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Hydrophilic emulsifier is commonly supplied as a 100% using a refractometer (Figure 1). As an NDT professional
active concentrate, which is diluted in water before use, to working for an aerospace company, I check the concentration
emulsify and remove excess of non-water-based penetrants of our hydrophilic emulsifier every week per ASTM E 1417/E
(method D). The percentage of concentration depends on 1417M-13 using a handheld refractometer (ASTM, 2013b).
the application technique. The general spray concentration I have found that there is not much information available
is up to 5% remover-to-water, and 20% remover-to-water regarding this subject, and so this article presents a brief
for immersion dip applications. Concentration measurement walkthrough on how the process works.
is performed at initial makeup, during additions, and at The use of a refractometer is suitable and practical for
intervals during use. measuring the concentration of hydrophilic emulsifier,
Most nondestructive testing (NDT) standards require a also referred to as a remover, and also for water-based
weekly check of the hydrophilic emulsifier concentration water-washable penetrant.
Method of Operation
Adjustment to zero (null): place two to three drops of distilled or
Figure 4. Through the eyepiece we can see that the scale reads
reverse osmosis water on the refractometer’s main prism (Figure 3).
zero (that is, calibrated to null).
The water must spread across the surface of the prism without any
AUTHOR
Abhishek Wakaskar: ASNT NDT Level III; Aerospace Precision, Inc.,
2851 Evans St., Hollywood, Florida 33020; (954) 923-3213; fax (954)
923-3223.
Figure 5. Through the eyepiece we can see that the scale reads 4%. REFERENCES
ASTM, ASTM D 6304, Standard Test Method for Determination of Water in
Petroleum Products, Lubricating Oils, and Additives by Coulometric Karl Fischer
Now that the refractometer calibration is complete, measure the Titration, ASTM International, West Conshohocken, Pennsylvania, 2007.
emulsifier sample in the same manner as for calibration. Clean the prism ASTM, ASTM D 95, Standard Test Method for Water in Petroleum Products
using a microfiber cloth. Add two to three drops of emulsifier onto the and Bituminous Materials by Distillation, ASTM International, West
prism, again making sure that the emulsifier spreads evenly across the Conshohocken, Pennsylvania, 2013a.
surface without any bubbles and wait for 30 s. Then look through the ASTM, ASTM E 1417/E 1417M-13, Standard Practice for Liquid Penetrant
eyepiece and read the corresponding scale on the light/dark boundary. Testing, ASTM International, West Conshohocken, Pennsylvania, 2013b.