Kelompok : 3

Sintesis : dihidropirimidon

Pembagian Tugas Kelompok Dalam Melakukan Sintesis

Jabatan dalam Nama Tugas

Kelompok
Ketua Diah Nurhayati Menimbang benzaldehida
Menyaring kristal
Anggota Chelsea Stefani P Menimbang etil asetoasetat
Rekristalisasi
Anggota Deri Priatna Menimbang urea
Anggota Farah Hazmatulhaq Memeras jeruk
Anggota Saskia Teja Widya Memasukkan semua bahan
kedalam wadah
Mengukur titik leleh
Chemical and Physical Properties of the Compound

1. Benzaldehid

Property Name Property Value

Molecular Weight 106.124 g/mol

Topological Polar Surface Area 17.1 A^2

Monoisotopic Mass 106.042 g/mol

Exact Mass 106.042 g/mol

Physical Description

BENZALDEHYDE is a clear colorless to yellow liquid with a bitter almond odor. Flash
point near 145°F. More denser than water and insoluble in water. Hence sinks in water.
Vapors are heavier than air. The primary hazard is to the environment. Immediate steps
should be taken to limit spread to the environment. Easily penetrates the soil to
contaminate groundwater and nearby waterways. Used in flavoring and perfume
making.

Boiling Point

354° F at 760 mm Hg (NTP, 1992)

from CAMEO Chemicals
178.7 deg C
Haynes, W.M. (ed.). CRC Handbook of Chemistry and Physics. 95th Edition. CRC Press LLC, Boca
Raton: FL 2014-2015, p. 3-24
from HSDB
179°C
from ILO-ICSC
354°F
from OSHA Occupational Chemical DB
Melting Point

-15° F (NTP, 1992)

from CAMEO Chemicals
-57.12 deg C
Haynes, W.M. (ed.). CRC Handbook of Chemistry and Physics. 95th Edition. CRC Press LLC, Boca
Raton: FL 2014-2015, p. 3-34
from HSDB
-26 °C
from Human Metabolome Database (HMDB)
-26°C
from ILO-ICSC
-15°F
from OSHA Occupational Chemical DB
Solubility
less than 0.1 mg/mL at 67.1° F (NTP, 1992)
from CAMEO Chemicals

In water, 6950 mg/L at 25 deg C

Yalkowsky, S.H., He, Yan, Jain, P. Handbook of Aqueous Solubility Data Second Edition. CRC Press,
Boca Raton, FL 2010, p. 367

from HSDB

Approximately 0.6% wt. at 20 deg C

Opgrande JL et al; Benzaldehyde. Kirk-Othmer Encyclopedia of Chemical Technology. (1999-2016). New
York, NY: John Wiley & Sons. Online Posting Date: 16 May 2003

from HSDB

Miscible with alcohol, ether, fixed and volatile oils

Larranaga, M.D., Lewis, R.J. Sr., Lewis, R.A.; Hawley's Condensed Chemical Dictionary 16th Edition.
John Wiley & Sons, Inc. Hoboken, NJ 2016., p. 150

from HSDB

Soluble in liquid ammonia

Weast, R.C. (ed.). Handbook of Chemistry and Physics. 60th ed. Boca Raton, Florida: CRC Press Inc.,
1979., p. C-140

from HSDB

Solubility of water in benzaldehyde at 20 deg C, wt%: 1.5

Opgrande JL et al; Benzaldehyde. Kirk-Othmer Encyclopedia of Chemical Technology. (1999-2016). New
York, NY: John Wiley & Sons. Online Posting Date: 16 May 2003

from HSDB

6.95 mg/mL at 25 °C
from Human Metabolome Database (HMDB)

