Академический Документы
Профессиональный Документы
Культура Документы
Laboratory is the place of training and working that force of a high responsible for it
users. There are rules below that necessary to know and obey, for the students or praktikan:
• Come on time, latest at 5 minutes before the practice is start. The late tolerance is 15
minutes. There is no practice for the students that has been late after 30 minutes.
• Sign in the attendance list that has prepared on the table when the students arrive and
leave from the laboratory. If the students cannot follow the practice because of sickness
and the other case, they must give the doctor’s letter to the lecturer / assistant / co.
assistant and they must collect the experimental report by themselves from the data of
their group. The rules of absence is had arranged in the lecture’s contract completely.
• Before practice, every group has given with the practice equipments according to each
experiment, all of the member’s group must check the amount and condition of their
equipments. The borrowed equipments must in clean condition. If this equipments is
broken or damaged, it must be the responsibility of a group in order to replace it
equipments by the same equipments and be accompanied by the invoice form. If at
the limiting time that has been determined, the student still does not replace the
equipment, so there is no permission to join in Final Test in this Semester and
automatically, the score of Final Test is zero.
• Make a estimation report that substituent with the form that has determined and has
signed by the assistant or lecturer after the experiment is done.
• Do carefully, far away from the dangerous treatment, such as in doing combustion, take
or pour the dangerous substances.
• The residual of insoluble substances and papers , must be throwing into the prepared
place, don’t throw into the washing box. If the substance is strong acid or strong base,
water faucet in the sink must be opened for few times.
• Don’t bring the bag and others in the experimental table, except practice instruction
book, journal book and writing tools.
• Praktikan must to wear practice coat, closed shoes, and if the hair is long, bonds it.
• When practice, don’t be capricious, and use cellular phone or doing the others
unrelated.
1. Read and learn practical instruction that related with your experiment .
2. Do according to time planning that has arranged by your self, so you can do the
experiment on time.
3. After knowing and learning the experiment carefully, borrow the equipments that
used for practice in laboratory assistant with the equipment bill, then arrange the
equipments in your table.
4. Do the experiment according to the practical instruction and record all the result of
experiment in report book and report it to lecturer / assistant.
5. Do calmly and carefully. Safety and happiness in practice will increase as you follow
all of the instructions. Misunderstanding instruction can be asked to assistant /
lecturer of experiment.
6. After doing experiment, come back the equipments in clean condition with the
equipment bill.
7. Leave the laboratory after you finished the experiment and the table must be in
clean condition.
A. OBJECTIVE: Students/praktikan be able to know a few simple equipments and its uses
in the basic chemistry laboratory
B. INTRODUCTION:
Activity recognition equipments is an important once performed as a laboratory
for basic knowledge for students to perform laboratory work properly and to avoid or
reduce the things that are not desirable, for example an error of principle in using the
equipments so that the results become inaccurate. In table 1 are presented some simple
equipments used in basic chemistry laboratory.
Conical flask
3. For solution distillation (separating
liquid mixture based on boiling point)
Measuring Flask
7 - Place to react the substances on small
quantity
Test tube
8 - To measure the volume of solution/ liquid/
water is roughly.
Graduated Cyllinder
9 - To measure/ delivery solutions drop wise
carefully in the titration process.
Burette
No Name and picture of equipments Uses
10 - Shed a reagent/ substance
- Add solution
Pipette
11 - For cooling substance in the process of
distillation, which is connected with other
equipment: distillation flask tube
connector.
Liebig Condenser
12 - Filtering solution
- Transform liquid/ solid samples into the
measuring flask
Glass funnel
13 - Burn/ heating the substance directly on the
fire
- Compose a substance on the gravimetric
method
Porcelain crucible
14 - evaporated the solution
Evaporation cup
No Name and picture of equipments Uses
15 - Smooth the substances that are still rough a
fine powder
Watch glass
17 Measure temperature of solution
Thermometer
Bunsen Burner
Spirit Burner
No Name and picture of equipments Uses
20 Weighing substance roughly
Coarse Weights
Vacuum Desiccators
Desiccators
24. Proper
Stative
No Name and picture of equipments Uses
25. Buret Holder
Clam
Holder/boss head
Petri dish
Porcelain Triangle
No Name and picture of equipments Uses
31 Heating equipment
Wire Gauze
Triangle
Iron Ring
Spatula
Substance spoon
PART III
A. EXPERIMENT 1
1. TITLE : DISTILLATION
2. PURPOSE : 1. Separating and purifying the liquid
2. Determining boiling point of the liquid
3. BASIC THEORY:
Distillation is a widely used method for separating mixtures based on differences in the
conditions required to change the phase of components of the mixture. To separate a
mixture of liquids, the liquid can be heated to force components, which have different
boiling points, into the gas phase. The gas is then condensed back into liquid form and
collected. Although the term is most commonly applied to liquids, the reverse process
can be used to separate gases by liquefying components using changes in temperature
and/or pressure. Distillation is used for many commercial processes, such as production
of gasoline, distilled water, xylene, alcohol, paraffin, kerosene, and many other liquids.
