DAD1 A, Sig 254,4 Ref Off (CHEM112 - 211 - 7S - A7.D)

Data File C:\CHEM32\1\DATA\CHEM112A_09_21_16 2016-09-21 13-10-19\CHEM112_211_7S_A7.
D
Sample Name: Shin_Aspirin
=====================================================================
Acq. Operator : SYSTEM Seq. Line : 36
Acq. Instrument : HPLC #3 Location : Vial 35
Injection Date : 9/21/2016 5:49:15 PM Inj : 1
Inj Volume : 1.000 µl
Sequence File : C:\Chem32\1\DATA\CHEM112A_09_21_16 2016-09-21 13-10-19\CHEM112A_09_21_16.S
Method : C:\CHEM32\1\DATA\CHEM112A_09_21_16 2016-09-21 13-10-19\CHEM112A_FALL2013.M
(Sequence Method)
Last changed : 9/21/2016 1:10:20 PM by SYSTEM
Method Info : CHEM112A
DAD1 A, Sig=254,4 Ref=off (CHEM112_211_7S_A7.D)
1.884
mAU
15
12.5
1.228
10
7.5
5
2.857
2.5
0
1 2 3 4 5 6 min
DAD1 C, Sig=230,4 Ref=off (CHEM112_211_7S_A7.D)
1.884
mAU
150
100
1.204
2.856
50
1.427
0.465
0.867
1.369
1.384
0.933
0.961
1.494
1.520
1.009
1.293
-50
-100
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000
Do not use Multiplier & Dilution Factor with ISTDs
Signal 1: DAD1 A, Sig=254,4 Ref=off
Peak RetTime Type Width Area Height Area

# [min] [min] [mAU*s] [mAU] %
----|-------|----|-------|----------|----------|--------|
1 1.228 BV 0.0510 35.14568 9.75200 31.4762
2 1.884 BB 0.0571 70.50314 18.44792 63.1421
3 2.857 BB 0.0704 6.00899 1.05604 5.3816
Totals : 111.65780 29.25596
HPLC #3 9/21/2016 5:56:23 PM SYSTEM Page 1 of 2

Data File C:\CHEM32\1\DATA\CHEM112A_09_21_16 2016-09-21 13-10-19\CHEM112_211_7S_A7.D
Sample Name: Shin_Aspirin
Signal 2: DAD1 C, Sig=230,4 Ref=off

----|-------|----|-------|----------|----------|--------|
1 0.465 VV 0.0350 5.85883 2.07110 0.2452
2 0.867 BV 0.1825 48.28283 3.11155 2.0208
3 0.933 VV 0.0220 45.83679 28.19768 1.9184
4 0.961 VV 0.0233 73.52323 39.41235 3.0772
5 1.009 VB 0.0685 322.47324 57.42269 13.4965
6 1.204 BV 0.1038 782.52240 91.00563 32.7509
7 1.293 VV 0.0198 75.84682 47.12201 3.1744
8 1.369 VV 0.0476 124.95281 33.80834 5.2296
9 1.384 VV 0.0183 44.31154 30.85798 1.8546
10 1.427 VV 0.0542 110.99875 24.34637 4.6456
11 1.494 VV 0.0124 9.45559 9.69296 0.3957
12 1.520 VB 0.0173 5.29763 4.48319 0.2217
13 1.884 BV 0.0515 670.86292 173.94873 28.0776
14 2.856 VV 0.0613 69.09231 13.47422 2.8917
Totals : 2389.31568 558.95480
=====================================================================
*** End of Report ***

Sample Name: Shin_Acetaminophen
=====================================================================
(Sequence Method)

1.228
mAU
500
400
300
200
100
1.887
0
1 2 3 4 5 6 min
1.228
mAU
300
200
1.888
100
1.434
1.402
2.867
1.489
1.512
2.441
6.512
1.012
2.826
4.274
0.939
0.966
-100
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.228 BB 0.0407 1545.30200 560.58130 99.4380
2 1.887 BB 0.0533 8.73363 2.32871 0.5620
Totals : 1554.03563 562.91001

Sample Name: Shin_Acetaminophen

----|-------|----|-------|----------|----------|--------|
1 0.939 BV 0.0106 5.04212 6.81722 0.1857
2 0.966 VV 0.0533 98.24077 21.90499 3.6180
3 1.012 VB 0.0552 221.01016 48.02845 8.1393
4 1.228 BV 0.0625 2121.37915 471.03854 78.1252
5 1.402 VV 0.0120 27.43922 30.58197 1.0105
6 1.434 VV 0.0433 91.21534 25.18001 3.3592
7 1.489 VV 0.0137 11.49178 11.42049 0.4232
8 1.512 VV 0.0132 7.38543 7.09026 0.2720
9 1.888 VV 0.0497 93.54330 24.13156 3.4450
10 2.441 VV 0.0397 12.33679 3.72072 0.4543
11 2.826 BV 0.0276 5.54459 2.62703 0.2042
12 2.867 VV 0.0279 9.53204 4.21165 0.3510
13 4.274 VV 0.0315 5.10114 1.95067 0.1879
14 6.512 VV 0.0372 6.09714 1.96313 0.2245
Totals : 2715.35898 660.66669
=====================================================================

Sample Name: Shin_Caffeine
=====================================================================
(Sequence Method)

1.382
mAU
1200
1000
800
600
400
1.886
1.228
200
2.858
0
1 2 3 4 5 6 min
1.382
mAU
1000
800
600
1.886
400
1.220
2.865
200
1.555
2.437
1.033
0.389
0.999
0.967
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.228 BV 0.0423 92.50227 31.94587 2.2357
2 1.382 VV 0.0449 3885.64575 1280.67615 93.9115
3 1.886 VB 0.0614 145.93983 34.79269 3.5272
4 2.858 BB 0.0713 13.47352 2.37227 0.3256
Totals : 4137.56138 1349.78697

Sample Name: Shin_Caffeine

----|-------|----|-------|----------|----------|--------|
1 0.389 BV 0.0327 5.26143 1.96581 0.0818
2 0.967 VV 0.0165 16.77150 13.53661 0.2606
3 0.999 VV 0.0211 42.10341 32.43705 0.6542
4 1.033 VB 0.0457 208.23958 54.31047 3.2359
5 1.220 BV 0.1100 862.74133 94.08807 13.4062
6 1.382 VV 0.0509 3844.88501 1109.11792 59.7461
7 1.555 VV 0.0130 6.14998 6.83526 0.0956
8 1.886 BV 0.0570 1258.31970 315.50067 19.5532
9 2.437 VB 0.0269 6.34004 2.85220 0.0985
10 2.865 VV 0.0767 184.56430 29.63674 2.8680
Totals : 6435.37628 1660.28079
=====================================================================

Data File C:\CHEM32\1\DATA\CHEM112A_09_21_16 2016-09-21 13-10-19\CHEM112_211_29S_B3.D
Sample Name: Eivazi_Aspirin
=====================================================================
(Sequence Method)
DAD1 A, Sig=254,4 Ref=off (CHEM112_211_29S_B3.D)
1.888
mAU
50
40
30
20
1.227
2.865
10
1 2 3 4 5 6 min
DAD1 C, Sig=230,4 Ref=off (CHEM112_211_29S_B3.D)
1.888
mAU
500
400
300
200
1.202
2.870
0.712
0.676
1.424
100
1.310
1.340
0.908
0.949
0.980
1.284
1.019
-100
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.227 BV 0.0587 24.36948 5.71930 8.8649
2 1.888 BB 0.0576 238.90977 61.80112 86.9087
3 2.865 BB 0.0819 11.61819 1.96796 4.2264
Totals : 274.89745 69.48838

Sample Name: Eivazi_Aspirin

----|-------|----|-------|----------|----------|--------|
1 0.676 BV 0.0346 8.94826 3.15271 0.2629
2 0.712 VV 0.0206 5.14146 3.31877 0.1511
3 0.908 BV 0.0270 14.36069 6.58181 0.4219
4 0.949 VV 0.0219 44.50240 25.45828 1.3074
5 0.980 VV 0.0171 52.98182 39.63795 1.5565
6 1.019 VB 0.0595 285.08270 56.85289 8.3754
7 1.202 BV 0.0971 592.45636 73.44484 17.4057
8 1.284 VV 0.0132 22.76168 21.73309 0.6687
9 1.310 VV 0.0167 15.85496 13.54259 0.4658
10 1.340 VB 0.0333 9.61699 4.19330 0.2825
11 1.424 VV 0.0196 5.51041 3.75803 0.1619
12 1.888 VV 0.0612 2210.14893 552.29126 64.9318
13 2.870 VV 0.0701 136.43253 23.55793 4.0082
Totals : 3403.79920 827.52344
=====================================================================

Sample Name: Eivazi_Acetaminophen
=====================================================================
(Sequence Method)

1.227
mAU
2500
2000
1500
1000
500
1.887
0
1 2 3 4 5 6 min
1.229
mAU
1200
1000
800
600
400
1.886
2.846
2.863
2.879
0.979
1.029
1.487
1.499
200
0
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.227 BV 0.0430 8068.92725 2812.20166 99.5868
2 1.887 VB 0.0711 33.47939 6.49607 0.4132
Totals : 8102.40663 2818.69773

Sample Name: Eivazi_Acetaminophen

----|-------|----|-------|----------|----------|--------|
1 0.979 VV 0.0359 117.86088 39.98238 1.7751
2 1.029 VB 0.0549 279.54596 62.25220 4.2101
3 1.229 BV 0.0548 5928.45215 1463.32776 89.2861
4 1.487 VV 0.0129 16.91550 17.28400 0.2548
5 1.499 VB 0.0281 34.48865 14.86218 0.5194
6 1.886 VV 0.0512 225.95709 55.87928 3.4031
7 2.846 BV 0.0255 12.42343 6.02923 0.1871
8 2.863 VV 0.0164 8.93248 7.00472 0.1345
9 2.879 VB 0.0291 15.25860 6.45611 0.2298
Totals : 6639.83475 1673.07786
=====================================================================

Sample Name: Eivazi_Caffeine
=====================================================================
(Sequence Method)

1.228
mAU
40
30
20
1.382
10
1 2 3 4 5 6 min
1.222
mAU
1.384
1.422
1.888
1.445
6.940
20
0.977
1.020
0.991
-20
-40
-60
-80
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.228 BV 0.0422 141.75433 49.01120 82.6494
2 1.382 VB 0.0527 29.75860 8.03352 17.3506
Totals : 171.51293 57.04472

