Accura Operation Manual Version 2.0 20160621

PAC
ACCURA
OPERATION MANUAL
Version 2.0
www.paclp.com
APPLICATION MANUAL
GENERAL DISCLAIMERS AND NOTICES
Thank you for purchasing a PAC™ product. This manual contains confidential and proprietary
information that is the property of PAC, L.P. The information contained in this document is subject
to change without notice. This document is for information only. The manufacturer accepts no
liability for errors contained herein or for incidental or consequential damages arising from the
furnishing, performance, or use of this material.
Unless otherwise specified, each reference to names or individual trademarks and service marks has
the sole purpose of illustrating the product described here. Contents of this publication may not be
reproduced in any form or by any means (including electronic storage and retrieval or translation
into a foreign language) without prior agreement and written consent from the copyright owner.
All rights reserved.
The instructions given herein cover generally the description, installation, operation, and
maintenance of subject equipment. PAC reserves the right to make engineering refinements that
may not be reflected in this manual. Should any questions arise which may not be answered
specifically by these instructions, they should be directed to PAC for further detailed information
and technical assistance.
Your satisfaction and safety are important to PAC, and a complete understanding of this manual is
necessary to attain these objectives. As the ultimate user of this apparatus, it is your responsibility
to understand its proper function and operational characteristics. This instruction manual should be
read thoroughly and all operators should be given adequate training before attempting to place this
unit in service. Consult your company’s training program(s) for correct training. Awareness of the
stated Cautions, Dangers, Notes, Warnings, etc., in this document and compliance with
recommended operating and maintenance parameters are important for safe and satisfactory
operation, preventive maintenance or service.
This unit should be used only for its intended operation; alterations will void the Warranty.
This manual contains confidential and proprietary information that is the property of PAC L.P. This
manual and all information disclosed herein shall not be used to manufacture, construct, or
fabricate the goods disclosed herein; shall not be exploited or sold; shall not be copied or
otherwise reproduced in whole or in part and shall not be revealed or disclosed to others or in any
manner made public without the express written permission of PAC L.P.
Copyright ©2015, by PAC, LP Houston, Texas.

All rights reserved.
Contents of this publication may not be reproduced in any form
without permission of the copyright owner.
01.03.2015
Page 2 of 64 ACCURA Operation Manual – Version 2.0 www.paclp.com

APPLICATION MANUAL
Accura Operation Manual

Edition: English
Version: 2016 2.0
Printed in The Netherlands

AC Analytical Controls B.V.
Innsbruckweg 35
3047 AG Rotterdam

APPLICATION MANUAL
TABLE OF CONTENTS
CONTACT US ................................................................................................................... 12
SYMBOLS, CAUTIONS, AND WARNINGS ...................................................................... 14
HANDLING SOLVENTS .................................................................................................... 15
SAFETY............................................................................................................................. 16
PART NUMBERS IN THIS MANUAL ................................................................................ 18
TECHNICAL INFORMATION ............................................................................................ 20
1. CHAPTER ONE: INTRODUCTION ........................................................................... 22
1.1 Gas/Liquefied Gas Sampling Inlet System .............................................................. 22
1.2 Model Configurations: GC and Elemental ............................................................... 22
2. CHAPTER TWO: ACCURA - MULTITEK INSTALLATION ...................................... 25
2.1 Rear Panel Connections ............................................................................................ 26
2.2 Electrical connections ............................................................................................... 30
3. CHAPTER THREE: ACCURA - MULTITEK OPERATION ....................................... 31
3.1 Connect power to Accura: ........................................................................................ 31
3.2 Default Parameters .................................................................................................... 31
3.3 Adjusting flow correction value................................................................................ 32
3.4 Sample Introduction Procedure................................................................................ 33
3.5 Multi-loop .................................................................................................................... 36
4. CHAPTER FOUR: SAMPLE INTRODUCTION ON GC ............................................ 39
4.1 Installation .................................................................................................................. 39
4.1.1 Connect Accura to GC ...................................................................................... 40
4.1.2 Connect Accura to Vent ................................................................................... 42
4.1.3 Connect Power to Accura ................................................................................ 43
4.2 Accura Settings .......................................................................................................... 43
4.2.1 Vaporizer Flow ................................................................................................... 43
4.2.2 Vaporizer Temperature ..................................................................................... 44
4.2.3 Purge Valve ........................................................................................................ 44
4.2.4 Flow Correction Value ...................................................................................... 44
4.3 Sample Introduction Procedure................................................................................ 45
5. CHAPTER FIVE: ACCURA SCREENS .................................................................... 49
6. CHAPTER SIX: PREVENTIVE MAINTENANCE/TROUBLESHOOTING .................. 59
6.1 Preventive Maintenance/Service Table .................................................................... 59
6.2 Troubleshooting ......................................................................................................... 60
6.3 Troubleshoot Table .................................................................................................... 61
APPENDIX A: CERTIFICATIONS ..................................................................................... 63

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APPLICATION MANUAL
POLICY STATEMENT
This is the property of PAC L.P. This manual and all information disclosed herein shall not be used
to manufacture, construct, or fabricate the goods disclosed herein; shall not be exploited or sold;
shall not be copied or otherwise reproduced in whole or in part and shall not be revealed or
disclosed to others or in any manner made public without the express written permission of PAC
L.P.
GENERAL INFORMATION
Disposal
Correct disposal of Waste Electrical and Electronic Equipment in the end-of life
Applicable in the European Union and other European countries with separate collection
systems
This product is designed for exclusive professional use by commercial companies. This marking
shown on the product or its literature, indicates that it should not be disposed with other
household wastes at the end of its working life.
To prevent possible harm to the environment or human health from uncontrolled waste disposal,
please separate this from other types of wastes and recycle it responsibly to promote the
sustainable reuse of material resources.
Business users should contact the producer or the importer and check the terms and conditions of
the purchase contract. If you have a separate agreement with your producer or importer such that
you will take care of end-of-life disposal on your own, please ensure an environmentally sound
disposal according to the legal regulations for electric and electronic waste equipment in your
country.
WARNING: This product should not be mixed with other commercial wastes for disposal.
The above WEEE-symbol is the official marking for equipment under the WEEE-scope. In some EC-
Member states, "pure B2B equipment" is not necessarily marked with the waste bin-symbol. To
provide a homogenous EC-wide procedure, PAC uses the marking in all EC-Member states.

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APPLICATION MANUAL
Warranty
STANDARD LIMITED WARRANTY

