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MATERIAL SPECIFICATION
PDVSA N° TITLE
APPRD. Eliecer Jiménez DATE DIC.97 APPRD. Oscar Adrianzén DATE DIC.97
PDVSA
REVISION FECHA
SUPPLEMENTARY SPECIFICATION OF PDVSA
SEAMLESS STEEL TUBULARS 3 DIC.97
FOR SOUR SERVICE Página 1
.Menú Principal Indice manual Indice volumen Indice norma
Index
1 SCOPE . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
2 REFERENCES . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
3 DEFINITIONS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
4 PROCESS OF MANUFACTURE . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
4.1 General . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
4.2 Heat Treatment . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
4.3 Straightening . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
4.4 Steel Deoxidation Process and Inclusion Content Determination . . . . . . 4
4.5 Traceability . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
5 MATERIAL REQUIREMENTS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5
5.1 Chemical Requirement . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5
5.2 Mechanical Property Requirements . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5
6 TOLERANCES ON DIMENSIONS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
6.1 Wall Thickness . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
6.2 Ovality . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
6.3 Dimensions and Weights . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
7 TESTING OF MECHANICAL PROPERTIES . . . . . . . . . . . . . . . . . . . . 9
7.1 Frecuency of Testing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
8 HYDROSTATIC TESTING . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
8.1 Pressure Recorder Calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10
9 THREADING . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10
10 VISUAL INSPECTION . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10
11 NON DESTRUCTIVE INSPECTION (NDI) . . . . . . . . . . . . . . . . . . . . . . 10
11.1 Qualification of Inspection Personnel . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
11.2 Inspection Process Control . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
11.3 Full Body Ultrasonic Inspection (Full Body UT) . . . . . . . . . . . . . . . . . . . . . . 11
12 COUPLING MAKEUP AND THREAD PROTECTION . . . . . . . . . . . . 14
13 MARKING . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14
14 DOCUMENTS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14
15 CERTIFICATION . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15
16 MANUFACTURER CLASSIFICATION . . . . . . . . . . . . . . . . . . . . . . . . . 15
17 SHIPPING . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15
17.1 Release for Shipment . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15
MATERIAL SPECIFICATION PDVSA EM–18–00/01
PDVSA
REVISION FECHA
SUPPLEMENTARY SPECIFICATION OF PDVSA
SEAMLESS STEEL TUBULARS 3 DIC.97
FOR SOUR SERVICE Página 2
.Menú Principal Indice manual Indice volumen Indice norma
PDVSA
REVISION FECHA
SUPPLEMENTARY SPECIFICATION OF PDVSA
SEAMLESS STEEL TUBULARS 3 DIC.97
FOR SOUR SERVICE Página 3
.Menú Principal Indice manual Indice volumen Indice norma
1 SCOPE
This is a supplementary specification to API Specification 5CT, fifth edition, April
1, 1995 (hereinafter referred to as API 5CT), and covers PDVSA’s requirements
for seamless steel tubular of API Group 2 and special sour grades (including
90SS, C100SS and C110SS). Where conflicts arise between this supplementary
specification and API 5CT, the requirements of this specification shall govern.
The manufacturer shall have his quality assurance program in accordance with
ISO 9000. The manufacturer is responsible for complying with all the provisions
of this specification. PDVSA may make any investigation necessary to ensure
compliance and may reject any material or cancel any order for failure to meet this
specification.
All material shall be furnished to meet the requeriments of this specification.
Exception can be made only if permission is garanted by PDVSA in writing.
NOTE: The numbers of this specification are followed by the numbers, in
parenthesis corresponding to the API 5CT paragraphs when there are
modifications to what is stated on API specification.
2 REFERENCES
References given in API 5CT, fifth edition, section 2 shall apply with the following
additions:
S NACE TM0177 last edition, Laboratory Testing of Metals for Resistance to
Sulfide Stress Cracking in H2S Enviroments.
S ISO Guide 22–1982, Information on supplier’s declaration of conformity with
standards or other Technical Specifications.
3 DEFINITIONS
Definitions given in API 5CT, fifth edition, section 3 shall apply with the following
additions:
Lot Size: 100 or fewer lenghts of pipe or coupling stock with the same specified
dimensions and Specified minimun yield strength (SMYS) which are heat treated
in a continuous operation and are from a single heat of steel.