Sample Name: Eivazi_Caffeine

----|-------|----|-------|----------|----------|--------|
1 0.977 BV 0.0163 19.82289 15.08521 1.4430
2 0.991 VV 0.0113 21.55946 24.38827 1.5695
3 1.020 VB 0.0563 202.96948 44.00977 14.7756
4 1.222 BV 0.1104 884.42560 101.26693 64.3836
5 1.384 VV 0.0771 188.79184 29.14438 13.7435
6 1.422 VV 0.0133 17.37241 16.46888 1.2647
7 1.445 VB 0.0213 17.90587 11.08977 1.3035
8 1.888 VV 0.0500 14.81289 3.63664 1.0783
9 6.940 VV 0.0348 6.02074 2.17184 0.4383
Totals : 1373.68118 247.26169
=====================================================================

Sample Name: Bhargava_Caffeine
=====================================================================
(Sequence Method)

1.383
mAU
500
400
300
200
100
1.885
1.228
0
1 2 3 4 5 6 min
1.383
mAU
400
300
200
1.885
1.204
100
2.837
2.860
0.905
0.927
0.965
0.979
1.008
1.023
-100
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.228 BV 0.0639 18.63195 3.92708 1.1158
2 1.383 VB 0.0442 1620.64197 544.57574 97.0510
3 1.885 BB 0.0555 30.61329 8.20603 1.8333
Totals : 1669.88721 556.70886

Sample Name: Bhargava_Caffeine

----|-------|----|-------|----------|----------|--------|
1 0.905 BV 0.0222 10.18663 5.73334 0.2862
2 0.927 VV 0.0403 52.28462 15.70441 1.4689
3 0.965 VV 0.0137 27.42053 33.45429 0.7703
4 0.979 VV 0.0177 57.23561 39.97015 1.6079
5 1.008 VV 0.0179 65.67419 53.19644 1.8450
6 1.023 VB 0.0419 207.07091 59.75542 5.8173
7 1.204 BV 0.1005 783.60419 92.33727 22.0142
8 1.383 VV 0.0520 2009.15881 558.39917 56.4443
9 1.885 VV 0.0548 308.39807 79.41468 8.6640
10 2.837 BV 0.0330 18.27703 6.77263 0.5135
11 2.860 VV 0.0377 20.23475 6.70009 0.5685
Totals : 3559.54535 951.43789
=====================================================================

Sample Name: Bhargava_Acetaminophen
=====================================================================
(Sequence Method)

1.227
mAU
2500
2000
1500
1000
500
1.884
1.609
0
1 2 3 4 5 6 min
1.227
mAU
1200
1000
800
600
400
1.883
1.424
2.848
2.860
1.477
1.509
0.942
2.240
2.430
0.833
0.848
0.874
0.914
0.928
0.979
1.032
200
0
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.227 BV 0.0424 7876.27393 2796.11475 98.7777
2 1.609 VV 0.0918 25.11524 3.37535 0.3150
3 1.884 VB 0.0622 72.34533 16.80033 0.9073
Totals : 7973.73450 2816.29043

Sample Name: Bhargava_Acetaminophen

----|-------|----|-------|----------|----------|--------|
1 0.833 BV 0.0189 7.84975 6.59658 0.1112
2 0.848 VV 0.0155 13.86809 11.56836 0.1965
3 0.874 VV 0.0379 64.95135 20.52217 0.9203
4 0.914 VV 9.35e-3 22.58235 33.56264 0.3200
5 0.928 VV 0.0119 33.90533 38.13273 0.4804
6 0.942 VV 0.0101 31.48251 42.94497 0.4461
7 0.979 VV 0.0434 198.32776 54.52271 2.8102
8 1.032 VB 0.0590 248.08211 70.07586 3.5152
9 1.227 BV 0.0515 5705.28662 1463.06409 80.8411
10 1.424 VV 0.0309 65.76353 26.98198 0.9318
11 1.477 VV 0.0157 16.45325 13.04891 0.2331
12 1.509 VB 0.0176 7.43880 5.93350 0.1054
13 1.883 VV 0.0547 578.80109 151.23244 8.2013
14 2.240 BV 0.0413 8.00118 2.31915 0.1134
15 2.430 VB 0.0279 6.05286 2.67743 0.0858
16 2.848 BV 0.0353 22.54237 8.41142 0.3194
17 2.860 VB 0.0366 26.01997 8.65597 0.3687
Totals : 7057.40891 1960.25090
=====================================================================

Sample Name: Bhargava_Aspirin
=====================================================================
(Sequence Method)
1.884
mAU
35
30
25
20
15
10
5
0
1 2 3 4 5 6 min
1.884
mAU
300
250
200
150
100
1.200
2.862
1.261
5.861
2.405
2.433
3.816
6.494
0.572
0.965
1.021
1.031
50
0
-50
-100
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.884 BB 0.0574 146.00117 37.90136 100.0000
Totals : 146.00117 37.90136

Sample Name: Bhargava_Aspirin

----|-------|----|-------|----------|----------|--------|
1 0.572 VV 0.0266 5.28931 2.40622 0.2398
2 0.965 BV 0.0562 36.12344 7.91721 1.6374
3 1.021 VV 0.0191 67.93274 45.09563 3.0792
4 1.031 VB 0.0349 146.89792 51.29329 6.6585
5 1.200 BV 0.0901 482.50049 65.39245 21.8705
6 1.261 VV 0.0154 21.26186 17.85707 0.9637
7 1.884 VV 0.0568 1356.68481 349.56662 61.4951
8 2.405 VV 0.0243 7.34258 3.76155 0.3328
9 2.433 VV 0.0331 9.91045 3.91275 0.4492
10 2.862 VV 0.0661 55.61210 10.11723 2.5208
11 3.816 VV 0.0290 5.01650 2.08734 0.2274
12 5.861 VV 0.0433 6.21290 1.71239 0.2816
13 6.494 BB 0.0355 5.38172 1.81934 0.2439
Totals : 2206.16682 562.93908
=====================================================================

Sample Name: Young_Acetaminophen
=====================================================================
(Sequence Method)

1.228
mAU
700
600
500
400
300
200
1.886
100
0
1 2 3 4 5 6 min
1.227
mAU
400
300
200
1.886
2.858
100
1.436
0.975
1.000
1.027
1.494
0.892
0.903
0.944
5.648
0
-100
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.228 BB 0.0409 2074.10132 747.99463 98.7991
2 1.886 BB 0.0568 25.21023 6.63648 1.2009
Totals : 2099.31154 754.63111

Sample Name: Young_Acetaminophen

----|-------|----|-------|----------|----------|--------|
1 0.892 BV 0.0158 10.32564 10.16985 0.3117
2 0.903 VV 0.0149 17.34571 15.13382 0.5235
3 0.944 VV 0.0272 67.78304 31.43303 2.0459
4 0.975 VV 0.0244 88.83979 44.29331 2.6814
5 1.000 VV 0.0258 108.18690 54.18707 3.2653
6 1.027 VB 0.0348 185.66763 65.01269 5.6039
7 1.227 BV 0.0570 2444.33569 594.04108 73.7760
8 1.436 VV 0.0603 101.42623 20.30394 3.0613
9 1.494 VB 0.0139 7.43487 7.00688 0.2244
10 1.886 BV 0.0514 240.54440 63.13742 7.2602
11 2.858 VV 0.0545 32.85183 7.51088 0.9915
12 5.648 VV 0.0408 8.44256 2.50531 0.2548
Totals : 3313.18429 914.73527
=====================================================================

Sample Name: Young_Aspirin
=====================================================================
(Sequence Method)
1.886
mAU
20
15
10
1.134
1.228
2.861
5
1 2 3 4 5 6 min
1.886
mAU
200
150
100
1.201
2.858
1.436
2.417
50
3.217
5.631
0.637
0.437
1.306
1.344
1.374
0.931
0.973
0.995
1.013
0.892
0.872
-50
-100
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.134 BV 0.0416 9.31227 3.23556 7.5251
2 1.228 VB 0.0609 9.36883 2.01051 7.5708
3 1.886 BB 0.0575 98.09443 25.44125 79.2684
4 2.861 BB 0.0703 6.97421 1.21796 5.6357
Totals : 123.74974 31.90528

Sample Name: Young_Aspirin

----|-------|----|-------|----------|----------|--------|
1 0.437 VB 0.0294 5.02449 2.06161 0.2234
2 0.637 VV 0.0463 10.94487 2.88331 0.4867
3 0.872 BV 0.0206 6.38109 4.01147 0.2837
4 0.892 VV 0.0341 33.92410 11.95992 1.5084
5 0.931 VV 0.0337 77.76773 27.77705 3.4579
6 0.973 VV 0.0209 72.74810 43.72836 3.2347
7 0.995 VV 9.24e-3 34.58775 52.15495 1.5379
8 1.013 VB 0.0539 261.65067 59.33819 11.6342
9 1.201 BV 0.1029 639.11121 77.33325 28.4179
10 1.306 VV 0.0211 38.56123 22.33220 1.7146
11 1.344 VV 0.0339 32.01800 11.35650 1.4237
12 1.374 VB 0.0304 7.07631 2.85527 0.3146
13 1.436 VV 0.0274 6.53708 2.94018 0.2907
14 1.886 VV 0.0556 907.85016 237.57278 40.3673
15 2.417 VV 0.0372 9.52765 3.15668 0.4236
16 2.858 VV 0.0702 91.90821 15.94736 4.0867
17 3.217 VV 0.0281 6.41534 2.76499 0.2853
18 5.631 VB 0.0389 6.93922 2.19152 0.3086
Totals : 2248.97320 582.36561
=====================================================================

Sample Name: Young_Caffeine
=====================================================================
(Sequence Method)

1.383
mAU
140
120
100
80
60
40
1.888
1.228
20
0
1 2 3 4 5 6 min
1.383
mAU
150
100
1.888
1.200
50
1.468
2.859
2.833
2.431
1.020
1.006
5.499
0.984
1.037
0.471
-50
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.228 BV 0.0992 12.39673 1.49629 2.3286
2 1.383 VB 0.0448 505.74625 167.25806 94.9995
3 1.888 BB 0.0546 14.22434 3.76155 2.6719
Totals : 532.36732 172.51590

