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Andreas Liessem
Europipe GmbH
Mülheim, Germany
560
N° 3: X70 (5“, 350°C)
540
420
400
0,00 0,02 0,04 0,06 0,08 0,10
pipeline engineering strain [ - ]
General C H nH . (5a)
In recent years, within Europipe GmbH significant efforts have been
undertaken in order to assess stress-strain behavior of UOE line pipe. It is important to notice that the stiffness parameter CH in Eq. (5a) is not
Motivated by the fact that with increasing steel grade (material) and, identical to the one of Eq. (4). Unlike the Ludwik strength parameter CL
with it, circumferential elongation (structure) is gradually decreasing, the Hollomon strength parameter CH can be directly associated with the
first, a huge research campaign was conducted in order to assess stress- ultimate engineering strength UTS of the material. CH is calculated as:
strain data in transverse direction including thermal ageing effects.
nH
Besides, part of this information was critical for optimizing forming e
processes within Europipe production route. Stimulated by customer C H UTS , (5b)
requests and the general development targeting at Strain Based Design nH
approaches, this was then followed by a campaign, which has been
directed towards axial stress-strain behavior and which still is in progress. where e = 2.178… is the natural number. In the range of large strains,
In both campaigns a total of four modeling approaches were applied to the Ludwik power law (4) does not fit experimental data any better than
experimental data and thoroughly analyzed, the individual approaches it is achieved by using Eq. (5). A representation, which accounts for
being: possible pre-straining is the one of Swift dating back to 1952 (Thomas,
Hollomon (1949) 2001):
Ludwik (1909)
Swift 1952, mentioned in Thomas (2001) C S 0 S ,
n
(6)
Ramberg Osgood (1943)
While the first three approaches are representations of true stress-true where CS and ns are, again, stiffness parameter and strain hardening
strain information, the latter one is capable of representing engineering exponent respectively. The idea of introducing a residual strain, which
stress-strain data. might be left over from cold forming, is interesting notably in the
Furthermore, a prediction method has been developed context of UOE pipe production. One may think, for instance of plastic
enabling fast assessment of strain hardening exponents of Hollomon strains evoked in the O-forming or the expansion procedure.
type in terms of Y/T. Currently, the method is limited to evaluating The formulae introduced above do not consider the elastic
strain hardening exponents of stress-strain behavior in transverse branch of the stress-strain diagram. Nevertheless, this part of the
direction. However, it is the intent to extend this tool for longitudinal constitutive relation may become important when dealing with sheet
stress-strain behavior in the near future. forming as encountered in the production of UOE pipes. Although large
This is particularly interesting because, in early stages of deformations are prevailing when forming sheet, generally, residual
design, stress-strain data is frequently unavailable. Comparison with stresses are induced, causing spring-back behavior. This is detrimental
results from best fit analysis shows that the approximate expression for because spring-back commonly entails significant deviations from the
strain hardening exponent calculation is simple to operate and efficient shape, which is actually targeted at. Likewise, it is reasonable to
for a wide range of pipeline steel material. account for the elastic contribution when designing according to Strain
Based Design principles because the notion of Strain Based Design
does not encompass strains greater than approximately 2%. Within this
Constitutive Equations for Representing Strain Hardening
range the elastic contribution might contribute to a significant amount
For representing constitutive behavior up to strains smaller than or
to total strain.
equal the uniform elongation a large variety of approaches are available
The linear elastic branch of the stress-strain diagram can be
in the literature, see above. The abovementioned models were selected
taken into account by superposing elastic and plastic strain
under the premise of taking care that these have relevance for
contributions as proposed as early as 1943 by Ramberg & Osgood:
engineering practice. Most simply, material behavior is described by
empirical relationships. All equations to be introduced below will nRO
represent material behavior, and strain hardening behavior in particular, * *
* *p * (7a)
solely by mere mathematical treatment. Hence the equations are
E
empirical in nature and, thus, do not resort to the causes encountered on p
micro-structural level.
