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Perfil de disolución referencia medio HCl 0.1 N pH 1.

2
Producto y fabricante:
Lote:
Aparato:
Fecha de caducidad:
Medio: HCl 0.1 pH 1.2
Tiempo: 75 min
Velocidad: 100 rpm

Resultados
Referencia
Tabla 1. Absorbancias por tiempo

absorbancia
tiempo v1 v2 v3 v4 v5 v6
2 0.02 0.025 0.03 0.022 0.027 0.021
5 0.043 0.051 0.04 0.039 0.073 0.064
10 0.096 0.091 0.089 0.097 0.095 0.084
15 0.105 0.198 0.109 0.111 0.117 0.112
20 0.167 0.189 0.171 0.175 0.186 0.191
30 0.281 0.3 0.301 0.207 0.234 0.305
45 0.289 0.373 0.356 0.364 0.296 0.313
60 0.321 0.307 0.313 0.319 0.328 0.305
75 0.339 0.389 0.333 0.319 0.405 0.315

Tabla 2. Concentraciones (µg/mL)

Concentración (µg/mL)
v1 v2 v3 v4 v5 v6
0.57681601 0.709697564 0.842579118 0.62996863 0.76285019 0.60339232
1.188071158 1.400681644 1.108342226 1.08176592 1.98536048 1.74617368
2.596615629 2.463734075 2.410581454 2.62319194 2.57003932 2.2776999
2.835802426 5.307399328 2.942107669 2.99526029 3.15471816 3.0218366
4.483533694 5.068212531 4.589838937 4.69614418 4.9884836 5.12136515
7.513233122 8.018183027 8.044759338 5.54658612 6.26414652 8.15106458
7.725843608 9.958253713 9.50645643 9.71906692 7.91187778 8.36367507
8.576285553 8.204217202 8.363675067 8.52313293 8.76231973 8.15106458
9.054659147 10.38347469 8.895201282 8.52313293 10.8086957 8.41682769
Tabla 3. Cantidad en miligramos

cantidad (mg)
v1 v2 v3 v4 v5 v6
25.81251646 31.758966 37.7054155 28.1910963 34.1375458 27.0018064
52.86916654 62.33033317 49.3212291 48.1385832 88.3485414 77.704729
115.5493955 109.6361663 107.270875 116.732041 114.36675 101.357646
124.7753067 233.5255704 129.452737 131.791453 138.807599 132.96081
196.1545991 221.7342982 200.805453 205.456308 218.246157 224.059725
326.8256408 348.7909617 349.947031 241.276496 272.490373 354.571309
332.2112752 428.2049097 408.777626 417.919877 340.210745 359.638028
366.6362074 350.7302854 357.547109 364.363933 374.589168 348.458011
384.8230137 441.2976741 378.046054 362.23315 459.369565 357.715177

% disuelto
v1 v2 v3 v4 v5 v6
5.162503293 6.3517932 7.54108311 5.63821926 6.827509163 5.40036127
10.57383331 12.46606663 9.86424581 9.62771664 17.66970828 15.5409458
23.1098791 21.92723327 21.4541749 23.3464083 22.87334993 20.2715291
24.95506135 46.70511409 25.8905475 26.3582906 27.76151977 26.5921621
39.23091982 44.34685965 40.1610907 41.0912616 43.64923149 44.8119451
65.36512816 69.75819233 69.9894062 48.2552993 54.49807469 70.9142619
66.44225503 85.64098193 81.7555253 83.5839755 68.04214894 71.9276056
73.32724148 70.14605708 71.5094218 72.8727866 74.91783368 69.6916022
76.96460275 88.25953483 75.6092109 72.4466299 91.87391309 71.5430354

Graficas de referencia

vaso 1
0.4
0.35
0.3
absorbancia

0.25 y = 0.0045x + 0.0527


0.2 R² = 0.8708
0.15
0.1
0.05
0
0 10 20 30 40 50 60 70 80
Tiempo

vaso 1