Sample Name: Young_Caffeine

----|-------|----|-------|----------|----------|--------|
1 0.471 VV 0.0251 5.67680 2.80952 0.3982
2 0.984 BV 0.0237 55.17284 28.29728 3.8703
3 1.006 VV 0.0158 50.23748 41.08735 3.5241
4 1.020 VV 0.0151 57.43318 49.20158 4.0288
5 1.037 VB 0.0370 128.80510 58.01790 9.0354
6 1.200 BV 0.0947 434.27762 58.40945 30.4637
7 1.383 BV 0.0403 493.90512 167.86255 34.6464
8 1.468 VV 0.0130 5.16215 5.48901 0.3621
9 1.888 BV 0.0510 143.96454 37.74607 10.0988
10 2.431 VV 0.0393 12.81879 3.90042 0.8992
11 2.833 BV 0.0292 12.06578 5.28036 0.8464
12 2.859 VV 0.0361 19.20337 6.66473 1.3471
13 5.499 VV 0.0332 6.83524 2.51902 0.4795
Totals : 1425.55802 467.28524
=====================================================================

Sample Name: Kim_Aspirin
=====================================================================
(Sequence Method)

1.228
mAU
40
30
1.887
20
1.383
10
1.620
2.858
4.112
0
1 2 3 4 5 6 min
1.886
mAU
100
1.224
75
2.854
50
4.099
1.390
1.440
1.615
1.998
1.462
5.226
2.440
1.021
1.008
25
0
-25
-50
-75
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.228 BV 0.0425 129.64728 45.15274 56.7761
2 1.383 VB 0.0504 16.68122 4.69747 7.3052
3 1.620 BB 0.0476 9.04780 2.73540 3.9623
4 1.887 BB 0.0567 54.02757 14.25306 23.6602
5 2.858 BB 0.0838 7.44807 1.28118 3.2617
6 4.112 BB 0.1101 11.49625 1.32001 5.0345

Sample Name: Kim_Aspirin
Totals : 228.34819 69.43987

----|-------|----|-------|----------|----------|--------|
1 1.008 BV 0.0113 5.51839 7.41634 0.2814
2 1.021 VB 0.0719 128.08722 21.22842 6.5324
3 1.224 BV 0.1140 947.06488 100.46610 48.2997
4 1.390 VV 0.0576 134.29300 27.93188 6.8489
5 1.440 VV 0.0339 43.57961 15.95919 2.2225
6 1.462 VB 0.0191 14.99974 9.95606 0.7650
7 1.615 VV 0.0210 6.58165 3.84159 0.3357
8 1.886 VV 0.0531 515.37073 136.36736 26.2836
9 1.998 VB 0.0327 7.05356 3.59725 0.3597
10 2.440 VB 0.0326 7.31738 2.93007 0.3732
11 2.854 VV 0.0648 90.74667 16.71283 4.6280
12 4.099 VV 0.0790 55.04642 8.23378 2.8073
13 5.226 VV 0.0424 5.14966 2.02323 0.2626
Totals : 1960.80892 356.66409
=====================================================================

Sample Name: Kim_Acetaminophen
=====================================================================
(Sequence Method)

1.228
mAU
2000
1500
1000
500
1.886
2.858
0
1 2 3 4 5 6 min
1.228
mAU
1200
1000
800
600
400
1.886
2.866
1.433
1.421
1.444
0.912
0.924
0.950
0.992
2.694
5.430
200
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.228 BV 0.0418 7083.82666 2522.80103 98.6383
2 1.886 VB 0.0637 85.72824 19.54490 1.1937
3 2.858 BB 0.0742 12.06135 2.10977 0.1679
Totals : 7181.61625 2544.45570

Sample Name: Kim_Acetaminophen

----|-------|----|-------|----------|----------|--------|
1 0.912 BV 0.0148 10.09538 9.60220 0.1545
2 0.924 VV 0.0138 16.16217 15.37735 0.2473
3 0.950 VV 0.0139 28.52031 26.81871 0.4364
4 0.992 VB 0.0923 359.86530 46.21947 5.5058
5 1.228 BV 0.0551 5233.60938 1400.97583 80.0724
6 1.421 VV 0.0141 11.57319 13.63315 0.1771
7 1.433 VV 0.0117 8.68197 11.03705 0.1328
8 1.444 VB 0.0116 7.44891 8.23052 0.1140
9 1.886 BV 0.0559 683.22668 177.33624 10.4531
10 2.694 VV 0.0265 6.06765 2.82972 0.0928
11 2.866 VV 0.0766 165.66312 26.08010 2.5346
12 5.430 BV 0.0395 5.18116 1.57064 0.0793
Totals : 6536.09523 1739.71098
=====================================================================

Sample Name: Kim_Caffeine
=====================================================================
(Sequence Method)

1.383
mAU
80
70
60
50
40
30
20
1.228
1.886
10
0
1 2 3 4 5 6 min
1.383
mAU
60
1.200
1.883
40
2.861
0.928
0.945
0.993
1.013
0.763
4.835
1.300
20
0
-20
-40
-60
-80
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.228 BV 0.0574 23.58846 5.74157 7.7995
2 1.383 VB 0.0448 272.10080 90.00719 89.9695
3 1.886 BB 0.0533 6.74741 1.77761 2.2310
Totals : 302.43667 97.52638

Sample Name: Kim_Caffeine

----|-------|----|-------|----------|----------|--------|
1 0.763 VB 0.0393 6.86294 2.33171 0.3723
2 0.928 VV 0.0238 38.33031 21.53422 2.0791
3 0.945 VV 0.0439 105.13346 28.56598 5.7026
4 0.993 VV 0.0133 49.48552 48.76204 2.6842
5 1.013 VB 0.0534 245.60143 57.39932 13.3218
6 1.200 BV 0.1080 780.19098 88.76910 42.3188
7 1.300 VV 0.0199 48.63808 40.73252 2.6382
8 1.383 VB 0.0561 471.63776 113.17117 25.5824
9 1.883 VV 0.0499 74.58421 18.36983 4.0456
10 2.861 VV 0.0370 17.24706 5.59519 0.9355
11 4.835 VV 0.0302 5.89058 2.52312 0.3195
Totals : 1843.60232 427.75421
=====================================================================

Data File C:\CHEM32\1\DATA\CHEM112A_09_21_16 2016-09-21 13-10-19\CHEM112_211_75S_C2.D
Sample Name: Douglas_Aspirin
=====================================================================
(Sequence Method)
DAD1 A, Sig=254,4 Ref=off (CHEM112_211_75S_C2.D)
1.893
mAU
40
30
20
1.229
10
2.883
0
1 2 3 4 5 6 min
DAD1 C, Sig=230,4 Ref=off (CHEM112_211_75S_C2.D)
1.893
mAU
400
300
200
1.201
2.886
100
2.421
2.459
0.928
0.976
1.008
1.274
1.347
0.912
-100
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.229 BV 0.0562 26.97577 6.53508 11.6988
2 1.893 BB 0.0583 194.79649 49.66458 84.4788
3 2.883 BB 0.0722 8.81396 1.53083 3.8224
Totals : 230.58623 57.73049

Sample Name: Douglas_Aspirin

----|-------|----|-------|----------|----------|--------|
1 0.912 BV 0.0170 5.64429 4.38060 0.1888
2 0.928 VV 0.0102 9.80072 12.36848 0.3278
3 0.976 VV 0.0312 88.86422 34.88177 2.9721
4 1.008 VB 0.0630 265.72177 50.00943 8.8870
5 1.201 BV 0.0951 587.79657 74.43031 19.6588
6 1.274 VV 8.78e-3 16.86290 29.02128 0.5640
7 1.347 VV 0.1113 72.01964 7.90302 2.4087
8 1.893 VV 0.0592 1814.65735 453.63235 60.6911
9 2.421 BV 0.0250 5.71496 2.77855 0.1911
10 2.459 VB 0.0227 6.24336 3.51207 0.2088
11 2.886 BB 0.0701 116.66375 19.83302 3.9018
Totals : 2989.98953 692.75089
=====================================================================

Sample Name: Douglas_Caffeine
=====================================================================
(Sequence Method)

1.385
mAU
600
500
400
300
200
1.230
1.894
100
0
1 2 3 4 5 6 min
1.385
mAU
600
500
400
300
200
1.894
1.205
2.892
1.295
2.452
2.868
0.938
0.992
1.016
100
0
-100
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.230 BV 0.0504 39.06920 10.87310 1.6693
2 1.385 VV 0.0454 2279.39551 741.00977 97.3918
3 1.894 VB 0.0668 21.97464 4.72083 0.9389
Totals : 2340.43935 756.60369

Sample Name: Douglas_Caffeine

----|-------|----|-------|----------|----------|--------|
1 0.938 BV 0.0171 5.59338 4.17932 0.1415
2 0.992 VV 0.0301 77.47126 33.99290 1.9594
3 1.016 VB 0.0582 222.81931 47.98768 5.6355
4 1.205 BV 0.1075 800.07013 91.02578 20.2353
5 1.295 VV 0.0131 39.90216 50.86386 1.0092
6 1.385 VV 0.0517 2609.53857 730.54834 66.0002
7 1.894 VV 0.0534 171.87978 42.71347 4.3472
8 2.452 VB 0.0253 5.66528 2.72001 0.1433
9 2.868 BV 0.0346 13.50992 4.69178 0.3417
10 2.892 VV 0.0188 7.38731 4.97373 0.1868
Totals : 3953.83711 1013.69687
=====================================================================

Sample Name: Douglas_Acetaminophen
=====================================================================
(Sequence Method)

1.221
1.231
mAU
3000
2500
2000
1500
1000
1.896
2.889
500
0
1 2 3 4 5 6 min
1.223
1.245
mAU
1200
1.896
1000
800
600
400
2.894
0.560
0.602
1.031
2.440
0.961
0.986
200
0
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.221 BV 0.0229 5187.76465 3407.40063 35.2171
2 1.231 VV 0.0321 9117.78809 3418.35254 61.8960
3 1.896 VB 0.0628 406.35410 94.26265 2.7585
4 2.889 BB 0.0802 18.91109 3.18771 0.1284
Totals : 1.47308e4 6923.20353

Sample Name: Douglas_Acetaminophen

----|-------|----|-------|----------|----------|--------|
1 0.560 BV 0.0238 5.38358 2.94193 0.0441
2 0.602 VV 0.0387 9.81700 3.03478 0.0805
3 0.961 BV 8.67e-3 5.03263 8.80387 0.0413
4 0.986 VV 0.0305 58.11091 23.81299 0.4764
5 1.031 VB 0.0473 194.51245 51.77470 1.5948
6 1.223 BV 0.0337 4236.29004 1533.43103 34.7326
7 1.245 VV 0.0386 4153.10010 1511.12073 34.0506
8 1.896 VV 0.0622 3308.22095 784.38007 27.1235
9 2.440 VV 0.0448 12.70802 3.42642 0.1042
10 2.894 VV 0.0695 213.68681 36.67479 1.7520
Totals : 1.21969e4 3959.40129
=====================================================================