OF
PETROLEUM ANALYZER COMPANY, L.P.
I. Limited Warranty
1. Limited Warranty. For each product sold, PAC offers to the original owner (“BUYER”) a limited warranty against failure to
conform to the product specifications or any defects in material and workmanship for a period of twelve (12) months from the date
of installation of the product or eighteen (18) months from date of invoice, whichever is less (the “Initial Warranty”). If a failure to
conform to specifications or a defect in materials or workmanship is discovered within the Initial Warranty period, BUYER must
promptly notify PAC in writing, which notification, in any event must be received no later than 14 months from the date of
installation of the product. Within a reasonable time after such notification, PAC will correct any failure to conform to
specifications or any defect in materials or workmanship, or in lieu of such repair, and at its sole option, shall replace the product,
F.O.B. PAC’s city of shipment or refund the purchase price, less a reasonable reduction in such purchase price as determined by PAC.
In no event shall PAC be liable for consequential or special damages, or for transportation, installation, adjustment or other
expenses, which may arise in connection with such products or warranty claim. Products and parts sold by authorized PAC
Distributors are covered by the Distributor’s terms and conditions.
During the Initial Warranty period, PAC offers a limited warranty on each part or product repaired or replaced by a PAC service
person for a period ending the later of (a) the remaining term of the product’s Initial Warranty or (b) ninety (90) days from the date
of repair or replacement whichever is longer. After expiration of the Initial Warranty period, PAC offers a ninety (90) day limited
warranty on each part or product repaired or replaced by a PAC service person. PAC further warrants that the products and parts it
sells will conform to PAC’s written specifications therefor. The foregoing limited warranties cover parts and labor only and PAC does
not warrant and will not reimburse the BUYER for any other costs relating repairing or replacing the product at issue. The foregoing
limited warranties apply only to the repair or replacement of defective parts and/or products and such determination will be in the
sole discretion of PAC. The limited warranties of this Section I.1 are further subject to those warranty exclusions set forth below.
2. Aftermarket. The use of third party parts in the operation or maintenance of the product or repairs or servicing by unauthorized
service personnel immediately voids all further warranty obligations of PAC. PAC genuine consumables are sold on an as-is basis and
have no warranty beyond being shipped in good working order.
3. Limited Warranty Exclusions. Other than the warranties set forth in Section I.1., PAC disclaims any and all express or implied
warranties, including but not limited to the warranty of merchantability, fitness for a particular purpose and non-infringement of the
intellectual property of others. Provided, however, this Intellectual Property Warranty shall apply to the product only so long as
BUYER (i) does not modify the product, combine the product with other elements or use the product in a practice or a process, and
such modification, combination or practice of which the product forms a part is the subject of such claim or allegation of
infringement and (ii) uses the product under ordinary conditions and for their intended purposes. PAC makes no warranty, express or
implied, as to the design, sale, installation or use of its products. PAC’s warranties will not be enlarged by, nor will any obligation
or liability of PAC arise due to PAC providing technical advice, facilities or service in connection with any product. PAC disclaims any
and all other warranties and representations and PAC provides no warranty on the oral representations made by its personnel while
they are undertaking Services for BUYER.
There is no warranty by PAC with respect to any product’s: (i) uninterrupted or error-free operation; (ii) actual performance, other
than the product’s capability to meet PAC’s specifications therefor; (iii) removal or installation from a worksite or process;
(iv) electronic components or associated accessories (including without limitation circuit boards and integrated circuits);
(v) maintenance (including without limitation gasket and seal replacements, adjustments, minor repairs and other inspection
requirements, preventative or otherwise); (vi) use under inappropriate conditions or not in accordance with operating instructions;
or (vii) use in connection with the operation of a nuclear facility. There is no warranty for products determined to be, in PAC’s sole
discretion, damaged or impaired as a result of (a) misuse, neglect or accident; (b) improper application, installation, storage or use;
(c) improper or inadequate maintenance or calibration; (d) operation outside of the published environmental specification;
(e) improper site preparation or maintenance; (f) unauthorized repairs or replacements; (g) modifications negligently or otherwise
improperly made or performed by persons other than PAC; (h) BUYER-supplied software or supplies; (i) use in conjunction with or
interfacing with unapproved accessory equipment; (j) use of ABC-style or dry powder fire suppression agents; or (k) leaked sample
materials. To the extent a PAC product is used in connection with the operation of a nuclear power facility, BUYER agrees to
indemnify and hold PAC harmless from any and all actions, claims, suits, damages and expenses arising from such use. PAC provides
no warranty on the oral representations made by its personnel while they are attempting to assist BUYER in the operation of a
product. This Standard Limited Warranty
does not apply to items consumed by the products during their ordinary use, including but not limited to fuses, batteries, paper,
septa, fittings, screws, fuses, pyrolysis, dryer or scrubber tubes, sample boats, furnaces or lamps. This warranty is valid only if
genuine PAC parts, consumables and standards are used in PAC products.
4. Resale products are goods (that are sold with PAC’s products) which are not manufactured by PAC and which are supplied as an
accommodation to BUYER. PAC MAKES NO WARRANTY FOR RESALE PRODUCTS, EITHER EXPRESS OR IMPLIED, INCLUDING WARRANTIES
OF MERCHANTABILITY AND FITNESS FOR A PARTICULAR PURPOSE. THE SOLE WARRANTY SHALL BE THAT OF THE RESALE PRODUCT
MANUFACTURER.

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BUYER agrees that PAC has no liability for resale products beyond the services within PAC’s direct control necessary to reasonably
discharge the above stated responsibility and that PAC shall not be liable for delays caused by resale product manufacturer. PAC
does not warrant products it does not manufacture except to the extent the warranty of the manufacturer of the product at issue
passes through or is otherwise assigned to PAC. BUYER further agrees that BUYER’s SOLE AND EXCLUSIVE REMEDY for PAC’s breach of
the stated responsibility shall be limited to the difference between the resale product manufacturer’s price to PAC and PAC’s price
to BUYER for resale products.
5. Expenses for Non-Warranty Work. All repairs or replacements by PAC after the expiration of any applicable limited warranty
period will be performed in accordance with PAC’s standard rate for parts and labor. Further, if upon PAC’s inspection and review,
PAC determines the condition of the product for which a warranty claim is submitted is not caused by a defect in PAC’s material and
workmanship, but is the result of some other condition, including but not limited to damage caused by any of the events or
conditions set forth in Section I.3., BUYER shall be liable for all expenses incurred by PAC to conduct the inspection and review of
the product.
6. Exclusive Remedy. The limited warranty contained herein constitutes BUYER’s exclusive remedy with respect to products sold by
PAC and PAC’s liability shall be exclusively limited to the written limited warranty specified herein. No employee, representative or
agent of PAC is authorized to either expressly or impliedly modify, extend, alter or change any of the limited warranties expressed
herein to BUYER.
7. Procedure and Costs. All limited warranty claims must be made in writing promptly following discovery of any failure to conform
to specifications or any defect in materials or workmanship. BUYER must hold products for inspection by PAC. If requested by PAC,
BUYER must send the product to PAC for inspection. Any such returns by BUYER will be at BUYER’s expense and BUYER will remain
liable for any loss of or damage to the product during such product’s transportation to PAC. No products will be sent to PAC for
inspection unless PAC has authorized BUYER to do so.
8. Terms and Conditions. PAC’s General Terms and Conditions are incorporated herein by reference and BUYER accordingly agrees
to be bound by the terms thereof.
II. Limitations on PAC Liability
1. In General. BUYER agrees that in no case shall PAC be liable for any special, incidental, consequential, or punitive damages based
upon any legal theory whether or not such damages are foreseeable. such damages include, but are not limited to, loss of profits,
loss of savings or revenue, loss of use of the product or any associated equipment, cost of capital, cost of any substitute equipment,
facilities or services, downtime, the claims of third parties including customers, injury to property and, unless precluded under
applicable state law, bodily and personal injury. PAC’s total liability for any and all losses and damages arising out of any and all
causes whatsoever including, without limitation, defects in the product(s), services, software, or documentation supplied or breach
of this agreement, shall in no event exceed the purchase price of the applicable product(s). BUYER agrees these limitations on PAC’s
liability are reasonable and reflected in the amounts charged by PAC for its products.
2. BUYER Data. If any data supplied by BUYER, whether in the form of BUYER specifications or pursuant to any purchase order or
other documentation, proves to be inaccurate, any warranties or other related obligations of PAC relying thereon will be void.
3. Force Majeure. This Standard Limited Warranty does not cover and PAC shall not be liable for either direct or consequential
damage caused, either directly or indirectly, as a result of: (i) any act of God, including but not limited to natural disaster, such as
floods, earthquakes, or tornadoes; (ii) damages resulting from or under the conditions of labor disputes, strikes or riots, insurrection,
civil commotion or war; (iii) damages or improper operation due to intermittent power line voltage, frequency, electrical spikes or
surges, unusual shock or electrical damage; (iv) accident, fire or water damage, neglect, corrosive atmosphere or causes other than
ordinary use; (v) failure of supplies or transportation, or governmental action or; or (vi) any other causes beyond Seller’s reasonable
control.
4. Limitation on Warranty Claims. Prior to any obligation of PAC to perform any limited warranty service as set forth herein, BUYER
must have: (i) paid all invoices to PAC in full, whether or not they are specifically related to the product at issue; and (ii) notified
PAC of the limited warranty claim within sixty (60) days from the date BUYER knew or had reason to know of the defect.
III. Compliance
1. In General. These Warranty Terms are subject to change without notice. PAC also retains the right to modify these warranty
terms in order to comply with policy or laws governing warranty issues in states or countries having specific remedies differing or
additional to those described within this document.
2. Severability. If any one or more of the provisions or subjects contained in the Agreement shall for any reason be held invalid,
illegal, or unenforceable, it shall not affect the validity and enforceability of any other provisions or subjects.