Solubility in water at 25°C: poor

from ILO-ICSC
 Density
1.046 at 68° F (USCG, 1999)
from CAMEO Chemicals

1.050 at 15 deg C/4 deg C

O'Neil, M.J. (ed.). The Merck Index - An Encyclopedia of Chemicals, Drugs, and Biologicals. Cambridge,
UK: Royal Society of Chemistry, 2013., p. 186

from HSDB

Relative density (water = 1): 1.05

from ILO-ICSC

1.046
from OSHA Occupational Chemical DB

2. 2- Naftol

Property Name Property Value

Molecular Weight 144.173 g/mol

Topological Polar Surface Area 20.2 A^2

Monoisotopic Mass 144.058 g/mol

Exact Mass 144.058 g/mol

XLogP3 2.7

Physical Description
1. DryPowder
2. Liquid
from EPA Chemicals under the TSCA
Solid
from Human Metabolome Database (HMDB)
WHITE-TO-YELLOWISH-WHITE CRYSTALS WITH CHARACTERISTIC ODOUR.
from ILO-ICSC
Color
White, lustrious, bulky leaflets or white powder. Darkens with age
Lewis, R.J. Sr.; Hawley's Condensed Chemical Dictionary 15th Edition. John Wiley & Sons, Inc. New
York, NY 2007., p. 874
from HSDB
Boiling Point
285 deg C
Lewis, R.J. Sr.; Hawley's Condensed Chemical Dictionary 15th Edition. John Wiley & Sons,
Inc. New York, NY 2007., p. 874
from HSDB
285°C
from ILO-ICSC
Melting Point
121.6 deg C
Lewis, R.J. Sr.; Hawley's Condensed Chemical Dictionary 15th Edition. John Wiley & Sons,
Inc. New York, NY 2007., p. 874
from HSDB
123 °C
from Human Metabolome Database (HMDB)
122°C
Solubility
In water, 7.55X10+2 mg/L at 25 deg C
Yalkowsky, S.H., He, Yan, Jain, P. Handbook of Aqueous Solubility Data Second Edition.
CRC Press, Boca Raton, FL 2010, p. 651
from HSDB
Soluble in alcohol, ether, chloroform, glycerol, oils, alkaline solutions
Lewis, R.J. Sr.; Hawley's Condensed Chemical Dictionary 15th Edition. John Wiley & Sons,
Inc. New York, NY 2007., p. 874
from HSDB
Very soluble in ethanol, ethyl ether; soluble in benzene, chloroform; slightly soluble
in ligroin
Haynes, W.M. (ed.). CRC Handbook of Chemistry and Physics. 95th Edition. CRC Press
LLC, Boca Raton: FL 2014-2015, p. 3-406
from HSDB
1 gram dissolves in 1000 mL water, 80 mL boiling water, 0.8 mL alcohol, 17
mL chloroform, 1.3 mL ether
O'Neil, M.J. (ed.). The Merck Index - An Encyclopedia of Chemicals, Drugs, and Biologicals.
Cambridge, UK: Royal Society of Chemistry, 2013., p. 1189
from HSDB
Solubility in water, g/100ml at 25°C: 0.074
from ILO-ICSC
Density
1.28 g/cu cm at 20 deg C
Haynes, W.M. (ed.). CRC Handbook of Chemistry and Physics. 95th Edition. CRC Press
LLC, Boca Raton: FL 2014-2015, p. 3-406
from HSDB
1.28 g/cm³
from ILO-ICSC

3. 1-Phenilazo-2-Naphtol
 Property Name Property Value

Molecular Weight 248.285 g/mol

Topological Polar Surface Area 41.5 A^2

Monoisotopic Mass 248.095 g/mol

Exact Mass 248.095 g/mol

XLogP3-AA 3.6

Physical Description
PHYSICAL DESCRIPTION: Dark reddish-yellow leaflets or orange powder. Slight
odor. (NTP, 1992)
from CAMEO Chemicals
Color
BRICK-RED CRYSTALS (LEAFLETS FROM ETHANOL)
IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Humans.
Geneva: World Health Organization, International Agency for Research on Cancer, 1972-
PRESENT. (Multivolume work). Available
at:http://monographs.iarc.fr/ENG/Classification/index.php , p. V8 225 (1975)
from HSDB
Boiling Point
greater than 212° F at 760 mm Hg (sublimes) (NTP, 1992)
from CAMEO Chemicals

