dioxide. We feed pure oxy-
gen into the exhaust from a tank on the
truck and the nonpoisonous gases that
come out of the pipe are swept away by
normal mine ventilation. The drivers and
miners work all day in perfect safety.
In European mines where adequate ven-
tilation exists or ean be created, air com-
pressors, bulldozers and hundreds of in-
Ponel control feeds on
into sabenety comrent
yon from tank under oor
Tome ete vie dhonibe:
POPULAR MECHANICS
wane.107207017
‘Sirkand Float Separation Process
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Fichest ores become exhausted.
doesn’t mean, says the mining industry,
that the United States is approaching the
status of a “have not” nation, in reserves.
‘Temporary shortages in such metals as
copper have been due to a high demand
plus rising extraction costs, factors that
eventually level themselves out.
‘The fact is that vast amounts of metallic
and nonmetallic minerals are still in the
ground, in many cases in quantities suffi-
Gient for our needs for centuries. Some of
these reserves, however, are in the form of
low-grade ores that cannot be worked
profitably by methods used in the past.
More efficient and safer ways of handling
the material underground and better ways
of concentrating and refining it. are being
developed,
‘The, exhaust purifier is one innovation
in underground tratfsport; another is
use of rubber conveyor belts for moving
ore from a working face through the tun:
nel system and up to the surface. The end-
less belts follow the configuration of seams,
can carry materials around sharp corners,
and can boost heavy loads up steep grades
to the surface.
One immense conveyor belt, half a mile
long, is being installed by Goodyear Tire
& Rubber Company in an Alabama coal
imine. It will raise 600 tons of coal per hour
to the surface from 715 feet underground,
perhaps the greatest climb ever attempted
by a conveyor belt.
Forty-two inches wide and weighing 42
tons, the belt is reinforced by 980 sicel
cables in its carcass in place of the usual
fabrie cords. Two 300-horsepower motors
rotate the belt, which will carry its load
up a slope of approximately 17 degrees.
‘Underground air conditioning is receiv-
ing considerable study as a safety measure
in gaseous or dusty mines and for greater
‘comfort. In some deep mines without air
conditioning, the constant temperature
Sands at 100 degrees or higher. ‘Tele:
phones are replacing pipe-rapping an
thor malceshife signaling methads and in
some mines electric eyes sound horns at
tunnel intersections to warn of the ap-
proach of ore trains.
Tungsten-earbide points on rock drills
are being adopted because they permit
faster drilling with fewer hit changes. Mine
timbers can be set by a new machine that
does the work of a gang of men, and push-
button elevators in some of the mines are
saving travel time as well as eliminating
hpe:wn9t metal largist.comblog/sinlot-seperation process.
116‘Sirkand Float Separation Process
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2S
\
practically all ladder climbing. In open-
cut operation on the surface, massive
pieces of equipment that take bigger bites
‘or handle bigger loads than ever are in use
An electric cable that won't spark when
short-cireuited may help prevent coal-
mine explosions, A fine:strand of copper
wire between two layers of insulation
catches any current “leaks” before an are
can occur. The wire carries current to a
circuit breaker which cuts off the power.
The flotation process that gleans the val-
uable ingredients from a wide range of
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New chemicals have been added for float-
ing minerals, other chemicals that assist
n depressing unwanted materials have
been found, and wetting agents such as
‘Aerosol are being employed to increase the
‘efficiency of the operation.
A development hailed as one of the most
Important since flotation eame into use is
the recent adaptation to big-seale opera
tions of the “sink float” concentrating
process, which is a method formerly used
aly in the laboratory
Sink-float process automatically sorts
the useless and lowest grade materials
from an ore, leaving s concentrate that ean
be milled ai minimum expense.
When coarse preliminary crushing of a
ore and the sinke-loat separation are per
formed underground, as is contemplated,
the cost of hoisting tons of useless material
to the surface, transporting it to the mill,
and running it through the mill will be
avoided entirely.
Tho sink-float process consists of passing
an ore through a bath composed of a heavy
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54
Source: This article is a reproduction of an excerpt of “In the Public Domain” documents held in
91.1 Metallurgy Corp's private library.
By David Michaud | June 9th, 2016 | Categories: Flowsheets & Flowcharts, Gravity Concentration | Tags: Dense Mecia Separation,
DMS, Heavy Media Separation, HMS | Comments Off
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