Deformations in metal and steel are usually large, notably Therein, E is the elastic modulus and *p is a “proof stress”.
close to the ultimate failure event. Resorting to this observation, Commonly, the proof stress is conveniently chosen either as Rp0.1, Rp0.2,
Ludwik (1909) postulated that small elastic strains could be considered or, if applicable, as Rt0.5. The strain *p corresponds to the plastic strain
as negligible. He then proposed a power law representing purely plastic correlating with Rp0.1 or Rp0.2. The strain hardening exponent nRO is
behavior. The power law takes the form: determined by fixing the plastic part of the Ramberg-Osgood curve at
the technical yield point (*y | *p) and requiring that it passes through Table 2: Pipe material in virgin state (as formed): mechanical properties
the ultimate point (*UTS | *UTS). Thus, in longitudinal direction
Herein, *y is the total strain at yield, *UTS is the engineering tensile 600
strength and *UTS stands for uniform elongation. The graphs of the
proposals of Ludwik, Hollomon and Swift show infinite gradients for
550
stress are bounded and, hence, stress-strain curves must feature an 300
RO (X56) X56
strains. This fact corroborates the procedure pursued. 400 Eng. stress-eng. strain
Stress-strain data was analyzed for a total of six types of pipeline steel. 300 RO (X60) X60
The qualities of the material were ranging from API 5L grade X56 up
RO (X70) X70
to grade X100. The stress-strain behavior in longitudinal direction was 250
600
True stress-true strain
Longitudinal direction Table 2 summarizes pipe material taken in
axial direction along with corresponding mechanical parameters. Per 550
grade two different diameter-to-wall thickness ratios D/t were analyzed.
500
true stress [MPa]
Table 1: Pipe material in virgin state (as formed): mechanical properties 450
in transverse direction 400
H (X56)
N o
Grade Y/T UTS [ % ] 350 H (X65)
600
True stress-true strain 800
750
550
700
500 650
true stress [MPa]
300 400
X60 X100.1 RO (X100.1)
350
250 X70
300
200 250
0,00 0,02 0,04 0,06 0,08 0,10 0,00 0,01 0,02 0,03 0,04 0,05 0,06
true strain [ - ] Engineering strain [ - ]
Fig. 6: Hollomon representation of true stress-true strain behavior in Fig. 7: Ramberg-Osgood representation of eng. stress-eng. strain
transverse direction of X60 and X70 line pipe steel behavior in longitudinal direction of X80 and X100 line pipe steel
o 850
N Grade Ludwik Hollomon Swift Ram.-Osg.
800
nL nH nS nRO
750
1 X56 0.1467 0.1467 0.1483 12.2
700
2 X60 0.1328 0.1259 0.1275 14.8 650
600
3 X65 0.1222 0.1054 0.1083 19.0
true stress [MPa]
550
True stress-true strain of strain hardening. Besides, Y/T merely addresses singular points of
500
individual stress-strain behavior, namely the onset of yielding and
450
Longitudinal direction material tensile strength. For some mechanical analyses this might be
400
X80.2 H (X80.2)
insufficient.
350
Despite all implications with other material characteristics,
300 X100.2 H (X100.2)
experimental evidence has shown that both yield and tensile strength of
250
a material have significant effect on impending failure of pipelines. It is
0 0,01 0,02 0,03 0,04 0,05 0,06
anticipated that, inherently, the yield-to-tensile ratio is closely related to
true strain [ - ]
strain hardening of pipeline material. Taking this as a natural starting
Fig. 10: Hollomon representation of true stress-true strain behavior in point, the next section theoretically explores the possibilities of
longitudinal direction of X80 and X100 line pipe steel correlating strain hardening exponents and Y/T based on a proposal of
Zhu and Leis (2004). As will be seen at a later juncture, the Hollomon
Discussion approach will emerge as a successful, yet simple, approach for
Based upon the results that were made throughout this research some achieving this goal under the sole condition that the material obeys
general conclusions can be drawn. Comprehensive discussion of all power-law plasticity.
constitutive equations towards representing stress-strain behavior and
issues of refining modeling methodologies goes well beyond the scope Strain hardening exponent as a function of Y/T
of this paper. The findings can be summarized as follows: Due to the presence of cold forming within the UOE production route
The Ludwik representation is prone to characterize well large the stress-strain diagram of current Europipe material features a smooth
plastic strains while still being sufficiently accurate in the vicinity trace in transverse direction. This fact permits true stress-true strain
of true yield strength. However, within our investigation, it did not curves be reproduced by power-law approximations without loss of
add significantly to overall accuracy of the plastic flow curve crucial constitutive information. The simplest form of a power law
representation curve is the one of Hollomon, which proved to be an excellent
Rather, the traces of Ludwik stress-strain approximations can be representation of experimental true stress-true strain curves in the
closely reproduced by the Hollomon approach for most line pipe regime of uniform plastic deformation. Moreover, it is well-suited for
steels. plastic collapse analysis of pipelines.