4 (5)PROCESS OF MANUFACTURE
4.1 (5.1) General
4.1.1 (5.1.2) Steel shall be fully killed. All products shall be seamless (S) only. Pup joints
and connectors may be made from standard casing or tubing or by machining
heavy wall seamless pipe. Machining from bar stock is not allowed. Couplings
MATERIAL SPECIFICATION PDVSA EM–18–00/01
PDVSA
REVISION FECHA
SUPPLEMENTARY SPECIFICATION OF PDVSA
SEAMLESS STEEL TUBULARS 3 DIC.97
FOR SOUR SERVICE Página 4
.Menú Principal Indice manual Indice volumen Indice norma
shall only be made from fully processed (heat treated) seamless pipe as defined
in API Specification 5CT, Section 5.1.3. Individually processed (heat treated)
coupling blanks are not allowed.
4.1.2 (5.1.5) The manufacturer shall submit a manufacturing and inspection plan,
complete with aim and accept/reject limits. The written approval of the purchaser
is required for the manufacturing and inspection plan prior to the start of
production.
h v 1 1ń 2
t v 2
PDVSA
REVISION FECHA
SUPPLEMENTARY SPECIFICATION OF PDVSA
SEAMLESS STEEL TUBULARS 3 DIC.97
FOR SOUR SERVICE Página 5
.Menú Principal Indice manual Indice volumen Indice norma
verifiable until the pipe is run into the ground. The number shall identify the
sequence in which the length was tempered to allow analysis of the data, or further
testing if required.
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ÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁ
ÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁ
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Grade Yield Strength Tensile Strength % Minimum
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ÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁ
(ksi) (ksi) Elongation
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min max min
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L–80
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80 95 95 18
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90SS
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90 105 100 18
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T–95 95 110 105 18
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C–100SS
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100 115 110 18
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C–110SS
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110 125 120 18
PDVSA
REVISION FECHA
SUPPLEMENTARY SPECIFICATION OF PDVSA
SEAMLESS STEEL TUBULARS 3 DIC.97
FOR SOUR SERVICE Página 6
.Menú Principal Indice manual Indice volumen Indice norma
at least 95 Ksi, 105 and 115 Ksi, for the grades 90SS, 100SS y 110SS,
respectively.
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ÁÁÁÁÁ
ÁÁÁÁÁÁÁÁÁ ÁÁÁÁ
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ToughnessÁÁÁÁ
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Specimen L80 90SS T95 C100SS C110SS
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Type
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Mean value of 5
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10x10mm 160 160 160 150 130
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ÁÁÁÁ ÁÁÁÁ
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longitudinal specimens
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10x5mm 80 80 80 75 65
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Mean value of 5
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ÁÁÁÁ ÁÁÁÁÁ
10x10mm 120 120 120 115 100
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ÁÁÁÁ ÁÁÁÁ
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transversal specimens
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10x5mm 60 60 60 57 50
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Minimum longitudinal
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10x10mm 120 120 120 100 97
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ÁÁÁÁÁÁÁÁÁ ÁÁÁÁ
ÁÁÁÁÁ ÁÁÁÁ
individual value
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Minimum transversal
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10x5mm
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10x10mm
60
90
60
90
60
90
56
86
48
75
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ÁÁÁÁÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁ
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individual value ÁÁÁÁ ÁÁÁÁÁ
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10x5mm 45 45 45 43 47
a. Hardness Maximums
1. If any hardness reading exceeds the value established in table 3, the entire
lot shall be rejected.
MATERIAL SPECIFICATION PDVSA EM–18–00/01
PDVSA
REVISION FECHA
SUPPLEMENTARY SPECIFICATION OF PDVSA
SEAMLESS STEEL TUBULARS 3 DIC.97
FOR SOUR SERVICE Página 7
.Menú Principal Indice manual Indice volumen Indice norma
Upset tubing:
For hardness testing (HRC), ring specimens are taken from both upset ends of
every 50 joints. One quadrant from both upset ends shall be tested. All the tubings
shall be tested externally in the following sequence:
The first tube: pin end upset
The second tube: pin end body
The third tube: Box end upset
The fourth tube: Box end body
Non upset casing and tubing:
For hardness testing (HRC), ring specimens are taken from alternate ends of
every casing joint.
