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Reinforcement of recycled PP fibre in concrete footpaths and precast panels was studied.
Post-cracking performance of fibre reinforced concrete was assessed by CMOD and RDPT.
Recycled PP fibre has good alkali resistance in concrete and other alkaline environments.
Recycled PP fibre shows comparable post-cracking reinforcement with virgin PP fibre.
a r t i c l e i n f o a b s t r a c t
Article history: Use of macro recycled plastic fibres in reinforcing concrete footpaths and precast panels offers significant
Received 1 July 2015 economic and environmental benefits over traditionally used virgin plastic fibres or steel fibre and mesh.
Received in revised form 3 March 2016 However, wide adoption of recycled plastic fibres by construction industries has not yet been seen due to
Accepted 25 March 2016
limited data available on their durability, mechanical properties and performance in concrete. This paper
reports findings from a laboratory study on the alkali resistance and performance of recycled polypropy-
lene (PP) fibres in the 25 MPa and 40 MPa concretes, used for footpaths and precast panels, respectively.
Keywords:
The recycled PP fibre was proven to have very good alkali resistance in the concrete and other alkaline
Recycled polypropylene fibre
Fibre reinforced concrete
environments. The recycled PP fibre showed excellent post-cracking performance in concrete, bringing
Mechanical properties in significant ductility. In the 40 MPa concrete the effectiveness of reinforcement of PP fibres depended
Post-cracking performance on their Young’s modulus and tensile strength in the crack mouth opening displacement (CMOD) test.
Since the recycled PP fibre was found to have lower tensile strength but higher Young’s modulus than
those of virgin PP fibre, the recycled PP fibre produced similar or slightly lower reinforcement than that
of virgin PP fibre. In the 25 MPa concrete, the Young’s modulus of fibres was more effective on their
reinforcement than the tensile strength, thus the recycled PP fibre produced better reinforcement than
that of virgin PP fibre.
Ó 2016 Elsevier Ltd. All rights reserved.
http://dx.doi.org/10.1016/j.conbuildmat.2016.03.162
0950-0618/Ó 2016 Elsevier Ltd. All rights reserved.
S. Yin et al. / Construction and Building Materials 114 (2016) 134–141 135
In order to promote development of concrete industry, recycled surface fibres, 0.8–0.9 mm in diameter, were then produced followed by indenta-
tion on the surface using an indenting roller die. After that, the fibres were winded,
plastic fibres have started attracting attention around the world
polywrapped and finally cut into a specific length. Both recycled and virgin PP fibres
[8]. Ochi et al. [1] and Fraternali et al. [9] produced recycled PET were produced by the same processes, thus having same geometry and dimensions
fibres though a serial processes of extrusion, spinning and stretch- (1.5 mm in width, 0.7 mm in thickness, and 47 mm in length), as shown in Fig. 1.
ing. The recycled PET fibres produced in both their studies Tests on recycled and virgin PP fibres for tensile strength and Young’s modulus
achieved a tensile strength of over 450 MPa. Kim et al. [10] and were carried out as per ASTM D3822-07 [17]. The tensile tests were undertaken
using United Calibration Corporation United STM ‘Smart’ Test Machine (STM-50
Kim et al. [11] produced recycled PET fibre by melting waste PET
KN) with a 2 kN load cell and a data acquisition software. 30 samples of each fibre
bottles first, then pressing and rolling them into roll-type sheets, type were tested at room temperature of 20 ± 2 °C. Gauge length of 25.4 mm was
before slitting the sheets into thin strands. The recycled PET fibres used with extension speed set at 60% of the gauge length/min (15.24 mm/min)
produced in this way had a tensile strength of more than 400 MPa for all the tests.
A brittle mode of failure can be seen in both types of fibres (Fig. 2), with a short
and a Young’s modulus of 10 GPa. de Oliveira and Castro-Gomes
elastic phase of steep slope and a progression of sharply rising stress until fracture.
[12] and Foti [5] produced recycled PET fibres by simply cutting Averages of the tensile strength and Young’s modulus are shown in Table 1 as well
waste PET bottles, but these fibres had limited strength. Although as the elongation at break and their standard deviations. As can be seen, the recy-
recycled PET fibres have recently become a focus of research, cled PP fibre shows lower tensile strength (284.1 MPa) but much higher Young’s
research on mechanical properties of recycled PP fibre and their modulus (4582 MPa) than those of virgin PP fibre. It is noteworthy that the recycle
PP fibre is not featured to have higher Young’s modulus than that of virgin PP fibre.
effectiveness as reinforcement in concrete is very limited.