APPLICATION MANUAL
Return Policy
No product may be returned, whether in warranty or out of warranty, without first obtaining
approval from PAC, L.P. No replacements will be provided nor repairs be made for products
returned without such approval. A return authorization number must accompany any returned
product. The buyer will pay for the expense of returning the unit to PAC, L.P. for service. The
status of any product returned later than 30 days after the issuance of a return authorization
number will be subject to review. Products may not be returned that are contaminated by
radioactive materials, infectious agents, or other materials constituting health hazards to PAC,
L.P.'s employees.
Returned Product Warranty Determination

After PAC, L.P.’s examination, warranty or out-of-warranty status will be determined. If a
warranted defect exists, the product will be repaired at no charge and shipped pre-paid back to the
buyer. Warranty repairs do not extend the original warranty period. If an out-of-warranty defect
exists, the buyer shall be notified of the repair cost. At such time, the buyer must issue a valid
purchase order to cover the cost of the repair and freight, or authorize the product to be shipped
back as is, at the buyer’s expense. Failure to obtain a purchase order number approval within
fifteen days of notification will result in the product being returned as is, at the buyer’s expense.
On-Site Repairs
If a PAC L.P. product cannot be made functional by telephone assistance or by installing
replacement parts, and cannot be returned to PAC L.P. for repair, the following policy applies:
PAC L.P. will provide an on-site field service representative in a reasonable amount of time,
provided that the customer issues a valid purchase order to PAC L.P. covering all transportation,
subsistence, and prevailing labor costs, including travel time, necessary to complete the repair. For
warranty field repairs, the customer will not be charged for the cost of transportation, labor, or
materials. Special service rates may apply when service is rendered at times other than normal
work periods.
Assumptions
The Accura is generally installed onsite by a trained service technician. However, on occasion, it
may be necessary to move the hardware or reinstall the software, if applicable. The hardware and
software installations require the following for many PAC products; your product may differ in
general needs:
 Familiarity with the installation components, such as cabling, stainless steel or copper tubing
for gas lines, connectors, and fittings
 An apparatus with ability to lift and transport at least the weight of the product(s)
 A working knowledge of computers and associated equipment (keyboard, mouse, and monitor)
 An understanding of scientific benchmarks for contaminates
 A knowledge of storage, handling, and use of specialty gases, such as argon, oxygen, helium,
and hydrogen

APPLICATION MANUAL
Inspection
This instrument was thoroughly inspected and carefully packed before leaving our factory.
Responsibility for its safe delivery was assumed by the carrier upon acceptance of the shipment.
Claims for loss or damage sustained in transit must be made to the carrier by the recipient as
follows.
Visible Loss or Damage

Note any external evidence of loss or damage on the freight bill or express receipt, and have it
signed by the carrier’s agent. Failure to adequately describe such external evidence of loss or
damage may result in the carrier’s refusing to honor your damage claim. The form required to file
such a claim will be supplied by the carrier.
Concealed Loss or Damage

Concealed loss or damage means loss or damage which becomes apparent when the merchandise is
unpacked and inspected. Should concealed loss or damage occur, make a written request for
inspection by the carrier’s agent within 15 days of the delivery date, then file a claim with the
carrier since the damage is the carrier’s responsibility. By following these instructions carefully,
we guarantee our full support of your claim to be compensated for loss from shipping damage.
NOTE: When shipping the Accura, remove all samples and accessories from the Accura, remove and
clean any glass jars, remove any loose deposits from ovens, lids, exhaust tubes or other parts or
sections.
DO NOT - for any reason - return the instrument without first obtaining authorization. In any
correspondence to PAC, please supply the nameplate data, including catalog number and serial
number. The name label is located on the rear of the instrument housing.
Record of Serial Number and Purchase Date
Catalog Number: ________________________________________
Serial Number: __________________________________________
Purchase Date: ______________________________________

APPLICATION MANUAL
CONTACT US
If you have any questions about your product, contact us using the information below:
U.S. Contacts
PAC L.P.
8824 Fallbrook Drive
Houston, TX 77064
Main Number: +1 281 940-1803
Service: +1 800 444-TEST (8378) or +1 281 580-0339
Fax Number: +1 281 580-0719
European Contacts
AC Analytical Controls B.V.
Innsbruckweg 35
3047 AG Rotterdam
Main Number: +31 10 462 4811
WEB: http://www.paclp.com
Email Support: sales@paclp.com
service@paclp.com

APPLICATION MANUAL
Table 1. Contact Information
Web: http://www.paclp.com
Phone: USA +1 281 940 1803
France +33 231 264 300
Germany +49 9343 6400
Singapore +65 6412 0890
Netherlands +31 10 462 4811
Russia & CIS +7 495 617 10 86
China +86 10 65072236
South Korea +82 2 785 3900
Thailand +66 2 627 9410
Abu Dhabi +971 2 446 9671
Fax: USA +1 281 580 0719
France +33 231 266 293
Germany +49 9343 640 101
Singapore +65 6412 0899
Netherlands +31 10 462 6330
Russia & CIS +7 495 913 97 65
China +86 10 65072454
South Korea +82 2 785 3977
Thailand +66 2 627 9401
Abu Dhabi +971 2 446 9672
Sales: USA mailto:Sales@paclp.com
France mailto:Sales.France@paclp.com
Germany mailto:Sales.Germany@paclp.com
Singapore mailto:Asia-Sales@paclp.com
Netherlands mailto:Sales.Netherlands@paclp.com
Russia & CIS mailto:Alexander.sungurov@paclp.com
China mailto:Asia-Sales@paclp.com
South Korea mailto:Asia-Sales@paclp.com
Thailand mailto:Asia-Sales@paclp.com
Abu Dhabi mailto:Sales.MiddleEast@paclp.com
Service: USA mailto:Service@paclp.com

France mailto:Service.France@paclp.com
Germany mailto:Service.Germany@paclp.com
Singapore mailto:Asia-Service@paclp.com
Netherlands mailto:Service.Netherlands@paclp.com
China mailto:Asia-Service@paclp.com
South Korea mailto:Asia-Service@paclp.com
Thailand mailto:Asia-Service@paclp.com
Abu Dhabi mailto:Service.MiddleEast@paclp.com

APPLICATION MANUAL
SYMBOLS, CAUTIONS, AND WARNINGS
The following symbols, notes, cautions, warnings, etc., are/may be used in this manual. The below
legend explains each type of basic entry. There can be various types of Warnings for gas leaks, fire
hazards and other dangerous hazards. Not all types of Warnings will be listed below. However,
each WARNING carries the same basic message that there is a possibility of injury or death to
humans due to the described conditions. READ ALL SYMBOL INFORMATION CAREFULLY.
NOTE: A note pictogram denotes helpful information about a topic or task.
CAUTION: Failure to follow the instructions and procedures contained in this manual
could result in poor performance of equipment or loss of data.
!!WARNING: Failure to follow the instructions and procedures contained in this manual
could result in death or serious injury to humans. Also, injury to equipment is possible.
The instructions and procedures must be performed by qualified and trained personnel
only. Do not perform installation or maintenance operations or procedures outside the
scope of this manual.
WARNING: This symbol (three wavy lines over a straight line in a triangle) indicates a
hot surface. During operation, the Accura surfaces get hot. To prevent burns exercise
caution when operating the knob of the Accura.
TIP: A tip pictogram denotes a recommendation that can help in understanding how to
operate or service the apparatus.

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IMPORTANT: Important means information that is more critical than NOTE information.
!!WARNING: Some procedures in this manual may involve handling flammable liquids and
exposure to skin irritants and harmful vapors. Wear protective clothing, gloves and
mask (PPE: personal protective equipment) when setting up and performing procedures
and tests. Ensure flames and spark producing materials are kept well away from test
areas. Use standard safety procedures at all times. Consult material safety data sheets
(MSDS) for product safety, storage, and handling information.
HANDLING SOLVENTS
!!WARNING: Procedures in this manual may involve handling flammable liquids and
exposure to skin irritants and harmful vapors. Wear protective clothing, gloves and
mask when setting up and performing Accura tests. Ensure flames and spark producing
materials are kept well away from the Accura test area. Use standard safety
procedures at all times.
OTHER SAFETY AND USAGE STATEMENTS
This instruction manual contains information, Warnings, and Cautions that must be followed to
insure safe operation and to maintain the equipment is safe operating condition. Use of this
product in a manner not specified may impair the protection provided by the equipment.
Safety glasses should be worn by the operator and anyone in the vicinity of the equipment for
protection from splashed materials. Non-flammable heat resistant gloves as well as non-flammable
clothing should be worn when using this equipment. Tests performed with this equipment may
involve hazardous materials. This instruction manual does not purport to address all safety concerns
associated with these tests. It is the responsibility of the user of this equipment to establish
appropriate safety and health practices and to determine applicability limitations prior to use.
For safe operation, this equipment must be electrically grounded by way of the protective
grounding connection in the power cord. Do not, under any circumstances, defeat the protective
grounding connection.

