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Int J Adv Manuf Technol (2015) 77:2181–2195

DOI 10.1007/s00170-014-6617-6

ORIGINAL ARTICLE

Effect of backing plate material in friction stir butt and lap


welding of 6063-T4 aluminium alloy
Murshid Imam · Vikranth Racherla · Kajal Biswas

Received: 6 March 2014 / Accepted: 20 November 2014 / Published online: 3 December 2014
© Springer-Verlag London 2014

Abstract 6063-T4 aluminum alloy plates were friction stir rail cars, military, and aviation (Threadgill et al. [2]). The
butt and lap welded using three different backing plate solid-state nature of FSW process avoids problems of hot
materials: mild steel, stainless steel, and asbestos. Effects cracking, porosity, element loss, etc., which are common to
of backing plate material on macrostructure, peak mid- aluminum fusion welding processes (Mishra and Ma. [3]).
section temperatures in heat affected and weld nugget Furthermore, absence of ultraviolet or electromagnetic haz-
zones, and weld mechanical properties were obtained for ards, high penetration depths, reduced energy requirements,
each of the cases. Effect of backing plate material was seen absence of shielding gas, elimination of consumables such
to be more significant in lap than butt welding. While lap as rods and grinding pastes are some of the key additional
welds obtained even at a low welding speed, for mild steel benefits of the process over traditional fusion welding tech-
and stainless steel backing plates, contained multiple weld niques (Nandan et al. [4]). The presence of an exit hole at
defects leading to failure in lap shear tests from weld nugget the end of weld from where the probe is withdrawn and large
zone, corresponding welds obtained with asbestos backing clamping forces needed to hold the workpiece steady during
plate were defect free resulting in failure from base metal the process are crucial demerits of this welding technique.
region. In butt as well as lap configuration, asbestos backing Process parameters such as welding speed, tool rota-
plate which had the lowest thermal diffusivity was observed tional speed, axial (forge axis) force, and tool tilt angle
to provide the largest process window within which defect significantly affect the FSW process as heat generation rate,
free welds could be obtained. resultant temperatures, material flow, dynamic recrystal-
lization, and mechanical integrity of the joint are directly
Keywords Macrostructure · Backing plate materials · affected by these parameters. He et al. [5], Hui et al. [6], and
6063-T4 · Sheet positioning · Process window Imam et al. [7] reported that hardness in FSW of 6061-T6
and 6063-T4 aluminum alloys tends to be lower in the heat
affected zone on the retreating side, which then becomes
1 Introduction the location of tensile fracture for transverse weld specimen.
Ren et al. [8] reported that tensile strength increases with
Friction stir welding (FSW), which is already in use in rou- increasing welding speed in friction stir welding of 6061-T6
tine as well as critical applications, is an effective solid aluminum alloys. Lim et al. [9] showed that microhard-
state joining technique for aluminium alloys (Cam and Mist- ness distribution in weld cross-section changes with welding
ikoglu [1]). Presently, commercial applications of this weld- speed and tool rotational speed in 6061-T6 aluminum alloy.
ing technique have been reported across many industries, They also reported that strength and ductility decrease with
such as shipbuilding, automobile, high speed aluminium decreasing welding speed and increasing tool rotational
speed. Sato et al. [10] and Heinz et al. [11] reported that,
in 6063-T5 and 6061-T6 aluminium alloys, hardness dis-
M. Imam · V. Racherla () · K. Biswas
tribution across weld cross-sections depends on grain size
Department of Mechanical Engineering,
Indian Institute of Technology, Kharagpur 721302, India distribution and state of precipitates. They also reported
e-mail: vikranth.racherla@mech.iitkgp.ernet.in that coarsening/dissolution of strengthening precipitates in
2182 Int J Adv Manuf Technol (2015) 77:2181–2195