The tensile properties of fibres mainly depend on the material properties and pro-
Effectiveness of the fibres in reinforcing concrete is generally cessing conditions. Our previous research [18] has shown that the recycled PP fibre
assessed through crack mouth opening displacement (CMOD) test has lower molecular weight and shorter molecular chains than those of virgin PP
and round determinate panel test (RDPT), which assess post- fibre. Under the same processing conditions, the shorter molecular chains make
the recycled PP fibre easier to be crystallised, thus producing higher Young’s mod-
cracking performance of fibre reinforced concrete. The CMOD test
ulus. The shorter molecular chains of recycle PP fibre have less molecular entangle-
is suitable for determining how the fibres control the cracks, as it ment and hence, producing lower tensile strength under the same processing
demonstrates an association between cracking behaviour and conditions with the virgin PP fibre. However, if the processing conditions or meth-
residual flexural strength. The CMOD test evaluates capacity of ods are changed, the properties of fibres will be changed, which is out of the scope
the fibres to bridge the cracks formed and redistribute the stresses of this paper.
[13]. The RDPT is also an effective method of assessing the perfor-
mance of fibre reinforced concrete. This test is desirable because 2.2. Concrete mix design
panels are subjected to a mixture of stress actions that more accu-
Based on industry practise, standard mix designs for 40 MPa and 25 MPa con-
rately reflect the in-situ behaviour of concrete than other labora- crete were used in this study (as shown in Table 2). For the 40 MPa concrete mix
tory based small-specimen mechanical tests. Significantly lower design, 0.67% in volume of PP fibres (6 kg/m3) were mixed with concrete, which
variability can be seen in the results of RDPT than that of other
tests and hence, the RDPT is considered one of the most reliable
test methods of post-cracking performance assessment [14].
Durability of plastic fibres in highly alkaline cement matrix is
another important factor that needs proper consideration. Brown
et al. [15] exposed virgin PP fibres to an ionic environment of
sodium and chloride ions created by salt water at 71 °C and
7 °C for six months, tensile properties of the PP fibres remained
unchanged. Elasto Plastic Concrete (EPC) Company [16] subjected
virgin PP fibres to an alkaline solution simulating alkaline environ-
ment of concrete mix. They reported that the PP fibres can last up
to 100 years in an alkaline environment without any reduction in
strength. While it is clearly demonstrated that the long-term dura-
bility is not a problem for the virgin PP fibres, the durability of
recycled PP fibres in the alkaline environment of concrete is still
unknown.
Fig. 1. Recycled (a) and virgin (b) PP fibres.
This research, therefore, assessed the alkali resistance of recy-
cled PP fibre in four different alkaline solutions to study degrada-
tion of the recycled PP fibre in different pH ranges and types. The
post-cracking performance of recycled PP fibre reinforced con-
cretes was also quantified and compared with that of virgin PP
fibre reinforced concretes through the CMOD test and RDPT. In this
study, two volume percentages of fibres were chosen to reinforce
40 MPa and 25 MPa concretes, which are the standard grades of
concrete used in precast panels and concrete footpaths, respec-
tively. The effectiveness of the recycled PP fibres as reinforcement
of the two different grades of concrete were assessed in this
research.
2. Materials properties
In this study the recycled PP fibres were produced by extruding, spinning and
stretching recycled PP granules, which were made of industrial PP waste (scrap
off-cuts and off-specification items in the manufacturing industry that are not used
by the consumer). Initial extrusion of the PP granules was carried out at 210–250 °C,
spinning and stretching at 140–170 °C, then stabilisation at 110–140 °C. Smooth Fig. 2. Typical stress-strain curves of PP fibres in tension.
136 S. Yin et al. / Construction and Building Materials 114 (2016) 134–141
Table 1
Mechanical properties of PP fibres.
PP compositions Tensile strength (MPa) Young’s Modulus (MPa) Elongation at break (%)
Average Standard deviation Average Standard deviation Average Standard deviation
Virgin PP Fibre 356.4 30.6 3129 564 12.6 2.8
Recycled PP Fibre 284.1 21.0 4582 1661 6.2 2.2
Table 2 on AS 1012.8.1:2014 [20], concrete beams, cylinders and round panel slabs were
Concrete mix proportions. removed from the moulds after 24 h. All specimens were then cured in water at
23 ± 2 °C for 28 days.
