LAPORAN PERHITUNGAN

DIFUSIVITAS INTEGRAL
(D5)

Menentukan Volume pipa kapiler

Suhu Aquqdes 28 C
Densitas Aquades 0.9962657 gr/ml

No Panjang pipa Berat pipa kosong Berat pipa isi Berat Aquades Volume pipa
( cm ) ( gr ) ( gr ) ( gr ) ( ml )
1 9.8 8.0176 10.5836 2.566 2.575618131
2 9.8 8.0709 10.6562 2.5853 2.594990473
3 9.9 8.1347 10.8032 2.6685 2.678502331
4 9.9 8.2407 10.9017 2.661 2.670974219
5 9.6 7.9304 10.398 2.4676 2.476849298

Standarisasi Larutan
NaOH
Normalitas Asam Standard 1 N
Volume NaOH rata2 10.83333333 ml

No Volume NaOH Volume Asam Normalitas

( ml ) Standard ( ml ) NaOH ( ml )
1 12.2 10 0.819672
2 10 10 1.000000
3 10.3 10 0.970874
 Standarisasi Asam Oksalat X1 & X2
Normalitas NaOH 0.930181973 N

No Volume Asam Oksalat Volume NaOH Normalitas Asam Oksala

x1 x2 x1 x2
1 10 7 3.6 0.651127381 0.33486
2 10 7 3.7 0.651127381 0.34416
3 10 7 3.6 0.651127381 0.33486
1.953382142 1.01389
Normalitas x1 rata2 = 0.651127381 N
Normalitas x2 rata2 = 0.337966117 N

Standarisasi Asam Oksalat X1 setelah difusi

Normalitas
NaOH 0.930181973 N
Selang waktu 10 Menit

No waktu Volume NaOH ( ml ) Volume Asam Normalitas Asam Oksalat

(menit) setelah Difusi Oksalat ( ml ) Sesudah Difusi
1 10 1.6 10 0.148829
2 20 1.5 10 0.139527
3 30 1.4 10 0.130225
4 40 1.4 10 0.130225
5 50 1.3 10 0.120924

Standarisasi Asam Oksalat X2 setelah difusi

Normalitas
NaOH 0.930181973 N
Selang waktu 10 Menit

No waktu Volume NaOH ( ml ) Volume Asam Normalitas Asam Oksalat

(menit) setelah Difusi Oksalat ( ml ) Sesudah Difusi
1 10 1 10 0.093018
2 20 0.9 10 0.083716
3 30 0.8 10 0.074415
4 40 0.7 10 0.065113
5 50 0.6 10 0.055811
Presentase Asam Oksalat sisa X1
No N No E
1 0.148829 0.651070 22.85915733
2 0.139527 0.651070 21.43045999
3 0.130225 0.651070 20.00176266
4 0.130225 0.651070 20.00176266
5 0.120924 0.651070 18.57306533

Presentase Asam Oksalat sisa X2

No N No E
1 0.093018 0.337936 27.52533024
2 0.083716 0.337936 24.77273803
3 0.074415 0.337936 22.02044174
4 0.065113 0.337936 19.26784953
5 0.055811 0.337936 16.51525733

Menentukan koefisien
difusifitas
y = ax + b
y=2 log100-E/200
x=Log πt/L^2
a=1

b = log DAB

Asam Oksalat X1
No x y Yhit % Kesalahan
1 -0.485522503 -0.827491234 -0.828439365 0.114579046
2 -0.184492508 -0.81155157 -0.809504579 0.252231849
3 -0.017219486 -0.795899155 -0.798983106 0.387480032
4 0.10771925 -0.795899155 -0.791124459 0.599912213
5 0.231357186 -0.780523819 -0.783347633 0.361784438
-0.348158061 -4.011364934 -4.011399142 1.715987578

Y= 0.0629 x+ -0.7979
% kesalahan rata = 0.343197516 %

b = log DAB = -0.7979

DAB = 0.159257539
Asam Oksalat X2
No x y Yhit % Kesalahan
1 -0.485522503 -0.881687501 -0.8903729 0.985088164
2 -0.184492508 -0.849309481 -0.838866668 1.229565096
3 -0.017219486 -0.81809845 -0.810246254 0.95981063
4 0.10771925 -0.787966949 -0.788869236 0.114508215
5 0.231357186 -0.758845766 -0.767714785 1.16875131
-0.348158061 -4.095908147 -4.096069844 4.457723415

Y= 0.1711 x+ -0.8073
% kesalahan rata = 0.891544683 %

b = log DAB = -0.8073

DAB = 0.155847557