weld zones for these alloys are sensitive to welding thermal al. [18], friction stir lap welding does not produce good
cycles they experience. Recently, Imam et al. [12] reported quality welds with the same ease as friction stir butt weld-
that peak temperatures in weld regions could be used as ing. In addition to factors that influence quality of friction
one of the monitoring parameters to evaluate friction stir stir butt welds, clamping arrangement, sheet positioning,
weld joints properties, particularly in heat treatable alloys. and pin height play an important role in FSW in lap con-
Rajakumar et al. [13] showed that lower weld zone tempera- figuration. For example, Buffa et al. [19] show that shorter
tures in FSW can result in weld defects such as voids, worm pins (significantly smaller than the combined thickness of
holes, cracks, etc., in butt welds. Additionally, as observed the two sheets welded in lap configuration) with sheet place-
by Yadava et al. [14], cold lap and hook defects can occur ment and clamping as shown in Fig. 1 result in better quality
in lap welds at lower weld temperatures. Thus, one needs lap welds. Failure of friction stir lap welds, under mono-
to find ways of maintaining required weld zone tempera- tonic or cyclic loading, is seen to be strongly influenced by
tures to avoid cold weld defects. Even though, choice of the hook and cold lap defects that form at the interface between
backing plate material has a direct and significant effect on stir/thermo-mechanically affected zone and the HAZs. In
resultant temperatures in FSW, relatively few works exist this connection, Yazdanian et al. [20] observed that the
on quantifying their effect, particularly in lap welding. This height of hook and cold lap defects, which directly influ-
work aims to shed light on this aspect through investigation ence the lap shear strength, increased with increasing tool
of microstructure and mechanical properties of butt and lap rotational speed and decreasing welding speed.
welds of 6063-T4 AA obtained using mild steel, stainless In this work, friction stir welds were obtained using
steel, and asbestos backing plates. 6063-T4 aluminum alloy plates. 6063-T4 is a medium
Rosales et al. [15] studied the effect of backing plate in strength, naturally aged Al-Mg-Si alloy with good post weld
friction stir butt welding of 4-mm-thick 6013-T6 and 3.2- formability characteristics and resistance to stress corrosion
mm-thick 2024-T351 aluminum alloy plates. Three backing cracking. Edwards et al. [21] reported that age hardening
plate materials were considered in their study: steel, cop- in this alloy occurs from Mg-Si precipitates appearing in
per, and ceramic. While, defect free welds were obtained different forms: GP zones (Si-Mg vacancy clusters), fine
with steel backing plate, tunnel defects and excess flash needle-shaped β  , rod-shaped β  , and cube/plate shaped
formation were observed with copper and ceramic backing β-Mg2 Si precipitates. Interestingly, relatively few works
plates, respectively. Upadhyay and Reynolds [16] inves- exist on friction stir welding of this alloy in naturally
tigated the effects of forge axis force and backing plate aged condition as compared to artificially aged condi-
thermal diffusivity on friction stir butt welding of 4.2-mm- tion, despite the fact that friction stir welded blanks of
thick 6056-T451 aluminum alloy plates. Three millimeter artificially aged Al-Mg-Si alloys present difficulties in
thick aluminum alloy 2099, tool steel, Al6XN (Allegheny post weld forming, e.g., inability to achieve high draw-
Ludlum super austenitic stainless steel), Ti-6-4, and ceramic ing depths and tight bending radii, etc., in as welded
floor tile were used as backing plates. It was found that condition. For this alloy, in naturally aged condition, as
peak, mid-section, stir zone temperatures for ceramic back- reported, e.g., by Simar et al. [22], while higher heat
ing plate were about 40, 35, and 25o C higher than that affected zone temperatures result in overaging of HAZs,
for aluminum, steel, and Al6XN backing plates, respec- higher stir zone temperatures result in higher grain sizes
tively. Stir zone temperatures were found to be sensitive which reduce the amount of hardening occurring from grain
to forge axis force, tool rpm, welding speed, and backing refinement.
plate material. While tunnel defects were found for peak, Elangovan and Balasubramanian [23] showed that square
mid-section, stir zone temperatures of around 360-400o C, pin profile gives better quality welds at least among tapered
excess flash formation was observed when mid-section tem- cylindrical, threaded cylindrical, triangular, and square pin
peratures exceeded around 450o C. Recently, Zhang et al. profiles. Additionally, Imam et al. [24] showed that square
[17] observed the effect of backing plates on friction stir pin profile gives better quality welds than tapered square
butt welding of 3.2-mm-thick 2024-T3 aluminium alloy and tapered cylindrical pin profiles. Thus, in this work,
sheets at 600 rpm and 200 mm/min welding speed for cop- friction stir welds were obtained using stainless steel tools
per, medium carbon steel, and granite backing plates. Steel with square tool pin profile. Asbestos is chosen as one of
backing plate was seen to give the highest joint efficiency the backing plate materials for its low thermal diffusivity,
of about 90 %, while granite and copper backing plates moderate toughness, and availability. Marble and granite
resulted in significantly lower joint efficiencies. While the were also tried as alternate backing plate materials but dis-
presence of a tunnel defect was responsible for the loss of carded due to occurrence of fracture during the tests. Results
weld strength for copper backing plate, softening in HAZ obtained with asbestos are also expected to hold true for
could be responsible for loss of weld strength for granite any other backing plate with low thermal diffusivity, mod-
backing plate. Separately, as observed by Soundararajan et erate rigidity and toughness, and melting point much above
Int J Adv Manuf Technol (2015) 77:2181–2195 2183

Fig. 1 a schematic of the tool


used in welding. h denotes the
pin height. All dimensions are in Shank
millimeter, b and c sheet
positioning and clamping 44 Tool
19 shoulder
arrangement used in lap Adv
anc
welding, d geometry of lap weld ing
side
specimen used in shear tests, The
r
and e geometry of butt weld coup mo-
specimen, prepared according to les
24 20 Ret
r
ASTM:E8M-11 guidelines, used Welding side eating
in uniaxial tensile tests. While 3 direction
and 6 mm sheets were used in
h
butt welding, only 3 mm sheets
were used in lap welding
60
Base metal (BM)

(a) (b)

Clamping force
Air gap
Support plates

Base metal (BM)

