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Abstract:
This is article addresses the effects of Al alloys by using different quenching media(water,
distilled water, brine, soybean oil, palm oil, cotton seed oil, olive oil, palm kernel oil, apple
juice, polymer quenching, clay and caster oil etc;) quenching time, quenching temperature
and mechanical properties like (Ultimate tensile strength, yield strength and hardness) and its
micro structure studies. By using different quenching media the micro structure is refined,
mechanical properties were improved at certain percentage of quenching media, quenching
temperature and quenching time not only Al alloys and other metals also. Ultimately the
property of fatigue is enriched with the refinement of micro structure.
Key words: Quenching media, quenching temperature, quenching time and micro structure.
I. INTRODUCTION:
Piston head is the most crucial components of an automobile engine. Lot of research work
was reported in the literature on the design of piston head, materials and manufacturing of
piston heads, temperature distribution over the surfaces of the piston head etc; A detailed
damage analysis of engine parts was also reported in the literature. The damage mechanism
includes, wear, temperature and fatigue failures. Extensive work was reported in the
literature on the wear and wear mechanism on pistons. However, there were only discrete
references in the literature on the fatigue strength analysis of piston heads. An attempt is
made in the proposed work to study fatigue strength analysis of piston heads and to optimize
the design of piston head from fatigue strength considerations. The two important fatigue
failures of piston heads are thermal fatigue failure either at room temperature or at elevated
temperatures and mechanical fatigue failure. The operating temperatures during working
stroke and the thermal fatigue failure are considered. The main focus was on determining
the mechanical properties of piston head material and the quenching process used to obtain
the required mechanical properties and micro structure.
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ISSN: 2278 – 7798
International Journal of Science, Engineering and Technology Research (IJSETR)
Volume 5, Issue 4, April 2016
M. Sakthivel et al.,(2013) did extensive work on Evaluation of EN8 steel in different quenching
medium.
They conducted experiment on EN8 MEDIUM Carbon steel using different quenching medium (oil,
water and air) in a gas carburizing furnace of heating temperature between 900 o C -9300 C. The
objectives of this experimentation was to improve hardness and wear resistance.
Based on the results, the hardness of the quenched materials was improved over the raw
materials and also improve the wear resistance of the quenched materials. Finally the water quenched
material has the best mechanical properties in hardness and wear resistance when compared to the
other quenched materials.
S.No
TYPE OF HARDNESS MEAN
QUENCHA (HRC) VALUE(HRC)
NT
1. As received 12,13,12,14,13,14, 12
12,12,13,14,12,14,12
2. Air 19,20,20,22,19,20, 21
21,22,21,20,19,22,20
3. Oil (open) 34
4,33,30,33,35,32
34,32,30,32,33,30,31
4. Oil (closed) 42,40,40,41,39,41, 42
41,42,40,39,40,42,41
5. Water 42,45,42,44,43,45, 46
42,43,42,44,43,42,44
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ISSN: 2278 – 7798
International Journal of Science, Engineering and Technology Research (IJSETR)
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Fig.5 Microstructure of Water quenched material
O. E. Joseph et al., (2015) have done hardening and characterisation of 0.45%C steel using
Clay/water as quenchant.
From experimental work they were the morphologies and mechanical properties of
0.45%C steel when different amount of clay was added to water for quenching operation.
The result obtained from present work was compared with the earlier work, which showed a
great improvement in the mechanical properties. Poor mechanical properties obtained for
higher additions of clay to water, lower amount of clay in water was considered by them.
Joshua. T. O. Et al., (2014) have done pioneering work on effects of various quenching media
on the mechanical properties of Medium Carbon Steel.
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International Journal of Science, Engineering and Technology Research (IJSETR)
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of each specimen was evaluated. Grains were fine them when quenched in distilled water
with high strength and hardness value was obtained in quenched distilled water, while for
strength and toughness palm kernel oil will be the best. Hence palm kernel oil has proved
better hardness value, tensile strength value and microstructure.
Fig .6 Microstructure of Medium Carbon Steel rod at 8000C held for 1 hour and quenched in
coldwater at x 200
Fig.7 Microstructure of Medium Carbon Steel rod 7900C, held for 1 hour and quenched in
palm kernel oil at x 200
A. AbdulmuminA et al., (2012) investigate the effect of water temperature on the mechanical
properties of water quenched Mn steel.
