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ABSTRACT
This study focuses on developing a ternary blended self-compacting concrete (SCC) for use in small repair works. Three
different SCC mixes were designed using fly ash, metakaolin and PCE superplasticizer based on experimental investigation
by varying its filler cement ratio and paste volume. The concrete mixes were tested for workability parameters such as
resistance to segregation, filling and passing ability by conducting slump flow, V-funnel, L-Box and U-Box tests to ascertain
its suitability for repair works. Mechanical properties of concrete mixes were found by conducting compressive strength test,
flexural strength test, split tensile strength test and young’s modulus test as per Indian Standards. Durability tests conducted
includes accelerated corrosion test, rapid chloride penetration test (RCPT) and sorptivity test by following Indian /ASTM
Standards / Guidelines of premier research institutions. It is found that all the developed mixes offer appreciable performance
against segregation, slump flow and filling ability. The concrete mix SCC-M1 with increased cement and metakaolin content
offered improved strength and durability properties as compared to other mixes which may be due to enhanced hydration
reaction and improved microstructure of concrete.
Keywords: Repair, self-compacting concrete, ternary blend, mechanical properties, durability properties.
1.Introduction
controlled by the micro-structural characteristics of the
materials used in the concrete [3,4]. The porosity and
The repair, rehabilitation and strengthening of reinforced
pore size distribution in concrete are the critical
concrete structures has become a routine activity of
components of the microstructure of hydrated cement
construction industry in the recent times. The need for
paste that largely influences durability. In order to
repair of these concrete structures arises from the
achieve high strength, low permeability and durable self-
deterioration caused mainly by corrosion of
compacting concrete, it is essential to reduce the porosity
reinforcement bars which is due to inappropriate
of cement paste in appropriate level. It is known that the
durability design, aggravated further by penetration of
incorporation of pozzolana materials refines the porosity
chloride ions and carbonation. India is incurring a loss of
and pore size distribution of the paste. Fly ash is known
Rs. 2,50,000 crores annually due to corrosion which
to be a good pozzolanic material for use in concrete and
reveals the significant contribution of distressed concrete
many researchers have established its effect on the
structures towards this. The engineers and specification
physical properties and pore structure of concrete.
makers have ample choice of materials for repair but lack
However, the pore structure changes due to variations in
in guidance and knowledge on their properties and long
fly ash fineness are not well established. Study conducted
term performance. The composition of a repair material
by Dinakar et. al [4] shows that self-compacting concrete
especially in concrete is not realistically possible without
has significant durability performance when compared
much understanding. There is a need to establish a set of
with normal vibrated concrete. Self-compacting concrete
requirements which should be based on performance
has the ability to gain strength at the early ages of curing.
related properties of the repair material. The set of
The gain in compressive strength at early ages for
procedures / specifications for a particular repair is not
different grade of SCC mixes and its relation to the
readily available and is location specific [1,2]. Self-
conventional concrete values as per BIS: SP 23-1982 was
compacting concrete (SCC) is one of the most widely
studied by Binu et. al [5]. Aruz [6] ascertained the extend
used repair material. In the design of self-compacting
of service life of chloride - exposed concrete structure by
concrete, durability has to be given much emphasis in
addition of fly ash in the concrete. The increase in initial
addition to its ability to resist expected loading
strength and durability of concrete due to addition of
conditions. The service life and durability of concrete
Metakaolin was established [7,8]. Metakaolin is also a
structure is strongly depending on properties such as
highly reactive pozzolanic material and has been
permeability, sorptivity and diffusivity which are
subjected for several studies especially in ternary
controlled by the micro-structural characteristics of the
blending mainly due to its capacity to react vividly with
materials used in the concrete [3,4]. The porosity and
Ca(OH)2 by-products occurred during cement hydration.
1 pore size distribution in concrete are the critical
Student, mohamedrayan1994@gmail.com Due to its high pozzolanic activity, the addition of
2 components of the microstructure of hydrated cement metakaolin enhances the mechanical and durability
Student, jeelanbasha1@gmail.com
3 paste that largely influences durability. In order to properties of cement based materials.
Professor and Dean, hajisheik@bsauniv.ac.in
achieve high strength, low permeability and durable self-
compacting concrete, it is essential to reduce the porosity
of cement paste in appropriate level. It is known that the
incorporation of pozzolana materials refines the porosity
and pore size distribution of the paste. Fly ash is known
to be a good pozzolanic material for use in concrete and
many researchers have established its effect on the
physical properties and pore structure of concrete.