(c)
Backing plate

130

(d)
18

Transverse Specimen AS

Crown R 12.5

100

12.5
Thermocouple
50 Rolling direction

RS
20
(e)
2184 Int J Adv Manuf Technol (2015) 77:2181–2195

that of material being welded. Thermal diffusivity of stain- designed fixture for rigidly holding the sheets/plates to the
less steel lies in between that of mild steel and asbestos backing and support/clamping plates. For lap welds, tem-
backing plate. Thus, to see if weld temperatures and weld peratures in heat affected zones (HAZs) and weld nugget
properties varied monotonically with thermal diffusivity of zone (WNZ) were measured using K-type thermocouples
backing plate material, welds were obtained for mild steel, inserted in 2 mm deep, 1.5 mm diameter blind holes drilled
stainless steel, and asbestos backing plate materials. In addi- from top, at a distance of 14 and 0 mm from the weld
tion, there is a greater chance of getting cold weld defects line, respectively. For butt welds, temperatures were mea-
when welding thinner aluminium sheets as compared to sured in WNZ and in HAZ on the retreating side. Once
thicker ones due to lower weld temperatures for smaller again, K-type thermocouples inserted in 1.5-mm-diameter
sheet thicknesses (Imam et al. [12]). On the other hand, blind holes drilled from top were used to measure the tem-
full penetration can sometimes be an issue for higher thick- peratures. While the holes used for inserting thermocouples
ness plates. Consequently, to show the effectiveness of using were 3 mm deep for 6 mm plates, they were 2 mm deep
lower diffusivity backing plate, butt welds were obtained for for 3 mm sheets. It may be noted that temperature varies
3 as well as 6-mm-thick plates. It has been shown in the lit- relatively sharply in weld nugget zone. Consequently, peak
erature that lap welds result in different set of defects and temperature measured by the thermocouple in WNZ is only
are in general more difficult to successfully obtain than butt the peak temperature at sheet mid-section along the weld
welds. Thus, in addition to butt welds, lap welds were also line. There would be regions within the WNZ that experi-
obtained for different backing plate materials. The main aim ence lower as well as higher peak temperatures than that
of this work is to experimentally investigate the effect of measured by the thermocouple. Separately, thermocouples
backing plate material on friction stir butt and lap welds. To in HAZs are placed close to WNZ and gradient in temper-
this end, microstructural and mechanical characterization is ature field in this zone is relatively moderate. Thus, peak
carried out for welds obtained with different backing plates temperatures measured by thermocouples in HAZs can be
and sheet thicknesses. thought of as peak temperatures in these zones.
To prepare specimen for microstructural analysis and
hardness testing, weld cross sections of specimen cut out
2 Experimental procedure from welded plates were polished on a disc polishing
machine, using different grades of emery paper and a dia-
6063-T4 aluminium alloy plates of 100 x 100 mm sourced mond compound. Microhardness measurements on polished
from Hindalco Industries Ltd, India, were friction stir weld cross sections were taken using a Vicker’s microhard-
welded at process parameters shown in Table 1. The weld- ness tester at 50 gf and 15 s dwell time. The polished
ing speeds were chosen through initial trails such that defect specimen was etched with Kellers reagent (150 ml H2 O,
free welds could be obtained with all three backing plates 3 ml HNO3 , 6 ml HF, and 6 ml HCL), for approximately
at the lowest speed and such that defect free welds could be 30 s, to reveal the underlying microstructure. Morpholo-
obtained, even at the highest welding speed considered, for gies of weld cross sections were studied using a stereozoom
low diffusivity backing plate. To highlight that weld defects Leica microscope. Shape, size, and distribution of precip-
can occur even at a low welding speed, butt welds were also itates in different weld regions were investigated using a
obtained at two tool rotational speeds. The tool rpm levels FEI-TECNAI transmission electron microscope operating
were chosen based on options available on the machine used at 200 kV. Samples for transmission electron microscope
for this work. Further, while 3 mm sheets were used in lap (TEM) study were polished until their thickness reduced to
welding, butt welding was done for 3 and 6 mm plates. In about 50 microns. A disc-punch machine was then used to
each case, welding was carried out using three backing plate cut 3-mm-diameter specimen which were electro-polished,
materials: mild steel, stainless steel, and asbestos. Thermo- in 30 % HNO3 , 70 % CH3 OH mixture at -30o C and 40 V,
physical properties of different backing plate materials are using a Struers Tenupol-2 twin-jet electro-polisher, before
given in Table 2. It may be noted that the thermal conductiv- being analyzed using TEM. Microstructural and mechani-
ity of stainless steel lies in between mild steel and asbestos cal characterization was typically carried out within 2 weeks
backing plate material. Schematics of the SS 316 tool used, of preparation of the welds. Shear strength of lap welds
sheet positioning and clamping arrangement for lap welds, was determined using tensile tests on specimen of the form
and specimen used in lap shear tests and tensile tests are shown in Fig. 1d. On the other hand, mechanical response
shown in Fig 1. Chemical composition of the plates obtained of butt welds in transverse loading was characterized using
from energy dispersive X-ray spectroscopy, done using a tensile tests on specimen prepared as per ASTM: E8-M11
scanning electron microscope with Oxford EDS detector, is guidelines (see Fig. 1e). Tensile tests were conducted on
given in Table 3. Weldings were done on a 7.5 HP, Hin- a computer controlled universal tensile testing machine
dustan ltd. make, vertical milling machine using a specially INSTRON 8862 at a crosshead speed of 2 mm/min.
Int J Adv Manuf Technol (2015) 77:2181–2195 2185

Table 1 Process parameters used in this work

Tool pin profile Rotational Welding Pin Plunge Tool


speed (rpm) speed (mm/min) height (mm) depth (mm) tilt angle (o )

