- Guy am < _WgVERSIOADE REOIONAL DO NOROF TE COESTADO 00 RIO GRANOE 00 6UL ‘vontaas pe hr ons -0 La, eae pn aes Mo al ‘en arp ments -OOU.itunbesteleon Ne OOU sets ee Central Analitica : ‘Registro CRQ 5* Regio 4,022 . Cortiicado de Cadactro FEPAM NF 34/2005D1, 1DeBQ- Departamento d Blologia e Quimica RELATORIO DE aNAtise a N° @0307 TWPO De ANALISE | Gieo Essencial DENTIFICAGAO DA AMOSTRA, Citronela (Cymbopogon nerdus) NOMERO| eee 8 3 2 OATAEHORADE REZEDIMENTO 080007 PERlo00 D§ REALIZAGAO DA ANALISE 2/0207 a 23101007 DATADE EMIS8AO 0D RELATORIO 22/03/07 Janauise | unioabe | __RESULTADO méTODO Citronetal | © ha She 924 reraagafo Goso80 iCitronetol : % 9,56. Cromatografia Gasosa_ i jot Zi & 1998 Cromatogratia Gasosd ures Cx Cromatografia Gasosa ‘OBS: A amostra foi ‘Beavia Walber ‘CRO S*Regiso N° 05201584 prob a repredco cll Ou paca deste documento, sem » ateriacdo Tria dese taocatii. sc rialids desl couse etre meet aach iin eratmentoe masters: orn aaa ‘CAMPUS ul Ftva do Comercio. 3000 Caka Pora! 660 CEP 98700-000 Fone: bux (58) 8332 0442 E-mal: egab@unjuthe br IDEN eee nero. Deere Egat do ree 0 Ee WANTENEDON | Poa 20\ Title : Andlisc de Oleos Essenciais Run File C:\STAR\MODULEL6\CAABAO30 . RUN Method Pile : :\STAR\MODULE16\METODOS\CAADANE .MTH Sample IP + ‘Citrpnela Injection Date: 15-MAR-7 3:23 PM calculation Date: 21-MAR~7 4:12 BM Operator = Anagilda Detector Type: ADCB (10 volts) Workstation: Bus Address : 16 Instrument : Varian stax #1 Sample Rate + 10.00 Hz Channel A=A) Run Time 62.002 min seereeeneee Star Chromatography Worketation ******* Version 4,5 *#ft¥shusessee Chart Speed = 0.61 cm/min Attenuation = 1100 Baro offset = 5% Start Time = 0 min gfind Time 33.000 min, Min / Tick, = 1.00Print Date: Wed Mar 21 16:15:49 2007 Page 1 of 2 Title 1 Andlise de Oleos Essenciais Run File ; C:\STAR\MODULW16\CAADA030, RUN Method File : C:\S'tAR\MODULHi6\MBTODOS\CAADANS . MTH Sample ID Citronela Injection Date: 15-298-7 3:23 PM Calculation pate: 21-MAR-7 4:12 PM Operator: Anagilda Detector Type: ADCB (10 volts) Workstation: Bus Address : 16 Instrument : Varian star #1 Sample Rate : 10.00 Hz chamel =: A= A Run Time : 62.002 min seennereees star Chromatography Workstation ++###6+. Version a.5 teérrereestenre Run Node : Analysis é Peak Measurement: Peak Area Calculation Type: Percent Ret. ‘Time width Peak Result Time Offset area Sep, 1/2 Status Name 0 (min) (min) (counts) Code (sec) Codes 0.2766 2.786 0.000 15964 BB 1.8 0.0032 3.613 0.000 184 BB 1.6 . 00,0224 3.948 0.000 1278 BB 2.1 0.0098 4.534 0.000 363 BB 2.4 0.0266 4,807 0.000 1534 BV 2.8 0.1248 4.922 0.000 7203 Ve 3.3 0.0086 «8.177 0,000 326 «BY 26 | 0.0106 §.251 0.000 612 VB 2.5 0.0053 §.569 0.000 308 BB 2.4 0.0025 8.767 0.000 was BY 2.8 i | 3.0256 5,898 0.000 174632) VB 3.4 0.0099 6.159 0.000 573 TS 0.0 0.0216 6.464 0.000 1248 BY. ae 0.0746 6.595 -0,000 4308 VB a. 0.0106 6.761 0.000 611 . BB 3.2 0.0058 7.187 9.000 337 BB 3.4 0.0577 7.697 , 0.000 3328 BB 4.2 E 0.6103 8.092 0.000 35228 BB 4.3 2.0148 B.472 0.000 BS4 BV 4.2 0.0064 8.592 0.000 3710 vB 0.0 0.0431 9-149 0.000 2487 BB 4.6 0.0056 9.413 0.000 322 BP 37g 0.6431 9.670 0.000 37121 PY 510 citronelal 43.2358 10,083 0.003 2a9ss26 BCG. 0,0238 10.390 0.000 1374 TS 0.0 0.0266 10.583 0.000 1533 «TS 0.0 : 0.0326 ' 10.853 0.900 1884 TS 0.0 0.0349 «41.116 0.000 2015 Ts 0.0 0.0442 11.390 9,900 2549 BV 5.0 00,0168 11.550 0.000 369 VB a7 0.0925 12.019 0.000 5340 BB Sub 0.0155 12,580 0.000 393 «BB 4,9 citronelol 9.5620 13.023 0,003 SS191L BB. 5.5 0;4950 13.410 0,000 28568 TS 0.0 Geraniol ‘19.9844 14.138 0.000 1153479 BB 6.3 0.8752 14.645 0.000 39029 «TS 0.0 0.0064 15.172 0.000 370 BB rey 0.0123 16.001 0,000 655 BB