APPLICATION MANUAL
!!WARNING: Do not use this equipment in a hazardous atmosphere or near flammable

materials. Do not use this equipment with hazardous materials for which it is not
designed. Protection provided by this equipment may be impaired if used with
accessories not provided or recommended by the manufacturer or used in a manner not
specified by the manufacturer.
SAFETY
The system and its components have been designed with safety in mind. The design applies to the
use, the conditions and the instructions described in the documentation.
If the user makes changes or modifications that are not expressly approved by PAC, the company
reserves the right to void the user’s authority to operate the equipment.
During performance or routine maintenance, the system operator may be exposed to potentially
dangerous chemicals, temperatures, electrical voltages and/or other hazards. In order to reduce
the personal risk involved, the user must follow established guidelines and accepted standards for
general analytical laboratory operation.
For established safety requirements, government safety and disposal standards, please refer to the
corresponding Material Safety Data Sheet (MSDS) for each PAC-supplied product and also reference
the corresponding vendor supplied MSDS for each sample and standard utilized with the product.
!!WARNING: Failure to follow the instructions and procedures contained in this manual
could result in death or serious injury. The instructions and procedures must be
performed by qualified and trained personnel only. Do not perform installation or
maintenance operations or procedures outside the scope of this manual.
ENVIRONMENTAL PROTECTION
Observe all local regulations and recommendations for the disposal and recycling of parts and
materials that have been used or replaced during installation, operation, and maintenance tasks.

APPLICATION MANUAL
REFERENCES
Document Name
Agilent 6890/7890 Operation Manual

PAC ANTEK 9000 User’s Manual
PAC MultiTek Operation Manual
DEFINITIONS OF TERMS
The following terms are/may be used in this manual:
Term Definition
Select To pick an item that begins an action (this includes menu commands
and buttons)
Click To press the left mouse button once
Right-click To press the right mouse button once
Double-click To press the left mouse button twice in rapid succession without
moving the mouse
Dialog box A temporary window that contains options or information you can
edit, select, or use
Preventive Maintenance Maintenance performed or parts replaced on a routine basis to keep
the product operating correctly and efficiently. The customer
generally retains the product on-site.
Service Non-routine maintenance performed for specific repairs or more
technical maintenance needs. The customer may have Service work
performed
on-site with PAC approval, or the product may have to be shipped to
PAC for service.
PAC L.P. is also referred to as PAC throughout the chapters and appendices of this manual.

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PERSONAL PROTECTION EQUIPMENT NEEDED
Consult your company’s training standards for correct PPE usage. The following PPE (but not
limited to) should be used while operating or servicing the unit. Exercise caution at all times.
PPE View Description of PPE
Protective eyewear
Nitrile powder-free exam gloves, or equivalent
LOCK-OUT/TAG-OUT PROCEDURES
Follow all of your company’s lock-out/tag-out procedures at all times. Exercise caution at all
times.
ACRONYMS AND ABBREVIATIONS

Acronym Definition
GC Gas Chromatograph
LPG Liquefied Petroleum Gas
MFC Mass Flow Controller
MT MultiTek
PART NUMBERS IN THIS MANUAL

This section contains a list of part numbers of the major consumable items for the PAC Accura.
Consumables
Part Number Description Quantity
71238T Filter, 0.5 Micron Treated 1 (MT)

10.10.161 In-line filter, 0.5 micron, 1/8“, SS 1 (GC)

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Parts
Part Number Description Quantity
10.10.222 Valve, Relief, 1/4", 24-50 bar, assy 1
10.10.254 Pressure regulator, KCP, treated – (vaporizer) 1
10.11.240 Valve, 2/3, NO, assy 1
10.10.104 Bulkhead union, 1/8”, SS 1
40.02.016 Temperature sensor, IC 1
20.10.003 Thermostat, Bi-metallic, NC, 65C 1
20.15.105 Fan 24V (40 x40 x 20mm), assy 1
10.11.241 Valve, 2prt, 86 Bar, assy 1
36.01.154 PCB, Accura, inclusive touchscreen 1
40.01.057 Heater/Sensor set, 24V/60W, Pt100 1
40.02.013 Pressure Sensor 0-40 Bar, assy 1
20.08.101 6.3A T fuse 2
21040.003 Ferrule,Delrin®, 10 pcs reduction 1/8”to 1/16” 1
10.20.132 MFC, Mass Flow Controller, 1-50 mls/min 1 (MT)
10.25.029 Valve, rotary, 6-port 1 (MT)
10.10.104T Bulkhead union, 1/8”, SS Treated 1 (MT)
35.01.425 Motor & Actuator for Valve 1 (MT)
10.35.027 O-ring, Viton, 013, 10,82x1,78 1 (MT)
10.45.044 Spider for jaw coupling, 19mm 1 (MT)
31054 Ferrule, Teflon, 1/4 , 10 pcs 1 (MT)

APPLICATION MANUAL
TECHNICAL INFORMATION
The Accura has been designed and tested in accordance with recognized safety standards and is
designed for use indoors. If the instrument is used in a manner not specified by the manufacturer,
the protection provided by the instrument may be impaired.
Item Definition/Explanation
Voltage range 110-230 Vac,50- 60 Hz, 240VA

Fuse ratings 6.3A T (2X)
Altitude Up to 2000 m
Operating temperatures 15 to 40 °C (59 to 104°F)
Maximum relative 80 % for temperatures up to 31 °C decreasing linearly to 50 %
humidity relative humidity at 40 °C.
Recommended 50 to 60%, non-condensing.
IP class IP21
Safety class Class I
Over voltage category CAT II
Power connection Grounded outlet fused at max. 16A within 1.5 meter of the
instrument with a grounded power cable
Ventilation requirements The Accura is cooled by air flow which enters the unit at the top
back side and exits trough the bottom back side. Do not obstruct
the air flow at the inlet and outlet.
Keep at least 10 cm free around the unit.
Main switch location At the top rear side of the unit
Cleaning To clean the unit, disconnect the power and wipe down with a
damp, lint-free cloth.
Sound level 50 dBA
Weight 15 kg Elemental version , 12 kg GC version
Carrier Gas, maximum 600kPa (6 bar , 87psi) Helium or Argon at 99.99% (Grade 4)
pressure
Carrier Gas, minimum 300kPa (3 bar, 43psi)
pressure
Sample Gas/ Liquid/ LPG, 3000kPa (30 bar, 435 psi)
maximum pressure
Sample Gas/ Liquid/ LPG, 200 kPa (2bar, 29psi)
minimum pressure
System Pressure Test
A pressure test is performed at a maximum pressure of 3000 kPa of the high pressure side. The
maximum allowed pressure drop is 10 kPa per 10 minute @ 3000 kPa.

APPLICATION MANUAL
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APPLICATION MANUAL
1. CHAPTER ONE: INTRODUCTION
1.1 Gas/Liquefied Gas Sampling Inlet System
The Accura is an automated Gas/Liquid Sampling Inlet Systems that is used to introduce gas or LPG
samples into a PAC Analyzer. Two models are distinguished, one for Elemental analysis with the
PAC MultiTek Analyzer (MT) and the other for Gas Chromatography (GC). Sampling for other
analyzers may also be accomplished, but is not described in this manual.
The two models start with the same high pressure flow path; both have a vaporizer to convert the
liquefied LPG into a gas. The vaporized liquid then enters a gas sample loop, which is connected to
a rotary valve. In case of GC the valve is located in the GC. For the MultiTek the rotary valve is
located inside the Accura.
When the injection pulse is given, the valve is switched and the contents of the sample loop is
transferred to the analyzer for analysis. In case of the MultiTek, a built-in Mass flow controller
(MFC) takes care of this. For the GC configuration the flow is provided by the Electronic pressure
control (EPC) of the GC.
NOTE: The Accura is intended to be used for the vaporization of liquefied gases
(liquids under pressure) prior to analysis by Multitek or GC. Liquefied gases typically
are LPG type samples, hydrocarbons heavier than C5 must be lower than 2 volume
% (D-1835-13).
NOTE: Direct injection of gases can also be done with the Accura. However, high
concentrations of heavy hydrocarbons (>C5) may result in condensation and thus loss,
giving lower results for the subsequent Multitek or GC analysis.
1.2 Model Configurations: GC and Elemental
The Accura is available in two models a GC version and Elemental version (MultiTek). The
difference is the presence of a 6-port injection valve with peripherals in the Elemental version. See
following Figure 1 (different configuration).