Square 450, 635 18, 38, 64 2.65, 4.85, 5.65 2.7, 4.9, 5.7 0

3 Results and discussion fraction of heat generated during welding, lost to backing
plate would be higher for 3 mm sheets. Thereby, peak tem-
3.1 Butt welds peratures for 3 mm sheets would be smaller. Note that this
observation is in line with the observation made by Imam et
Cross-sectional macrographs of butt welds for 3 mm sheets, al. [12]. Effect of peak mid-section temperature along weld
obtained at three different welding speeds, for mild steel, center line on mean grain size in this region for 3 and 6 mm
stainless steel, and asbestos backing plates, are shown sheets, for different backing plates, is shown in Fig. 4a.
in Fig 2. Also shown in the figure are the underlying The following observations can be made from the figure:
microstructures in some of the weld regions. Note from the (i) in line with earlier works, e.g., Sato et al. [28], aver-
figure that asbestos backing plate gives defect free welds age grain size in WNZ increases exponentially with peak
at all welding speeds considered. On the other hand, tun- temperature in this region, (ii) different static grain growth
nel defects can be seen at 64 mm/min welding speed for relations are obtained for 3 and 6 mm sheets. For a given
stainless steel and at 32 and 64 mm/min welding speeds peak temperature, faster cooling rates for 3 mm sheets result
for mild steel backing plates. Note from Fig. 3 that tunnel in smaller grain sizes for 3 than 6 mm sheets, (iii) aver-
defects appear when peak temperature at sheet mid-section age grain size is largest for asbestos and smallest for mild
in WNZ goes below 400o C. Average grain size in WNZ is steel backing plates, and (iv) for a given set of process con-
seen to be smallest for mild steel and largest for asbestos ditions and tool profile, average grain size is smaller in 3
backing plates. This is on anticipated lines, as asbestos and than 6 mm sheets as WNZ temperatures are lower in 3 mm
mild steel backing plates are expected to give the highest sheets. Figure 4b shows relation between average micro-
and lowest WNZ temperatures, respectively, and as aver- hardness and average grain size in WNZs. It can be seen that
age grain size in weld nugget zone is expected to be higher microhardness increases with decreasing grain size as per
for higher peak WNZ temperatures. Interestingly, average Hall-Petch relation, implying that for this alloy hardening in
grain size in HAZ on RS for asbestos backing plate is much WNZ in as welded condition is predominantly from grain
larger than mean grain size for the base metal. Further, peak refinement.
temperatures in WNZ are about 50o C higher for asbestos Cross-sectional micrographs of butt welds obtained for
than that for mild steel backing plate. Peak temperatures 3 and 6 mm sheets, at a lower tool rotational speed of
in HAZs on retreating side are shown in Fig. 3d. It is evi- 450 rpm, are shown in Fig. 5. It can be seen from this figure
dent that higher HAZ temperatures for asbestos backing that a tunnel defect appears for mild steel backing plate
plate are responsible for larger grain sizes in these regions. for 3 mm sheets welded at 450 rpm, even at a low weld-
It may be further noted from Fig. 3 that peak mid-section ing speed of 18 mm/min, whereas all welds obtained at this
temperatures along the weld center line are higher in 6 welding speed are defect free for tool rotational speed of
than 3 mm sheets by about 40o C. Smaller heat capacity 635 rpm. It is evident from Fig. 6 that peak mid-section weld
of 3 mm sheets is believed to be the underlying cause for nugget zone much below 400o C, for the case where 3 mm
this. Since conduction heat loss to backing plate primar- sheets are welded with mild steel backing plate at 450 rpm
ily depends on temperatures reached at sheet-backing plate and 18 mm/min, is responsible for the formation of tunnel
interface, it would be nearly unaffected by the sheet thick- defect. For the aluminum alloy used in this work, Imam et al.
ness. However, as 3 mm sheets have a smaller heat capacity, [12] show that softening from overaging is expected to occur

Table 2 Thermo-physical properties of different backing plate mate-


rials used in this work (Kumzerov et al. [25], Kusiorowski et al. [26],
and Charde et al. [27]) Table 3 Chemical composition of 6063-T4 aluminium alloy sheets
used in this work
Properties Mild steel Stainless steel Asbestos
Element Si Mg Cu Fe Zn Cr Al
Density (g/cm3 ) 7.85 8.0 2.6
Thermal conductivity (W/mK) 54 16.2 2.5 Weight % 0.72 0.57 0.13 0.61 0.02 0.09 97.88
Specific heat (J/gK) 0.620 0.530 0.024 Atomic % 0.69 0.63 0.05 0.29 0.01 0.04 98.26
2186 Int J Adv Manuf Technol (2015) 77:2181–2195

100 µm WNZ 100 µm


WNZ

MS v = 18 mm/min SS v = 18 mm/min

v = 38 mm/min v = 38 mm/min
Tunnel Defect

3000 µm
3000 µm
v = 64 mm/min v = 64 mm/min

(a) Tunnel Defect Tunnel Defect (b)

WNZ HAZ BM

100 µm 100 µm 100 µm

AS RS

ASB v = 18 mm/min

v = 38 mm/min

3000 µm
v = 64 mm/min

(c)
Fig. 2 Optical macrographs and WNZ microstructures for butt welds obtained at 635 rpm for 3 mm sheets with a mild steel, b stainless steel, and
c asbestos backing plates

when heat affected zone temperatures go above 410o C. Transmission electron microscopy (TEM) image taken
Thus, it is expected that for welds obtained at 450 rpm and from the base metal region along with selected area diffrac-
18 mm/min, except for 6 mm sheets welded using asbestos tion pattern (SADP) for this region is shown in Fig. 7a
backing plate, where the peak heat affected zone tempera- and b. TEM images for the base metal are conspicu-
ture on retreating side is around 425o C, overaging will not ous by the absence of grain boundaries, pile ups, or
occur in any other case. precipitates. SADP for the BM confirms the absence of
Int J Adv Manuf Technol (2015) 77:2181–2195 2187

550 550
t = 3 mm
ASB t = 6 mm

Peak Temperature ( O C)
Peak Temperature ( C)
500 A S B WNZ 500 ASB WNZ
SS

O
MS
SS ASB
450 SS
MS ASB 450 MS
ASB SS
SS MS
400 MS
400
SS
350 MS 350

300 300

250 250
18 64 18 38 64
38
Welding Speed (mm/min) Welding Speed (mm/min)
(a) (b)