Material 40 MPa 25 MPa
Concrete Concrete
0.6–4.75 mm Coarse sand (kg/m3) 350 410 3. Alkali resistance of the recycled PP fibre
6.7–9.5 mm Concrete aggregate (kg/m3) 950 260
0.3–5 mm Crusher dust (kg/m3) 220 200
Alkali resistance test was conducted to study possible degrada-
0.075–0.3 mm Fine sand (kg/m3) 290 350
9.5–19 mm Concrete aggregate (kg/m3) – 690 tion of the recycled PP fibre in concrete alkaline environment. The
Fly ash (kg/m3) 130 134 recycled PP fibre was immersed into a Lawrence solution [0.48 g/l
Cement (kg/m3) 256 186 Ca(OH)2 + 3.45 g/l KOH + 0.88 g/l NaOH, pH = 12.9], which is con-
Polyheed 8190 admixture (ml/100 kg 337 281
sidered to simulate pore water composition of a fully hydrated
cementitious materials)
Air entrapment admixture (ml/100 kg – 22 cement paste [21]. The recycled PP fibre was also immersed in
cementitious materials) three other alkaline solutions with pH value ranging from 12.3 to
Water (l/m3) 105 116 13.5 to study degradation of the fibre in different pH ranges and
PP fibre (kg/m3) 6 4 types. These three alkaline solutions used were Ca(OH)2 saturated
solution (pH = 12.3), 0.068 mol/l KOH solution (pH = 12.83), and
0.28 mol/l NaOH solution (pH = 13.45). The recycled PP fibre was
is normal dosage of PP fibres for 40 MPa concrete construction of precast panels. For immersed into these four solutions for 28 days at ambient temper-
the 25 MPa concrete, 0.45% in volume of PP fibres (4 kg/m3) were mixed. This
design is commonly used to construct concrete footpaths. Delivery of concrete
ature. The tensile strength and Young’s modulus of recycled PP
was carried out in a standard concrete truck from a Holcim Australia Pty. Ltd. batch fibre were measured before and after immersion.
plant and without PP fibres. Average slump was 60 mm for the 40 MPa concrete and As can be seen from Fig. 3, all the curves representing fibre
100 mm for the 25 MPa concrete, based on AS 1012.3.1-2014 [19]. The PP fibres immersion in the alkaline solutions nearly overlap with the curves
were then mixed with concrete in a drum mixer before casting specimens. The
of fibre without immersion, indicating that the recycled PP fibre
fibres were gradually added to avoid clumping and ensure good dispersion. Based
has outstanding alkali resistance in the various alkaline environ-
ments. However, there still are some minor changes on the
mechanical properties after immersion. As shown in Table 3, the
NaOH solution slightly embrittles the recycled PP fibre, thus
decreasing the tensile strength and increasing the Young’s modu-
lus of fibre, due to its higher pH value. The KOH solution slightly
decreases the tensile strength of fibre. However, there is nearly
no change after immersing the fibre in the Lawrence solution
which simulates a fully hydrated cement paste. Overall, the recy-
cled PP fibre shows good alkali resistance in all the alkaline envi-
ronments tested.
Table 3
Mechanical properties of the recycled PP fibre before and after immersion in the alkaline solutions.
Fig. 6. Load-CMOD curves for (a) 0.67% PP fibre reinforced 40 MPa concrete, (b) 0.45% PP fibre reinforced 25 MPa concrete, and (c) 0.45% recycled PP fibre reinforced 25 MPa
and 40 MPa concrete.
Fig. 8. Residual flexural tensile strength of 0.67% fibre reinforced 40 MPa concrete and 0.45% fibre reinforced 25 MPa concrete beams at (a) CMOD1, (b) CMOD2, (c) CMOD3
and (d) CMOD4.
Fig. 9. Fracture surfaces of PP fibres reinforced concrete beams: (a) 0.67% recycled PP fibre, (b) 0.67% virgin PP fibre, (c) 0.45% recycled PP fibre, and (d) 0.45% virgin PP fibre.
140 S. Yin et al. / Construction and Building Materials 114 (2016) 134–141
Fig. 11. Energy absorption and load curves from Round Determinate Panel Tests: (a) 0.67% PP fibre reinforced 40 MPa concrete, and (b) 0.45% PP fibre reinforced 25 MPa
concrete.
S. Yin et al. / Construction and Building Materials 114 (2016) 134–141 141
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