Sample Name: Yiv_Aspirin
=====================================================================
(Sequence Method)
1.895
mAU
15
12.5
1.230
10
7.5
5
1.385
2.894
2.5
0
1 2 3 4 5 6 min
1.895
mAU
150
100
1.203
2.895
50
1.388
1.443
2.962
5.129
0.823
3.002
0.799
0.876
0.914
0.936
0.950
1.296
0.964
0.985
1.018
-50
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.230 BV 0.0524 32.97670 8.76443 27.6516
2 1.385 VB 0.0624 9.08167 2.02211 7.6152
3 1.895 BB 0.0592 69.41708 17.52796 58.2076
4 2.894 BB 0.0729 7.78237 1.28883 6.5257
Totals : 119.25783 29.60332

Sample Name: Yiv_Aspirin

----|-------|----|-------|----------|----------|--------|
1 0.799 BV 0.0234 10.19431 5.43625 0.4972
2 0.823 VV 0.0530 54.99727 12.45032 2.6826
3 0.876 VV 0.0299 49.01619 27.35375 2.3908
4 0.914 VV 0.0234 69.02769 38.75074 3.3669
5 0.936 VV 0.0120 42.32031 44.73655 2.0642
6 0.950 VV 0.0123 45.23610 48.95371 2.2065
7 0.964 VV 0.0162 66.08158 52.48930 3.2232
8 0.985 VV 0.0244 115.87110 57.87007 5.6518
9 1.018 VB 0.0423 234.98260 66.44288 11.4616
10 1.203 BV 0.0996 561.51721 69.61393 27.3888
11 1.296 VV 0.0168 16.23835 12.38015 0.7920
12 1.388 BV 0.0332 9.59593 3.47903 0.4681
13 1.443 VB 0.0223 6.35908 3.56886 0.3102
14 1.895 VV 0.0546 659.06628 166.72755 32.1469
15 2.895 VV 0.0660 90.91728 16.31987 4.4346
16 2.962 VV 0.0201 5.46796 4.53497 0.2667
17 3.002 VV 0.0295 7.22003 3.00403 0.3522
18 5.129 BB 0.0342 6.06112 2.16245 0.2956
Totals : 2050.17041 636.27441
=====================================================================

Sample Name: Yiv_Caffeine
=====================================================================
(Sequence Method)

1.386
mAU
20
15
10
1.230
1 2 3 4 5 6 min
1.201
1.385
mAU
1.884
20
2.451
6.784
6.833
1.266
0.981
1.021
1.001
1.279
-20
-40
-60
-80
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.230 VV 0.0607 12.47027 2.78556 12.7515
2 1.386 VB 0.0467 85.32442 26.77584 87.2485
Totals : 97.79470 29.56139

Sample Name: Yiv_Caffeine

----|-------|----|-------|----------|----------|--------|
1 0.981 BV 0.0182 23.65368 16.07762 2.7195
2 1.001 VV 0.0192 41.40583 28.84338 4.7605
3 1.021 VB 0.0473 165.97569 42.28671 19.0827
4 1.201 BV 0.0918 494.04584 65.67780 56.8018
5 1.266 VV 0.0101 11.26468 16.24640 1.2951
6 1.279 VB 0.0142 10.95969 10.47185 1.2601
7 1.385 VV 0.0392 82.89108 26.72877 9.5302
8 1.884 VV 0.0546 19.32189 4.20390 2.2215
9 2.451 VV 0.0283 7.13669 3.16881 0.8205
10 6.784 VV 0.0271 5.90086 2.68891 0.6784
11 6.833 VV 0.0363 7.21531 2.38534 0.8296
Totals : 869.77124 218.77948
=====================================================================

Sample Name: Yiv_Acetaminophen
=====================================================================
(Sequence Method)

1.230
mAU
2000
1500
1000
500
1.897
0
1 2 3 4 5 6 min
1.230
mAU
1200
1000
800
600
400
1.897
1.374
1.438
5.897
2.146
2.427
2.882
0.964
0.999
200
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.230 BV 0.0422 6674.72314 2342.99512 99.5171
2 1.897 VB 0.0715 32.38542 6.45678 0.4829
Totals : 6707.10857 2349.45190

Sample Name: Yiv_Acetaminophen

----|-------|----|-------|----------|----------|--------|
1 0.964 BV 0.0366 64.42210 21.09101 1.1403
2 0.999 VB 0.0727 247.70616 40.28102 4.3844
3 1.230 BV 0.0541 5006.42871 1353.94153 88.6139
4 1.374 VV 0.0315 78.24464 30.45599 1.3849
5 1.438 VB 0.0182 16.24660 11.33505 0.2876
6 1.897 VV 0.0487 208.13268 54.96431 3.6840
7 2.146 VV 0.0327 5.89941 2.20922 0.1044
8 2.427 VV 0.0497 12.33170 3.04922 0.2183
9 2.882 VV 0.0293 5.03381 2.07741 0.0891
10 5.897 VB 0.0258 5.26671 2.57720 0.0932
Totals : 5649.71252 1521.98196
=====================================================================

Sample Name: Alfaraj_Caffeine
=====================================================================
(Sequence Method)

1.384
mAU
400
300
200
1.229
100
1.892
0
1 2 3 4 5 6 min
1.384
mAU
400
300
200
1.891
1.222
100
2.877
1.527
1.540
0.995
1.021
0.949
0.922
-100
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.229 BV 0.0425 124.56164 42.77562 7.8544
2 1.384 VV 0.0453 1423.06750 464.38409 89.7333
3 1.892 VB 0.0630 38.25595 8.75753 2.4123
Totals : 1585.88509 515.91724

Sample Name: Alfaraj_Caffeine

----|-------|----|-------|----------|----------|--------|
1 0.922 VV 0.0123 8.95223 10.62764 0.2664
2 0.949 VV 0.0165 30.43950 23.69745 0.9059
3 0.995 VV 0.0387 145.04567 45.53801 4.3169
4 1.021 VB 0.0592 204.34027 57.53453 6.0816
5 1.222 BV 0.1046 873.80695 98.89273 26.0063
6 1.384 VV 0.0516 1700.97400 477.11102 50.6246
7 1.527 VV 0.0182 13.31825 9.58907 0.3964
8 1.540 VB 0.0187 7.39590 6.58733 0.2201
9 1.891 BV 0.0543 309.61502 79.75027 9.2148
10 2.877 BV 0.0619 66.08787 12.76413 1.9669
Totals : 3359.97565 822.09217
=====================================================================

Sample Name: Alfaraj_Aspirin
=====================================================================
(Sequence Method)
1.891
mAU
12
10
4
1.227
1 2 3 4 5 6 min
1.892
mAU
100
75
1.202
50
2.872
2.846
2.444
1.013
1.002
1.025
1.283
25
0
-25
-50
-75
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.227 BB 0.0914 9.39491 1.26085 15.7340
2 1.891 BB 0.0573 50.31613 12.96604 84.2660
Totals : 59.71104 14.22689

Sample Name: Alfaraj_Aspirin

----|-------|----|-------|----------|----------|--------|
1 1.002 BV 9.95e-3 5.88027 9.84537 0.4854
2 1.013 VV 9.84e-3 15.41557 21.57568 1.2724
3 1.025 VB 0.0495 132.19621 32.12880 10.9119
4 1.202 BV 0.0922 515.36499 68.20767 42.5398
5 1.283 VV 0.0359 25.87685 12.01007 2.1360
6 1.892 VV 0.0521 491.74908 124.53264 40.5905
7 2.444 BV 0.0343 8.51612 2.98000 0.7029
8 2.846 BV 0.0192 5.13296 3.47656 0.4237
9 2.872 VB 0.0314 11.35657 4.50504 0.9374
Totals : 1211.48863 279.26183
=====================================================================

Sample Name: Alfaraj_Acetaminophen
=====================================================================
(Sequence Method)

1.230
mAU
300
250
200
150
100
1.896
50
0
1 2 3 4 5 6 min
1.229
mAU
200
150
100
1.896
1.382
1.417
1.436
1.462
2.436
3.304
0.970
1.001
1.015
3.839
50
-50
-100
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.230 BB 0.0415 1005.51385 360.52734 99.3801
2 1.896 BB 0.0543 6.27228 1.65344 0.6199
Totals : 1011.78613 362.18078

Sample Name: Alfaraj_Acetaminophen

----|-------|----|-------|----------|----------|--------|
1 0.970 BV 0.0177 14.18688 13.05105 0.6820
2 1.001 VV 0.0200 53.60625 33.77264 2.5768
3 1.015 VB 0.0751 193.39084 42.89188 9.2962
4 1.229 BV 0.0671 1619.42334 325.23166 77.8448
5 1.382 VV 0.0283 61.46111 26.77630 2.9544
6 1.417 VV 0.0180 28.03115 19.20950 1.3474
7 1.436 VV 0.0198 22.92619 15.49861 1.1020
8 1.462 VB 0.0142 10.35170 9.18216 0.4976
9 1.896 BV 0.0451 60.30268 16.12799 2.8987
10 2.436 VV 0.0250 5.46768 2.71285 0.2628
11 3.304 VV 0.0293 5.65945 2.37466 0.2720
12 3.839 BB 0.0323 5.51646 2.05927 0.2652
Totals : 2080.32374 508.88855
=====================================================================

Sample Name: Chyn_Aspirin
=====================================================================
(Sequence Method)

mAU
1.229
0.5
-0.5
-1
1 2 3 4 5 6 min
1.202
mAU
1.003
0.983
5.648
0.941
1.395
0.881
0.911
1.270
4.724
0
-20
-40
-60
-80
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.229 BB 0.0925 8.97043 1.21714 100.0000
Totals : 8.97043 1.21714

Sample Name: Chyn_Aspirin

----|-------|----|-------|----------|----------|--------|
1 0.881 BV 0.0231 20.76271 12.07957 1.9716
2 0.911 VV 0.0184 30.32332 22.94524 2.8794
3 0.941 VV 0.0405 112.12083 34.46706 10.6468
4 0.983 VV 0.0155 61.98917 49.99889 5.8864
5 1.003 VB 0.0640 296.80084 57.68711 28.1836
6 1.202 BV 0.0944 496.93384 65.60997 47.1878
7 1.270 VV 0.0161 18.00374 14.42220 1.7096
8 1.395 BV 0.0358 6.01559 2.07671 0.5712
9 4.724 BV 0.0273 5.09291 2.26003 0.4836
10 5.648 VB 0.0283 5.05488 2.28503 0.4800
Totals : 1053.09784 263.83181
=====================================================================