500 500
t = 3 mm t = 6 mm
Welding

Peak temperature ( O C)
Peak temperature ( O C)

direction HAZ RS HAZ RS


ASB
450 450
30 mm SS
ASB Thermocouple
ASB
400 ASB 400 SS
SS ASB MS
ASB
MS SS MS
350 350 SS
MS MS
SS
MS
300 300
18 38 64 18 38 64
Welding Speed (mm/min) Welding Speed (mm/min)
(c) (d)
Fig. 3 Peak temperatures at thermocouple locations in WNZ and three different backing plate materials: asbestos (ASB), stainless steel
HAZ on RS, in friction stir butt welding of a and c 3 and b and d 6- (SS), and mild steel (MS). Note that tool rotational speed is 635 rpm
mm-thick 6063-T4 AA plates obtained at different welding speeds, for

precipitates in this region. Similar observations were also from Fig. 7c that for this case HAZ on RS is free of pre-
made by Heinz and Skrotzki [11] for 6013-T4 aluminum cipitates. Figure 7d shows that dynamic recrystallization in
alloy. TEM images taken in HAZ on RS and WNZ for WNZ results in the formation of sub-grains. The WNZ too
6 mm sheets butt welded using stainless steel backing plate appears to be free of precipitates. TEM images for 6 mm
at 450 rpm tool rotational speed and 18 mm/min welding sheets butt welded using asbestos backing plate at 450 rpm
speed are shown in Fig. 7c and d, respectively. It is evident and 18 mm/min are shown in Fig. 8. Note from Fig. 6 that

Fig. 4 a Effect of peak 25 80


temperatures in WNZ on mean Red 3 mm ASB SS MS
6 mm
grain size and b Effect of mean 3 mm Green 6 mm
Mean Grain Size (µm)

grain size on average hardness 20 ASB 70


Hardness (Hv)

of WNZ for friction stir welds SS


15 MS
obtained at 635 rpm for 3 and
6 mm sheets by using three 60
backing plate materials: 10 -1/2
Hv = 48 + 46.6 d
Asbestos, stainless steel, and
mild steel, respectively 50
5 f = 635 rpm f = 635 rpm
v = 18 mm/min v = 18 mm/min
0 40
400 425 450 475 500
525 550 0.2 0.25 0.30 0.35 0.40
o
Peak WNZ Temperature ( C) -1/2
d (µm -1/2 )
(a) (b)
2188 Int J Adv Manuf Technol (2015) 77:2181–2195

Fig. 5 Optical macrographs of AS RS


weld cross-sections obtained AS RS
ASB
with different backing plates for ASB
friction stir butt welding of (a) 3
5 mm
and (b) 6 mm sheets. Note that 5 mm
tool rotational and welding
speeds are 450 rpm and 18
mm/min, respectively SS SS

MS
MS

Tunnel Defect
(a) (b)

peak temperatures in WNZ and HAZ on RS for this case contains a range of features (Su et al. [29]). Greater peak
are around 475 and 420o C, respectively. Rod shaped precip- WNZ temperatures in the case of asbestos backing plate
itates indicating overaged condition can be seen in HAZ on result in greater recovery and lower dislocation densities.
RS in Fig. 8b and c. This is in line with works of Sato et al. Solute depletion caused by preferential grain boundary pre-
[28] and Zhang et al. [31] who too observed significantly cipitation results in precipitate free zone (PFZ) near to grain
overaged precipitates in HAZs when peak temperatures in boundaries (Shastry and Judd [32]). As seen from Fig. 8 f,
HAZ reach around 420o C. Figure 8d–f shows that the WNZ needle-shaped precipitates aligned with < 100 > directions

Fig. 6 Peak temperatures at


thermocouple locations in a and
b WNZ and c and d HAZ on RS,
in friction stir butt welding of 3
and 6 mm sheets at 18 mm/min
welding speed for two different
tool rotational speeds
Int J Adv Manuf Technol (2015) 77:2181–2195 2189

Fig. 7 a Transmission electron


microscopy (TEM) image of BM BM
base metal, b Selected area
diffraction pattern of base metal,
c and d TEM images taken of
HAZ on RS and WNZ,
respectively, for 6-mm-thick
6063-T4 AA plates welded at
18 mm/min and 450 rpm using
stainless steel backing plate

200 nm
(a) (b)
HAZ RS WNZ

Sub grain
Dislocation tangle boundary

200 nm 200 nm

(c) (d)

