FARABI YANBU P

PETROCHE
EMICALS CO
OMPANY

FARAB
BI NORMALL PARAFFIN
N AND DERIIVATIVES
COMPL
LEX, YANBU
U, KINGDOM
M OF SAUDDI ARABIA

G446-082
28-2810-QA
A-0100-0050
PMMI PROCEDDURE
FOR DEMIN
NERALIZATIO
ON PACKAG
GE

EMPLOYER R : FARABI Y
YANBU PET TROCHEMICCALS COMP PANY
PROJECT : FARABI N
NORMAL PA ARAFFIN ANND DERIVAATIVES COM
MPLEX
EPC CONTRRACTOR : L&T HYDRROCARBON N ENGINEERING
LTHE JOB NO : G446
PR NO : G446-2810
0-MR-0100-0005
VENDOR
V NAME : ION EXCHHANGE IND
DIA LIMITED
D
ITEM DESC
CRIPTION : DEMINERRALIZATIONN PACKAGEE (810-ME-01)
ITEM TAG : 810-ME-01
1

DOCUMENT
CATEGOORY APPROVA
AL CODES / REVIEW APP
PROVAL COODES / REVIIEW
(USE TICK MARK) ST
TATUS- LTH
HE STA
ATUS- PMC / EMPLOYEER

[CODE 1] REEJECTED [CODE 11] REJECTEED

R
Revise and Resubmit.
R Revise a
and Resubmit.
A
[CODE 2] COOMMENTS A AS NOTED [CODE 22] COMMEN NTS AS NOT TED
W
Work may prroceed subje
ect to Work maay proceed subject
s to
c
compliance w and inco
with orporation off nce with and incorporatio
complian on of
R c
comments. comments.

[CODE 3] NOO COMMENNTS [CODE 3

3] NO COMM MENTS
W
Work may prroceed. Work ma
ay proceed.
I
[CODE 4] INFORMATIO ON ONLY [CODE 44] INFORMA ATION ONLY Y
A
Accepted forr information only. Accepted
d for informa
ation only.
LTHE APPROVAL EMPLOYER Approval
A
DISCIPLINE Quality DISCIPLINE
PREPARED BY --- SIGNATURE
REVIEWED BY Ritesh Datta mm-yy)
DATE ( dd-m
APPROVED BY CODE
Date ( dd-mm-yy) 16-Dec-17
Code Code-3 This approvval does not abso olve the CONTRA ACTOR
from meetinng their contractuual obligation of delivering
d a
This review / apprroval does not re
T elieve the vendor complete, sa afe and efficiently operating unit/ffacilities
/ manufacturer of the full responsibility as to design
n meeting all rrequirement of thhe contract
mensions & comp
correctness of dim pliance with all
a
applicable regulattions and with the
e requirements
m
made in purchaseer specifications.

Issu
ued for Review
w
02
0 29-No
ov-17 GP NT
T M
MR SG RS
(IFR)
Issu
ued for Review
w
01
0 14-Se
ep-17 GP NT
T M
MR SG RS
(IFR)
PREPAR
RED REVIEWWED ROVED
APPR VIEWED
REV AP
PPROVED
Rev
R Datte DE
ESCRIPTION
BY BYY B
BY BY BY

ALL
A RIGHTS RESERVE
VED
TH
HIS DOCUMENT ANDD ANY DATA AND IN NFORMATION CONT TAINED THEREIN AR
RE CONFIDENTIAL AN ND THE PROPERTY OF L&T HYDROCAR RBON ENGINEERING (LTHE) AND
TH
HE COPYRIGHT THER
REIN IS VESTED IN LTC NO PART OF THIS
S DOCUMENT, DATA,, OR INFORMATION SHALL
S BE DISCLOSE
ED TO OTHERS OR RE
EPRODUCED IN ANY MANNER
M OR
USED FOR ANY PURPO
OSE WHATSOEVER E EXCEPT WITH THE PRIOR
P WRITTEN PERM
MISSION OF LTC
 FARABI YANBU PETROCHEMICALS COMPANY

FARABI NORMAL PARAFFIN AND DERIVATIVES

COMPLEX, YANBU, KINGDOM OF SAUDI ARABIA

G446-0828-2810-QA-0100-0050
PMI PROCEDURE
FOR DEMINERALIZATION PACKAGE

REVISION HISTORY SHEET

S. Rev. Page Clause /
No. No. Line No. Brief Description / Reason of Revision Remarks
No.
1 01 - - Issued For Review
2 02 1-8 - Revised as per Contractors Comments