Sample Name: Chyn_Acetaminophen
=====================================================================
(Sequence Method)

1.229
mAU
500
400
300
200
100
1.890
1.135
0
1 2 3 4 5 6 min
1.229
mAU
400
300
200
100
1.890
1.363
1.423
1.435
0.912
1.463
2.870
0.938
0.987
2.894
1.028
5.067
0
-100
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.135 BV 0.0361 5.72062 2.29675 0.3422
2 1.229 VB 0.0409 1660.52527 598.31720 99.3248
3 1.890 BB 0.0492 5.56766 1.45413 0.3330
Totals : 1671.81356 602.06808

Sample Name: Chyn_Acetaminophen

----|-------|----|-------|----------|----------|--------|
1 0.912 BV 0.0189 5.70443 3.81701 0.2120
2 0.938 VV 0.0723 71.87591 16.57382 2.6708
3 0.987 VV 0.0200 64.33673 40.67086 2.3907
4 1.028 VB 0.0474 238.23737 60.54879 8.8526
5 1.229 BV 0.0588 2081.20288 492.41336 77.3349
6 1.363 VV 0.0272 74.20884 34.35135 2.7575
7 1.423 VV 0.0247 37.71519 19.83535 1.4014
8 1.435 VV 0.0199 25.43040 17.31796 0.9450
9 1.463 VB 0.0185 14.72159 10.08128 0.5470
10 1.890 VV 0.0454 57.92286 15.75192 2.1523
11 2.870 BV 0.0290 7.90700 3.61532 0.2938
12 2.894 VV 0.0303 6.50818 2.78191 0.2418
13 5.067 BB 0.0358 5.38642 1.83224 0.2002
Totals : 2691.15779 719.59117
=====================================================================

Sample Name: Chyn_Caffeine
=====================================================================
(Sequence Method)

1.385
mAU
700
600
500
400
300
200
1.230
1.891
100 2.874
0
1 2 3 4 5 6 min
1.384
mAU
600
500
400
300
200
1.893
1.224
2.876
1.558
1.589
1.625
0.955
0.988
1.001
1.018
1.301
1.698
4.556
4.635
1.035
100
0
-100
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.230 BV 0.0421 135.45836 47.06934 5.3493
2 1.385 VV 0.0452 2355.04053 769.00897 93.0023
3 1.891 VB 0.0689 31.46000 6.50575 1.2424
4 2.874 BB 0.0705 10.28097 1.77684 0.4060
Totals : 2532.23986 824.36090

Sample Name: Chyn_Caffeine

----|-------|----|-------|----------|----------|--------|
1 0.955 BV 0.0279 26.65723 12.25774 0.6103
2 0.988 VV 0.0175 38.79874 31.27353 0.8883
3 1.001 VV 8.62e-3 23.31029 38.19654 0.5337
4 1.018 VV 0.0167 64.81279 48.22296 1.4839
5 1.035 VB 0.0320 145.32602 56.49928 3.3272
6 1.224 BV 0.1007 912.88086 107.36622 20.9004
7 1.301 VV 9.99e-3 36.05398 52.65797 0.8255
8 1.384 VV 0.0519 2708.56128 754.64191 62.0125
9 1.558 VV 0.0193 24.64742 16.16373 0.5643
10 1.589 VV 0.0147 11.99969 10.25121 0.2747
11 1.625 VB 0.0209 6.23148 3.95213 0.1427
12 1.698 BV 0.0579 5.18668 1.07254 0.1187
13 1.893 VV 0.0502 230.54802 57.64518 5.2784
14 2.876 VV 0.0660 121.46959 21.97625 2.7810
15 4.556 BV 0.0303 5.77134 2.33653 0.1321
16 4.635 VV 0.0309 5.51215 2.14812 0.1262
Totals : 4367.76756 1216.66185
=====================================================================

Data File C:\CHEM32\1\DATA\CHEM112A_09_21_16 2016-09-21 13-10-19\CHEM112_212_2B_C1.D
Sample Name: Altobelli_Aspirin
=====================================================================
(Sequence Method)
DAD1 A, Sig=254,4 Ref=off (CHEM112_212_2B_C1.D)
1.885
mAU
80
70
60
50
40
30
20
2.857
1.226
10
0
1 2 3 4 5 6 min
DAD1 C, Sig=230,4 Ref=off (CHEM112_212_2B_C1.D)
1.886
mAU
600
500
400
300
200
1.201
2.859
2.039
2.785
0.929
1.285
1.312
0.986
1.009
100
0
-100
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.226 BB 0.0809 9.66829 1.50682 2.7635
2 1.885 BB 0.0571 331.93436 86.78871 94.8763
3 2.857 BB 0.0686 8.25736 1.48093 2.3602
Totals : 349.86002 89.77647

Sample Name: Altobelli_Aspirin

----|-------|----|-------|----------|----------|--------|
1 0.929 BV 0.1018 64.85001 7.50302 1.6204
2 0.986 VV 0.0178 51.02607 36.52896 1.2750
3 1.009 VB 0.0582 233.76628 48.51590 5.8412
4 1.201 BV 0.1006 558.91534 71.20434 13.9658
5 1.285 VV 0.0143 17.80662 15.57182 0.4449
6 1.312 VB 0.0140 6.47581 6.05466 0.1618
7 1.886 BV 0.0577 2955.07178 745.49670 73.8391
8 2.039 VV 0.0351 13.72602 6.50913 0.3430
9 2.785 BV 0.0249 9.43816 4.70404 0.2358
10 2.859 VV 0.0602 90.96601 18.40652 2.2730
Totals : 4002.04209 960.49509
=====================================================================

Sample Name: Altobelli_Acetaminophen
=====================================================================
(Sequence Method)

1.226
mAU
500
400
300
200
1.882
100
0
1 2 3 4 5 6 min
1.226
mAU
400
300
200
1.883
100
2.423
2.849
2.862
3.637
6.366
6.430
1.383
0.492
0.940
0.991
1.008
-100
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.226 BB 0.0404 1693.91626 619.61523 98.0633
2 1.882 BB 0.0573 33.45413 8.81559 1.9367
Totals : 1727.37039 628.43082

Sample Name: Altobelli_Acetaminophen

----|-------|----|-------|----------|----------|--------|
1 0.492 VV 0.0428 7.52323 2.10129 0.2767
2 0.940 VV 0.0184 17.26347 12.67395 0.6349
3 0.991 VV 0.0252 80.17395 39.40759 2.9484
4 1.008 VB 0.0616 249.49236 48.46255 9.1752
5 1.226 BV 0.0555 1982.26660 497.00235 72.8985
6 1.383 VV 0.0117 7.60595 8.26933 0.2797
7 1.883 VV 0.0530 325.13416 84.34639 11.9569
8 2.423 BV 0.0271 8.39873 3.98391 0.3089
9 2.849 VV 0.0326 11.14190 4.70185 0.4097
10 2.862 VB 0.0298 11.03181 4.55101 0.4057
11 3.637 VV 0.0371 5.63337 2.08301 0.2072
12 6.366 VV 0.0423 8.07090 2.33895 0.2968
13 6.430 VV 0.0302 5.47794 2.18932 0.2015
Totals : 2719.21438 712.11150
=====================================================================

Sample Name: Altobelli_Caffeine
=====================================================================
(Sequence Method)

1.381
mAU
15
12.5
10
7.5
5
2.5
0
1 2 3 4 5 6 min
1.201
1.381
mAU
0.960
1.001
1.028
0.982
1.306
0.567
0.581
-20
-40
-60
-80
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.381 BB 0.0436 52.94738 18.13626 100.0000
Totals : 52.94738 18.13626

Sample Name: Altobelli_Caffeine

----|-------|----|-------|----------|----------|--------|
1 0.567 VV 0.0230 6.26300 3.48650 0.4306
2 0.581 VB 0.0466 12.52962 3.20433 0.8615
3 0.960 BV 0.0335 13.70784 6.81653 0.9425
4 0.982 VV 9.03e-3 13.84976 21.46287 0.9523
5 1.001 VV 0.0137 35.47350 33.94521 2.4391
6 1.028 VB 0.0475 201.48621 51.69030 13.8539
7 1.201 BV 0.1040 771.79950 89.56609 53.0677
8 1.306 VV 0.0191 68.31060 45.30848 4.6969
9 1.381 VV 0.0812 330.94907 48.78048 22.7555
Totals : 1454.36909 304.26078
=====================================================================

Sample Name: Flores_Aspirin
=====================================================================
(Sequence Method)
1.884
mAU
20
15
10
5
1.227
1 2 3 4 5 6 min
1.884
mAU
200
150
100
1.198
2.852
2.865
2.418
2.428
1.437
4.062
50
0.948
0.992
4.508
0.974
1.019
1.031
1.301
-50
-100
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.227 BB 0.0977 7.91019 1.01182 7.3756
2 1.884 BB 0.0571 99.33780 26.00885 92.6244
Totals : 107.24799 27.02067

Sample Name: Flores_Aspirin

----|-------|----|-------|----------|----------|--------|
1 0.948 BV 0.0249 10.85150 5.41991 0.5740
2 0.974 VV 0.0125 17.66271 20.54514 0.9342
3 0.992 VV 0.0249 63.05184 31.41307 3.3350
4 1.019 VV 9.97e-3 34.41301 47.40594 1.8202
5 1.031 VB 0.0476 155.56281 54.45488 8.2281
6 1.198 BV 0.0962 566.21442 70.90511 29.9485
7 1.301 VV 0.0165 12.50659 9.74771 0.6615
8 1.437 BB 0.0359 8.34881 2.87288 0.4416
9 1.884 BV 0.0574 932.08478 242.13008 49.3003
10 2.418 BV 0.0249 7.20937 3.92376 0.3813
11 2.428 VV 0.0293 9.25238 3.87750 0.4894
12 2.852 BV 0.0370 32.84209 10.95915 1.7371
13 2.865 VB 0.0434 27.46727 10.55847 1.4528
14 4.062 BB 0.0417 7.39146 2.17406 0.3910
15 4.508 VB 0.0306 5.76640 2.31375 0.3050
Totals : 1890.62544 518.70140
=====================================================================

Sample Name: Flores_Caffeine
=====================================================================
(Sequence Method)