form in WNZ. Note from the fact that stable Mg2 Si precip- β  precipitates, lower dislocation densities from enhanced
itates dissolve in Al matrix above 520o C and from Figs. 6, recovery, and grain coarsening. These results are in line with
7, 8 that WNZ is precipitate free only when peak temper- works of Heinz and Skrotzki [11], Zhang et al. [31], and Lee
atures are below 450 or above 520o C. Precipitates form in et al. [32] who reported loss of hardness in HAZs, experi-
WNZ, in as welded condition, only in a narrow temperature encing peak temperatures of around 420o C, from formation
window around 475o C. of overaged β  Mg2 Si precipitates. The absence of softening
Vicker’s microhardness contours at approximately weld in HAZs for 3 mm sheets or 6 mm sheets welded with stain-
mid-sections for 3 and 6 mm sheets welded at 450 rpm and less steel and mild steel backing plate indicates that peak
18 mm/min are shown in Fig. 9. Three millimeter sheets temperatures of about 385o C or less in HAZs do not result
welded with mild steel backing plate contain a big tunnel in overaging of these regions for this alloy.
defect and consequently hardness contour has not been Magnitudes of joint efficiency, yield strength, and per-
obtained for this case. Note from Fig. 8c that HAZs for centage elongation (at load maximum) of welds in trans-
6 mm sheets welded with asbestos backing plate, which verse loadings are shown in Fig. 10. Note that the ultimate
experience peak temperatures of around 420o C, are softer tensile strength, yield strength, and percentage elongation at
than BM by about 10 Hv. Further, the average hardness of load maximum for base metal, not shown in the figure, are
WNZ for this case is slightly less than that for stainless 140 MPa, 88 MPa, and 20 %, respectively. The following
steel backing plate. It may be noted that hardening in stir are evident from the Fig. 10: (i) In nearly all cases, maxi-
zone in as welded condition is believed to be from dynamic mum percentage elongation is achieved for welds obtained
recrystallization induced grain refinement and from for- with asbestos backing plate. Percentage uniform elongation
mation of dislocation cells. Lower hardeness in SZ in of transverse weld specimen is significantly lower (about
the case of asbestos backing plate is believed to be from 60 % or smaller) than that for corresponding base metal
lower dislocation densities from higher recovery and grain specimen. It may be noted that loss of ductility is due to
coarsening. These observations are in line with that made non-uniform weld zone properties. More specifically, higher
in literature, e.g., Sato et al. [28]. Separately, softening hardness of WNZ and lower hardness of HAZs result in
in HAZs in this case is from the formation of overaged strain localization in HAZs leading to reduced elongation
2190 Int J Adv Manuf Technol (2015) 77:2181–2195

HAZ RS HAZ RS HAZ RS


ASB ASB ASB

Dislocation Rod Rod


tangle
Dislocation
tangle

200 nm 200 nm 200 nm

(a) (b) (c)

Dislocation WNZ WNZ [010] WNZ


line ASB ASB ASB
Dislocation
network
[100]

Precipitate
Sub grain free zone
boundary
200 nm 200 nm 100 nm

(d) (e) (f)


Fig. 8 Transmission electron microscopy images taken in a–c HAZ on RS and d-f WNZ, for 6-mm-thick 6063-T4 AA plates welded at 18 mm/min
and 450 rpm using Asbestos (ASB) backing plate

at load maximum for transverse weld specimen, (ii) Joint that temperatures in WNZ, for asbestos backing plate, are
efficiencies of about 100 % or more are typically achieved higher than that for mild steel and stainless steel backing
when there is no softening in HAZs and when there are plates by about 100 and 50o C, respectively. Further note that
no tunnel defects in WNZ, (iii) For 3 mm sheets welded the temperatures shown for WNZs are measured along weld
at 450 rpm, asbestos backing plate gives the best joint effi- center line at about 2 mm from the top. Peak temperatures
ciency, yield strength, and percentage uniform elongation. reached at the bottom of the bottom plate (i.e., at about 5 to
Note that for this case, temperatures in HAZ and WNZ are 6 mm from top) would be much smaller than that measured
about 380 and 430o C, respectively, and that there is no soft- by the thermocouples, particularly for mild steel backing
ening in HAZ and no weld defects in WNZ, and (iv) Effect plate. Lower weld zone temperatures for mild steel and
of backing plate, particularly on percentage elongation and stainless steel backing plates appear to result in tun-
joint efficiency, is highest at the lower tool rpm and lower nel defects. Higher thermal diffusivity of mild steel
sheet thickness. is expected to result in significant heat loss from the
plates being welded, thereby resulting in lower weld zone
3.2 Lap welds temperatures.
Interestingly, difference in heat affected zone temper-
Cross-sectional optical macrographs of lap welds obtained atures for different backing plates is much smaller as
with different backing plates are shown in Fig. 11. Note compared to difference in weld nugget zone temperatures.
from the figure that while tunnel defects appear in lap welds, Further, peak temperatures on advancing side are higher
for mild steel and stainless steel backing plates, even at a than that on the retreating side. Note that this has got to
low welding speed of 18 mm/min, defect free lap welds are do with sheet placement and temperatures would have been
obtained with asbestos backing plate for welding speeds at higher on retreating side if the sheet placement were to be
least up to 64 mm/min. Reasons for the formation of tun- reversed and the top sheet was on retreating side. As noted
nel, cold lap, and hook defects particularly for mild steel earlier, for the aluminium alloy used in this work, Imam
backing plates can be seen in Fig. 12. Note from Fig. 12a et al. [16] show that softening from overaging is expected
Int J Adv Manuf Technol (2015) 77:2181–2195 2191

Fig. 9 Vickers microhardness


contours at weld mid-sections
for a and b 3 mm and c-e 6 mm
sheets. Note that the tool
rotational speed is 450 rpm and
welding speed is 18 mm/min

to occur when heat affected zone temperatures go above unit width) of lap welds obtained with MS, SS, and ASB
410o C. Thus, overaging in HAZs is not expected in any of backing plates was found to be 290, 350, and 360 N/mm,
the lap welds obtained here. Photographs of failed lap shear respectively.
test specimen prepared from welds obtained with different
backing plates are shown in Fig. 13. Note from the figure
that while welds obtained with mild steel and stainless steel 4 Summary and conclusions
backing plates fail from WNZ, welds obtained with asbestos
backing plate fail from the base metal. The presence of cold Friction welds were obtained for 3 and 6 mm thick 6063-T4
lap defect for MS and SS backing plates can be confirmed aluminum alloy sheets, under butt and lap configurations,
from Fig. 13a and b. Average strength (maximum load per using asbestos, stainless steel, and mild steel backing plates.
2192 Int J Adv Manuf Technol (2015) 77:2181–2195

