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Article history: This paper presents an extensive experimental study to investigate the possibility of using sugarcane
Received 2 February 2018 bagasse ash (SCBA) as a partial replacement of cement in ordinary, lightweight, and self-compacting con-
Received in revised form 30 May 2018 cretes. For this purpose, specimens containing 5, 10, 15, 20, and 25% SCBA in addition to a control spec-
Accepted 17 June 2018
imen were prepared. To evaluate the mechanical properties of concrete specimens, compressive strength,
tensile strength, impact resistance, workability, water absorption, and ultrasonic pulse velocity (UPV)
tests were performed. The results indicated that improvements in strength and impact resistance in light-
Keywords:
weight concrete are observed as compared with the control sample when cement was replaced with
Sugarcane bagasse ash
Ordinary concrete
bagasse ash at 5%. It was also found incorporation of BA improved durability and quality of SCC.
Lightweight concrete Ó 2018 Published by Elsevier Ltd.
Self-compacting concrete
Mechanical properties
Impact resistance
Ultrasonic pulse velocity
https://doi.org/10.1016/j.conbuildmat.2018.06.153
0950-0618/Ó 2018 Published by Elsevier Ltd.
S.A. Zareei et al. / Construction and Building Materials 184 (2018) 258–268 259
2.1.2. SCBA
Bagasse burns at temperature levels between 500 and 550 °C Sugarcane bagasse consists of approximately 50% of cellulose,
and produces raw bagasse ash. It is found that for every ten tons 25% of hemicelluloses, and 25% of lignin [34]. Each ton of sugarcane
of sugarcane crushed in a sugar mill, generally about three tons generates approximately 26% of bagasse at a moisture content of
of bagasse is produced [20]. The main constituents of SCBA include 50% and 0.62% of the residual ash [35]. The chemical composition
cellulose, hemicellulose, lignin, ash, and wax [21]. It is shown that of the residual ash mainly consists of silicon dioxide (SiO2) [24].
improvements in mechanical properties such as tensile and flexu- The ash used in this study was brought from Seven Hills Province
ral strength, flexural modulus, hardness, and impact resistance can located in Khuzestan city, Iran. The ash was dry and black and it
be obtained by optimizing the processing methods, or applying was heated at 700 °C for 1 h and then it was used to replace cement
chemicals to produce modified supplementary materials [22]. at different percentages. Fig. 2 shows the raw and burnt SCBA
Raw bagasse ash (BA) with large particle size and high porosity material. Fig. 3 shows the X-ray diffraction (XRD) of as-received
requires more water, which results in lower compressive strength SCBA, where the high amount of quartz and calcite indicates bio-
of concrete; however, when ground up into small particles the mass burnt at a high temperature, which was in agreement with
compressive strength significantly increases [23]. It was observed the results obtained by Arif et al. [36], whose XRD data showed a
that the compressive strength of concrete containing 15% BA as predominance of quartz with no or little pozzolanic activity. The
partial replacement of cement had improved [24]. Radkeh et al amount of quartz in SCBA is due to the presence of sand adhered
showed that strength properties slightly changed by replacing to the sugarcane. The amount of sand is about 2% in weight even
cement with up to 10% BA and then the strength decreased with after washing the harvested sugarcane bagasse [37], which
higher values of BA. Rukzon et al. [25,26]. increases after the loss of organic matter. Scanning electron micro-
Results of some studies [25–28] reported improvements in scopy (SEM) was used to examine the microstructure of BA as
durability. Chemical and physical properties of hardened concrete shown in Fig. 4. Burnt silica particles with irregular structure cause
such as the compressive strength, splitting tensile strength, and lesser fluidity. The similar results were observed in the previous
water absorption indicated the effects of incorporating SCBA in studies on fly ash with spherical shape as the reason of better
concrete. Chusilp et al. [29] evaluated the mechanical properties workability [38] or in the case of silica-fume and metakoaline, with
of concrete containing BA ranging from 3 to 10% and reported lesser fluidity [39,40].
