Linseis Application

Laboratory
Thermal Analysis

Date: 6/8/2015
Operator: Default User
Sample: Aspirin

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The LINSEIS STA Platinum Series (simultaneous thermal analysis) can be used to determine simultaneous changes of mass (TG) and
energetic effects (DTA/DSC) of a sample in the temperature range 150 1750°C. The top loading STA can be easily equipped with
various TG, TG-DTA and TG-DSC sensors.The unique characteristics of this product are high precision, high resolution and long term
drift stability. The Platinum Series was especially developed to meet the high demands of the high temperature as well as low
temperature applications. To cover this broad range several specifically designed furnace types are available. Furthermore MS (mass-
spectrometer) and FTIR spectrometer couplings can be added to receive unique additional information. Due to its superior
performance, user friendliness and modularity, the STA Platinum Series is an indispensable tool for every thermo analytical user.

If there should be any question concerning the evaluation please do not hesitate to contact us!

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 Info
Date: 6/4/2015 2:54:56 PM
Operator: Default User
Laboratory:
Sample name: Aspirin
Sample weight: 16.7867 mg
Atmosphere: unknown
Flowrate: 0 l/h
Crucible: Alumina
Measurement type: TG-HDSC

Comment

Temperature profile plot

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 Temperature profile table
Rate (K/min) Temperature (°C) Dwell (min) DAQ Relay 1 Relay 2 Relay 3 Relay 4
10 32 0 on off off off off
10 250 0 on off off off off
30 40 0 on off off off off

Coefficients
Temperature (°C) Rel. mass change (%)
40 -0.0813
50 0.4591
60 0.8273
70 1.1250
80 1.3430
90 1.5162
100 1.6658
110 1.7737
120 1.7667
130 1.6550
140 1.3635
150 0.6175
160 -0.9101
170 -3.6793
180 -7.8527
190 -13.1257
200 -18.6592
210 -23.5397
220 -27.4231
230 -30.3745
240 -32.8358
250 -34.9037
260 -36.6968

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