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International Journal of Science, Engineering and Technology Research (IJSETR)
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Graph 2 :Effect of Water Temperature Impact Strength of the Quenched Steel Samples
Graph 3:Effect of Water Temperature Tensile Strength of the Quenched Steel Samples
Alim sabur Ajibola et al., (2012) did extensive work on production and micro structural analysis of
as Cast and heat treated aluminium alloy (Al-20%wt Mg).
Their experimental work consisted of 16 samples were cast and heat treated at 450 0C for 1
hr and the samples were annealed, and quenched in water and used engine oil. Also they estimated
tensile, fatigue and hardness values. In case of the used engine oil quenched sample, the cooling rate
is slower compared to that of water. This slow cooling rate reduces the possibilities of defect
formation. The rate of cooling experienced in annealing is the slowest of all the sluggishness gives
room for poor formation.
Dr. Jassim Mohammed Salman A. M et al.,(2014) did extensive work on the effect of heat
treatments, polymer quenching and additions (Zr & Ag) on mechanical properties of (6061)
aluminium alloy.
Graph 4:Variation of energy absorbed of alloy sample ( quenching in water medium and
35% polyethylene glycol medium ) with aging time at 180°C aging temperature for A and B
alloys.
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International Journal of Science, Engineering and Technology Research (IJSETR)
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Fig 8:Microstructure of A alloy after aging treatment in 1800C alloy quenched in water.800X
Fig9: Microstructure of B alloy after ageing treatment in 1800C alloy quenched in polymer.
800X
M. Dauda et al., (2015) did experiments of effects of various quenching media on mechanical
properties of annealed 0.509wt % C – 0.178wt% Mn steel.
They evaluated palm kernel oil, cotton seed oil and olive oil as quenching media of
0.509Wt% C medium carbon steel. The machined specimen of the steel was heated at 8800C
and then quenched in water, engine oil, palm kernel oil, cotton seed oil and olive oil. They
also estimated strength properties and micro structure of the quenched samples were used to
determine the quench severity of the oils.
(1)The olive oil, palm kernel oil and cotton seed oil have hardness values less than that of water and
SAE 40 engine oil.
(2) Palm kernel oil, cotton seed oil and olive oil can be used to improve the toughness and these
quench media gave higher impact energy values than water
Fig 10:Microstructure of as-received structure of 0.509% carbon steel showing pearlite (dark)
in ferric (white) matrix X200
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ISSN: 2278 – 7798
International Journal of Science, Engineering and Technology Research (IJSETR)
Volume 5, Issue 4, April 2016
Fig 11: Microstructure of 0.509% carbon steel quenched in engine oil, showing full marten
site (dark) X200
Fig 12: Microstructure of water quenched microstructure of 0.509% carbon steel showing
marten site structure (dark) with retained austenite (white) X200
Fig 13:Micrograph of 0.509% carbon steel quenched in cotton seed oil, showing low
proportion of marten site structure (dark) in ferric (white) matrix X 200
Fig 14:Micrograph of 0.509% carbon steel quenched in palm kernel oil, showing low
proportion of marten site structure (dark) in ferric (white) matrix X200
Fig 15: Micrograph of 0.509% steel quenched in olive oil, showing low proportion of marten
site structure (white) with retained austenite(dark)
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ISSN: 2278 – 7798
International Journal of Science, Engineering and Technology Research (IJSETR)
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O.K. Abubakre et al., (2009) have done Investigations of the Quenching properties
of selected media on 661 aluminium alloy.
From the result based alloy at 5300C water quenched has highest tensile strength and
yield strength as well as highest value in hardness. Toughness property of the alloy was
better at 5300C for specimen quenched in sheanut oil and low impact strength was observed
in specimen quenched in water at 4000C water among the quenching media proved to have
the highest cooling rate followed by sheanut oil
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ISSN: 2278 – 7798
International Journal of Science, Engineering and Technology Research (IJSETR)
Volume 5, Issue 4, April 2016
Nikolai I.K et al., (2010) have done experiments on vegetable oil quenchants: Calculation
and comparison of the cooling properties of a series of vegetable oils, was undertaken by
them.
Vegetable oils were taken as quenching medium (canola, soya bean, corn, cotton seed
and sunflower oils) by blending oils with minimum viscosity variations. The heat transfer
using the oils occurs only by convection. Vegetate oils have better heat conducting properties
than petroleum oil based quenchants.