improvements in strength compared to the reference sample. The
optimum percentage of BA was obtained equal to 30%, which led 2.1.3. Micro-silica
to higher compressive strength and lower water permeability at The amount of micro-silica was controlled to be constant in all
the ages of 28 and 90 days [30]. mixes at 10% with particle size of 0.1 lm. As stated before, the poz-
Payá, J., J. et al. reported that combustion produces ashes with zolanic properties of sugarcane bagasse ash is partly due to the
high amount of unburnt matter, silicon, and aluminum oxides high volume of silica [29,41–43]. Paya et al. showed that combus-
[31]. The pozzolanic materials contain high amount of amorphous tion produces ashes with high amount of unburnt matter, silicon,
silica, which possibly react with the free lime produced from the and aluminum oxides [31]. Because of proper pozzolanic activity,
hydration of cement, leading to the formation of new silicate bagasse ash has been suggested as an excellent alternative com-
hydrate, which significantly improves the mechanical properties pendious material in some studies.
as well as the durability of concrete [28,32,33]. Furthermore, it was found that the particle size has a significant
The purpose of this research is to utilize the sugarcane bagasse effect on the pozzolanic activity of the ash, i.e., the smaller the par-
ash (SCBA) as partial replacement of cement in concrete to reduce ticle size the larger the surface area, resulting in a greater reactivity
the environmental impacts of disposing this waste material. For [44]. Cordeiro et al. concluded that a good correlation exists
this purpose, concrete specimens with 5, 10, 15, 20, and 25% SCBA between the specific surface area, that is, the surface area
were manufactured for three types of concretes including ordinary, associated with the measured particle size distribution, and the
Table 1
The physical properties of cement, SCBA, and micro-silica.
Properties Density Specified surface Compressive strength Bulk density Fineness Water Particle size
(g/cm3) area of Blain (g/cm2) at 28 days (MPa) (g/cm3) modulus absorption (lm)
Cement 3.17 3800 40.3 1.13 – – 13
SCBA 1.51 2600 – – 1.04 0.8 0.4 0.5
Micro-silica 2.33 2 105 – 0.65 – – 0.1 0.2
260 S.A. Zareei et al. / Construction and Building Materials 184 (2018) 258–268
was shown that BA particles are smaller than that of cement, while
Q Q: Quartz micro-silica particles are much smaller than that of BA and cement.
C: Crystobalite
Ca Ca: Calcite It was found that the particle size has a significant effect on the
pozzolanic activity of the ash, i.e., the smaller the particle size the
larger the surface area resulting in a greater reactivity [44].
X-ray counts
pozzolanic activity of the residual RHA. Fig. 5 shows the particle 2.1.4. Aggregates
size distribution of SCBA [42]. The particle size distribution was Crushed gravel with particle size of 4.75–19 mm and density of
obtained by using a LA-960 Laser Particle Size Analyze HORIBA. It 2650 kg/m3 were used as coarse aggregates for ordinary and
100 micro-silica were considered for all concrete mixtures. In the mix-
90 ing process, dry materials were firstly poured in the mixer to be
80 mixed for 2 min. Then, half of the required water and cementitious
Passing percentage (%)
70 materials were added to the mixture and mixed for 3 min. Finally,
60 a solution made from remaining water and the super-plasticizer
50 were added to be mixed for 5 min. The paste preparation method,
40 type of mixer, and time of adding super-plasticizer are among the
30 key factors influencing cement and super-plasticizer interaction
20
[46]. The cast specimens were demoulded after 24 h and were
10
immersed in water at 23 °C to be cured until the required age,
0
1 10 100 i.e., 28 days. The concretes mix designs are presented in Table 3.
Sieve mesh size (µm)
Cement Silica fume SCBA
2.3. Methods
Fig. 5. Particle size distribution of cement, silica fume, and SCBA.