APPLICATION MANUAL
Figure 1. GC and Multitek configuration
Right panel Back panel

Supply
MFC
Maximum
45-150 °C 8bar / 87 PSI
Left panel
1 To Analyzer
45 -150°C 2 6
Inlet Filter
3 5
Vaporizer 4
Sample in Gas loop 10mL

From Analyzer
(Liquid and Gas)

Pressure sensor
( 0-4000 kPa)
Sample vent
Flowsensor
Relief valve
3200kPa
Purge vent
Purge valve
High pressure; Liquid and Gas side Low pressure; Gas only side
MultiTek Configuration (part # 36.00.001)
Back panel
Left panel
Right panel
45 -150°C
Inlet Filter To Analyzer
Vaporizer
Sample in
(Liquid and Gas) From Analyzer
Pressure sensor
( 0-4000 kPa)
Sample vent
Flowsensor
Relief valve
3200kPa Purge vent
Purge valve
High pressure; Liquid and Gas side Low pressure; Gas only side
GC Configuration (Part # 36.00.002)

APPLICATION MANUAL
Accura Overview:
Figure 2. Accura MultiTek (36.00.001)
4
3
1. Display
2. Flow adjust knob
3. From Analyzer – To Analyzer
4. Sample in
Figure 3. Accura GC (36.00.002)
4
3
1. Display
2. Flow adjust knob
3. Sample in
4. From Analyzer – To Analyzer

APPLICATION MANUAL
2. CHAPTER TWO: ACCURA - MULTITEK INSTALLATION
The Accura is intended for use in the introduction of gases and vaporized liquefied petroleum gases
into the furnace of the PAC 9000/MultiTek® System.
The following text will focus on the general aspects of installation and operation.
TIP 1: Place the unit on a sturdy flat surface, with the screen facing the front.
Check for leaks after making connections.
TIP 2: When placing the Acura, please make sure that the Flow adjust knob is easily
accessible.
This is a global overview how to connect the Accura to a MultiTek (Figure 4).
Figure 4. Connections Overview

APPLICATION MANUAL
WARNING: Possible shock hazard: take all necessary precautions, disconnect power if
needed; Located at the rear side of the instrument there is an M5 stud that can be used
to connect a grounding wire to ground the sample cylinder / sample line.
Figure 5. Rear side of Accura and M5 Stud
CAUTION: When electrically connecting the Accura to another device, make sure this
device is CE certified or equivalent.
2.1 Rear Panel Connections

1. Place the unit next to the MultiTek. (preferably on the right-hand side)
2. Use the T-piece supplied in the start-up kit to split the carrier gas supply to both MultiTek and
Accura. This supply (Argon or Helium) should be pure (99.99%) dry gas, regulated below 600
kPa. (6 bar/ 87 psi)
3. Connect the carrier gas to the “supply” connection at the rear side of the Accura (figure 12,
item F)

APPLICATION MANUAL
NOTE: This carrier gas does not replace the carrier gas supply to the analyzer. The
carrier gas supply to the analyzer should be continued as if the instrument were being
operated without Accura.
4. Connect the Vent connections at the rear side of the Accura to a fume hood or outside vent
with the double vent line. (figure 12, item D and E)
CAUTION: Do not use a t-piece to connect Purge Vent (D) and Sample Vent (E) with a
single line to a fume hood or outside vent, but leave both lines separated!
NOTE: Do not hold the End of the vent line(s) in a beaker glass with liquid, this may
cause the liquid to be drawn into the Accura
!!WARNING: Do not vent into the lab atmosphere. An explosion hazard may exist.
5. On the Left hand side of the Accura, connect the carrier from the “From Analyzer“ port to the
“Carrier in” connection at the rear side of the MultiTek, (Figure 6) using Stainless steel
capillary tubing (preferably “jumper tube”; 1/16 inch tubing sleeved to 1/8 inch end).

APPLICATION MANUAL
Figure 6. Rear side of the MultiTek and Left handside of the Accura
From Analyzer
Carrier In
To Analyzer
6. On the MultiTek, remove the Right hand side panel that allows access to the furnace.
7. Connect the supplied tubing (#30.30.807) to the Pyro tube (figure 6). Connect to the side which
leads the gas just below the septum.
Figure 7. Connection tubing to Pyro tube (part # 30.30.807)
NOTE: After disconnection, this tubing needs to be capped

APPLICATION MANUAL
Figure 8. MultiTek (Vertical) Figure 9. MultiTek (Horizontal)
Pyrotube
connection Pyrotube
connection
8. Feed the 1/16” line/tube through a vent hole out towards the “To Analyzer” port on the Left
hand side of the Accura using a reducing ferrule (Delrin® ferrule p/n 21040.003, see Figure 11).
9. Connect the in-line filter to the “Sample In” port, see figure 10. Please use a treated 0.5 µm
inlet filter (part # 71238T) for protection of the hardware inside the instrument.
Figure 10. Accura Right hand side panel
Sample in
Figure 11 shows a low pressure connections to the Accura. Slide a nut and the Delrin® ferrule
(21040.003) over the tubing. Tighten like a normal Swagelok® fitting. Use only for pressures less
than 300 kPa (3 bar/43 psi).
Figure 11. Low Pressure Fittings

APPLICATION MANUAL
NOTE: Use the supplied tubing to connect the Accura to the Multitek. Incorrect tubing
can result in pressure build-up in the Multitek !
2.2 Electrical connections

1. Connect the mains wire to a wall socket and Accura. The wall socket has to be fused at 16A.
2. Connect the I/O port to the “734 port” on the rear side of the MultiTek using the
Communication Cable (part # 40.02.011)
NOTE: If this Communication cable is not connected to both MultTek and Accura, the
Accura will not function!
Figure 12. Accura MultiTek Rear Panel
A. Fan inlet
C. Mains On/Off
switch and fuse holder
B: I/O port (2 x 6.3A T)
E. Sample vent: 1/8”

compressed fitting for
gas sample vent.
F. Supply: 1/8”
compressing fitting
for carrier gas
connection
D. Purge vent: 1/8”

compressed fitting for
purge gas vent.

APPLICATION MANUAL
!!WARNING: Exhaust venting must comply with all local environmental and safety codes.
Contact your Environmental Health & Safety (EHS) specialist.
3. CHAPTER THREE: ACCURA - MULTITEK OPERATION
This chapter describes the use of the Accura system for sample introduction on a MultiTek.
Once the Accura is properly installed, the following steps should be taken to place the system into
operation:
3.1 Connect power to Accura:

1. Connect the Accura to a fused 16A wall socket. To protect users, the metal instrument panels
and cabinet are grounded through the three-conductor power line cord in accordance with
International Electrotechnical Commission (IEC) requirements.
IMPORTANT: The three-conductor power line cord, when plugged into a properly
grounded receptacle, grounds the instrument and minimizes shock hazard. A properly
grounded receptacle is one that is connected to a suitable earth ground. Be sure to verify
proper receptacle grounding. The Accura requires an isolated ground.
2. Plug the power cord into the rear side of the Accura and the power outlet (figure 12).
WARNING: Before switching the unit ON, check the mains wire for damages and replace
immediately if damages are noticed. Replace only with a similar type mains wire.
3.2 Default Parameters
To run the Accura, the default parameters are used. If the repeatability value of analyses results
(RSD) is above 5% then increase the vaporizer temperature 10°C (18°F). The target vaporizer flow
is 60 ml/minute, this will make sure that the loop is flushed. Keep the loop temperature as low as
possible to allow for maximal peak area.