1.380
mAU
1200
1000
800
600
400
1.226
1.881
1.132
200 2.853
0
1 2 3 4 5 6 min
1.379
mAU
1000
800
600
400
1.882
1.203
200
2.844
1.593
0.908
1.003
1.013
1.031
1.296
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.132 BV 0.0415 8.67513 2.93133 0.2102
2 1.226 VV 0.0438 35.06531 11.41447 0.8497
3 1.380 VV 0.0452 4033.99463 1336.42554 97.7482
4 1.881 VB 0.0657 43.14168 9.45525 1.0454
5 2.853 BB 0.0690 6.04696 1.06016 0.1465
Totals : 4126.92371 1361.28674

Sample Name: Flores_Caffeine

----|-------|----|-------|----------|----------|--------|
1 0.908 VV 0.0487 5.42517 1.43264 0.0977
2 1.003 BV 0.0104 10.04302 13.18394 0.1809
3 1.013 VV 0.0145 25.98287 23.26604 0.4680
4 1.031 VB 0.0384 125.62373 39.75763 2.2625
5 1.203 BV 0.1057 802.09869 93.38003 14.4459
6 1.296 VV 0.0147 54.96532 52.73903 0.9899
7 1.379 VV 0.0532 4122.63281 1152.26233 74.2493
8 1.593 VV 0.0250 16.09470 9.14563 0.2899
9 1.882 BB 0.0539 312.59958 83.07915 5.6300
10 2.844 VV 0.0636 76.95598 14.35297 1.3860
Totals : 5552.42188 1482.59939
=====================================================================

Sample Name: Flores_Acetaminophen
=====================================================================
(Sequence Method)

1.226
mAU
1200
1000
800
600
400
1.882
200
0
1 2 3 4 5 6 min
1.226
mAU
800
600
400
1.881
200
2.852
1.369
2.870
1.436
2.410
2.443
0.977
1.032
2.050
3.337
0.927
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.226 BV 0.0406 3924.28687 1427.29102 98.7180
2 1.882 VB 0.0630 50.96439 11.77977 1.2820
Totals : 3975.25125 1439.07078

Sample Name: Flores_Acetaminophen

----|-------|----|-------|----------|----------|--------|
1 0.927 BV 0.0171 5.68393 4.25823 0.1289
2 0.977 VV 0.0496 127.45152 30.57655 2.8912
3 1.032 VB 0.0408 199.74498 58.52500 4.5312
4 1.226 BV 0.0502 3497.92432 990.60443 79.3504
5 1.369 VV 0.0258 55.39503 26.58015 1.2566
6 1.436 VB 0.0354 24.92647 8.82738 0.5655
7 1.881 BV 0.0557 424.02719 108.25249 9.6191
8 2.050 VB 0.0258 5.40130 2.53880 0.1225
9 2.410 VV 0.0301 9.73321 4.10813 0.2208
10 2.443 VB 0.0277 7.65965 3.40893 0.1738
11 2.852 VV 0.0410 31.30383 9.25112 0.7101
12 2.870 VV 0.0211 13.31753 7.93062 0.3021
13 3.337 VV 0.0284 5.63307 2.40070 0.1278
Totals : 4408.20202 1257.26252
=====================================================================

Data File C:\CHEM32\1\DATA\CHEM112A_09_21_16 2016-09-21 13-10-19\CHEM112_212_30B_A5.D
Sample Name: Khamnei_Acetaminophen
=====================================================================
(Sequence Method)
DAD1 A, Sig=254,4 Ref=off (CHEM112_212_30B_A5.D)

1.226
mAU
600
500
400
300
200
1.889
100
0
1 2 3 4 5 6 min
DAD1 C, Sig=230,4 Ref=off (CHEM112_212_30B_A5.D)
1.225
mAU
400
300
200
1.889
100
1.374
1.437
2.888
1.406
1.005
1.026
4.267
0.954
0.972
-100
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.226 BB 0.0404 1904.43250 697.02673 98.6933
2 1.889 BB 0.0565 25.21508 6.76206 1.3067
Totals : 1929.64757 703.78879

Sample Name: Khamnei_Acetaminophen

----|-------|----|-------|----------|----------|--------|
1 0.954 BV 0.0161 6.02501 4.81057 0.2081
2 0.972 VV 0.0297 31.04378 17.42727 1.0723
3 1.005 VV 0.0189 61.14851 39.75508 2.1121
4 1.026 VB 0.0399 174.25723 52.95961 6.0189
5 1.225 BV 0.0561 2246.71875 556.30377 77.6020
6 1.374 VV 0.0186 40.49937 26.78582 1.3989
7 1.406 VV 0.0228 26.55288 19.43170 0.9171
8 1.437 VV 0.0251 27.93376 13.50014 0.9648
9 1.889 VV 0.0517 253.04535 65.35121 8.7402
10 2.888 VV 0.0559 22.56294 4.79070 0.7793
11 4.267 VV 0.0340 5.39477 1.96523 0.1863
Totals : 2895.18235 803.08110
=====================================================================

Sample Name: Khamnei_Caffeine
=====================================================================
(Sequence Method)

1.384
mAU
140
120
100
80
60
40
1.227
20
0
1 2 3 4 5 6 min
1.384
mAU
150
100
1.202
50
1.886
1.896
0.563
0.975
0.989
1.010
1.029
1.298
0.915
-50
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.227 BV 0.0925 13.63675 1.81798 2.6548
2 1.384 VB 0.0441 500.03271 166.40959 97.3452
Totals : 513.66947 168.22757

Sample Name: Khamnei_Caffeine

----|-------|----|-------|----------|----------|--------|
1 0.563 VV 0.0359 8.40767 2.85471 0.4183
2 0.915 VV 0.0122 10.82873 11.23682 0.5387
3 0.975 VV 0.0305 96.93178 38.93029 4.8225
4 0.989 VV 0.0150 53.10635 45.76465 2.6421
5 1.010 VV 0.0179 77.16045 55.01558 3.8389
6 1.029 VB 0.0342 178.21037 63.57636 8.8663
7 1.202 BV 0.1077 778.41376 89.70425 38.7275
8 1.298 VV 0.0145 50.95959 44.12170 2.5353
9 1.384 VV 0.0539 738.12744 191.85678 36.7232
10 1.886 BV 0.0254 9.20983 4.49438 0.4582
11 1.896 VV 0.0267 8.62246 4.16398 0.4290
Totals : 2009.97843 551.71952
=====================================================================

Sample Name: Khamnei_Aspirin
=====================================================================
(Sequence Method)
1.889
mAU
10
4
1.226
1 2 3 4 5 6 min
1.890
mAU
100
75
1.199
50
2.868
2.429
0.632
1.283
1.015
1.001
0.966
25
0
-25
-50
-75
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.226 BB 0.1039 9.88524 1.16015 17.1574
2 1.889 BB 0.0573 47.72972 12.55670 82.8426
Totals : 57.61496 13.71685

Sample Name: Khamnei_Aspirin

----|-------|----|-------|----------|----------|--------|
1 0.632 VB 0.0289 5.22361 2.22256 0.4044
2 0.966 BV 0.0276 18.73228 8.54263 1.4501
3 1.001 VV 0.0158 33.22786 32.89754 2.5723
4 1.015 VB 0.0556 198.84962 42.49427 15.3937
5 1.199 BV 0.0949 544.89972 70.32104 42.1827
6 1.283 VV 0.0181 17.29853 12.94533 1.3391
7 1.890 VV 0.0563 458.82513 119.54778 35.5193
8 2.429 VV 0.0287 8.30358 3.70062 0.6428
9 2.868 VV 0.0282 6.40159 2.96349 0.4956
Totals : 1291.76193 295.63527
=====================================================================

Sample Name: Khamnei_Mixed
=====================================================================
(Sequence Method)

1.227
mAU
30
25
20
1.888
15
10
1.383
1 2 3 4 5 6 min
1.888
mAU
100
75
1.217
50
2.861
2.890
1.438
1.386
1.424
5.514
0.996
1.290
2.453
5.493
1.017
2.423
0.965
0.935
25
0
-25
-50
-75
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.227 BV 0.0431 98.47431 33.22136 62.3565
2 1.383 VB 0.0581 11.28224 2.65386 7.1442
3 1.888 BB 0.0567 48.16489 12.56470 30.4993
Totals : 157.92145 48.43992

Sample Name: Khamnei_Mixed

----|-------|----|-------|----------|----------|--------|
1 0.935 BV 0.0143 13.34422 13.20262 0.8457
2 0.965 VV 0.0189 39.67992 28.23825 2.5147
3 0.996 VV 0.0238 85.65974 44.79465 5.4286
4 1.017 VB 0.0503 231.16354 54.68305 14.6498
5 1.217 BV 0.1004 644.63855 75.67300 40.8535
6 1.290 VV 0.0203 31.30011 19.44502 1.9836
7 1.386 BV 0.0256 7.88543 4.06579 0.4997
8 1.424 VV 0.0219 5.03430 3.02751 0.3190
9 1.438 VB 0.0170 5.69732 4.14282 0.3611
10 1.888 BB 0.0520 475.02887 120.42457 30.1046
11 2.423 VV 0.0244 5.90975 3.14657 0.3745
12 2.453 VV 0.0297 8.17522 3.50399 0.5181
13 2.861 BV 0.0209 6.41156 3.94846 0.4063
14 2.890 VB 0.0215 6.55576 3.92180 0.4155
15 5.493 VV 0.0329 5.12287 2.03069 0.3247
16 5.514 BB 0.0368 6.31986 2.05670 0.4005
Totals : 1577.92702 386.30549
=====================================================================

Sample Name: Rivas_Caffeine
=====================================================================
(Sequence Method)
1.891
mAU
80
60
40
20
1.226
2.879
0
1 2 3 4 5 6 min
1.891
mAU
700
600
500
400
300
200
1.201
2.876
2.074
2.452
3.323
0.858
1.307
1.323
1.019
1.034
100
0
-100
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.226 BV 0.0640 18.97985 3.95536 4.8330
2 1.891 BB 0.0569 363.22769 95.50464 92.4916
3 2.879 BB 0.0734 10.50657 1.83263 2.6754
Totals : 392.71411 101.29263

Sample Name: Rivas_Caffeine

----|-------|----|-------|----------|----------|--------|
1 0.858 VB 0.0638 8.64002 1.63167 0.2096
2 1.019 VV 0.0129 18.21576 18.61864 0.4418
3 1.034 VB 0.0359 100.11057 33.90945 2.4282
4 1.201 BV 0.1030 612.85535 73.73173 14.8650
5 1.307 VV 0.0168 17.17544 13.12532 0.4166
6 1.323 VB 0.0202 11.08499 7.51423 0.2689
7 1.891 VV 0.0606 3204.57886 801.50287 77.7279
8 2.074 VB 0.0242 6.90964 3.80396 0.1676
9 2.452 BV 0.0398 10.63838 3.24113 0.2580
10 2.876 VV 0.0663 126.49583 22.61173 3.0682
11 3.323 BV 0.0355 6.11296 2.12768 0.1483
Totals : 4122.81779 981.81841
=====================================================================