Table 4 presents the standard test methods used to evaluate the
fresh and hardened concrete properties. For the fresh ordinary and
Table 2 lightweight concrete, slump test was conducted according to ASTM
The chemical composition of cement, SCBA, and micro-silica. C143/C143M-12 [47] and fresh density was determined based on
Compound Na2 O Cao K2O Fe2 O3 SiO2 Al2 O3 MgO ASTM C138/C138M-14. For the fresh self-compacting concrete
Cement 0.1 66.1 0.6 2.5 21.5 6 2 (SCC) some specific tests were conducted. These tests are designed
SCBA 0.87 8.17 1.32 5.47 64.23 9.08 2.97 to evaluate the fresh SCC in terms of filling ability, passing ability,
Micro-silica 0.29 0.11 0.25 1.1 95 1.12 0.14 and resistance to segregation. In this study, T50, V funnel, and
L-Box tests were carried out to determine the fresh self-
self-compacting concretes. High durable pumice with the density compacting concrete properties. Further, for the hardened concrete
of 700 kg/m3 was used for the lightweight concrete. Graded river different tests were performed to determine the mechanical prop-
sand brought from Sofeh mine located in Isfahan with the particle erties of each concrete. To investigate the effects of bagasse ash on
size of 0–5 mm and specified weight of 2570 kg/m3 was used as compressive strength of concrete, three cubic samples with the
fine aggregate. Crushed limestone with fineness modules less than dimensions of 15 15 15 cm were prepared for each mixture,
125 lm was used as coarse aggregates to increase the powdered resulting in 54 specimens and were tested at the age of 28 days
materials in SCC mixtures. according to ASTM C39/C39M-14 standard test method [48]. A
total number of 54 cylindrical samples with the dimensions of
15 30 cm were used to evaluate the tensile strength of concrete
2.2. Concrete mix design specimens in accordance with ASTM C496/C496M-11 [49]. To
determine the impact resistance of concrete, two samples with
An extensive experimental study was conducted on concretes the dimensions of 10 10 10 cm were made for each mixture
containing sugarcane bagasse ash. For this purpose, cement was to test the impact resistance of concrete specimens according to
partially replaced with 5%, 10%, 15%, 20%, and 25% bagasse ash in ASTM G544 [50]. Water absorption ratio was evaluated using 18
three types of concrete including ordinary, lightweight, and self- cubic specimens with the dimensions of 15 15 15 cm at the
compacting. A constant water to cement ratio of 0.4 and 10% age of 28 days according to ASTM C642-13 [51].
Table 3
Concrete mix design.
Concrete Mix code W/b BA (%) Cement Micro- Water Gravel Pumice (kg/m3) Sand Limestone Super Plasticizer
(kg/m3) silica (%) (kg/m3) (kg/m3) (pumice) (kg/m3 ) powder plasticizer (kg/m3 )
(kg/m3 )
OCBA CTL 0.40 0 400 10 180 900 – 760 – – 15
OCBA5 0.40 5 380 10 180 900 – 760 – – 15
OCBA10 0.40 10 360 10 180 900 – 760 – – 15
OCBA15 0.40 15 340 10 180 900 – 760 – – 15
OCBA20 0.40 20 320 10 180 900 – 760 – – 15
OCBA25 0.40 25 300 10 180 900 – 760 – – 15
LWCBA CTL 0.40 0 450 10 200 – 360 500 – – 15
LWCBA5 0.40 5 428 10 200 – 360 500 – – 15
LWCBA10 0.40 10 405 10 200 – 360 500 – – 15
LWCBA15 0.40 15 383 10 200 – 360 500 – – 15
LWCBA20 0.40 20 360 10 200 – 360 500 – – 15
LWCBA25 0.40 25 338 10 200 – 360 500 – – 15
SCCBA CTL 0.40 0 450 10 198 350 – 520 150 20 –
SCCBA5 0.40 5 428 10 198 350 – 520 150 20 –
SCCBA10 0.40 10 405 10 198 350 – 520 150 20 –
SCCBA15 0.40 15 383 10 198 350 – 520 150 20 –
SCCBA20 0.40 20 360 10 198 350 – 520 150 20 –
SCCBA25 0.40 25 338 10 198 350 – 520 150 20 –
CTL: control.
OCBA: ordinary concrete in which SCBA was used in partial substation for cement by weight.
LWCBA: lightweight concrete in which SCBA was used in partial substation for cement by weight.
SCCBA: SCC in which cement was replaced partially with SCBA by weight.
262 S.A. Zareei et al. / Construction and Building Materials 184 (2018) 258–268
Table 4 80
Standard test methods to determine concrete properties in fresh and hardened states.
percent
compared to cement, thus, replacing a part of cement with SCBA -20
decreases the density of the mixture Figs. 8 and 9 -30
For the self-compacting concrete some specific tests were con- -40
ducted. T50 test measures the time for the fresh concrete flow to -50
reach 500 mm in diameter. The V funnel test measures the time -60
that a defined volume of SCC passes a narrow opening. L-box test -70
method aims to evaluate the passing and blocking ability of SCC. SCBA percent
In this test, after the gate of the test equipment is released, the
OCBA LWCBA SCCBA
time that the concrete spreads along 200–400 mm in vertical part
is measured. Table 5 presents the fresh concrete test results for the Fig. 9. Compressive strength variations.
self-compacting concrete.