Melting Point
268 to 271° F (NTP, 1992)
from CAMEO Chemicals

134 DEG C
IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Humans.
Geneva: World Health Organization, International Agency for Research on Cancer, 1972-
PRESENT. (Multivolume work). Available
at:http://monographs.iarc.fr/ENG/Classification/index.php , p. V8 225 (1975)
from HSDB

Solubility
less than 0.1 mg/mL at 64° F (NTP, 1992)
from CAMEO Chemicals
SOL IN ETHANOL, ACETONE, ETHER & BENZENE; INSOL IN WATER
IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Humans.
Geneva: World Health Organization, International Agency for Research on Cancer, 1972-
PRESENT. (Multivolume work). Available
at:http://monographs.iarc.fr/ENG/Classification/index.php , p. V8 225 (1975)
from HSDB
SOL IN PETROLEUM ETHER, CARBON DISULFIDE, CONCN HYDROCHLORIC
ACID
Weast, R.C. (ed.). Handbook of Chemistry and Physics. 60th ed. Boca Raton, Florida: CRC
Press Inc., 1979., p. C-132
from HSDB
Density
0.18 (NTP, 1992)
from CAMEO Chemicals

4. Thiamin Hydroklorida

Property Name Property Value

Molecular Weight 337.263 g/mol

Topological Polar Surface Area 104 A^2

Monoisotopic Mass 336.058 g/mol

Exact Mass 336.058 g/mol

Color
Crystals from water
Lewis, R.J. Sr. (ed) Sax's Dangerous Properties of Industrial Materials. 11th Edition. Wiley-
Interscience, Wiley & Sons, Inc. Hoboken, NJ. 2004., p. 3441
from HSDB
Odor
SLIGHT, CHARACTERISTIC
Osol, A. and J.E. Hoover, et al. (eds.). Remington's Pharmaceutical Sciences. 15th ed.
Easton, Pennsylvania: Mack Publishing Co., 1975., p. 962
from HSDB
Melting Point
164 deg C
Lide, D.R. CRC Handbook of Chemistry and Physics 88TH Edition 2007-2008. CRC Press,
Taylor & Francis, Boca Raton, FL 2007, p. 3-482
from HSDB
Solubility
In water, approximately 5.0X10+5 mg/L, temp not specified
Budavari, S. (ed.). The Merck Index - An Encyclopedia of Chemicals, Drugs, and Biologicals.
Whitehouse Station, NJ: Merck and Co., Inc., 1996.
 from HSDB
Vapor Pressure
1.8X10-10 mm Hg at 25 deg C (est)
US EPA; Estimation Program Interface (EPI) Suite. Ver. 4.0. Jan, 2009. Available from, as
of Feb 16, 2010:http://www.epa.gov/oppt/exposure/pubs/episuitedl.htm

from HSDB
Stability
Stable under normal storage conditions; it is degraded in neutral and alkaline
solutions (even at room temp)
Furia, T.E. (ed.). CRC Handbook of Food Additives. 2nd ed. Cleveland: The Chemical Rubber
Co., 1972., p. 89
from HSDB