Page 2 of 9
 FARABI YANBU PETROCHEMICALS COMPANY

FARABI NORMAL PARAFFIN AND DERIVATIVES

COMPLEX, YANBU, KINGDOM OF SAUDI ARABIA

G446-0828-2810-QA-0100-0050
PMI PROCEDURE
FOR DEMINERALIZATION PACKAGE

CONTENT

1.0 Purpose…………………………………………………………………………………………….4

2.0 Scope & Extent of PMI………..………………………………………………………………….4

3.0 References…………………………………………………………………………………………5

4.0 Requirements………………………………………………………………………………………5

5.0 Time of Examinations……………………………………………………………………………..6

6.0 Method of Identification……………………………………………………………………………6

7.0 Alloy Acceptance ………………………………………………………………………………….7

8.0 Traceability………………………………………………………………………………………….8

9.0 PMI Certificate ……………………………………………………………………………………..8

Appendix 1: Sample Report Format: PMI………............................................................…….…...9

Page 3 of 9
 FARABI YANBU PETROCHEMICALS COMPANY

FARABI NORMAL PARAFFIN AND DERIVATIVES

COMPLEX, YANBU, KINGDOM OF SAUDI ARABIA

G446-0828-2810-QA-0100-0050
PMI PROCEDURE
FOR DEMINERALIZATION PACKAGE

1.0 PURPOSE

This procedure defines basic requirements for conducting Positive Material Identification (PMI) test to
verify that the elemental composition of Alloy Materials is as specified in the purchase document, and
that the materials, equipment are marked and stamped to indicate the proper alloy. PMI is the
process by which alloy composition is verified and is independent of any material certification and
material control requirements. PMI shall not be considered a substitute for material certification.

2.0 SCOPE

The following items shall be conducted Positive Material Identification (PMI) testing and reports shall be
included into final documentation.

TAG NO DESCRIPTION MOC EXTENT OF PMI

Shell – 02 readings
Cover – 02 readings
Nozzle – All
Flanges – All
810-TK-01 NaOH Dosing Tank SS 316 Each Weld – 1 Reading
Welding consumable – 1
Reading per Batch
Other Attachments - All
Rod – 01 Reading
810-ME-04 Agitator for NaOH Dosing Tank SS 316 Impeller blade – 01 Reading
Other attachment – 01 Reading
Rod – 01 Reading
810-ME-05 Agitator for Antiscalent Dosing Tank SS 316 Impeller blade – 01 Reading
Other attachment – 01 Reading
Rod – 01 Reading
810-ME-06 Agitator for SMBS Dosing Tank SS 316 Impeller blade – 01 Reading
Other attachment – 01 Reading
Shell – 02 readings
Cover – 02 readings
Nozzle – All Flanges
– All
810-ME-01 A/B Micron Cartridge Filter SS 316 Each Weld – 1 Reading
Welding consumable – 1
Reading per Batch
Other Attachments - All
Shell – 02 readings
Cover – 02 readings
Nozzle – All
Flanges – All
810-ME-03 Cartridge Filter for RO Cleaning SS 316 Each Weld – 1 Reading
Welding consumable – 1
Reading per Batch
Other Attachments - All
810-P-01 A/B RO Feed Pumps – Casing & Weld SS 316 100%

Page 4 of 9
 FARABI YANBU PETROCHEMICALS COMPANY

FARABI NORMAL PARAFFIN AND DERIVATIVES

COMPLEX, YANBU, KINGDOM OF SAUDI ARABIA

G446-0828-2810-QA-0100-0050
PMI PROCEDURE
FOR DEMINERALIZATION PACKAGE

810-P-04 A/B NaOH Dosing Pumps – Casing & Weld SS 316 100%
810-P-02 A/B RO High Pressure Pumps - Casing & Weld SS 316L 100%
810-P-03 A/B Cleaning Pumps - Casing & Weld SS 316 100%
Unloading Pump for NaOH - Casing &
810-P-08 Weld
SS 316 100%
AS PER DRG. - Welds of Piping Spools SS 316 100%
- Components forming part of SS 316 100%
fabricated piping spools
AS PER DRG. Tank Internal & External attachments SS 316 100%
AS PER
Instruments
DATASHEET
- Conductivity, ORP, pH Transmitter –
Flow through chamber
SS 316 100%
- Differential pressure transmitter -
Manifold
SS 316 100%
- Differential pressure flow transmitter
– orifice & Manifold
SS 316 100%
- Pressure Indicator – Snubber &
Diaphragm
SS 316 100%

- Pressure Transmitter - Manifold SS 316 100%

NA Fasteners SS 316 100%

Note: 1] If any other alloy material is identified/added in this specific package, same shall be PMI Tested
according to this procedure.
.

