Factor 1 Factor 2 Factor 3 Factor 4 Response 1

Run Block A:oil to methanol (v/v) B:NaOH(%) C:Temperature

D:Time(hr) %BD yield

1 Block 1 7.00 2.25 57.50 3.50

2 Block 1 7.00 2.25 57.50 3.50
3 Block 1 9.00 3.00 55.00 2.00
4 Block 1 7.00 2.25 57.50 3.50
5 Block 1 5.00 3.00 60.00 5.00
6 Block 1 5.00 1.50 55.00 2.00
7 Block 1 5.00 3.00 60.00 2.00
8 Block 1 5.00 3.00 55.00 2.00
9 Block 1 9.00 1.50 55.00 5.00
10 Block 1 7.00 2.25 57.50 3.50
11 Block 1 9.00 3.00 60.00 5.00
12 Block 1 9.00 3.00 55.00 5.00
13 Block 1 7.00 2.25 62.50 3.50
14 Block 1 7.00 2.25 52.50 3.50
15 Block 1 9.00 1.50 60.00 5.00
16 Block 1 9.00 1.50 55.00 2.00
17 Block 1 5.00 3.00 55.00 5.00
18 Block 1 7.00 2.25 57.50 3.50
19 Block 1 3.00 2.25 57.50 3.50
20 Block 1 9.00 1.50 60.00 2.00
21 Block 1 7.00 2.25 57.50 6.50
22 Block 1 7.00 3.75 57.50 3.50
23 Block 1 7.00 2.25 57.50 0.50
24 Block 1 9.00 3.00 60.00 2.00
25 Block 1 7.00 0.75 57.50 3.50
26 Block 1 5.00 1.50 55.00 5.00
27 Block 1 5.00 1.50 60.00 2.00
28 Block 1 11.00 2.25 57.50 3.50
29 Block 1 7.00 2.25 57.50 3.50
30 Block 1 5.00 1.50 60.00 5.00

Factor 1 Factor 2 Factor 3 Factor 4 Response 1

 A:oil to methanol (v/v) B:NaOH(%) C:Temperature D:Time(hr) %BD
yield

7.00 2.25 57.50 3.50

7.00 2.25 57.50 3.50
9.00 3.00 55.00 2.00
7.00 2.25 57.50 3.50
5.00 3.00 60.00 5.00
5.00 1.50 55.00 2.00
5.00 3.00 60.00 2.00
5.00 3.00 55.00 2.00
9.00 1.50 55.00 5.00
7.00 2.25 57.50 3.50
9.00 3.00 60.00 5.00
9.00 3.00 55.00 5.00
7.00 2.25 62.50 3.50
7.00 2.25 52.50 3.50
9.00 1.50 60.00 5.00
9.00 1.50 55.00 2.00
5.00 3.00 55.00 5.00
7.00 2.25 57.50 3.50
3.00 2.25 57.50 3.50
9.00 1.50 60.00 2.00
7.00 2.25 57.50 6.50
7.00 3.75 57.50 3.50
7.00 2.25 57.50 0.50
9.00 3.00 60.00 2.00
7.00 0.75 57.50 3.50
5.00 1.50 55.00 5.00
5.00 1.50 60.00 2.00
11.00 2.25 57.50 3.50
7.00 2.25 57.50 3.50
5.00 1.50 60.00 5.00

Factor 1 Factor 2 Factor 3 Factor 4 Response 1

Run Block A:oil to methanol (v/v) B:NaOH(%) C:Temperature D:Time(hr)
%BD yield

5 Block 1 5.00 3.00 60.00 5.00

6 Block 1 5.00 1.50 55.00 2.00
7 Block 1 5.00 3.00 60.00 2.00
8 Block 1 5.00 3.00 55.00 2.00
9 Block 1 9.00 1.50 55.00 5.00
10 Block 1 7.00 2.25 57.50 3.50
11 Block 1 9.00 3.00 60.00 5.00
12 Block 1 9.00 3.00 55.00 5.00
13 Block 1 7.00 2.25 62.50 3.50
14 Block 1 7.00 2.25 52.50 3.50
15 Block 1 9.00 1.50 60.00 5.00
16 Block 1 9.00 1.50 55.00 2.00
17 Block 1 5.00 3.00 55.00 5.00
18 Block 1 7.00 2.25 57.50 3.50
19 Block 1 3.00 2.25 57.50 3.50
20 Block 1 9.00 1.50 60.00 2.00
21 Block 1 7.00 2.25 57.50 6.50
22 Block 1 7.00 3.75 57.50 3.50
23 Block 1 7.00 2.25 57.50 0.50
24 Block 1 9.00 3.00 60.00 2.00
25 Block 1 7.00 0.75 57.50 3.50
26 Block 1 5.00 1.50 55.00 5.00
27 Block 1 5.00 1.50 60.00 2.00
28 Block 1 11.00 2.25 57.50 3.50
29 Block 1 7.00 2.25 57.50 3.50
30 Block 1 5.00 1.50 60.00 5.00