5. Etil Asetoasetat

Property Name Property Value

Molecular Weight 130.143 g/mol

Topological Polar Surface Area 43.4 A^2

Monoisotopic Mass 130.063 g/mol

Exact Mass 130.063 g/mol

XLogP3 0.2

Physical Description
ETHYL ACETOACETATE is a colorless liquid with a fruity odor. Flash point 185°F.
Boiling point 365°F. May cause adverse health effects if ingested or inhaled. May
irritate to skin, eyes and mucous membranes. Used in organic synthesis and in
lacquers and paints.
from CAMEO Chemicals
Liquid
from EPA Chemicals under the TSCA, Human Metabolome Database (HMDB)
COLOURLESS LIQUID WITH CHARACTERISTIC ODOUR.
from ILO-ICSC
Color
COLORLESS LIQUID
Hawley, G.G. The Condensed Chemical Dictionary. 9th ed. New York: Van Nostrand
Reinhold Co., 1977., p. 351
from HSDB
Odor
PLEASANT GREEN, FRUITY, RUM ODOR
Furia, T.E. (ed.). CRC Handbook of Food Additives. 2nd ed. Volume 2. Boca Raton, Florida:
CRC Press, Inc., 1980., p. 269
from HSDB
Taste
RIPE FRUIT TASTE
Furia, T.E. (ed.). CRC Handbook of Food Additives. 2nd ed. Volume 2. Boca Raton, Florida:
CRC Press, Inc., 1980., p. 269
from HSDB
Boiling Point
363° F at 760 mm Hg (USCG, 1999)
from CAMEO Chemicals
180.8 DEG C AT 760 MM HG
The Merck Index. 9th ed. Rahway, New Jersey: Merck & Co., Inc., 1976., p. 495
from HSDB
180.8°C
from ILO-ICSC
Melting Point
less than -112° F (USCG, 1999)
from CAMEO Chemicals
-45 DEG C
The Merck Index. 9th ed. Rahway, New Jersey: Merck & Co., Inc., 1976., p. 495
from HSDB
-45 °C
from Human Metabolome Database (HMDB)
-45°C
from ILO-ICSC
Solubility
SOL IN ABOUT 35 PARTS WATER
The Merck Index. 9th ed. Rahway, New Jersey: Merck & Co., Inc., 1976., p. 495
from HSDB

SOL IN BENZENE, & CHLOROFORM; MISCIBLE WITH ETHER, & ACETONE

Weast, R.C. (ed.). Handbook of Chemistry and Physics. 60th ed. Boca Raton, Florida: CRC
Press Inc., 1979., p. C-226
from HSDB

water solubility = 1.11X10+5 mg/l @ 17 deg C

Yalkowsky SH, Dannenfelser RM; The AQUASOL dATAbASE of Aqueous Solubility. Fifth
Ed, Tucson, AZ: Univ Az, College of Pharmacy (1992)
from HSDB

110 mg/mL at 17 °C
from Human Metabolome Database (HMDB)
Solubility in water, g/100ml at 20°C: 2.86
from ILO-ICSC

Density
1.028 at 68° F (USCG, 1999)
from CAMEO Chemicals

1.0282 AT 20 DEG C/4 DEG C

Weast, R.C. (ed.). Handbook of Chemistry and Physics. 60th ed. Boca Raton, Florida: CRC
Press Inc., 1979., p. C-226
from HSDB

Relative density (water = 1): 1.021

from ILO-ICSC

6. Urea

Property Name Property Value

Molecular Weight 61.048 g/mol

Topological Polar Surface Area 69.1 A^2

Monoisotopic Mass 61.036 g/mol

Exact Mass 61.036 g/mol

XLogP3-AA -1.4

Color
White crystals or powder
Lewis, R.J., Sr (Ed.). Hawley's Condensed Chemical Dictionary. 13th ed. New York, NY:
John Wiley & Sons, Inc. 1997., p. 1157
from HSDB

Tetragonal prisms
Budavari, S. (ed.). The Merck Index - An Encyclopedia of Chemicals, Drugs, and Biologicals.
Whitehouse Station, NJ: Merck and Co., Inc., 1996., p. 1683
from HSDB

Odor
MAY GRADUALLY DEVELOP SLIGHT ODOR OF AMMONIA, ESP IN PRESENCE
OF MOISTURE
Osol, A. and J.E. Hoover, et al. (eds.). Remington's Pharmaceutical Sciences. 15th ed.
Easton, Pennsylvania: Mack Publishing Co., 1975., p. 864
from HSDB

Almost odorless
Lewis, R.J., Sr (Ed.). Hawley's Condensed Chemical Dictionary. 13th ed. New York, NY:
John Wiley & Sons, Inc. 1997., p. 1157
from HSDB

Taste
Cooling, saline taste
Budavari, S. (ed.). The Merck Index - An Encyclopedia of Chemicals, Drugs, and Biologicals.
Whitehouse Station, NJ: Merck and Co., Inc., 1996., p. 1683
from HSDB

Boiling Point
Decomposes
Verschueren, K. Handbook of Environmental Data on Organic Chemicals. 3rd ed. New York,
NY: Van Nostrand Reinhold Co., 1996., p. 1876
from HSDB