Table 2: Physical properties of constituent materials
Properties of the constituent materials
Material used Specific Fineness Bulk density Blaine’s surface % of Zone
gravity modulus (Kg/l) fineness* (m2/Kg) Void
Cement (PPC) 3.2 - - 340 - -
Fly ash 2.2 - - 428 - -
Metakaolin 2.6 - - 2200 - -
Fine Aggregate 2.55 4.6 1.69 - 35 II
Course Aggregate 2.59 7.67 1.3 - 44 -
*Data obtained from the manufacturer
superplasticizer. Aggregate skeleton is composed of fine is noted. The time taken for 115mm spread shall be
and coarse aggregate. within 2-4 sec. The diameter of final spread shall be of
170-190mm. The paste prepared with different f/c value
The dosage of superplasticizer was optimized using of 0, 0.3, 0.4, 0.5 and 0.6 with superplasticizer dosage
marsh cone test as per EN 445 [17]. The tests were (sp/c) optimized from marsh cone test and a fixed water
conducted for different filler cement ratio (f/c) of 0, 0.3, binder ratio (w/b) of 0.4 is subjected to mini slump test.
0.4, 0.5 and 0.6 with fixed water binder ratio of 0.4. The Table 3 shows the observation on march cone test and
relation between the flow time and dosage of mini slump test. The optimized dosage of fly ash
superplasticizer (sp/b) for different f/c value is shown in considered for design of SCC is f/c=0.5; sp/b=1 and
Figure 2. The optimum dosage of superplasticizer at f/c=0.6; sp/b=1.09. The sand gravel ratio for SCC is
saturation point was identified as 0.8,0.8,0.9,1,1.09 for optimized using ASTM C29/ C 29M [18] method. The
f/c values 0,0.3,0.4,0.5 and 0.6 respectively. It can be relation of bulk density and percentage of void with
inferred that slurry with higher filler content requires varying sand content is shown in figure 3.
more dosage of superplasticizer.
Mix ID w/b Sp/b Slump flow T50cm slump V-funnel flow V-funnel flow L-Box U-Box
ratio ratio (mm) flow (s) at Tf (s) at t5 min (sec) h2/h1 (h2-h1)
Description Compressive strength Split tensile strength Modulus of rupture Young’s modulus
(MPa) (MPa) (GPa)
7 days 14 days 28 days
SCC-M1 39 43 48 2.5 3.8 26
SCC-M2 24 30 37 2.33 3.7 24
SCC-M3 22 28 36 2.1 3.5 22
SCC-M2 and SCC-M3 is 4.8 MPa, 4.3 MPa and 4.2 period. Although specimen with SCC-M3 was observed
MPa respectively which overestimates the experimental with minimum initial current development, this
tensile strength test results significantly. Flexural condition remains only for 1000 minutes and thereafter
strength values of 3.8 MPa, 3.7 MPa and 3.5 MPa was there is a gradual increase in current values upon time
observed for concrete beam specimens made of SCC- increment until failure of specimens. It can be
M1, SCC-M2 and SCC-M3 mix when tested at the age concluded that the specimens with mix SCC-M1 and
of 28 days. There is slightly improved flexural strength SCC-M2 offered significant resistance against
for SCC-M1 mix specimens as compared to other mix accelerated chloride ingress followed by SCC-M3
specimens. But flexural strength values calculated as per specimens. Control concrete specimen exhibited inferior
BIS 456:2000 is in the range of 4.8 MPa, 4.3 MPa and performance as compared to SCC mix specimens.
4.2 MPa for SCC-M1, SCC-M2 and SCC-M3 mix Figure 7 shows the comparison of cracking time for
respectively. This infers that theoretical values control and SCC mix specimens. It can be seen that
overestimate the experimental test results appreciably cracking time for control concrete specimen is 40 hours.
irrespective of the type of SCC mix. Whereas specimens made of SCC mix exhibited
resistance against cracking until 89 hours. This reveals
Modulus of elasticity of developed concrete mixes at that SCC specimens offered 2.2 times improved
the age of 28 days was observed as 26 GPa, 24 GPa and performance as compared to control concrete. This
22 GPa for SCC mix SCC-M1, SCC-M2 and SCC-M3 improved performance may be due to presence of high
respectively. This again reveals that there is a marginal content finer materials and well-designed particle size
increase in young’s modulus values for SCC-M1 as distribution, resulted in improved packing and
compared to other mixes. But theoretical value of elastic microstructure formation with optimum water content in
modulus estimated as per BIS 456:200 are 34 GPa, 30.4 the SCC mix which gave excellent resistance against
GPa and 30 GPa for SCC-M1, SCC-M2 and SCC-M3 accelerated chloride ingress.
mix respectively. This exhibits that theoretical values
overestimate the experimental results of the order of 25-
30% irrespective of type of SCC mix. Figure 5 shows
the stress –strain behavior of different mixes of SCC.