Coupling Stock:
For hardness testing, ring specimens are taken from both ends of each joint used
for machining coupling stock.
Hardness tests shall be conducted on each test ring as shown on
Fig. 13 of API 5CT specification. Hardness values (defined as the average of
three individual readings taken along a circunferential arc) shall be taken in each
of the four quadrants at the outer, mid wall and inner positions.
The maximum hardness value, reading and permisible variations within any one
quadrant are listed in Table 3.
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Grade
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ÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁ
ÁÁÁÁÁÁ ÁÁÁ
ÁÁÁÁÁÁÁÁÁÁÁÁ
Maximum Average
ÁÁÁ HRC reading MAX HRC VARIATION
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ÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁ
ÁÁÁÁÁÁ
ÁÁÁÁÁÁ ÁÁÁ
Hardness value, HRC
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max for wall thickness in inch
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ÁÁÁ
0.5 or less 0.5 to 1 1
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L–80
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22
ÁÁÁ 23 3 3.5 4
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90SS
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ÁÁÁÁÁÁ
ÁÁÁÁÁÁÁ
24
ÁÁÁ 26 3 3.5 4
ÁÁÁÁÁ
ÁÁÁÁÁÁÁÁÁÁ
T–95
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ÁÁÁÁÁÁ
ÁÁÁÁÁÁÁ
25
ÁÁÁ 26 3 3.5 4
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ÁÁÁÁÁÁÁÁÁÁ
ÁÁÁÁÁÁ
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ÁÁÁÁÁÁ
ÁÁÁÁÁÁ
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ÁÁÁ
C–100SS 26 28 3 3.5 4
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ÁÁÁÁÁÁÁÁÁÁ
C–110SS
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ÁÁÁÁÁÁ
ÁÁÁÁÁÁÁ
28
ÁÁÁ 30 3 3.5 4
PDVSA
REVISION FECHA
SUPPLEMENTARY SPECIFICATION OF PDVSA
SEAMLESS STEEL TUBULARS 3 DIC.97
FOR SOUR SERVICE Página 8
.Menú Principal Indice manual Indice volumen Indice norma
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Grade Threshold stress Threshold stress Test duration hours
% SMYS psi
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L–80*
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ÁÁÁÁÁÁÁÁ90 72000 720
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90SS
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ÁÁÁÁÁÁÁÁ90 81000 720
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T–95
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ÁÁÁÁÁÁÁÁ90 85500 720
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ÁÁÁÁÁÁÁÁÁ
ÁÁÁÁÁÁÁÁ
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ÁÁÁÁÁÁÁÁ
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C–100SS 85 85000 720
C–110SS 85 93500 720
PDVSA
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SEAMLESS STEEL TUBULARS 3 DIC.97
FOR SOUR SERVICE Página 9
.Menú Principal Indice manual Indice volumen Indice norma
6.2 Ovality
The maximum ovality on the pipe body shall be limited to 0,7% as determined by
the following formula:
% Ovality= ODmax–ODmin x 100
OD avr
OD: Outer diameter
The ovality testing procedure and frecuency is at the manufacture’s discretion.
PDVSA
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SEAMLESS STEEL TUBULARS 3 DIC.97
FOR SOUR SERVICE Página 10
.Menú Principal Indice manual Indice volumen Indice norma
or manufacturer specifications for API threads. For premium thread, pipe will be
hydrostatic pressure tested on plain end material. Each pipe shall be dried with
efficiency in order to avoid the start of surface corrosion.
Test pressure shall be held for a minimum of 10 seconds.
Pressure recording charts showing joint number, test pressure, and hold time
shall be maintained.
The pressure recorder used the record test pressure shall have a full scale
capacity on not more than 200% of the hydrotest pressure.
9 (7.13.6) THREADING
API pipe and coupling threads, gauging practice, and thread inspection shall
conform to the requirements of API Std. 5B. As a minimum, one (1) different
element of a thread shall be checked on each threaded end and one (1) out of ten
(10) joints shall receive 100% thread inspection in accordance with a documented
procedure. The documented procedure shall demonstrate that all aspects of the
product are within specification to a reliability of 98% (2% AQL) at a confidence
level of 95%. In addition, proprietary threads shall conform to PDVSA
Specification, Requirements for Proprietary Casing and Tubing Connections.