Melting Point
132.70 deg C
Lewis, R.J., Sr (Ed.). Hawley's Condensed Chemical Dictionary. 13th ed. New York, NY:
John Wiley & Sons, Inc. 1997., p. 1157
from HSDB

Solubility
10 ml 95% alc, 6 ml methanol, 1 ml boiling 95% alc, 20 ml abs alc, 2 ml glycerol;
almost insol in chloroform, ether; sol in concn HCl
Budavari, S. (ed.). The Merck Index - An Encyclopedia of Chemicals, Drugs, and Biologicals.
Whitehouse Station, NJ: Merck and Co., Inc., 1996., p. 1683
from HSDB

INSOL IN BENZENE; SOL IN ACETIC ACID

Weast, R.C. (ed.). Handbook of Chemistry and Physics. 60th ed. Boca Raton, Florida: CRC
Press Inc., 1979., p. C-536
 from HSDB

Sol in pyrimidine
Lide, D.R. (ed). CRC Handbook of Chemistry and Physics. 72nd ed. Boca Raton, FL: CRC
Press, 1991-1992., p. 3-509
from HSDB

In water, 5.45X10+5 mg/l @ 25 deg C

Yalkowsky SH; Arizona Database of Aqueous Solubilities. Univ of AZ, College of Pharmacy
(1989)
from HSDB

Density
1.3230 @ 20 deg C/4 deg C
Lide, DR (ed.). CRC Handbook of Chemistry and Physics. 81st Edition. CRC Press LLC,
Boca Raton: FL 2000, p. 3-328
from HSDB

7. Aniline

Property Name Property Value

Molecular Weight 93.129 g/mol

Topological Polar Surface Area 26 A^2

Monoisotopic Mass 93.058 g/mol

Exact Mass 93.058 g/mol

XLogP3 0.9

Physical Description
ANILINE is a yellowish to brownish oily liquid with a musty fishy odor. Melting
point -6°C; boiling point 184°C; flash point 158°F. Denser than water (8.5 lb / gal)
and slightly soluble in water. Vapors heavier than air. Toxic by skin absorption and
inhalation. Produces toxic oxides of nitrogen during combustion. Used to
manufacture other chemicals, especially dyes, photographic chemicals, agricultural
chemicals and others.
from CAMEO Chemicals

PelletsLargeCrystals
 from EPA Chemicals under the TSCA

Liquid
from Human Metabolome Database (HMDB)

COLOURLESS OILY LIQUID WITH CHARACTERISTIC ODOUR. TURNS BROWN

ON EXPOSURE TO AIR OR LIGHT.
from ILO-ICSC

Colorless to brown, oily liquid with an aromatic amine-like odor.

from OSHA Occupational Chemical DB

Colorless to brown, oily liquid with an aromatic amine-like odor. [Note: A solid
below 21°F.]
from The National Institute for Occupational Safety and Health (NIOSH)

Color
Oily liquid; colorless when freshly distilled, darkens in exposure to air and light.
O'Neil, M.J. (ed.). The Merck Index - An Encyclopedia of Chemicals, Drugs, and Biologicals.
Whitehouse Station, NJ: Merck and Co., Inc., 2006., p. 107
from HSDB

Colorless with a bluish fluorescence when freshly distilled

IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Humans.
Geneva: World Health Organization, International Agency for Research on Cancer, 1972-
PRESENT. (Multivolume work). Available
at:http://monographs.iarc.fr/ENG/Classification/index.php , p. V4: 27 (1974)
from HSDB

Colorless to brown, oily liquid [Note: A solid below 21 deg F]

NIOSH. NIOSH Pocket Guide to Chemical Hazards & Other Databases CD-ROM.
Department of Health & Human Services, Centers for Disease Prevention & Control.
National Institute for Occupational Safety & Health. DHHS (NIOSH) Publication No.
2005-151 (2005)
from HSDB