Morphology, microstructure, and mechanical properties of • Weld zone temperatures are significantly affected by
the welds were analyzed as a function of the backing plate the backing plate material, particularly in lap weld con-
material used. The following conclusions are drawn from figuration. While defect free lap welds were obtained
this work: with asbestos backing plate, tunnel, hook, and cold lap

140 140
t = 3 mm t = 6 mm
120 120
Joint Efficiency (%)

100

Joint Efficiency (%)


100
80 80
60 60
40 40
ASB SS MS ASB SS MS ASB SS MS ASB SS MS
20 20
0 0
450 635 450 635
Tool rotational speed (rpm) Tool rotational speed (rpm)
(a) (d)
1 00 1 00
t = 3 mm t = 6 mm
Yield Strength (MPa)
Yield Strength (MPa)

80 80

60 60

40 40

20 ASB SS MS ASB SS MS 20 ASB SS MS ASB SS MS

0 0
450 635 450 635
Tool rotational speed (rpm) Tool rotational speed (rpm)
(b) (e)
16 16
t = 3 mm t = 6 mm
14 14
12 12
Elongation (%)

Elongation (%)

10 10
8 8
6 6
4 4
ASB SS MS ASB SS MS
2 2
ASB SS MS ASB SS MS
0 0
450 635 450 635
Tool rotational speed (rpm) Tool rotational speed (rpm)
(c) (f)
Fig. 10 Joint efficiency, yield strength (0.2 % proof stress), and as the ratio of tensile strength of transverse weld specimen to that of
percentage uniform elongation for welds obtained at different tool similarly oriented base metal specimen. Also note that uniform elon-
rotational speeds and for different backing plate for a–c 3 and d–f gation is the engineering strain at load maximum. The welding speed
6 mm sheet thickness, respectively. Note that joint efficiency is defined is 18 mm/min
Int J Adv Manuf Technol (2015) 77:2181–2195 2193

Fig. 11 Optical macrographs AS RS AS RS


for lap welds obtained at MS SS
635 rpm for 3 mm sheets with a
mild steel, b stainless steel, and
c asbestos backing plates Hook 5000 µm 5000 µm
v = 18 mm/min v = 18 mm/min

Tunnel Defect Cold lap Tunnel Defect


(a) (b)
AS RS

ASB

5000 µm
v = 18 mm/min

5000 µm
v = 38 mm/min

5000 µm
v = 64 mm/min

(c)

Fig. 12 Peak temperatures in 550 550


weld nugget zone (WNZ), heat ASB f = 635 rpm WNZ ASB
affected zone on advancing side v = 18 mm/min WNZ f = 635 rpm
500 500
Peak Temperature ( oC)
Peak Temperature ( oC)

(HAZ AS), and heat affected SS


WNZ
zone on retreating side (HAZ 450 450 HAZ
RS) in mid-section of the top MS AS HAZ
sheet in lap welding of 3 mm ASB 400 HAZ
400 HAZ AS
sheets for welds obtained with a SS HAZ AS
RS HAZ
using the three backing plate MS ASB SS RS
350 350 RS
MS
materials and b only asbestos at
a tool rotational speed of 300 300
635 rpm and welding speeds of
18, 38, and 64 mm/min. 250 250
Thermocouples in HAZs are WNZ HAZ-AS HAZ-RS 18 38 64
placed at a distance of 14 mm Welding Speed (mm/min)
from weld center line
(a) (b)

Fig. 13 a–c Fractographs of MS SS


weld cross-sections of lap weld
tensile specimen just after
failure, obtained using asbestos Cold lap Hook
(ASB), stainless steel (SS), and AS RS AS RS
mild steel (MS) backing plates
for tool rotational speed of (a) (b)
635 rpm and welding speed of
18 mm/min ASB