10 (9.6)VISUAL INSPECTION
Visual inspection on tubes, coupling stock, pup joints and connector material shall
be conducted in accordance with API 5CT, paragraph 9.6.
Visual inspection on finished threads shall be conducted in accordance with the
manufacturer’s written procedure, as reviewed, amended and approved by
PDVSA.
PDVSA
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FOR SOUR SERVICE Página 11
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Inspection Requirements
Pipe Body Inspection: For all pipe, the EMI and / or the UT methods shall be used
to comply whith paragraph 9.7.2.1 (API 5CT). The first method is permitted to be
applied in pipes with thickness no greater than 0.5 inches.
MPI is not an aceptable pipe body inspection method. All inspections shall take
place after final heat treatment and hot rotary straightening operations or stress
relieving.
Pup joints: For pup joints machined from pipe, the required inspetions shall take
place after machining to final product dimensions.
Coupling Stock inspection: Coupling stock shall be inspected in the same manner
as pipe.
Pipe Inspetion coverage
Pipe upsets: Forged upsets (including the upset runout interval) on all grades shall
be inspected for transverse, outside and inside surface defects by wet MPI. The
inspection shall take place after all heat treatment.
PDVSA
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SEAMLESS STEEL TUBULARS 3 DIC.97
FOR SOUR SERVICE Página 12
.Menú Principal Indice manual Indice volumen Indice norma
standards shall be steel of the same nominal diameter, wall thickness, surface
finish and heat treatment as the production pipe.
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TABLE 5. CALIBRATION (REFERENCE) STANDARDS
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ÁÁÁÁÁÁÁÁÁÁ
PDVSA
ÁÁÁÁÁÁÁ
ÁÁÁÁÁÁÁÁ
Notches Notch Depth Notch wall area
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ÁÁÁÁÁÁÁÁÁÁ
Grades
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ÁÁÁÁÁÁÁÁ
required (% NWT) (% NWT)
ÁÁÁÁÁÁ
ÁÁÁÁÁÁÁÁÁÁ
All
ÁÁÁÁÁÁÁ
ÁÁÁÁÁÁÁÁ
Longitudinal OD & ID 5 93
ÁÁÁÁÁÁ
ÁÁÁÁÁÁÁÁÁÁ
ÁÁÁÁÁÁÁ
ÁÁÁÁÁÁÁÁ
Transverse OD & ID 5 93
c.
ÁÁÁÁÁÁ
ÁÁÁÁÁÁÁÁÁÁ
ÁÁÁÁÁÁÁ
ÁÁÁÁÁÁÁÁ
Oblique OD & ID 5 93
Reduced wall thickness area: Each calibration (reference) standard shall also
have an area of reduced wall thickness not larger than 1/2 inch by 1 inch. The
short dimension of the reduced wall thickness area shall be longitudinally oriented
relative to the pipe. The reduced wall thickness area will have the remaining wall
thickness given in Table 5 for each reference standard.
d. Dynamic calibration:
S Frequency: Dynamic calibration shall be performed on the full body ultrasonic
unit at the beginning and end of each production run, or if the vendor chooses,
at a shorter interval. If any calibration check fails, all material inspected since
the last successful calibration check must be reinspected.
S Procedure: The reference standard shall be scanned at the normal inspection
speed and helix a total of four times, once each with the standard entering the
scan unit at 12, 3, 6 and 9 o’clock positions. The signal from any reference
notch shall not be less than 90% of the reference level for that notch on any
dynamic calibration run. The signal from the reduced wall area shall indicate
not more than 1 % wall thickness above the thickness of the reduced wall area.
e. Scanning sensitivy level: Production scanning shall be performed at a gain setting
of 6 db above the reference level gain setting. Any indication that produces a
signal that equals or exceeds the signal from any reference notch shall be
evaluated (proven up).
f. Scanning: Other than the increased gain setting noted above, scanning shall be
performanced at the same speed and helical advance and with the same couplant
as was used for the dinamyc calibration.