Table 5
140 SCC test results.
120 Mixture T50 V funnel L Box
100 L Box (h2/h1) L Box (time to reach 200 mm)
Slump (mm)
2200
As shown in Fig. 6, the reduction of slump was apparent in OCBA,
2000 LWCBA, and SCCBA mixes for BA content of 10%. Filling ability
1800 measurements of SCC showed that the concrete with 10%–20%
1600 BA content exhibited high workability, i.e., slump values increased
1400 with an increase in BA content. The similar results were observed
1200
in concrete containing 15% and 20% SCBA.
1000
CTL 5 10 15 20 25
3.2. Compressive strength
SCBA percent
4.5
strength was observed in all three types of concrete by adding 20%
BA (29% reduction in OCBA, 11% in LWCBA, and 30% in SCCBA). The 4
maximum reduction occurred in specimens with BA content of y = 0.0855x - 0.7482
y = 0.0645x + 1.0437
25%, where 40% and 33% reduction occurred in OCBA and SCCBA, 3.5 R² = 0.9942
R² = 0.9295
respectively.
3
where ft is the impact resistance or tensile strength recorded in Linear (OCBA) Linear (LWCBA) Linear (SCCBA)
MPa, fc denotes the compressive strength recorded in MPa, and a Fig. 12. Correlation between compressive strength and tensile strength.
and b are constants.
6
70
5
Tensile strength (MPa)
60
Impact resistance (Mpa)
4 50
3 40
2 30
20
1
10
0
CTL 5 10 15 20 25 0
CTL 5 10 15 20 25
SCBA percent
SCBA percent
OCBA LWCBA SCCBA OCBA LWCBA SCCBA
Fig. 10. The results of tensile strength test. Fig. 13. The results of impact resistance test.
264 S.A. Zareei et al. / Construction and Building Materials 184 (2018) 258–268
100 ture of 105 °C and then their weights were measured. Then, the
80 specimens were submerged into the cold water for 1 h and they
60 were weighted again in order to determine the water absorption
variations by percent
coefficient.
Impact resistance
40
20 As seen, the water permeability ratio of concrete increased with
0 increasing bagasse ash content, especially for BA content higher
5 10 15 20 25 than 15% in concrete at early ages. The highest water permeability
-20
-40 was observed in LWCBA. The water permeability ratios of 72%,
-60 107%, and 156% were obtained respectively for OCBA, SCCBA, and
-80 LWCBA containing 25% BA. The increase in water absorption of
-100 the concrete specimens can be due to the fact that cement was
SCBA percent replaced with SCBA, which increased the voids in the sample and
produced a more porous specimen.
OCBA LWCBA SCCBA
4 by using this test [58]. This test was conducted after 28 days of
3.5 curing according to the provisions of ASTM C 137 and by using
3 Ultrasonic Concrete Tester 110–240 V 50/60 Hz 1Ph. The results
2.5 OCBA showed that addition of BA caused a slight reduction in UPV as seen
2 LWCBA in Fig. 16, which is in consistent with those reported in other works
1.5 SCCBA [59]. Some studies reported that any increase in the substitution of
1 cement by BA beyond 10% can negatively affect the compressive
0.5
strength of mortars and concretes [28,44,60–62]. UPV passing
through a solid is strongly influenced by density, elastic properties,
0
CLT 5 10 15 20 25 and phases involved inside the material [63,64]. In fact, the higher
SCBA percent the UPV is estimated, the material is denser. Furthermore, the sensi-
tivity of UPV is dependent on the age and strength of the concrete.
Fig. 15. Water absorption coefficient. The results of UPV test are given in Table 6 and Fig. 16.
4800
4600
4400 Perfect
4200
UPV (m/s)
4000
3800 Good
3600
3400
3200
Uncertain
3000
CTL 5 10 15 20 25
SBCA percent
Table 6
UPV test results at 28 days.