The Swift approach tends to represent high-strength line pipe steel Until the maximum load is attained plastic flow develops
best. Small discrepancies between experimental stress-strain curve uniformly. In this regime of large uniform deformation, true stress and
and approximation are seen for strains smaller than 1%. However, true strain can be expressed using engineering stress and strain :
these might be due to the necessity of estimating plastic pre-strains
* 1 * , ln1 *
Ramberg-Osgood approximations supply appropriate descriptions
(8)
of engineering stress-engineering strain data. With respect to the
accuracy of representations there seems to be no particular
difference between lower and higher strength material. Substitution of Eqs. (8) in to the Hollomon power law (5) and solving
Description of engineering stress-engineering strain curves by the for the true stress gives:
Ramberg-Osgood constitutive equation leads to values of strain
hardening exponent, which are conceptually different to those of
true stress-true strain approaches. While strain hardening exponent CH
ln1
* nH
(9)
of true-stress-true strain approaches is generally smaller than 0.5 1 *
strain hardening exponent of Ramberg-Osgood type models may go
to infinity as underlying stress-strain information tends to trace Generally, localization of deformation, that is to say necking, begins
perfectly elastic-perfectly plastic behavior when the maximum force is attained during tensile testing of a ductile
material. At this point, engineering stress and engineering strain take
Comparing Tables 3 and 4 it becomes apparent that specimens their ultimate values UTS and UTS. After the point of necking
machined in longitudinal direction feature stress-strain behavior, which initiation, the engineering stress decreases as the engineering strain
is convenient for strain based design. Yield-to-tensile ratio Y/T and increases. Thus, the instability condition is defined by (Zhu and Leis,
Ramberg-Osgood work hardening exponent nRO are even lower than 2004a, b, Law et al., 2004):
those upraised in transverse direction.
d *
SIMPLIFIED METHOD FOR COMPUTING STRAIN 0 (10)
HARDENING EXPONENTS d *
Substitution of Eq. (9) into Eq. (10) and assessing proves that the
General
Hollomon strain hardening exponents equals:
In addition to providing information on stress and strain, pipe
manufacturers can actively support the design process by supplying
strain hardening exponents. This section lays out a method for
n H ln 1 UTS
*
UTS , (11)
estimating strain hardening exponents of Hollomon type for transverse
where UTS is the true ultimate strain at necking initiation. If the in deriving an average absolute value Rp0,2/E from the lower and upper
corresponding true ultimate stress is denoted by UTS, from Eqs. (5a) limit case of yield strength Rp02, applying to UOE pipe production, and
and (11) one obtains: substituting it into Eq. (14). This certainly is an approximation, but as will
be shown later on, it provides sufficiently accurate estimates of strain
UTS C H UTS nH C H n H nH .
hardening exponent.
(12)
Within the scope of this investigation, steel has been
considered ranging from grade X56 up to grade X100. The yield
In the following the subscript “H ” is omitted for simplicity. Solving this strengths were 395 MPa and 786 MPa for steel grade X56 and X100
for the strength coefficient yields: respectively. Correspondingly, one derives strains at yield of y* = 0,0039
and y* = 0,00576 respectively. The average of total strain at yield for
C
UTS
UTS
*
1 UTS
*
. (13) grade X56 and X100 then amounts to y* = 0,00483. Substituting this into
n Eq. (14) and assessing gives:
n nn
n
Because ln (1+*UTS) = n there is (1+ *UTS) = en. Using this intermediary Y 0,01313 (19)
0,995
result, Eq. (13) takes the form of Eq. (5b): T n
n When plotting the relationship Y/T vs. n (17) for y* = 0,0039, y* =
e * .