3.0 REFERENCES

067401-0000 JSS 6300 004 A Positive Alloy Material Identification of Equipment and Piping
ASME Sec II A, B & C Material Specifications for Ferrous and Non-ferrous materials
API RP 578 Material verification program for new and existing alloy piping
Systems

4.0 REQUIREMENTS

4.1 Pressure Components

All pressure components shall be PMI tested as per mentioned in above section 2.0

4.2 Exemption from PMI

Following items are exempted from PMI
1) Internal parts for machinery and machinery auxiliary system, like pumps.
2) Metallic flexible hoses, hose couplings.
3) Gaskets (Except RTJ)

Page 5 of 9
 FARABI YANBU PETROCHEMICALS COMPANY

FARABI NORMAL PARAFFIN AND DERIVATIVES

COMPLEX, YANBU, KINGDOM OF SAUDI ARABIA

G446-0828-2810-QA-0100-0050
PMI PROCEDURE
FOR DEMINERALIZATION PACKAGE

4.3 Weld Examination

Welds shall be tested after removal of slag or oxide from the weld surface. On double-sided solid alloy
weld joints, both inside and outside weld surfaces shall be tested.
4.4 Personnel Qualification
Personnel operating the test instrument shall be registered with the Radiation Protection Inspectorate
and fully conversant with NITON XL or XLP series, X-Ray Fluorescence Analyzer’s Operation Manual.

5.0 TIME OF EXAMINATION

The positive material identification checks shall be performed during and / or after fabrication is
completed. Equipment internals and other items, shall be checked and verified just prior to installation to
avoid any substitutions. All checks shall be performed prior to any required heat treatment or other
special processing, at seller's option, but shall not be performed until all welding is completed.

6.0 METHODS OF IDENTIFICATION

6.1 General
The instruments or methods used for positive material identification shall have the capability to
Identify positively and to provide a quantitative measurement of the alloying elements listed in
Section 7.0.

6.2 Identification Equipment

6.2.1 For PMI verification, the following methods or their close equivalents shall be used and
also note that any one of instruments as below mentioned in (i) shall be used.
(i) Niton XL-800 series or XLP series multi-element analyser (XRF)
Texas Nuclear Analyser Models 9266/9277
Spectroport or Spectrotest 'F'
Metorex X-met 2000/3000
Metorex Arc-Met

6.2.2 Chemical spot tests, magnets, alloy sorters and methods are not performed.

6.2.3 All PMI instruments shall be calibrated, in accordance with the instrument manufacturer’s
recommendation, at the start of each working shift as a minimum.
6.2.4 Certified samples, with full traceability, of "known" alloy materials shall be available for use as a random
spot check on the instrument calibration. These samples are in addition to any standard manufacturer's
calibration.sample.

Page 6 of 9
 FARABI YANBU PETROCHEMICALS COMPANY

FARABI NORMAL PARAFFIN AND DERIVATIVES

COMPLEX, YANBU, KINGDOM OF SAUDI ARABIA

G446-0828-2810-QA-0100-0050
PMI PROCEDURE
FOR DEMINERALIZATION PACKAGE

6.2.5 Surfaces to be examined shall be prepared by light grinding or abrasive paper and solvent cleaning.
Evidence of ‘arc burn’ resulting from the examination shall be removed by light grinding or abrasive
paper.
6.2.6 When the portable analyzer is unable to identify the material, an approved laboratory method shall be
used to analyze the composition of the material. The laboratory procedures for sample removal,
identification and traceability to the original material shall be submitted to Purchaser for review prior to
start of testing.

7.0 ALLOY ACCEPTANCE

All materials shall comply with the requirements of the applicable material specification. Materials shall
be verified to ensure the correct major alloying elements and the correct percentages of each element
where applicable. A deviation of the alloying elements / or absence of the alloying elements with
respect to the required material specification shall be considered non acceptable. A detailed Chemical
analysis may be performed in a laboratory for the materials having very nominal deviation of Alloying
Elements from the acceptable limits, as a referee method, before rejecting the material. In such cases
a final decision to accept or reject is left to the Purchaser / Company. All rejected
materials that are identified shall be quarantined until an investigation is carried out.
As a minimum, the elements listed in Table 2 (given below) shall be verified.
Table 2
Material Elements
304 /304 L Cr, Ni, Mo, Nb (Cb), Ti
310 Cr, Ni, Mo, Nb (Cb), Ti
309/309 L Cr, Ni, Mo, Nb (Cb), Ti
309 Nb Cr, Ni, Mo, Nb (Cb), Ti
316 / 316 L Cr, Ni, Mo, Nb (Cb), Ti
321 Cr, Ni, Ti, Nb (Cb)
347 Cr, Ni, Nb (Cb), Ti
904 / 904L Ni,Cr,Mo, Cu
S31803 Cr,Ni,Mo
S32750 Cr,Ni,Mo
Inconel 182/82 Ni, Cr
Inconel 625 Ni, Cr, Mo, Nb(Cb) + Ta, Ti, Fe
Incoloy 825 Cr, Ni, Mo, Ti, Fe