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ISSN: 2278 – 7798
International Journal of Science, Engineering and Technology Research (IJSETR)
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Graph:8 Cooling curves data at 60ºC bath temperature. a) time - temperature, b) cooling
rate –Temperature
Mr. Rajkumar shinde et al.,(2013) analysed the Influence of petroleum and Biodegradable
quench ants on properties of medium carbon steels.
Their observed that medium carbon alloy steel it microstructure and composition
dependent on the heat treatment and quenching process used i.e petroleum , vegetable oils
and soya bean oil. The result showed biodegradable quenchants used in place of petroleum
oils with improved mechanical properties.
From the results it is concluded that the heat treatment of steel using soy bean
quenchant gives the better mechanical properties and micro structure than petroleum
quenchants showed graphically.
First specimen heated to 8600 2 hours and then quenched indifferent quenchants. After
quenching specimen are tempered at 5600C and finally evaluated mechanical properties and
micro structure examined.
Kahtan K.A et al.,(2011) did extensive work on the effect of poly metric quenching on wear
resistance of Eutectic modified aluminium silicon alloy.
In their study a master alloy of modified eutectic (Al-12% Si) was prepared and used
the specimens were quenched and heat treated in distilled water, food oil, machine oil (0.2 –
1.4_wt% concentrations of poly vinyl alcohol. The specimens were characterised for X-ray
diffraction, microstructure, hardness and wear rate.
From the results it has been concluded that he Al-Si alloy with (0.6)wt% PVA had
maximum hardness and slight decrease the wear rate. And maximum decrease in the wear
rate when (1.2)wt% PVA was compared to the reference cast alloy, polymer quench ants
affect positively decrease wear rate of eutectic Al-Si alloy over the traditional quenching
media.
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ISSN: 2278 – 7798
International Journal of Science, Engineering and Technology Research (IJSETR)
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Table 4: explains the effect of different quenching media on the hardness and wear rate of the
eutectic Al-Si alloy.
M. Riaz et al.,(2014) have done A study on the mechanical properties of S45C medium type
carbon steel specimens under lathe machining and quenching conditions.
From experimental process they determined the nature and behaviour of many
materials under study. In the experimental work there were 2 sets (5 samples each) of
medium type steel specimens S45C of 0.45% carbon. Quench media both water and iso rapid
oil that were selected. Substantial change in mechanical properties when material quenched
in water as compared to isorapid oil.
Table5: Results for stress, strain, and percentage elongation (430 RPM & 860 RPM/Water
quenching)
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International Journal of Science, Engineering and Technology Research (IJSETR)
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Graph: 15 Graph:16
S.B.Hassan et al., ((2013) Investigated the Evaluation of khaya seed oil (mahoganyoil) as
quenchant in the hardening process of plain carbon steel.
The main objective of their work was khaya seed oil as a quenchant for hardening
process of 0.34% C plain carbon steel was investigated. Compared to water and SAE engine
oil quenched properties of plain carbon steel in the annealed, normalized and quenched,
tempered conditions were also investigated. The samples heated to 8700C, soaked and
quenched different media and also mechanical properties investigated.
Based on results khaya seed oil hardness value less than that of water but higher
hardness value than that of SAE 40 engine oil. Khaya seed oil improved toughness of PCS
and high impact energy values than water. Khaya seed oil used for hardening process in
PCS properties in between that of water and SAE 40 engine oil.
Table 6: Details of Plain Carbon steel different heat treatment and its Micro structure
Quenched in Khaya oil and tempered (350°) Martensite present, retain austenite and slight
increase in bainite Tempered martensite
structure
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ISSN: 2278 – 7798
International Journal of Science, Engineering and Technology Research (IJSETR)
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Fig 30: Microstructure of Plain Carbon Steel Hardened in Khaya Oil and Tempered at 350°.
The Structure Reveals Tempered Martensite x500.
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ISSN: 2278 – 7798
International Journal of Science, Engineering and Technology Research (IJSETR)
Volume 5, Issue 4, April 2016
the Cooling Properties of a Series of vegetable Oils”, Strojniski vestnik – Journal of
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http://www.akamaiuniversity.us/PJST.htm Volume 14. Number 1. May 2013 (Spring)
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