It was also indicated that an increase in BA content led to higher in higher UPV. As it can be seen from the figures, the compressive
reductions of UPV in samples. Moreover, a significant beneficial strength positively contributes to UPV variations at 28 days, which
effect of the addition of 10% micro-silica on UPV was observed as can be translated into more reasonable relation found to be estab-
it was kept constant at a sufficient level. lished in later ages. Two factors are responsible for strength of OCBA
at early ages. First, the pozzolanic reaction can be highly activated
3.6.1. Correlation between UPV and compressive strength with small particle size, which increases the compressive strength
A sound correlation between UPV and compressive strength of the specimen. Second, filling ability of bagasse ash particles to fill
was observed as shown in Fig. 17. The following relationship is the voids and air spaces, which produces a denser concrete. If cali-
established between the aforementioned parameters: bration curve of specimens is provided at 90 days, compressive
strength estimations are closer to reality. At later ages variation of
f c ¼ aV b ð4Þ UPV cause significant changes in the compressive strength [65,66].
It was reported that incorporation of SCBA from 10% to 20% in the
where V refers to the ultrasonic pulse velocity recorded in m/s. mixture led to a reduction in UPV values [44].
As seen, for higher compressive strength value higher UPV was
obtained, especially in concrete samples with higher densities. Fur-
thermore, the effects of incorporating BA was more pronounced in 3.6.2. Correlation between UPV and water absorption coefficient
SCCBA in comparison with OCBA. The highest UPV was obtained in According to the results a negative correlation was observed
SCCBA as an indication of the direct relationship between UPV and between water absorption coefficient and UPV as shown in
compressive strength variations in self-compacting concrete sam- Fig. 18. Concrete containing bagasse ash showed less UPV values
ples with R-square of 0.88. The same trend was observed for LWCBA with increasing values of water absorption ratio due to the
samples: an increase in BA content in lightweight concrete resulted microstructure changes in the cementitious matrix. Higher ratios
65 51
Compressive strength (MPa)
45 y = 0.1931x - 824.72
R² = 0.8842
40
35
30
25
20
4350 4400 4450 4500 4550
UPV m/s
BMP Linear (BMP)
(c)
Fig. 17. Correlation between UPV and the compressive strength; (a) Ordinary concrete, (b) Lightweight concrete, (c) Self-compacting concrete.
266 S.A. Zareei et al. / Construction and Building Materials 184 (2018) 258–268
4500 4 3600 5
UPV m/s
UPV m/s
3
4300 2
2
3400
4200 1 1
3300 0
4100 0
UPV WA UPV WA
(a) (b)
4600 4
2
4400
1
4300 0
SCBA percent
UPV WA
(c)
Fig. 18. Correlation between UPV and water absorption coefficient; (a) Ordinary concrete, (b) Lightweight concrete, (c) Self-compacting concrete.
of water permeability led to lower quality of concrete texture, SCBA. Inability of SCBA to fill the pores of concrete was the rea-
especially in lightweight concrete samples. son of increased amount of water absorption.
- It was found that incorporation of SCBA up to 5% improved the
performance of concrete in terms of durability and impact
4. Conclusions resistance.
- UPV tests indicated that the optimum cement replacement of
The paper studied the effects of partial replacement of cement SCBA was 15%, 5%, and 10% in ordinary, lightweight, and self-
with sugarcane bagasse ash (SCBA) on the fresh and hardened con- compacting concretes, respectively.
crete properties. For this purpose, an extensive experimental pro- - Increase in water absorption in OCBA concrete is possibly due to
gram was designed in which mechanical properties of three the low ability of bagasse ash aggregates to fill the pores.
types of concrete including ordinary, lightweight, and self- - SCC specified tests indicated that concrete passing and flowabil-
compacting concrete containing different amounts of SCBA were ity increased with an increase in BA content. Accordingly, the
examined. To investigate the effects of SCBA on fresh concrete optimum amount of replacing cement with SCBA was deter-
properties, slump and fresh density tests were conducted on ordi- mined 5% for SCC.
nary and lightweight concretes, while T50, V funnel, and L-
Box tests were carried out on SCC samples. For the hardened con- 5. Conflict of interest
crete, mechanical tests including compressive strength, tensile
strength, impact resistance, water absorption, and ultrasonic pulse None.
velocity test were performed. Based on the experiment results, the
following conclusions were drawn:
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