APPLICATION MANUAL
Figure 13. Default Values MultiTek
Parameter Values
Vaporizer Temperature 125 °C (257°F)

Vaporizer flow (Target) 60 ml/min
Loop Temperature 100°C (212°F)
MFC flow 25 ml/min
Correction value: Nitrogen 100

Methane 35
C3/C4 60/40% 30
C3/C4 with some C5 and 23
heavier
Default Parameters
NOTE: The system pressure of the MultiTek will be higher compared to a 734
3.3 Adjusting flow correction value
The built-in flow sensor of the Accura needs to be adjusted for the matrix of the sample. The
Correction factor can be calculated in the following way:
Flow correction value:

𝐼𝑛𝑡𝑒𝑟𝑛𝑎𝑙 𝑣𝑎𝑙𝑢𝑒
𝐷𝑖𝑠𝑝𝑙𝑎𝑦𝑒𝑑 𝑣𝑎𝑙𝑢𝑒 = 𝑥 𝑓𝑎𝑐𝑡𝑜𝑟
100
Set factor to 100. Measure the flow at the vent. Multiply the flow on the flowmeter by 100 then
divide by the displayed value to get the factor.
Example: Displayed value =303, factor = 100
Measured with flowmeter = 70 mL/min
70*100 / 303 = 23.1  factor is 23
NOTE: The displayed flow value should be considered as indicative. The flow sensor is
not intended for precise flow measurement.

APPLICATION MANUAL
3.4 Sample Introduction Procedure

1. Turn ON the Accura system by switching the ON/OFF button at the rear side of the instrument.
2. Set the MFC flow to 25 mL/minute (The vaporizer flow can be optimized later).
3. Set the Accura to 125°C (257 °F) vaporizer temperature and 100°C (212 °F) Loop temperature.
Allow at least 30 minutes for the temperature to stabilize.
4. Let the system stabilize for 30 minutes. In particular the vaporizer needs some time to reach
the temperature set-point after start-up.
5. Actuate the sample valves several times to ensure proper working of the valve. This can be
done in the Service mode on the Accura display. (Without the sample being connected,
otherwise actual injections on the MultiTek are made!)
NOTE: The system status will indicate “Sample Load” when the unit is ready for
injections.
6. Ensure that all program parameters have been entered into the 9000/MultiTek system,
including timed events for manipulation of the valve of the Accura. Default values are visible in
the following table.
NOTE: During the operation the flow adjust knob may become warm
Figure 14. Table Run Parameters MultiTek
Parameter Value (mm:ss)

Cycle time 05:00
Inject time 00:50
Load 02:45

APPLICATION MANUAL
Figure 15. Method MultiTek
7. Verify the pressure of the sample cylinder. The pressure should be lower than the rating of the
Accura system (<30 bar / 435 psi).
!!WARNING: If the pressure inside the sample cylinder is higher than the rating of the
Accura system, damage to the system and possible dangerous situation might occur.
The Internal relief valve will vent the excess pressure to vent.
8. Using Stainless steel capillary tubing (preferably “jumper tube”, 1/16” inch tubing sleeved to
1/8” end # 30.20.008), connect the sample to the “Sample in” connection on the Right hand
side of the Accura, see Figure 10.
9. Turn the Flow adjust know counter clockwise (shut-off the flow).
10. Open the (liquid) sample cylinder slowly.
11. Purge the sample lines by using the Purge button on the Main Display. The purge button
activates the purge valve that opens and closes the samples lines to the purge vent for a fixed
period of time (e.g. 600 ms open / 1800 ms closed) for a fixed number of times (e.g. 6 times).
12. Turn the Flow adjust knob for regulating the vaporizer flow clockwise until the desired flow is
reached (e.g. 60 ml/min +/- 10 ml/min, recommended flushing time is 1 minute).

APPLICATION MANUAL
NOTE: The System Status will change to “Sample Load” if the Vaporizer flow reaches the
set flow within the set tolerances. Besides the Vaporizer flow, the Vaporizer
temperature should also be “ready”. The “prepare GC” button will be available if the
System Status is “ready”.
13. Prepare a 9000/MultiTek sequence.
Main Display
Figure 16. Sample Chromatogram

APPLICATION MANUAL
Disconnecting procedure:
1. Close the valve on the sample cylinder.
2. Turn the Flow adjust knob clockwise until mechanical stop, the flow increases.
3. Press the purge button. Repeat this until the status bar on the display is green indicating that
the pressure is below 200 kPa (2 bar/29psi).
4. Wait till the flow drops to zero.
5. Disconnect the sample cylinder.
TIP: Nitrogen can be used to purge the system for the time being, until the next sample
needs to be analyzed.
3.5 Multi-loop
The Multi-loop feature allows the Accura to inject the Loop volume multiple times. (under Method
on the display menu) The Sample is injected as normal, however now the Accura will turn the
injection valve back to the Load position, flush the Loop with sample and re inject the sample. The
peaks are visible one after another. The MultiTek method has to be long enough to allow all peaks
to elute. A method of ten multi Loop injections takes about 15 minutes run time.

APPLICATION MANUAL
Figure 17. Multiloop method MultiTek
Figure 18. Multi-loop Injection

APPLICATION MANUAL
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APPLICATION MANUAL
4. CHAPTER FOUR: SAMPLE INTRODUCTION ON GC
This chapter describes the use of the Accura system for sample introduction on the Agilent 6890
and Agilent 7890 A and B version Gas Chromatograph.
The Accura is a sampling module that allows the user to reproducibly introduce gaseous and
liquefied (LPG) samples into a gas chromatograph. A built-in heated vaporizer vaporizes the
liquefied samples, so they are introduced into the gas chromatograph in the gaseous state. The unit
is placed adjacent to the gas chromatograph and connected to the gas sample loop(s) of the GC.
Figure 19. Placement of Accura On the Left-Hand Side of the GC
4.1 Installation
The Sampling device must be placed adjacent to the gas chromatograph on the left-hand side. The
following will focus on the general aspects of installation and operation.
1. Place the unit on a sturdy flat surface, with the screen facing the front. Check for leaks after
making connections.
CAUTION: When electrically connecting the Accura to another device, make sure this
device is CE certified or equivalent.

APPLICATION MANUAL
WARNING: Located at the rear side of the instrument there is an M5 stud that can be
used to connect a grounding wire to earth the sample cylinder / sample line.
When placing the Accura, please make sure that the flow adjust knob is easy accessible.
4.1.1 Connect Accura to GC
2. Using Stainless steel capillary tubing (preferably “jumper tube, # 30.20.008”; 1/16 inch tubing
sleeved to 1/8 inch end), connect the “To Analyzer” connection on the Right hand side of the
Accura to the “Gas Sample in” of the GC.
3. Connect the “Gas sample out” from the gas chromatograph to the “From Analyzer” connection
on the Right hand side of the Accura, following Figure 20.
Figure 20. Connect the GC to the Right Hand Side of the Accura System
From Analyzer To Analyzer
4. Connect the dedicated remote cable (part # 40.02.012) from the I/O connection at the rear
side of the Accura (Fig. 21), to the “remote” connection at the rear side of the GC. (Fig. 21)

APPLICATION MANUAL
Figure 21. Connect Remote Cable to the I/O Connection (rear side)
Figure 22. Connect the Remote Cable to the Remote Connection At the rear side of the GC

APPLICATION MANUAL
4.1.2 Connect Accura to Vent

5. Connect the Vent connections at the rear side of the Accura to a fume hood or outside vent
with the double vent line. (figure 23, item D and E)
!!WARNING: Do not vent into the lab atmosphere. An explosion hazard may exist.
Figure 23. Direct both Vents (Purge- and Sample) to a Fume Hood
D. Purge vent: 1/8”

E. Sample vent: 1/8” compressed fitting for
compressed fitting for purge gas vent.
gas sample vent.
!!WARNING: Exhaust venting must comply with all local environmental and safety codes.
Contact your Environmental Health & Safety (EHS) specialist.