This shows the linear behavior for all the tested SCC
mixes. The reduction in young’s modulus values may be
due to increased past content and reduced coarse
aggregate content in the developed mixes.
100 89 89
CONTROL 87
90
Cracking Time (hrs)
80 SCC-M1
70 SCC-M2
60 SCC-M3
Figure 5: Stress and strain relationship of SCC 50 40
mixes 40
30
20
Figure 6 shows the time versus current behavior of 10
control concrete & SCC mixes in the accelerated 0
1 2 3 4
corrosion test during the test period. It can be seen that Type of Concrete mix
there is an increased initial current development for
control concrete as compared to SCC mixes followed by Figure 7: Comparison of cracking time for control
similar current values until 2000 minutes. Thereafter and SCC mix specimens
there is a steep increase in current values for the small Table 7 shows the observation on the rapid chloride
increment in time which indicates failure of specimen penetration test for the developed SCC mixes at the end
due to corrosion related cracking. Concrete specimen of 6-hour test period. It can be observed that the mixes
made of SCC-M1 and SCC-M2 mix was observed with SCC-M1, SCC-M2 and SCC-M3 exhibited current
minimum initial current development. This value is values of 1008, 1312 and 1353 coulombs respectively.
persisted until 5000 minutes and followed with gradual According to ASTM C 1202 [23], the values falls under
increase in current values during the remaining test 2000 coulombs falls under low permeability category.
Mix SCC-M1 offered improved resistance against
current development as compared to other SCC mixes. Figure 9 shows the relation between water
It can be concluded that the developed SCC mixes absorption and square root of time. It can be inferred
possess excellent impermeability characteristics. Figure that mix SCC-M1 exhibit less water absorption
8 shows the time versus current development behavior characteristics as compared to other tested SCC
of SCC mixes in RCPT test during the test period. concrete. The sorptivity value was estimated based on
Irrespective of the type of SCC mix, minimal current the slope of the best fit curve of water absorption and
development in the initial test period for all the mixes square root of time. It is found that sorptivity value of
followed by gradual increase in current values as the mix SCC-M1 is 572 x 10-4 mm/sec. Whereas mixes
time progress. SCC-M1 offered better resistance against SCC-M2 and SCC-M3 were observed with 665 x 10-4
current development as compared to other SCC mixes mm/sec and 1154 x 10-4 mm/sec respectively. The
which explicit its improved durability performance. mix SCC-M1 and SCC-M2 offered significant reduction
in sorptivity values as compared to SCC-M3. The
The improved performance of SCC mixes is due to the sorptivity values is attributed by the rise of water in the
fact that chloride ion penetration depends mainly on the specimen through capillary action which depends
chloride binding capacity of the constituent materials. presence of pores and its connectivity in the
Chlorides penetrate through concrete by diffusion along microstructure of concrete. The dense and well packed
water paths or open pores. Some of these chlorides react microstructure of SCC-M1 and SCC-M2 resulted in
with the cement compounds mainly tricalcium- excellent reduction in sorptivity.
aluminates (C3A), forming stable chloro complexes.
The excess free chloride leads to the initiation of the
corrosion process. The presence of fly ash content in
SCC leads to an increase in the amount of C3A due to
the higher amount of alumina present in the mix and
increases the calcium silicate hydrate content that is
formed in the pozzolanic reactions.
5.Conclusions
Over 100 specimens were subjected to workability,
strength and durability test to find the performance of
Figure 8: Time versus current behavior of SCC the optimized SCC mixes. The following conclusions
mixes in RCPT test were drawn based on the test results and further
analysis.
Thus, the chloride binding capacity of concrete tends to • All the tested SCC mixes showed an
increase with fly ash addition and consequently less free appreciable performance against segregation,
chloride is available to initiate the corrosion process as slump flow and filling ability.
observed by Dinakar et al. • The mix SCC-M1 offered significant increase
in compressive strength at all the tested ages as
Table 7: Observation on rapid chloride penetration compared with other tested mixes.
test • There is a marginally improved flexural
strength, split tensile strength and modulus of
Sl.No. Type of Charge passed (coulombs) elasticity values for SCC-M1 mix as compared
mix (at the end of test period) to other SCC mixes.
• Theoretical tensile strength and modulus of
1 SCC-M1 1008 elasticity values of SCC mixes overestimates
the experimental values appreciably.
2 SCC-M2 1312 • Accelerated corrosion test results revealed 2.2
times improved performance for SCC
3 SCC-M3 1353
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