C UTS 0,00576 and the mean value y*, mean = 0,00483, then it is seen that the
n latter one firmly interpolates between the boundaries correlating with
moderate and extreme values of yield strength, see Fig. 11. Likewise, the
If the “yield point” (y | y) of the true stress-true strain relation, where graphs in Fig. 11 give indication that, intrinsically, the strain hardening
y = ln (1+y*) and y = y (1+y*), is on the power law curve as given by exponent may not just be a function of Y/T alone but of the yield stress Y
Eq. (5a), one may write: as well. Furthermore, close inspection of the graphs reveals that the
curves do not reach down to n = 0 for Y/T → 1. This, at first sight,
*y 1 *y C ln 1 *y n
, (14)
surprising phenomenon is to be attributed to the fact that even for a
perfectly elastic-plastic engineering stress-engineering strain diagram the
associated true stress-true strain diagram has a finite slope not equal to
and further, employing relation (5b): zero. The horizontal grey line in Fig. 12 highlights this phenomenon.
Since Eqs. (17) and (19) are implicit in nature, these cannot be
solved for the strain hardening exponent n directly. In order to generate
n
e * n
*y 1 *y UTS ln 1 *y . (15) an explicit expression for the strain hardening exponent, it is attempted to
n represent Eq. (19) by a polynomial of order two. It was found that
0,0696
In fact, Eq. (16) establishes a functional relationship between the strain n 0,0293 0,0683 . (21)
hardening exponent and the yield-to-tensile ratio. Denoting, as usual, Y T
UTS* by T and y* by Y and respecting y* << 1, one may simplify as
follows: Relationship (21) has been evaluated and the corresponding graph
depicted in Fig. 12, along with the plot according to Eq. (19) and the data
n
n of Hollomon strain hardening exponent nH, taken from Table 3. It is to be
1
Y
1 *y (17) noted that each data point of Hollomon strain hardening exponent –
e *y represented as circular point in Fig. 12 - was determined based on the best
individual fit to the underlying true stress-strain curve received from
T transverse tensile testing on round bar specimens. Thus, these did not
originate from bare theoretical consideration. Comparing the final
According to German standards, the yield strength (Rp0,2) is commonly theoretical approximation (21) and the results from curve fitting reveals
defined at the 0,2% plastic offset strain. Hence, the total strain at yield is potential and efficacy of this approach. Nonetheless, there is still some
then: inaccuracy for Y/T ≥ 0,93 where the results obtained from best fit analysis
switch their locus from underneath to above the theoretical curve. This
R p 0, 2 might be due to specific architecture and composition of material
*y 0,002 * (18)
microstructures (uncommon alloying elements, etc.) associated with such
E
elevated yield-to-tensile ratios. From the fact that for yield-to-tensile
ratios Y/T ≥ 0,93 actual values of strain hardening exponent have their
It is clear from Eq. (15) that y* must depend upon the stress-strain
locus clearly above the theoretical curve, it is inferred that there is still
characteristic of the material under investigation. There is no unique
dormant potential for improvement of circumferential elongation of high-
solution covering all possible combinations of yield-to-tensile ratio and
strength line pipe.
yield strength. A practical solution of removing this dependence consists
0,16 were shown for both circumferential and longitudinal direction for a
n [-]
wide range of steel grades. Furthermore, experimental stress strain
0,14 information was approximated using well-accepted constitutive
approaches and corresponding work hardening parameters compiled.
0,12 A procedure for strain hardening exponent estimation was
developed for stress-strain behavior in transverse direction of UOE line
0,1 pipe. The mathematical approach supposes validity of the Hollomon
power law approximation and declares yield-to-tensile Y/T ratio as the
0,08 lower bound leading parameter. The correlation was evaluated exactly for two sorts
of n of steel (X56 and X100) featuring about the limit levels (lower and
0,06
upper bound) of yield strength of today’s UOE pipe production. In so
Rp0,2 = 395 MPa
0,04
doing, it became apparent that, indeed yield-to-tensile ratio is
Rp0,2 = 786 MPa prevailing, but not the only parameter controlling strain hardening
0,02
exponent. Specifically, yield strength might exert some additional
average: Rp0,2 = 590 MPa effect. Defining an average value for the complete range of yield
0 strength of current Europipe production conveniently decouples strain
0,65 0,70 0,75 0,80 0,85 0,90 0,95 1,00 hardening exponent from yield strength.