APPLICATION MANUAL
4.1.3 Connect Power to Accura
6. Connect the Accura to a fused 16A wall socket. To protect users, the metal instrument panels
and cabinet are grounded through the three-conductor power line cord in accordance with
International Electrotechnical Commission (IEC) requirements.
IMPORTANT: The three-conductor power line cord, when plugged into a properly
grounded receptacle, grounds the instrument and minimizes shock hazard. A properly
grounded receptacle is one that is connected to a suitable earth ground. Be sure to verify
proper receptacle grounding. The Accura requires an isolated ground.
7. Plug the power cord into the rear side of the Accura and the power outlet (figure 24).
Figure 24. Connect the Power Cable To the Accura
4.2 Accura Settings
For optimal performance, the Vaporizer and purge valve settings of the Accura system should be set
prior to sample introduction.
4.2.1 Vaporizer Flow
To prevent sample discrimination, and obtain proper flushing of the entire system (including GC
samples loop), the vaporizer flow should be accurately set.
1. Set the desired flow in the “Set Parameters” menu (e.g. 60 ml/min).
2. Adjust the flow tolerance settings in the “Tolerance Settings” menu (e.g. +/- 10 ml/min).

APPLICATION MANUAL
NOTE: The actual vaporizer flow can be monitored in the “Actuals menu” and “Main
menu”. If the actual flow is within the tolerance of the set value (in above example
between 50 – 70 ml/min), the flow setting will be “ready”. If the actual flow is outside
the specified flow tolerance, the flow will be “not ready”, and displayed in “red”
characters.
4.2.2 Vaporizer Temperature
To obtain proper vaporization and prevent samples discrimination, the vaporizer temperature
should be accurately set.
1. Set the desired temperature in the “Set Parameters” menu (e.g. 100 °C).
2. Adjust the flow tolerance settings in the “Tolerance Settings” menu (e.g. +/- 3 °C).
NOTE: The actual Vaporizer temperature can be monitored in the “Actuals menu”. If the
actual temperature is within the tolerance of the set value (in above example between
97 – 103 °C), the temperature setting will be “ready”. If the actual temperature is
outside the specified flow tolerance, the flow will be “not ready”.
4.2.3 Purge Valve
The purge valve in the Accura system is available if fast flushing of the sample lines to the
vaporizer is necessary. The purge valve is also a handy tool if the pressure in the sample lines
should be decreased to an acceptable level when disconnecting the sample after finishing sample
introduction.
1. Set the purge valve time to the desired value (e.g. 600 ms).
2. Set the purge valve count to 6 (e.g. 6 times).
4.2.4 Flow Correction Value
The built-in flow sensor of the Accura needs to be adjusted for the matrix of the sample. The
Correction factor can be calculated in the following way:
Flow correction value:

𝐼𝑛𝑡𝑒𝑟𝑛𝑎𝑙 𝑣𝑎𝑙𝑢𝑒
𝐷𝑖𝑠𝑝𝑙𝑎𝑦𝑒𝑑 𝑣𝑎𝑙𝑢𝑒 = 𝑥 𝑓𝑎𝑐𝑡𝑜𝑟
100
Set factor to 100. Measure the flow at the vent. Multiply the flow on the flowmeter by 100 then
divide by the displayed value to get the factor.
Example: Displayed value =303, factor = 100
Measured with flowmeter = 70 mL/min
70*100 / 303 = 23.1  factor is 23

APPLICATION MANUAL
NOTE: The displayed flow value should be considered as indicative. The flow sensor is
not intended for precise flow measurement.
4.3 Sample Introduction Procedure
The next procedure describes the step-by-step sample introduction done by the Accura system,
connected with remote cable to the Agilent 7890GC.
1. Turn ON the Accura system by switching the ON/OFF button at the rear side of the instrument.
Let the system stabilize for 30 minutes. In particular the vaporizer needs some time to reach
the temperature set-point after start-up.
2. Prepare the GC. Be sure the correct GC method is loaded and is in ready state (all
temperatures reached set-point and system is stabilized).
3. Verify the pressure of the sample cylinder. The pressure should be lower than the rating of the
Accura system (<30 bar / 435 psi).
!!WARNING: If the pressure inside the sample cylinder is higher than the rating of the
Accura system, damage to the system and possible dangerous situation might occur.
The Internal relief valve will vent the excess pressure to vent.
4. Using Stainless steel capillary tubing (preferably “jumper tube”, 1/16” inch tubing sleeved to
1/8” end, # 30.20.008), connect the sample to the “Sample in” connection on the Left hand
side of the Accura, see Figure 25.
!!WARNING: Use the provided inlet filter of 0.5 µm that will protect the instrument for
blockage due to solid particles in the samples.

APPLICATION MANUAL
Figure 25. Connect Sample To the Left hand Side On the Accura
5. Turn the Flow adjust know counter clockwise (shut-OFF the flow).
Figure 26. Turn the Flow adjust knob Counter-clockwise To Shut-Off the Flow
6. Open the (liquid) sample cylinder slowly.

7. Purge the sample lines by using the Purge button on the Main Display:

APPLICATION MANUAL
Figure 27. Main Display
The purge button activates the purge valve that opens and closes the samples lines to the purge
vent for a fixed period of time (e.g. 600 ms open / 1800 ms closed) for a fixed number of times
(e.g. 6 times).
8. Turn the Flow adjust knob for regulating the vaporizer flow clockwise until the desired flow is
reached (e.g. 60 ml/min +/- 10 ml/min, recommended flushing time is 1 minute)
NOTE: The System Status will change to “Ready” if the Vaporizer flow reaches the set flow within
the set tolerances. Besides the Vaporizer flow, the Vaporizer temperature should also be “ready”.
The “prepare GC” button will be available if the System Status is “ready”.
9. Flush the sample tubing and sample loop with the gas for approximately 1 minute with the set
flow.
10. Prepare the GC (the GC will set the desired split flows etc.) by using the “Prepare GC” Button
on the Main Display of the GC.
Figure 28. Prepare GC
11. When the GC is ready for analysis, press the “Start GC” button on the Main display to start the
analysis.

APPLICATION MANUAL
Disconnecting procedure:
12. Close the valve on the sample cylinder.
13. Turn the Flow adjust knob clockwise until mechanical stop, the flow increases.
14. Press the purge button. Repeat this until the status bar on the display is green indicating that
the pressure is below 200 kPa (2 bar/29psi).
15. Wait till the flow drops to zero
16. Disconnect the sample cylinder.
NOTE: The status bar on top of the display will change from Red to Green if the sample
pressure drops below 2 Bars (30 psi/200 kPa)
Figure 29. Purge Button
WARNING: Check if the pressure in the sample lines is reduced to ambient

pressure---and no gas is coming out of the GC sample outlet tubing---before
disconnecting any connection lines.

APPLICATION MANUAL
5. CHAPTER FIVE: ACCURA SCREENS
Home Screen
Figure 30. Home Screen
The color of the status bar at the top of the screen indicates the sample pressure, connected to the
instrument. Red/Orange means a pressure above 200 kPa (2 bar/29psi)
IMPORTANT: At this point it is NOT safe to disconnect the sample line between the instrument and
the sample container.
If the status bar is green, the pressure is lower than 200 kPa (2 bar/29psi).
Main Display 1
Main Display: This is the screen to operate the Accura.
The displayed Sample pressure is in barg. (see Setup menu / units). The vaporizer flow is an
indication of the gas flow that is generated by the vaporizer.

APPLICATION MANUAL
The color of the displayed vaporizer flow is an indication whether the flow is within the tolerance
of the set target. Blue is below target and Red is above target. White is within the tolerances
around the target. Multi-loop amount is the amount of times the loop is injected per injection
event (from the analyzer).
System status will show “Not Ready” when error or warnings are present.
Main Display 2
Here the flow is too high; Turn the Flow adjust knob counter-clockwise to reduce the flow.

APPLICATION MANUAL
Status
Figure 33. Status Screen 1
Status Screen: On the Status screens, the actual values of various parameters are displayed in
the units that are chosen (see Setup menu / units, following pages).

APPLICATION MANUAL

APPLICATION MANUAL
Report
Report screen: A snapshot is taken at each injection. When an injection is detected, the date and
time are noted together with the Sample pressure, Vaporizer Flow, Vaporizer temperature and
Loop temperature. Then, the valve is closed and two seconds nothing will happen; these seconds
are used to determine the loop pressure. After this, the actual injection is made. So the loop
pressure is the pressure in the loop in zero flow condition, just before injection.
All these settings are logged in the system and can be viewed in the Report screen.
Figure 38. Report
Service Mode and About
Figure 39. Service Mode
Service Mode:, the Injection valve and the Purge valve can be controlled manually.

