A.

Title of Experiment
B. Date and Time of Experiment
C. Purpose of Experiment

D. Basic Theories
E. Tools and Materials
F. Procedures
G. Result of Experiment
No. Procedures Result of Observation Hyphotesis/Reaction Conclusion
Exp Before After
1 Determine the Peroxide Number - Aquades: - Aquades + - H2O2(aq) + 2KI(aq)  Based on the
a. Blanco solution colorless acetic acid : I2(aq) + 2KOH(aq) experiment, it
5 grams of Aquades solution chloroform: - CH3(CH2)14COOH(aq) can conclude that

 Entered into erlenmeyer flask - Acetic acid : colorless + 2KI(aq) + H2O2(aq) blanco solution is
 Added 30 mL acetic acid : chloroform chloroform: solution  used as
(3:2)
 Shaken until homogenous colorless - + KI: soft CH3(CH2)14COOK(aq) comparison
 Added 0,5 mL saturated KI solutiom
solution yellow solution + I2(aq) + H2O2(aq) solution.
 Let it 20 minutes with shaken sometimes
 Added 30 mL aquades - Saturated - + Aquades: soft
 Titrated with Na2S2O3 until yellow color
change KI: light yellow solution Red: I2 + 2e  2I-
 Added 0,5 mL starch solution 1% yellow - + Na2S2O3:
 Titrated again with Na2S2O3 0,1N until
Oxd: 2S2O32-  S4O62-
colorless solution formed two + 2e
 Written the volume that needed
- Na2S2O3: layer. soft
Volume Na2S2O3 I2(aq) + 2S2O32-(aq) 
colorless yellow (++)
2I-(aq) + S4O62-(aq)
solution (top) and
- Starch yellow (down)
solution: V = 0,1 ml
 white turbid - + strach:
solution blackish purple
solution
- + Na2S2O3:
formed two
layer. soft
yellow (++)
(top) and
yellow (down)
V = 0,1 ml
Vtotal = 0,2 ml

b. Sample Solution - Oil: yellow - Oil + acetic - H2O2(aq) + 2KI(aq)  Based on the
solution acid : I2(aq) + 2KOH(aq) experiment, it
- Acetic acid : chloroform: - CH3(CH2)14COOH(aq) can conclude that
chloroform: yellow solution + 2KI(aq) + H2O2(aq) the peroxide
colorless - + KI: yellow  number is 105,34
solution solution CH3(CH2)14COOK(aq)
- KI: light - + aquades: + I2(aq) + H2O2(aq)
 yellow yellow soft Red: I2 + 2e  2I-
5 grams of oil/fat solution solution Oxd: 2S2O32-  S4O62-
 Entered into erlenmeyer flask - Na2S2O3: - Na2S2O3: + 2e
 Added 30 mL acetic acid : chloroform colorless formed two
(3:2) I2(aq) + 2S2O32-(aq) 
 Shaken until homogenous solution layer. yellow 2I-(aq) + S4O62-(aq)
 Added 0,5 mL saturated KI solutiom
- Aquades: soft (top) and
 Let it 20 minutes with shaken sometimes
 Added 30 mL aquades colorless yellow (down) H
CH2OH

O H H
CH2OH

O H


O

Titrated with Na2S2O3 until yellow color

O H O OH H
OH

change solution V1 = 0,3 ml H OH H OH

n(aq)
 Added 0,5 mL starch solution 1% - Starch: V2 = 0,9 ml + nI2(aq) →
 Titrated again with Na2S2O3 0,1N until CH2OH CH2OH

colorless white turbid V3 = 0,6 ml I

O
H

OH
O

H
H I

O
H

OH
O

H
H I

 Written the volume that needed H OH H OH n

solution - + starch: turbid

 Repeat 3x n(aq)
Volume Na2S2O3
(top) and
yellow (down) CH2OH CH2OH

I H O H I H O H I

O O O

- Na2S2O3:
OH H OH H

H OH H OH n n(aq)
formed two
+ 2Na2S2O3(aq) 
layer. yellow
2NaI(aq) + Na2S2O6(aq)
soft (top) and
yellow (down)
V1 = 4,9 ml
 V2 = 4,8 ml
V3 = 4,9 ml
Vtotal of Na2S2O3
V1 = 5,2 ml
V2 = 5,7 ml
V3 = 5,5 ml
2 Determine the Free Fatty Acid (FFA) - Aquades: - Aquades + Based on the
a. Blanco solution colorless ethanol: experiment, it

6 grams of Aquades solution colorless can conclude that

- Ethanol: solution blanco solution is
 Entered into erlenmeyer flask
 Added 10 mL alcohol 96% colorless - + PP: colorless used as
 Added 2 drops of PP indicator solution solution comparison
 Shaken
- PP: colorless - + NaOH: soft solution
 Titrated with NaOH 0,1N
 Written the volume that needed solution pink solution
- NaOH: V = 0,3 ml
Volume NaOH colorless
solution
b. Sample solution - Oil: yellow - Oil + ethanol: - CH3(CH2)14COOH(aq) Based on the
solution form two layer. + CH3CH2OH(aq)  experiment, it
 - Ethanol: turbid (top) and CH3(CH2)14COOCH2C can conclude that

6 grams of Aquades colorless yellow (down) H3(aq) + H2O(l) %FFA of oil is

solution - + PP: form two - CH3(CH2)14COOCH2C 0,163%
 Entered into erlenmeyer flask
 Added 10 mL alcohol 96% - PP: colorless layer. turbid H3(aq) + NaOH(aq) 
 Added 2 drops of PP indicator solution (top) and CH3CH2OH(aq) +
 Shaken
- NaOH: yellow (down) CH3(CH2)14COONa(aq
 Titrated with NaOH 0,1N
 Written the volume that needed colorless - + NaOH: pink )
 Repeat 3x solution solution (top) %FFA of oil is less than
and yellow 0,3%
Volume NaOH
(down)
 Calculated the % of FFA V1 = 0,4 ml
V2 = 0,6 ml
%FFA
V3 = 1 ml
H. Analysis and Explanation
I. Conclusion
References
Attacment
A. Answer of Question
B. Documentation
C. Calcutaion