Sample Name: Rivas_Acetaminophen
=====================================================================
(Sequence Method)

1.219
1.237
mAU
3000
2500
2000
1500
1000
1.890
1.617
2.875
500
0
1 2 3 4 5 6 min
1.216
1.228
mAU
1200
1.890
1000
800
600
400
2.879
1.616
2.094
0.972
0.987
1.007
1.018
1.034
200
0
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.219 BV 0.0223 6235.91406 3417.83057 41.9212
2 1.237 VV 0.0300 8165.58545 3401.64844 54.8935
3 1.617 VB 0.0721 37.55951 7.17499 0.2525
4 1.890 BB 0.0569 422.32462 112.31174 2.8391
5 2.875 BB 0.0670 13.93032 2.48102 0.0936
Totals : 1.48753e4 6941.44675

Sample Name: Rivas_Acetaminophen

----|-------|----|-------|----------|----------|--------|
1 0.972 BV 0.0126 13.74711 14.43020 0.1103
2 0.987 VV 0.0182 32.52700 24.14864 0.2611
3 1.007 VV 9.82e-3 27.17569 38.10889 0.2181
4 1.018 VV 0.0104 32.81457 45.50667 0.2634
5 1.034 VB 0.0347 152.99146 56.39431 1.2280
6 1.216 BV 0.0206 2491.19849 1521.04126 19.9953
7 1.228 VV 0.0452 5793.94238 1529.15747 46.5043
8 1.616 VB 0.0307 8.02849 3.20865 0.0644
9 1.890 VV 0.0587 3737.07373 913.51678 29.9951
10 2.094 VV 0.0183 6.79865 4.71265 0.0546
11 2.879 VV 0.0676 162.62924 29.12648 1.3053
Totals : 1.24589e4 4179.35200
=====================================================================

Sample Name: Rivas_Aspirin
=====================================================================
(Sequence Method)

1.227
1.383
mAU
30
25
20
15
10
1.890
1.481
1.150
5
0
1 2 3 4 5 6 min
1.219
1.381
1.890
mAU
1.481
20
1.529
1.014
0.988
1.037
2.883
0.482
1.303
-20
-40
-60
-80
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.150 BV 0.0427 5.17852 1.60383 2.3053
2 1.227 VV 0.0403 104.47045 37.78209 46.5065
3 1.383 VV 0.0438 97.59660 33.22420 43.4465
4 1.481 VB 0.0464 7.50518 2.30910 3.3410
5 1.890 BB 0.0544 9.88554 2.65461 4.4007
Totals : 224.63629 77.57384

Sample Name: Rivas_Aspirin

----|-------|----|-------|----------|----------|--------|
1 0.482 VV 0.0343 7.73343 2.70975 0.4588
2 0.988 VV 0.0368 35.51545 16.08511 2.1070
3 1.014 VV 0.0185 53.69094 35.83604 3.1853
4 1.037 VB 0.0293 124.48900 53.15658 7.3855
5 1.219 BV 0.1066 866.01038 96.63317 51.3772
6 1.303 VV 0.0121 37.52855 45.52945 2.2264
7 1.381 VV 0.0686 369.91544 64.84766 21.9457
8 1.481 VV 0.0418 67.57021 19.33149 4.0087
9 1.529 VB 0.0177 7.29131 6.84716 0.4326
10 1.890 VV 0.0474 101.37100 26.35630 6.0140
11 2.883 VV 0.0533 14.47643 3.32188 0.8588
Totals : 1685.59213 370.65461
=====================================================================

Sample Name: Rivas_Mixed
=====================================================================
(Sequence Method)

1.384
mAU
400
1.228
300
200
100
1.893
0
1 2 3 4 5 6 min
1.384
mAU
400
300
1.227
200
1.893
100
2.872
0.638
1.543
2.027
2.430
0.958
1.009
0.948
-100
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.228 BV 0.0398 614.82721 229.49463 29.6929
2 1.384 VB 0.0444 1411.94861 472.62131 68.1896
3 1.893 BB 0.0561 43.84680 11.73754 2.1176
Totals : 2070.62262 713.85347

Sample Name: Rivas_Mixed

----|-------|----|-------|----------|----------|--------|
1 0.638 VV 0.0290 5.15110 2.96029 0.1328
2 0.948 BV 0.0128 8.52177 11.08518 0.2196
3 0.958 VV 0.0239 33.49390 17.47437 0.8633
4 1.009 VB 0.0709 280.01755 47.10385 7.2173
5 1.227 BV 0.0733 1311.01636 237.88077 33.7906
6 1.384 VV 0.0504 1746.99268 492.26022 45.0276
7 1.543 VV 0.0188 10.11209 8.97863 0.2606
8 1.893 BV 0.0518 438.77585 112.93184 11.3092
9 2.027 VB 0.0253 5.96635 2.98216 0.1538
10 2.430 BV 0.0348 9.15874 3.20577 0.2361
11 2.872 VV 0.0587 30.61995 6.36117 0.7892
Totals : 3879.82632 943.22425
=====================================================================

Sample Name: Subramanian_Aspirin
=====================================================================
(Sequence Method)

1.228
mAU
800
600
400
200
1.891
1.379
1.133
1.622
2.871
0
1 2 3 4 5 6 min
1.228
mAU
600
500
1.891
400
300
200
2.876
1.375
1.434
1.616
1.141
2.422
1.000
1.014
1.029
100
0
-100
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.133 BV 0.0334 20.97041 9.24989 0.7207
2 1.228 VV 0.0407 2689.94263 988.72241 92.4472
3 1.379 VB 0.0522 37.77444 9.97638 1.2982
4 1.622 BB 0.0477 10.33922 3.28885 0.3553
5 1.891 BB 0.0575 144.16945 37.81985 4.9548
6 2.871 BB 0.0762 6.51052 1.14686 0.2238

Sample Name: Subramanian_Aspirin
Totals : 2909.70666 1050.20424

----|-------|----|-------|----------|----------|--------|
1 1.000 BV 0.0119 13.00419 13.93133 0.2890
2 1.014 VV 0.0142 25.65875 25.64679 0.5702
3 1.029 VB 0.0422 133.06598 39.13269 2.9572
4 1.141 BV 0.0426 234.48135 75.85176 5.2109
5 1.228 VV 0.0490 2552.01001 743.95251 56.7139
6 1.375 VV 0.0330 76.60497 28.39061 1.7024
7 1.434 VB 0.0170 11.90462 9.26131 0.2646
8 1.616 VB 0.0348 10.51072 3.98347 0.2336
9 1.891 VV 0.0572 1373.30090 350.28943 30.5192
10 2.422 VV 0.0273 6.19716 2.75269 0.1377
11 2.876 VB 0.0594 63.05972 12.80634 1.4014
Totals : 4499.79836 1305.99893
=====================================================================

Data File C:\CHEM32\1\DATA\CHEM112A_09_21_16 2016-09-21 13-10-19\CHEM112_212_66B_B1.D
Sample Name: Subramanian_Acetaminophen
=====================================================================
(Sequence Method)
DAD1 A, Sig=254,4 Ref=off (CHEM112_212_66B_B1.D)

1.383
mAU
500
400
300
200
1.228
1.889
100
2.868
0
1 2 3 4 5 6 min
DAD1 C, Sig=230,4 Ref=off (CHEM112_212_66B_B1.D)
1.383
mAU
500
1.889
400
300
200
1.224
2.870
1.566
1.583
0.865
0.906
0.930
100
0.525
0.980
1.025
-100
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.228 BV 0.0414 194.39850 69.02097 9.0611
2 1.383 VV 0.0456 1808.60901 592.95819 84.3011
3 1.889 VB 0.0596 133.42346 33.07991 6.2190
4 2.868 BB 0.0735 8.98497 1.55264 0.4188
Totals : 2145.41594 696.61171

Sample Name: Subramanian_Acetaminophen

----|-------|----|-------|----------|----------|--------|
1 0.525 VB 0.0304 6.16574 2.44518 0.1250
2 0.865 BV 0.0253 19.58721 10.46640 0.3972
3 0.906 VV 0.0303 64.04026 25.46577 1.2987
4 0.930 VV 0.0227 61.30797 32.95215 1.2433
5 0.980 VV 0.0484 199.50143 49.62404 4.0458
6 1.025 VB 0.0377 200.07253 64.54360 4.0574
7 1.224 BV 0.0991 982.95795 120.57536 19.9340
8 1.383 VV 0.0508 2127.29980 601.03693 43.1409
9 1.566 VV 0.0122 5.57418 7.08559 0.1130
10 1.583 VB 0.0203 5.60613 4.02455 0.1137
11 1.889 VV 0.0546 1163.24683 301.21384 23.5902
12 2.870 VV 0.0620 95.69345 18.61331 1.9406
Totals : 4931.05348 1238.04672
=====================================================================

Sample Name: Subramanian_Caffeine
=====================================================================
(Sequence Method)
1.891
mAU
30
25
20
15
10
1.228
5
0
1 2 3 4 5 6 min
1.891
mAU
300
250
200
150
100
1.202
2.866
2.034
1.257
1.439
1.008
1.022
3.806
0.985
1.276
6.515
50
0
-50
-100
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.228 BB 0.0811 10.24147 1.59166 6.9096
2 1.891 BB 0.0577 137.97858 35.64221 93.0904
Totals : 148.22005 37.23387

Sample Name: Subramanian_Caffeine

----|-------|----|-------|----------|----------|--------|
1 0.985 BV 0.0182 33.23355 23.89123 1.5767
2 1.008 VV 0.0182 52.69320 39.07594 2.4999
3 1.022 VB 0.0445 175.90834 47.77066 8.3456
4 1.202 BV 0.0913 473.99298 64.08404 22.4875
5 1.257 VV 0.0131 18.19859 18.28623 0.8634
6 1.276 VB 0.0107 7.39945 8.87440 0.3510
7 1.439 BV 0.0261 5.32583 2.63635 0.2527
8 1.891 BV 0.0569 1283.22400 329.83606 60.8796
9 2.034 VV 0.0193 5.30298 3.57407 0.2516
10 2.866 VV 0.0584 39.09248 8.15742 1.8547
11 3.806 VV 0.0291 5.38840 2.55762 0.2556
12 6.515 VB 0.0453 8.04720 2.12150 0.3818
Totals : 2107.80698 550.86552
=====================================================================