APPLICATION MANUAL
The About screen:
Figure 40. About screen
About: information on the s/w version

APPLICATION MANUAL
Method
Figure 41. Method
The method screens show the actual settings that are used.
In this screen, the flow correction factor can be adjusted.

APPLICATION MANUAL
Setup Menu
In the setup menu several parameters can be adjusted. Access is protected by password. The
default factory password is 12345.
Date/Time: Date and Time can be adjusted here
Operaton Mode: Displays whether the Accura is configured for MultiTek or for GC.
Display: The brightness of the display can be adjusted here as well as the use of a
screensaver for the display.
Units: Temperature can be set to either Celsius (°C) or Fahrenheit (F)
Pressure can be set to kPa, Bar or psi.
Valve: Two parameters for the Purge valve can be adjusted here: the Purge valve
time and the number of Purge valve switches per activation.
Tolerances: Tolerances for Temperature and Flow can be set here
Change Password: A new password can be entered here
Clear errors: Clears the errors on the display
Figure 42. Setup Menu
= restore to factory defaults also the password is reset to : 12345

APPLICATION MANUAL
Error messages
Here the heaters are not ready, check on the status display which heater is not ready
(vaporizer or loop)

APPLICATION MANUAL
Here the flow is too high (therefore displayed in red) and the heaters are not ready. Check
on the Status display which heater. After the system has been switched off, it may take a
while for the heaters to heat up and become constant.
On the report display several messages are displayed here.
 OVERPRESSURE: 38.5 bars – a sample has been connected and opened with a
pressure > 30 bars (435 psi). To protect the system, the relief valve that is set at
30 bars will be opened, sending the sample direct to the purge vent.
 PULSE DETECTED, NOT READY – Valve will not be actuated because either a
temperature or a flow setting is not ready. The MultiTek will start however.

APPLICATION MANUAL
6. CHAPTER SIX: PREVENTIVE MAINTENANCE/TROUBLESHOOTING
The Accura has no parts inside that require maintenance. Should maintenance or system
modification be necessary, the following guidelines should be carefully followed.
Servicing/preventive maintenance should only be performed by PAC qualified trained personnel or
PAC approved personnel.
WARNING: Ensure that the power cord has been unplugged from the power source before
continuing. If power is applied while servicing internal components, a severe electric
shock hazard may exist.
!!WARNING: Confirm proper tubing installation. Sample flow path leaks can result
in an explosion hazard.
6.1 Preventive Maintenance/Service Table
Preventive Maintenance Table

Routine Maintenance Performed (by lab technician, etc.) Interval
Pressure check. monthly

The inlet filter should be replaced once a year or thoroughly annually
cleaned.
Clean the unit. (To clean the unit, disconnect the power and Quarterly
wipe down with a damp, lint-free cloth.)
Check fan inlet for dust. Quarterly
Non-routine Maintenance Performed (more technical Interval
maintenance performed by PAC qualified technician or by a
qualified service technician)
Replace spider (10.45.044) Bi-annually

Leak check. annually
Pressure Check sampling path:
 Allow the Accura to be stable at temperature for at least 1 hour (internal temperature drift can
cause the pressure to deviate).
 Apply a pressure of 2500 – 3000 kPa N2 (25-30bar / 360 - 435 psi).
 Close the pressure source and observe if the pressure doesn’t drop more than 10 kPa per 10
minutes.

APPLICATION MANUAL
6.2 Troubleshooting
NOTE: The following guide is primarily concerned with troubleshooting

the Accura system. This guide should be used in conjunction with normal
gas chromatograph and/or Multitek troubleshooting guides. To use this
guide, simply locate the symptom in the left column and follow suggestions
for probable cause and solution. For detailed drawings of component
location, flow diagrams, parts lists, and servicing guidelines, refer to the appropriate
section of this manual.
Before attempting to perform any troubleshooting and before taking any action to remedy
an apparent problem, ensure all components of the analytical system and any accessories
are properly assembled.
To use this guide, simply locate the symptom in the left column and follow suggestions for
probable cause and remedy. Some symptoms may be addressed in each section. For
detailed drawings of component location, electronic schematics, flow diagrams, parts
lists, and servicing guidelines, please contact a PAC service representative.

APPLICATION MANUAL
6.3 Troubleshoot Table
Symptom Probable Cause Corrective Action

Accura doesn’t turn on Fuses blown Replace fuses
Error: no remote cable Cable not connected Connect cable and reset
connected Accura
Error: temperature Wrong remote cable Use correct cable for GC or
sensor MultiTek model
No Injection (no peaks) Accura ignored Injection pulse Check report section on
(from MultiTek) Accura display for cause and
adjust accordingly
Accura Valve not switching Manually switch the injection
valve on the Accura display
several times
Sample-out line not correctly Check configuration
attached to instrument
Sample shutoff valve closed (GC) Troubleshoot GC, disconnect
the Accura an perform GC
analysis only
Blockage in the system Check fittings, ferrules, and
vents for any restrictions
Gas leak Check fittings, ferrules, and
vents for Leaks.
Repair gas leak
Tailing peak (MT) Dead volume or absorption in Replace sample loop (contact
sample loop PAC)
Discrimination of Breakdown of components Vaporizer Temperature too
components (GC) high for unstable components
Non properly evaporation of Temperature too low for high
components boiling components
Low response Gas leak Check fittings, ferrules, and

vents for Leaks.
Repair gas leak
Troubleshoot instrument
Table continues on the next page

APPLICATION MANUAL
Symptom Probable Cause Corrective Action

High RSD on instrument Incorrect sample flow readout Measure flow on the Sample
results vent.
Adjust Flow correction value.
Sample pressure too low Increase sample pressure
Gas Leak Repair gas leak
Non-stable sample pressure - Replace purge valve

Leaking purge valve
Sample not completely vaporized, Increase vaporizer temp by

liquid to sample loop - 10°C (18°F).
Vaporizing temperature to low
Heaters don’t work – I/O cable Connect cable and reset

not connected Accura
Heaters don’t work – heater Replace heater, contact PAC

broken
Vaporizer Temperature Insulation not correctly installed Check and modify

unstable
Too tight tolerance setting Adjust tolerance setting or
restore factory default.(within
3 C)
Thermocouple not properly Check and properly insert
inserted in housing
After an error message, the error needs to be cleared on the display

APPLICATION MANUAL
APPENDIX A: CERTIFICATIONS

APPLICATION MANUAL
END OF DOCUMENT

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GENERAL DISCLAIMERS AND NOTICES

Copyright ©2015, by PAC, LP Houston, Texas.

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Accura Operation Manual

Printed in The Netherlands

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STANDARD LIMITED WARRANTY

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II. Limitations on PAC Liability

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Returned Product Warranty Determination

 An understanding of scientific benchmarks for contaminates

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Visible Loss or Damage

Concealed Loss or Damage

Record of Serial Number and Purchase Date

Catalog Number: ________________________________________

Serial Number: __________________________________________

Purchase Date: ______________________________________

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Main Number: +1 281 940-1803

Service: +1 800 444-TEST (8378) or +1 281 580-0339

Fax Number: +1 281 580-0719

AC Analytical Controls B.V.

Main Number: +31 10 462 4811

Email Support: sales@paclp.com

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Table 1. Contact Information

Service: USA mailto:Service@paclp.com

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SYMBOLS, CAUTIONS, AND WARNINGS

NOTE: A note pictogram denotes helpful information about a topic or task.

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OTHER SAFETY AND USAGE STATEMENTS

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!!WARNING: Do not use this equipment in a hazardous atmosphere or near flammable

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Agilent 6890/7890 Operation Manual

The following terms are/may be used in this manual:

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PERSONAL PROTECTION EQUIPMENT NEEDED

PPE View Description of PPE

Nitrile powder-free exam gloves, or equivalent

ACRONYMS AND ABBREVIATIONS

PART NUMBERS IN THIS MANUAL

71238T Filter, 0.5 Micron Treated 1 (MT)

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Voltage range 110-230 Vac,50- 60 Hz, 240VA

System Pressure Test

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1. CHAPTER ONE: INTRODUCTION

1.1 Gas/Liquefied Gas Sampling Inlet System

1.2 Model Configurations: GC and Elemental

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Figure 1. GC and Multitek configuration

Right panel Back panel

Sample in Gas loop 10mL