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Designation: D1411 − 09
1. Scope* uses, or both. How one applies the results obtained using this
1.1 These test methods are applicable to the determination standard is beyond its scope.
of water-soluble calcium, magnesium, and sodium chlorides 1.3 This standard does not purport to address all of the
used as admixtures in the preparation of graded aggregate road safety concerns, if any, associated with its use. It is the
materials. responsibility of the user of this standard to establish appro-
1.1.1 Method A, Total Chlorides—Add an excess of a priate safety and health practices and determine the applica-
standard silver nitrate solution to the filtered sample; back bility of regulatory limitations prior to use.
titrate the excess silver with a standard ammonium thiocyanate 1.4 This practice offers a set of instructions for performing
solution to a red-orange endpoint using Volhard indicator. one or more specific operations. This document cannot replace
1.1.2 Method B, Calcium Chloride—Calcium in an alkaline education or experience and should be used in conjunction with
solution is titrated with standard EDTA solution using calcein professional judgment. Not all aspects of this practice may be
modified as an indicator. The color change is from green to applicable in all circumstances. This ASTM standard is not
blue. intended to represent or replace the standard of care by which
1.1.3 Method C, Magnesium Chloride—Calcium and the adequacy of a given professional service must be judged,
magnesium, in a solution buffered to a pH of 10, are titrated nor should this document be applied without consideration of
with standard EDTA solution using eriochrome black T as an a project’s many unique aspects. The word “Standard” in the
indicator. The color change is from red to blue. Magnesium title of this document means only that the document has been
chloride is calculated by subtracting the EDTA calcium equiva- approved through the ASTM consensus process.
lent volume determined in the analysis for calcium chloride 1.5 The text of this standard references notes and footnotes
from the total EDTA volume used, to obtain the magnesium which provide explanatory material. These notes and footnotes
EDTA equivalent by difference. (excluding those in tables and figures) shall not be considered
1.1.4 Method D, Alkali Chloride—Alkali chlorides are cal- as requirements of the standard.
culated from the difference of the total chloride and calcium
and magnesium determinations. 2. Referenced Documents
NOTE 1—These test methods assume that the aggregate did not contain
significant amounts of the water-soluble chlorides in question before the 2.1 ASTM Standards:2
admixture was added. If significant amounts of these chlorides are known D653 Terminology Relating to Soil, Rock, and Contained
or suspected to be present, the aggregate shall be tested for these Fluids
constituents according to these test methods and the proper corrections D1193 Specification for Reagent Water
made. D3740 Practice for Minimum Requirements for Agencies
1.2 All observed and calculated values shall conform to the Engaged in Testing and/or Inspection of Soil and Rock as
guidelines for significant digits and rounding established in Used in Engineering Design and Construction
Practice D6026. D6026 Practice for Using Significant Digits in Geotechnical
1.2.1 The method used to specify how data are collected, Data
calculated, or recorded in this standard is not directly related to
the accuracy to which the data can be applied in design or other 3. Terminology
3.1 Except as follows in 3.2, all definitions are in accor-
dance with Terminology D653.
1
These test methods are under the jurisdiction of Committee D18 on Soil and
Rock and are the direct responsibility of Subcommittee D18.15 on Stabilization
2
With Admixtures. For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Current edition approved June 1, 2009. Published July 2009. Originally approved contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
in 1956. Last previous edition approved in 2004 as D1411 – 04. DOI: 10.1520/ Standards volume information, refer to the standard’s Document Summary page on
D1411-09. the ASTM website.
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D1411 − 09
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D1411 − 09
SUMMARY OF CHANGES
Committee D18 has identified the location of selected changes to this standard since the last issue (D1411–04)
that may impact the use of this standard.
(1) 1.1 was modified to summarize each of the test methods. (6) 6.1 was modified to clarify the materials that required
(2) 1.2, 1.4, and 1.5 were added to reflect caveats required by grinding.
Committee D18. (7) 7.1 was changed to an active voice.
(3) Section 2 was modified to include references to D3740 and (8) 14.1 was changed to eliminate an undesirable footnote.
D6026. (9) Section 24 “Reports: Records” was added.
(4) 3.1 was modified to include a delimiting phrase. (10) Updated Summary of Changes section.
(5) Note 2 was added highlighting Practice D3740 as required
by Committee D18.
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D1411 − 09
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