Odor
Hedonic tone; pungent
Verschueren, K. Handbook of Environmental Data on Organic Chemicals. Volumes 1-2. 4th
ed. John Wiley & Sons. New York, NY. 2001, p. V1: 202
from HSDB
Aromatic amine-like odor.
NIOSH. NIOSH Pocket Guide to Chemical Hazards & Other Databases CD-ROM.
Department of Health & Human Services, Centers for Disease Prevention & Control.
National Institute for Occupational Safety & Health. DHHS (NIOSH) Publication No.
2005-151 (2005)
from HSDB

Taste
Burning taste
O'Neil, M.J. (ed.). The Merck Index - An Encyclopedia of Chemicals, Drugs, and Biologicals.
Whitehouse Station, NJ: Merck and Co., Inc., 2006., p. 107
from HSDB

Boiling Point
363 to 367° F at 760 mm Hg (EPA, 1998)
from CAMEO Chemicals
184.1 °C
PhysProp
from DrugBank
184.1 deg C
Lide, D.R. CRC Handbook of Chemistry and Physics 88TH Edition 2007-2008. CRC Press,
Taylor & Francis, Boca Raton, FL 2007, p. 3-26
from HSDB
184°C
from ILO-ICSC
363°F
from OSHA Occupational Chemical DB, The National Institute for Occupational Safety and
Health (NIOSH)
Melting Point
21° F (EPA, 1998)
from CAMEO Chemicals
-6 °C
PhysProp
from DrugBank
-6.0 deg C
Lide, D.R. CRC Handbook of Chemistry and Physics 88TH Edition 2007-2008. CRC Press,
Taylor & Francis, Boca Raton, FL 2007, p. 3-26
from HSDB
-6 °C
from Human Metabolome Database (HMDB)
-6°C
from ILO-ICSC
21°F
from OSHA Occupational Chemical DB, The National Institute for Occupational Safety and
Health (NIOSH)
Solubility
10 to 50 mg/mL at 73° F (NTP, 1992)
from CAMEO Chemicals

Water Solubility
36000 mg/L (at 25 °C)
YALKOWSKY,SH & DANNENFELSER,RM (1992)
from DrugBank

Miscible with chloroform, other organic solvents

O'Neil, M.J. (ed.). The Merck Index - An Encyclopedia of Chemicals, Drugs, and Biologicals.
Whitehouse Station, NJ: Merck and Co., Inc., 2006., p. 107
from HSDB

Miscible in ethanol, ethyl ether, benzene and acetone

Lide, D.R. CRC Handbook of Chemistry and Physics 88TH Edition 2007-2008. CRC Press,
Taylor & Francis, Boca Raton, FL 2007, p. 3-26
from HSDB

Miscible with lipids; soluble in dilute hydrochloric acid

IARC. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Humans.
Geneva: World Health Organization, International Agency for Research on Cancer, 1972-
PRESENT. (Multivolume work). Available
at:http://monographs.iarc.fr/ENG/Classification/index.php , p. V4: 28 (1974)
from HSDB

MISCIBLE WITH VEGETABLE OILS, ESSENTIAL OILS

Lefaux, R. Practical Toxicology of Plastics. Cleveland: CRC Press Inc., 1968., p. 105
from HSDB

3.5 parts/100 parts water at 25 deg C; 6.4 parts/100 parts water at 90 deg C
Aminin B, Lowenkron S; Kirk-Othmer Encyclopedia of Chemical Technology. (2001). New
York, NY: John Wiley & Sons; Aniline & Its Derivatives. Online Posting Date: July 18,
2003.
from HSDB

In water, 36,000 mg/L at 25 deg C

Yalkowsky, S.H., He, Yan., Handbook of Aqueous Solubility Data: An Extensive
Compilation of Aqueous Solubility Data for Organic Compounds Extracted from the
AQUASOL dATAbASE. CRC Press LLC, Boca Raton, FL. 2003., p. 262
 from HSDB

36 mg/mL at 25 °C
from Human Metabolome Database (HMDB)

Solubility in water, g/100ml at 20°C: 3.4

from ILO-ICSC

4%
from The National Institute for Occupational Safety and Health (NIOSH)

Density
1.022 at 68° F (EPA, 1998)
from CAMEO Chemicals

1.0217 at 20 deg C/20 deg C

Lide, D.R. CRC Handbook of Chemistry and Physics 88TH Edition 2007-2008. CRC Press,
Taylor & Francis, Boca Raton, FL 2007, p. 3-26
from HSDB

