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Analysts: Alexandrea Apolinario, Kaitlin Keltner, Ryan Nakamura, & Margaret Shields

Sample: Deionized Water


Analysis : Data Analysis
Principle : Mastering the basic skills in the use of glassware and equipment to evaluate the skill of
the user. In addition, evaluating the reliability of such instruments and glassware by gathering
data from six determinations of the same procedure to generate the mean, standard deviation and a
confidence interval to further tell of accuracy, precision and validation.
Results :
  Volumetric Pipette Burette
  1ml 10ml 1ml 10ml
  Weight (g) Volume (mL) Weight (g) Volume (mL) Weight (g) Volume (mL) Weight (g) Volume (mL)
1 0.9954 0.9978 9.7396 9.7633 0.969 0.9714 9.9014 9.9255
2 0.989 0.9914 9.8976 9.9217 1.0345 1.0370 9.8227 9.8466
3 0.9919 0.9943 9.7814 9.8052 1.0721 1.0747 9.9324 9.9566
4 0.9902 0.9926 9.86 9.8840 0.9807 0.9831 9.9323 9.9565
5 1.0125 1.0150 9.8133 9.8372 1.0184 1.0209 9.9293 9.9535
6 0.9904 0.9928 9.8508 9.8748 0.9886 0.9910 10.0854 10.1100

  Weight (g) Volume (mL)


Water in Flask 99.6704 99.913
Water in Beaker 99.0816 99.323

𝑆𝐷 𝑋1 + 𝑋2 + ⋯ 𝑋𝑛 𝑥−𝑇𝑟𝑢𝑒 𝑉𝑎𝑙𝑢𝑒
𝐶𝐼 = 𝑥 ± 𝑡𝑣𝑎𝑙𝑢𝑒 × 𝑥 = % 𝐸𝑟𝑒𝑙 = 𝑥 100 ∑(𝑥 − 𝑥)^2
√𝑛 𝑛 𝑇𝑟𝑢𝑒 𝑉𝑎𝑙𝑢𝑒 𝜎=√
𝑀𝑎𝑠𝑠 𝑛−1
𝑉𝑜𝑙𝑢𝑚𝑒 = 𝐷𝑒𝑛𝑠𝑖𝑡𝑦

Conclusion:
  Volumetric Pipette Burette
  1ml 10ml 1ml 10ml
n=3  
Mean 0.9945 9.8477 1.0277 9.9096
SD 0.0032 0.0821 0.0523 0.0567
CV 0.0032 0.0083 0.0509 0.0057
%Erel -0.5483 -0.0152 0.0277 -0.0090
0.9945 ± 9.8477 ± 1.0277 ± 9.9096 ±
Cl 95% 0.0066 0.2307 0.1298 0.1407
n=6  
Mean 0.99732 9.84771 1.0130 9.9581
SD 0.00892 0.05756 0.03888 0.0855
CV 0.00895 0.00584 0.03838 0.0086
%Erel -0.00268 -0.01523 0.01301 -0.0042
0.9973 ± 9.8477 ± 1.013 ± 9.9581 ±
Cl95%   0.00936   0.0603   0.0408   0.0897

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