12 1 Block 1 9.00 10.00 55.00 90.00

27 2 Block 1 7.50 7.50 57.50 75.00
5 3 Block 1 6.00 5.00 60.00 60.00
25 4 Block 1 7.50 7.50 57.50 75.00
7 5 Block 1 6.00 10.00 60.00 60.00
30 6 Block 1 7.50 7.50 57.50 75.00
3 7 Block 1 6.00 10.00 55.00 60.00
16 8 Block 1 9.00 10.00 60.00 90.00
20 9 Block 1 7.50 12.50 57.50 75.00
17 10 Block 1 4.50 7.50 57.50 75.00
9 11 Block 1 6.00 5.00 55.00 90.00
24 12 Block 1 7.50 7.50 57.50 105.00
8 13 Block 1 9.00 10.00 60.00 60.00
21 14 Block 1 7.50 7.50 52.50 75.00
29 15 Block 1 7.50 7.50 57.50 75.00
11 16 Block 1 6.00 10.00 55.00 90.00
15 17 Block 1 6.00 10.00 60.00 90.00
1 18 Block 1 6.00 5.00 55.00 60.00
18 19 Block 1 10.50 7.50 57.50 75.00
19 20 Block 1 7.50 2.50 57.50 75.00
2 21 Block 1 9.00 5.00 55.00 60.00
4 22 Block 1 9.00 10.00 55.00 60.00
10 23 Block 1 9.00 5.00 55.00 90.00
22 24 Block 1 7.50 7.50 62.50 75.00
6 25 Block 1 9.00 5.00 60.00 60.00
14 26 Block 1 9.00 5.00 60.00 90.00
13 27 Block 1 6.00 5.00 60.00 90.00
23 28 Block 1 7.50 7.50 57.50 45.00
26 29 Block 1 7.50 7.50 57.50 75.00
28 30 Block 1 7.50 7.50 57.50 75.00

Factor 1 Factor 2 Factor 3 Factor 4 Response 1

Run Block A:Oil to methanol (v/v) B:H2SO4 (%) C:Temperature (oc)
D:Time(min) %FFA

5 1 Block 1 6.00 5.00 60.00 60.00

25 2 Block 1 7.50 7.50 57.50 75.00
26 3 Block 1 7.50 7.50 57.50 75.00
27 4 Block 1 7.50 7.50 57.50 75.00
3 5 Block 1 6.00 10.00 55.00 60.00
15 6 Block 1 6.00 10.00 60.00 90.00
22 7 Block 1 7.50 7.50 62.50 75.00
4 8 Block 1 9.00 10.00 55.00 60.00
16 9 Block 1 9.00 10.00 60.00 90.00
1 10 Block 1 6.00 5.00 55.00 60.00
21 11 Block 1 7.50 7.50 52.50 75.00
24 12 Block 1 7.50 7.50 57.50 105.00
23 13 Block 1 7.50 7.50 57.50 45.00
17 14 Block 1 4.50 7.50 57.50 75.00
13 15 Block 1 6.00 5.00 60.00 90.00
7 16 Block 1 6.00 10.00 60.00 60.00
2 17 Block 1 9.00 5.00 55.00 60.00
10 18 Block 1 9.00 5.00 55.00 90.00
12 19 Block 1 9.00 10.00 55.00 90.00
6 20 Block 1 9.00 5.00 60.00 60.00
8 21 Block 1 9.00 10.00 60.00 60.00
18 22 Block 1 10.50 7.50 57.50 75.00
9 23 Block 1 6.00 5.00 55.00 90.00
19 24 Block 1 7.50 2.50 57.50 75.00
30 25 Block 1 7.50 7.50 57.50 75.00
28 26 Block 1 7.50 7.50 57.50 75.00
14 27 Block 1 9.00 5.00 60.00 90.00
29 28 Block 1 7.50 7.50 57.50 75.00
11 29 Block 1 6.00 10.00 55.00 90.00
20 30 Block 1 7.50 12.50 57.50 75.00