Page 7 of 9
 FARABI YANBU P EMICALS CO
PETROCHE OMPANY

BI NORMAL
FARAB N AND DERIIVATIVES
L PARAFFIN
COMPL
LEX, YANBU
U, KINGDOM
M OF SAUDDI ARABIA

G446-082
28-2810-QA
A-0100-0050
PMMI PROCEDDURE
FOR DEMIN
NERALIZATIO
ON PACKAG
GE

Admiralty Brass Cu, Sn, As

s
Alum
minium Brass Cu, Al, Zn
Cuprro-nickel (70--30) Cu, Ni
Cuprro-nickel (90--10) Cu, Ni
Mone
el 400 Cu, Ni
Titan
nium Ti

Note: The ab
bove list of material
m is nott exhaustive, and shall no
ot be constru
ued as limiting
g the alloy m
materials
subjectt to PMI. Any
y repair and re-verification
r n of alloy con
ntent shall be
e at Supplier’’s expense unless the
materia
al has been supplied
s by Purchaser.
P

8.0 TRACEABILITY
PMI accepted material should be identified as "PMI". The preferred marking methods are low stress
stamps or vibra-etch. If not possible by this method, material shall be identified by permanent marker.
The marking shall be carried out with a water-soluble material that contains no harmful substance,
such as metallic pigments, sulphur or chlorides which would attack or otherwise harmfully effect
austenitic or nicked alloy steels at ambient or elevated temperatures.

9.0 PMI CERTIFICAT

TE
PMI Re
eport shall ha
ave following
g info as minimum or attacched sample ppendix 1 sha
e report in Ap all be
followe
ed.
P.O Nu
umber
Proced
dure Referen
nce
Item/co
omponent nu me & Drawin
umber or Nam ng Reference
e
Item Description
D
Materia
al Type
Materia
al Certificate
e No.
Materia
al Supplier
Qty per lot/heat
PMI Re
eport No. & Date
D
Accepttance & Reje
ection
Signature of Inspec ndent Inspecttor as applica
ctor/ Indepen able.

Above forms shall be

b prepared and signed b
by Supplier in
n accordance equirements.
e with ITP re
Reportts shall be file ection of Manufacturing Data Records.
ed in NDE Se
 FARABI YANBU PETROCHEMICALS COMPANY

FARABI NORMAL PARAFFIN AND DERIVATIVES

COMPLEX, YANBU, KINGDOM OF SAUDI ARABIA

G446-0828-2810-QA-0100-0050
PMI PROCEDURE
FOR DEMINERALIZATION PACKAGE

Appendix 1: Sample Report Format

POSITIVE ALLOY MATERIAL (PMI) IDENTIFICATION REPORT

REPORT REF : DATE OF TEST :

1. GENERAL DETAILS:
EMPLOYER :
PROJECT :
EPC CONTARCTOR :
(IEIL) JOB NO. :
(IEIL) P.O. REF. NO. :

2. ITEMS DESCRIPTION:
EQUIPMENT NAME :
TAG NO. :
MATERIAL GRADE :

3. REFERENCE DOCUMENTS:
DOCUMENT TITLE LTHE DOC. NO. IEIL DOC.NO. REV.
INSPECTION AND TEST PLAN :
PMI PROCEDURE NO. :
G.A.DRAWING NO. :

4. INSTRUMENT DETAIL:
INSTRUMENT NAME : CALIB. DUE DATE :
SERIAL NO : LAST SERVICE DATE :

5. TESTING DETAIL:
ALLOY CONTENT, WEIGHT PERCENTAGE / ACTUAL OBSERVATIONS
REMARKS
ELEMENTS
ACCD / REJD
SPECIFIED RANGE

ITEM IDENTIFICATION NO.

……..Shall be continued with additional sheets for additional

Details

PMI OPERATOR’S SIGN SUB SUPPLIER CLIENT / TPI

Page 9 of 9