AS Fracture Location RS

(c)
2194 Int J Adv Manuf Technol (2015) 77:2181–2195

defects were obtained with mild steel and stainless steel 12. Imam M, Biswas K, Racherla V (2013) On use of weld zone
backing plates. temperatures for online monitoring of weld quality, in friction
• stir welding of naturally aged aluminium alloys. Mater Des 52:
Microhardeness of weld nugget zone, for this alloy, is
730–739
predominantly controlled by the average grain size in 13. Rajakumar S, Muralidharan C, Balasubramanian V (2010)
weld nugget zone which is in turn controlled by the Establishing empirical relationships to predict grain size and
peak temperature and cooling rates in this region. tensile strength of friction stir welded AA 6061-T6 alu-
• Process window within which defect free butt or lap minium alloy joints. Trans Nonferrous Met Soc China 20:
1863–1872
welds can be obtained is larger for backing plate materi- 14. Yadava MK, Mishra RS, Chen YL, Carlson B, Grant GJ
als with lower thermal diffusivity. In this work, asbestos (2010) Study of friction stir welding joining of thin alu-
backing plate provided the largest process window minium sheets in lap joint configuration. Sci Tech Weld join 15:
within which defect free welds could be obtained. 70–75
• 15. Rosales MJC, Alcantara NG, Satos J, Zettler R (2010) The back-
Peak weld zone temperatures are lower for sheets of ing bar role in heat transfer on aluminium alloys friction stir
lower thickness. Thus, an appropriate choice of backing welding. Mater Sci Forum 636-637:459–464
plate is more important during friction stir welding of 16. Upadhyay p, Reynolds AP (2012) Effects of forge axis force and
thinner sheets. backing plate thermal diffusivity on FSW of AA6056. Mater Sci
• Eng A 558:94–402
Sheet positioning plays a crucial role in temperature
17. Zhang Z, Li W, Shen J, Chao YJ, Li J, Ma YE (2013)
asymmetry in lap welding. Peak HAZ temperature is Effect of backplate diffusivity on microstructure and mechan-
higher in the sheet placed on the top. ical properties of friction stir welded joints. Mater Des 50:
551–557
18. Soundararajan v, Yarrapareddy E, Kovacevic R (2007) Inves-
Acknowledgments The support provided by the Central Research tigation of the friction stir lap welding of aluminum alloys
Facility and Steel Technology Center at IIT Kharagpur is greatly AA 5182 and AA 6022. J Mater Eng Perform 16(4):
appreciated. The authors are also grateful to Maniram Chakraborty 477–484
for his help in carrying out experiments at welding laboratory in 19. Buffa G, Campanile G, Fratini L, Prisco A (2009) Friction
Mechanical Engineering Department at IIT Kharagpur. stir welding of lap joints: Influence of process parameters on
the metallurgical and mechnical properties. Mater Sci Eng A
519:19–26
20. Yazdanian S, Chen ZW, Littlefair G (2012) Effects of friction
References stir lap welding parameters on weld features on advancing side
and fracture strength of AA6060-T5 welds. J Mater Sci 47:
1. Mistikoglu CG (2014) Recent developments in friction stir weld- 1251–1261
ing of Al-alloys. J Mater Eng Performance 23:1936–1953 21. Edwards GA, Stiller K, Dunlop GL, Couper MJ (1998) The
2. Threadgill PL, Leonard AJ, Shercliff HR, Withers PJ (2009) precipitation sequence in Al-Mg-Si alloys. Acta Mater 46:3893–
Friction stir welding of aluminium alloys. Int Mater Rev 3904
54(2):49–93 22. Simar A, Brechet Y, De Meester B, Denquin A, Gallais C, par-
3. Mishra RS, MA ZY (2005) Friction stir welding and processing. doen T (2012) Integrated modeling of friction stir welding of
Mater Sci Eng R 50:1–78 6xxx series Al alloys: Process, microstructure and properties.
4. Nandan R, Debroy T, Bhadeshia HKDH (2008) Recent advances Prog Mater Sci 57:95–183
in friction-stir welding-process, weldment structure and proper- 23. Elangovan K, Balasubramanian V (2008) Influences of tool pin
ties. Prog Mater Sci 53:980–1023 profile and tool shoulder diameter on the formation of friction
5. He X, Gu F, Ball A (2014) A review of numerical analysis of stir processing zone in AA6061 aluminium alloy. Mater Des 29:
friction stir welding. Prog Mater Sci 65:1–66 362–373
6. Hui-jie L, Fujii H, Maeda M, Nogi K (2003) Tensile properties 24. Imam M, Biswas K, Racherla V (2013) Effect of weld mor-
and fracture locations of friction-stir welded joints of 6061-T6 phology on mechanical response and failure of friction stir
aluminum alloy. J Mater Sci Lett 22:1061–1063 welds in a naturally aged aluminum alloy. Mater Des 44:
7. Imam M, Racherla V, Biswas K (2014) Effect of post-weld 23–34
natural aging on mechanical and microstructural properties 25. Kumzerov YA, Parfen’eva LS, Smirnov IA, Krivchikov AI,
of friction stir welded 6063-T4 aluminium alloy. Mater Des Zvyagina GA, Fil VD, Misiorek H, Mucha J, Jezowski A (2005)
64:675–686 Thermal and acoustic properties of chrysotile asbestos. Phy Solid
8. Ren SR, Ma ZY, Chen LQ (2007) Effect of welding parameters State 47(2):370–373
on tensile properties and fracture behavior of friction stir welded 26. Kusiorowski R, Zarimba T, Piotrowski J, Adamek J (2014) Ther-
Al-Mg-Si alloy. Scrip Mater 56:69–72 mal decomposition of different types of asbestos. J Therm Ana
9. Lim S, Kim S, Lee CG, Kim S (2004) Tensile behavior of Calorim 109:693–704
friction stir welded Al 6061-T651. Metal Mater Trans A 35A: 27. Charde N, Yusof F, Rajkumar R (2014) Materials characteriza-
2829–2835 tion of mild steels, stainless steels, and both steel mixed joints
10. Sato YS, Kokawa H, Enomoto M, Shigetoshi J (2429) under resistance spot welding (2-mm sheets). Int J Adv Manuf
Microstructural evolution of 6063 aluminium alloy during fric- Tech
tion stir welding. Metall Mater Trans A:30A 28. Sato YS, Urata M, Kokawa H (2002) Parameters control-
11. Heinz B, Skrotzki B (2002) Characterization of a friction- ling microstructure and hardness during friction-stir welding
stir-welded aluminum alloy 6013. Metall Mater Trans A 33B: of precipitation-hardenable aluminum alloy 6063. Metall Mater
489–498 Trans A 33A:625–635
Int J Adv Manuf Technol (2015) 77:2181–2195 2195

29. Su JQ, Nelson TW, Stirling CJ (2005) Microstructure evolution 31. Zhang HJ, Liu HJ, Yu L (2012) Effect of water cooling on the
during FSW/FSP of high strength aluminium alloys. Mater Sci performances of friction stir welding heat-affected-zone. J Mater
Eng A 405:277–286 Eng Perform 21:118–227
30. Shastry CR, Judd G (1971) A study of grain boundary 32. Lee WB, Yeon YM, Jung SB (2003) Evaluation of the
precipitate-free zone formation in an Al-Zn-Mg alloy. Metal microstructure and mechanical properties of friction stir welded
Trans 2:3283–3287 6005 aluminum alloy. Mater Sci Tech 19:1513–1518

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