Y/T [ - ] Comparing with results from best fit analysis showed that the
final approximate expression is simple to operate and efficient for a
Fig. 11: Strain hardening exponent n vs. yield-to-tensile ratio Y/T, Eq.
wide range of pipeline steel material.
(19)
0,16
REFERENCES
n [-]
0,14
Bowker, J.T., Gianetto, J.A., Shen, G., Tyson W. and Horsley , D. (2006).
0,12
X70 material in the “Cross-Weld Tensile Properties of Girth Welds for Strain Based
sequel of artificial Designed Pipeline” Int Pipeline Conf, Calgary, Canada, IPC, Paper
0,1 ageing 10400.
CSZ Z662-03. Canadian Standards Association (2003). “Oil and Gas
0,08 Pipeline Systems”.
Hollom, JH (1949). “Tensile Deformation”. Transactions of the
0,06
average: Rp0,2 = 590 MPa American Institute of Mining, Metallurgical and Petroleum
0,04
Engineers, Vol 16, pp 268290.
Final approximation
Martin, R. (2006). "Investment in Oil and Gas Filed Materials
0,02 n acc. to ow n experiments Technology - The Key to a Secure Energy Supply”. Energy Materials,
Vol 1, pp 11-13.
0 Mohr, W. (2006). "Strain Based Design for Materials with HAZ
0,65 0,70 0,75 0,80 0,85 0,90 0,95 1,00 Softening” Int Pipeline Conf, Calgary, Canada, IPC, Paper 10424.
Y/T [ - ] Law, M., Bowie, G., Fletcher, L. (2004): Burst Pressure and Failure
Fig. 12: Strain hardening exponent n vs. yield-to-tensile ratio Y/T, Eq. Strain in Line Pipe, Part 3, Failure Pressure Calculated by the
(21) Method of Plastic Instability. The Journal of Pipeline Integrity, Vol.
3, pp 107-111
CONCLUSIONS Ludwik, P. (1909). Elemente der Technologischen Mechanik, 1st
edition, Springer.
Ramberg, W., Osgood, W.R. (1943). “Description of Stress-Strain
Limit State Design calls for application of advanced methods of
Curves by Three Parameters”. National Advisory Committee for
analyses, including advanced material solutions. This requires exact
Aeronautics (NACA), Technical Note No 902.
representations of constitutive behavior of line pipe steel and structural
Thomas, S. (2001): Konstitutive Gleichungen und Numerische
pipe behavior also beyond the onset of yielding, until the ultimate limit
Verfahren zur Beschreibung von Verformung und Schädigung.
state marked by bursting. The load bearing capacity, once yielding has
Dissertation, Technische Universität Darmstadt, Darmstadt
started, is strain based. One essential component of Strain Based
Zhou, J., Horsley, D. and Rothwell B. (2006). “Application of Strain-
Design is the material’s strain hardening behavior, which may be
Based Design for Pipelines in Permafrost Areas”. Int Pipeline Conf,
limited for line pipe steels of higher grades. Here the possible
Calgary, Canada, IPC, Paper 10054.
contribution of manufacturer comes into play: Next to basic parameters
Zhu, X.K., Leis, B.N. (2004a): Strength Criteria and Analytical
of the stress-strain-behavior like uniform elongation, yield strength,
Predictions of Failure Pressure in Corroded Line Pipes. International
tensile strength and yield-to-tensile ratio knowledge of strain hardening
Journal Offshore and Polar Engineering, Vol. 14, pp 125-131.
exponent is useful for any strain based assessment of safety. Strain
Zhu, X.K., Leis, B.N. (2004b): Accurate Prediction of Burst Pressure
capacity and, thus, strain hardening exponent can be relevant in axial as
for Linepipes. The Journal of Pipeline Integrity, Vol. 3, pp 195-206
well as in circumferential direction, depending on the type of loading
(pressure containment only or additional presence of external loads). In
this context, representative graphs of uni-axial stress-strain behavior