Relative density (water = 1): 1.02

from ILO-ICSC

1.02
from OSHA Occupational Chemical DB, The National Institute for Occupational Safety and
Health (NIOSH)

8. Benzoin

Property Name Property Value

Molecular Weight 212.248 g/mol

opological Polar Surface Area 37.3 A^2

Monoisotopic Mass 212.084 g/mol

Exact Mass 212.084 g/mol

XLogP3 2.1
Physical Description
PHYSICAL DESCRIPTION: Off-white to yellow-white crystalline solid with an odor
of camphor. Slightly acrid taste. When broken the fresh surfaces have a milky-white
color. (NTP, 1992)
from CAMEO Chemicals

DryPowder
from EPA Chemicals under the TSCA

Solid
from Human Metabolome Database (HMDB)

WHITE-TO-YELLOW CRYSTALS.
from ILO-ICSC

Color
REDDISH-BROWN GLOBULES
Hawley, G.G. The Condensed Chemical Dictionary. 9th ed. New York: Van Nostrand
Reinhold Co., 1977., p. 99
from HSDB

PALE YELLOW CRYSTALS

Sax, N.I. Dangerous Properties of Industrial Materials. 4th ed. New York: Van Nostrand
Reinhold, 1975., p. 443
from HSDB

WHITE CRYSTALS
Hawley, G.G. The Condensed Chemical Dictionary. 9th ed. New York: Van Nostrand
Reinhold Co., 1977., p. 99
from HSDB
Odor
VANILLA-LIKE ODOR
Hawley, G.G. The Condensed Chemical Dictionary. 9th ed. New York: Van Nostrand
Reinhold Co., 1977., p. 99
from HSDB
SWEET NON-DESCRIPT ODOR
Furia, T.E. (ed.). CRC Handbook of Food Additives. 2nd ed. Volume 2. Boca Raton, Florida:
CRC Press, Inc., 1980., p. 259
from HSDB
Taste
EXTRACTIVE TASTE: SPICY
Merory, J. Food Flavorings: Composition, Manufacture, and Use. 2nd ed. Westport, Conn.:
Avi Publishing Co., 1968., p. 90
from HSDB
SWEET NON-DESCRIPT TASTE
Furia, T.E. (ed.). CRC Handbook of Food Additives. 2nd ed. Volume 2. Boca Raton, Florida:
CRC Press, Inc., 1980., p. 259
from HSDB
Boiling Point
651° F at 760 mm Hg (NTP, 1992)
from CAMEO Chemicals
194
MSDS
from DrugBank
at 102.4kPa: 344°C
from ILO-ICSC
Melting Point
279° F (NTP, 1992)
from CAMEO Chemicals
60
MSDS
from DrugBank
134-138
MSDS
from DrugBank
137 °C
from Human Metabolome Database (HMDB)
137°C
from ILO-ICSC
Solubility
less than 0.1 mg/mL at 64° F (NTP, 1992)
from CAMEO Chemicals

Water Solubility
Insoluble
MSDS
from DrugBank

SOL IN WARM ALCOHOL & CARBON DISULFIDE; INSOL IN WATER

Hawley, G.G. The Condensed Chemical Dictionary. 9th ed. New York: Van Nostrand
Reinhold Co., 1977., p. 99
from HSDB

0.3 mg/mL at 25 °C
from Human Metabolome Database (HMDB)

Solubility in water, g/100ml: 0.03

from ILO-ICSC
Density
1.31 at 68° F (NTP, 1992)
from CAMEO Chemicals

1.31 g/cm³
from ILO-ICSC

6. Turunan Dihidropirimidon

Formula C14H16N2O

Molecular weight 228.2932 u

Hydrogen bond donors 2

Hydrogen bond acceptors 1

Percent composition

C 12.0107 u × 14 73.656 %

H 1.00794 u × 16 7.0643 %

N 14.0067 u × 2 12.271 %

O 15.9994 u × 1 7.0084 %