MATERIAL SPECIFICATION PDVSA EM–18–00/01
PDVSA
REVISION FECHA
SUPPLEMENTARY SPECIFICATION OF PDVSA
SEAMLESS STEEL TUBULARS 3 DIC.97
FOR SOUR SERVICE Página 13
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PDVSA
REVISION FECHA
SUPPLEMENTARY SPECIFICATION OF PDVSA
SEAMLESS STEEL TUBULARS 3 DIC.97
FOR SOUR SERVICE Página 14
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13 (10) MARKING
Markings shall be in accordance with appendix D of API Specification 5CT. The
products manufactured to this specification shall be marked only with paint
stencilling.
14 (13) DOCUMENTS
The manufacturer / vendor shall furnish a declaration of conformity, i.e. certificate
of compliance stating that the material has been manufactured, sampled, tested,
and inspected in accordance with this specification and has been found to meet
the specified requirements, as per ISO Guide 22–1982. API Specification 5CT,
Appendix BSR15 shall also apply to this specification.
MATERIAL SPECIFICATION PDVSA EM–18–00/01
PDVSA
REVISION FECHA
SUPPLEMENTARY SPECIFICATION OF PDVSA
SEAMLESS STEEL TUBULARS 3 DIC.97
FOR SOUR SERVICE Página 15
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15 (13.1) CERTIFICATION
The manufacturer shall submit a quality control certificate with the values of the
following test results for the pipe and the coupling.
S Inclusions level
S Grain size for each heat treated
S Chemical analysis for each heat
S Product chemical analyses for each heat
S Tensile tests including elongation
S Toughness test
S Hardness test.
S Sulfide stress corrosion cracking (SSCC) and metallography report of the
samples tested.
16 MANUFACTURER CLASSIFICATION
16.1 New manufacturer shall submit to PDVSA prior to order placement, the statistical
production reports (Histogram), of the following items:
S Mechanical properties: Sy, Su, elongation
S Hardness variations through the thickness
S Fracture toughness (transversal and longitudinal)
S Chemical composition.
S Sulfide stress corrosion cracking (SSCC)
16.2 In adition, the manufacturer shall submit a plan for quality control assesment to
be approved by PDVSA prior to order placement.
17 (14) SHIPPING
17.1 (14.1) Release for Shipment
Pipe may not be shipped until the certificate of compliance and the mill test report
have been received and reviewed by PDVSA. Review of the mill test report will
normally take a period of five(5) working days. This review, at the option of
MATERIAL SPECIFICATION PDVSA EM–18–00/01
PDVSA
REVISION FECHA
SUPPLEMENTARY SPECIFICATION OF PDVSA
SEAMLESS STEEL TUBULARS 3 DIC.97
FOR SOUR SERVICE Página 16
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PDVSA, may be conducted on preliminary mill test reports. The results of sulfide
stress corrosion cracking tests shall be available prior to shipment of the pipe. The
manufacturer (or processor) may ship the product prior to certification at their sole
risk.
19 REJECTS
PDVSA has the right to reject the products with mechanical propertier higher than
the evaluated pipe in the sulfide stress corrosion cracking test (SSCC). In this
case, a new test series is mandatory.
MATERIAL SPECIFICATION PDVSA EM–18–00/01
PDVSA
REVISION FECHA
SUPPLEMENTARY SPECIFICATION OF PDVSA
SEAMLESS STEEL TUBULARS 3 DIC.97
FOR SOUR SERVICE Página 17
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20 BIBLIOGRAPHY
LAGOVEN, Specification for seamless steel tubular, last edition.
CORPOVEN P2, Supplementary specification to API 5CT for seamless casing,
last edition.
MATERIAL SPECIFICATION PDVSA EM–18–00/01
PDVSA
REVISION FECHA
SUPPLEMENTARY SPECIFICATION OF PDVSA
SEAMLESS STEEL TUBULARS 3 DIC.97
FOR SOUR SERVICE Página 18
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1.APPENDIX A
The samples for the SSCC test must be taken from the hardest pipe of the
processed heat, and from the midwall part of the pipe as ilustrated in Fig. 1.
SSCC SPECIMEN
HARDNESS TEST RING