FIRST TASK:

PREPARATION OF CALCIUM SOLUTION:

What is Calcium Oxalate Precipitation:

 “creation of insoluble calcium oxalate precipitate from the solution, using calcium
chloride solution as the precipitant.”
 powdered ammonium oxalate monohydrate ((NH4)2C2O4.H2O) (eto yung
“oxalate”)
 Calcium chloride dihydrate (CaCl2.2H2O) (eto yung “calcium”)

Materials needed:
 1000mg of Calcium chloride dihydrate salts (to make 1000ppm of Calcium chloride
dihydrate soln)
 Distilled water (2.5L maybe)
 1L containers-10pcs (pwede na siguro yung mga lalagyan ng tubig? For storage to ng
solns)
 Stirrer
 Analytical balance

Preparation of 1000ppm CaCl2H2O: (di ko sure wahu)

Molarity concept: 1000 ppm= mg/L

1000𝑚𝑔 𝑥
=
𝐿 1𝐿
𝒙 = 𝟏𝟎𝟎𝟎𝒎𝒈 𝒐𝒇 𝑪𝒂𝑪𝒍𝟐 𝒊𝒏 𝟏𝑳 𝒐𝒇 𝑯𝟐𝑶
Serial Dilution of 1000ppm: 80,70,60,50,40,30,20 ppm:

80 ppm

of 1000 ppm Dilute to 460mL of H2O

70 ppm
of 80 ppm Dilute to 62.5mL of H2O

60 ppm

of 70 ppm Dilute to 72 mL of H2O

50 ppm

of 60 ppm Dilute to 90mL of H2O

40 ppm

of 50 ppm Dilute to 100mL of H2O

30 ppm

of 40 ppm Dilute to 125mL of H2O

20 ppm
of 30 ppm Dilute to 167mL of H2O

10 ppm
of 20 ppm
Dilute to 250mL of H2O

SECOND TASK:
PREPARATION OF 0.1M OXALATE SOLUTION

What is this for:

 Eto dapat yung mag pprecipitate sa soln

Materials needed:
 Distilled H2O
 Ammonium oxalate

Preparation of 0.1M Ammonium Oxalate Solution:

1𝑚𝑜𝑙 1
0.1𝑀(1𝐿) = 𝑋 ( ) ( ) (0.5𝐿)
142𝑔 1𝐿
𝑿 = 𝟐𝟖. 𝟒 𝒈 𝒐𝒇 𝒂𝒎𝒎𝒐𝒏𝒊𝒖𝒎 𝒐𝒙𝒂𝒍𝒂𝒕𝒆