Distillation is used to purify a compound by separating it from a non-volatile or less-
volatile material. When different compounds in a mixture have different boiling points,
they separate into individual components when the mixture is carefully distilled.
The boiling point is the temperature at which the vapor pressure of the liquid phase of a
compound equals the external pressure acting on the surface of the liquid. The external
pressure is usually the atmospheric pressure. For instance, consider a liquid heated in
an open flask. The vapor pressure of the liquid will increase as the temperature of the
liquid increases, and when the vapor pressure equals the atmospheric pressure, the
liquid will boil. Different compounds boil at different temperatures because each has a
different, characteristic vapor pressure: compounds with higher vapor pressures will
boil at lower temperatures.
Boiling points are usually measured by recording the boiling point (or range) on a
thermometer while performing a distillation. This method is used whenever there is
enough of the compound to perform a distillation. The distillation method of boiling
point determination measures the temperature of the vapors above the liquid. Since
these vapors are in equilibrium with the boiling liquid, they are the same temperature
as the boiling liquid. The vapor temperature rather than the pot temperature is
measured because if you put a thermometer actually in the boiling liquid mixture, the
temperature reading would likely be higher than that of the vapors. This is because the
liquid can be superheated or contaminated with other substances, and therefore its
temperature is not an accurate measurement of the boiling temperature.
4. DESIGN OF EXPERIMENT :
a) Equipments and Materials
• Equipment :
b) Procedure
a. Draw the distillation set complete with the name of apparatus in the blank space
bellow:
b. Write down the procedures by using flow cart !
1)……………………………………………………………………….
NaCl (aq)
Distillation flask
2) …………………………………………………………………………..
EXPERIMENT
RESULT
Dropped AgNO3 0,1M
and compared
Result of experiment
No. Experiment Prosedure
Before After
1.
2.
3.
4.
5.
6. DATA ANALYSIS
………………………………………………………………………………………………………………………………………………
……………………………………………………………………………………………………………………………………………..
………………………………………………………………………………………………………………………………………………
……………………………………………………………………………………………………………………………………………..
………………………………………………………………………………………………………………………………………………
……………………………………………………………………………………………………………………………………………..
………………………………………………………………………………………………………………………………………………
……………………………………………………………………………………………………………………………………………..
………………………………………………………………………………………………………………………………………………
……………………………………………………………………………………………………………………………………………..
………………………………………………………………………………………………………………………………………………
……………………………………………………………………………………………………………………………………………..
………………………………………………………………………………………………………………………………………………
……………………………………………………………………………………………………………………………………………..
………………………………………………………………………………………………………………………………………………
……………………………………………………………………………………………………………………………………………..
………………………………………………………………………………………………………………………………………………
……………………………………………………………………………………………………………………………………………..
7. DISCUSSION
………………………………………………………………………………………………………………………………………………
……………………………………………………………………………………………………………………………………………..
………………………………………………………………………………………………………………………………………………
……………………………………………………………………………………………………………………………………………..
………………………………………………………………………………………………………………………………………………
……………………………………………………………………………………………………………………………………………..
………………………………………………………………………………………………………………………………………………
……………………………………………………………………………………………………………………………………………..
………………………………………………………………………………………………………………………………………………
……………………………………………………………………………………………………………………………………………..
………………………………………………………………………………………………………………………………………………
……………………………………………………………………………………………………………………………………………..
8. CONCLUSION
………………………………………………………………………………………………………………………………………………
……………………………………………………………………………………………………………………………………………..
………………………………………………………………………………………………………………………………………………
……………………………………………………………………………………………………………………………………………..
Why the water flow into the liquefier with different direction in the distillate flow?
Answer :
………………………………………………………………………………………………………………………………………………
……………………………………………………………………………………………………………………………………………..
………………………………………………………………………………………………………………………………………………
……………………………………………………………………………………………………………………………………………..
REFERENCES
………………………………………………………………………………………………………………………………………………
……………………………………………………………………………………………………………………………………………..
B. Cfg
C. Hb
D. bh