Sample Name: Yuan_Acetaminophen
=====================================================================
(Sequence Method)

1.228
mAU
600
500
400
300
200
1.482
1.890
100
0
1 2 3 4 5 6 min
1.228
mAU
400
300
200
1.890
100
1.378
1.481
0.584
0.973
1.001
0.896
0.915
6.736
0
-100
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.228 BV 0.0408 1902.04639 686.84637 98.9180
2 1.482 VB 0.0542 8.19183 1.98204 0.4260
3 1.890 BV 0.0558 12.61380 3.36366 0.6560
Totals : 1922.85202 692.19207

Sample Name: Yuan_Acetaminophen

----|-------|----|-------|----------|----------|--------|
1 0.584 VV 0.0375 7.36982 2.38884 0.2642
2 0.896 VV 0.0151 17.84151 15.25434 0.6396
3 0.915 VV 0.0213 36.74664 22.18072 1.3173
4 0.973 VV 0.0364 127.61848 45.28887 4.5749
5 1.001 VB 0.0706 317.29446 56.42172 11.3744
6 1.228 BV 0.0548 2122.47437 540.54663 76.0868
7 1.378 VV 0.0204 19.49998 12.69058 0.6990
8 1.481 VV 0.0235 7.46194 3.96503 0.2675
9 1.890 VV 0.0498 128.08601 33.33139 4.5917
10 6.736 VV 0.0269 5.14875 2.36251 0.1846
Totals : 2789.54197 734.43063
=====================================================================

Sample Name: Yuan_Aspirin
=====================================================================
(Sequence Method)

1.383
mAU
80
1.228
60
40
1.133
1.888
20
1 2 3 4 5 6 min
1.383
1.887
mAU
100
1.224
75
50
2.864
1.134
2.044
0.588
0.633
1.489
6.641
0.977
0.997
0.961
0.987
1.031
25
0
-25
-50
-75
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.133 BV 0.0360 32.00410 13.11049 5.9180
2 1.228 VV 0.0404 175.56139 64.26882 32.4636
3 1.383 VB 0.0441 287.60477 96.96173 53.1819
4 1.888 BB 0.0567 45.62459 12.05215 8.4366
Totals : 540.79485 186.39319

Sample Name: Yuan_Aspirin

----|-------|----|-------|----------|----------|--------|
1 0.588 VV 0.0238 5.64080 3.40167 0.2429
2 0.633 VV 0.0301 9.35754 3.88514 0.4029
3 0.961 BV 0.0133 10.40254 9.88978 0.4479
4 0.977 VV 8.97e-3 13.57167 21.20703 0.5844
5 0.987 VV 9.29e-3 17.80960 26.66545 0.7669
6 0.997 VV 0.0139 35.43474 33.30531 1.5259
7 1.031 VB 0.0456 200.36586 54.20354 8.6281
8 1.134 BV 0.0438 288.75995 83.68984 12.4344
9 1.224 VV 0.0748 687.27435 115.72913 29.5951
10 1.383 VV 0.0595 531.00739 122.72407 22.8660
11 1.489 VB 0.0143 6.58021 6.22736 0.2834
12 1.887 BV 0.0534 450.09467 115.54919 19.3818
13 2.044 VV 0.0234 5.29106 2.81877 0.2278
14 2.864 VV 0.0575 55.18336 11.49387 2.3763
15 6.641 VB 0.0439 5.48548 1.51058 0.2362
Totals : 2322.25922 612.30072
=====================================================================

Sample Name: Yuan_Caffeine
=====================================================================
(Sequence Method)

1.383
mAU
1600
1400
1200
1000
800
600
400
1.889
1.228
1.134
200 2.865
0
1 2 3 4 5 6 min
1.383
mAU
1200
1000
800
600
1.889
400
1.203
2.866
1.568
0.838
0.866
0.901
0.929
0.945
0.965
1.285
2.431
2.463
3.028
1.024
1.034
3.044
200
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.134 BV 0.0421 6.83181 2.27200 0.1191
2 1.228 VV 0.0432 55.99093 18.80833 0.9763
3 1.383 VV 0.0455 5492.64893 1804.33557 95.7781
4 1.889 VB 0.0612 167.14224 40.00697 2.9145
5 2.865 BB 0.0680 12.15118 2.17968 0.2119
Totals : 5734.76509 1867.60255

Sample Name: Yuan_Caffeine

----|-------|----|-------|----------|----------|--------|
1 0.838 BV 0.0314 24.78268 10.00579 0.3031
2 0.866 VV 0.0287 45.77667 19.62563 0.5598
3 0.901 VV 0.0201 48.81591 30.62232 0.5970
4 0.929 VV 0.0169 49.80656 38.99804 0.6091
5 0.945 VV 9.23e-3 29.34636 44.31145 0.3589
6 0.965 VV 0.0469 196.67087 50.56952 2.4050
7 1.024 VV 0.0137 71.64642 68.37500 0.8761
8 1.034 VB 0.0291 171.37383 71.03148 2.0957
9 1.203 BV 0.1034 820.86041 96.79655 10.0381
10 1.285 VV 0.0145 65.35294 56.34821 0.7992
11 1.383 VV 0.0572 5046.32373 1333.35791 61.7103
12 1.568 VV 0.0400 39.80918 16.57315 0.4868
13 1.889 BV 0.0561 1370.18860 358.27890 16.7557
14 2.431 VV 0.0299 8.41537 3.58728 0.1029
15 2.463 VV 0.0221 5.20178 2.94209 0.0636
16 2.866 VV 0.0754 170.74179 28.31488 2.0880
17 3.028 VV 0.0232 6.82821 3.85066 0.0835
18 3.044 VV 0.0221 5.49705 3.04551 0.0672
Totals : 8177.43834 2236.63437
=====================================================================

Sample Name: Zeledon_Aspirin
=====================================================================
(Sequence Method)

1.228
mAU
300
250
200
150
100
1.888
1.383
1.619
1.133
2.862
2.679
50
0
1 2 3 4 5 6 min
1.227
1.888
mAU
200
150
100
2.862
1.381
1.614
2.437
1.423
1.435
0.522
0.574
0.912
0.817
0.849
0.900
4.692
0.967
1.000
1.016
50
-50
-100
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.133 BV 0.0363 13.79688 5.68685 1.2109
2 1.228 VV 0.0402 958.94165 353.36520 84.1625
3 1.383 VB 0.0555 22.54781 5.72240 1.9789
4 1.619 BB 0.0474 17.25062 5.23692 1.5140
5 1.888 BB 0.0565 107.22051 28.41540 9.4103
6 2.679 VV 0.0713 6.63103 1.14930 0.5820
7 2.862 VB 0.0720 13.00471 2.35167 1.1414

Sample Name: Zeledon_Aspirin

----|-------|----|-------|----------|----------|--------|
Totals : 1139.39322 401.92774

----|-------|----|-------|----------|----------|--------|
1 0.522 VV 0.0219 6.72923 3.84558 0.1893
2 0.574 VV 0.0436 13.87603 3.99022 0.3903
3 0.817 BV 0.0277 8.25357 3.68130 0.2322
4 0.849 VV 0.0405 46.03180 13.78576 1.2948
5 0.900 VV 0.0167 36.09618 30.65320 1.0154
6 0.912 VV 0.0240 64.32065 34.90278 1.8093
7 0.967 VV 0.0376 162.25917 51.67869 4.5642
8 1.000 VV 0.0195 84.59649 61.58978 2.3796
9 1.016 VB 0.0432 242.27731 67.01421 6.8151
10 1.227 BV 0.0653 1568.81116 319.60028 44.1295
11 1.381 VV 0.0365 72.98148 24.34251 2.0529
12 1.423 VV 9.83e-3 7.86800 11.02010 0.2213
13 1.435 VB 0.0149 8.55048 8.06881 0.2405
14 1.614 VV 0.0465 23.92813 6.41134 0.6731
15 1.888 VV 0.0581 1027.71606 265.87521 28.9089
16 2.437 VV 0.0268 8.75240 4.37482 0.2462
17 2.862 BV 0.0716 166.23311 28.49391 4.6760
18 4.692 BB 0.0470 5.73895 1.45502 0.1614
Totals : 3555.02018 940.78352
=====================================================================

Sample Name: Zeledon_Acetaminophen
=====================================================================
(Sequence Method)

1.228
mAU
1750
1500
1250
1000
750
500
1.382
1.991
1.887
1.697
2.834
0.996
2.675
3.615
250
0
1 2 3 4 5 6 min
1.227
mAU
1000
800
600
400
1.886
1.384
2.858
1.693
200
1.609
0.533
0.557
0.988
1.004
2.676
0.917
0.929
0.941
2.434
3.770
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 0.996 BB 0.0463 5.79588 1.65885 0.1008
2 1.228 BV 0.0402 5182.58496 1905.22559 90.1492
3 1.382 VB 0.0528 286.24582 77.13010 4.9791
4 1.697 BB 0.0462 29.45026 9.62702 0.5123
5 1.887 BV 0.0535 70.60677 19.84904 1.2282
6 1.991 VB 0.0614 113.07705 27.27047 1.9669
7 2.675 VV 0.0885 10.86223 1.69071 0.1889

Sample Name: Zeledon_Acetaminophen

----|-------|----|-------|----------|----------|--------|
8 2.834 VB 0.1031 32.49070 4.79318 0.5652
9 3.615 BV 0.1277 17.78129 1.69789 0.3093
Totals : 5748.89495 2048.94283

----|-------|----|-------|----------|----------|--------|
1 0.533 BV 0.0352 5.71921 2.10346 0.0888
2 0.557 BB 0.0596 9.67698 1.92794 0.1502
3 0.917 BV 0.0151 16.26573 13.91837 0.2525
4 0.929 VV 8.98e-3 12.18807 19.00113 0.1892
5 0.941 VV 0.0199 37.33137 24.38490 0.5795
6 0.988 VV 0.0275 106.62055 47.82912 1.6550
7 1.004 VB 0.0580 264.83038 54.21155 4.1107
8 1.227 BV 0.0522 4374.18555 1225.22546 67.8963
9 1.384 VV 0.0737 602.74792 108.71671 9.3559
10 1.609 VV 0.0261 7.15020 3.32652 0.1110
11 1.693 VB 0.0405 39.74966 11.89717 0.6170
12 1.886 VV 0.0577 757.09814 193.13680 11.7517
13 2.434 VV 0.0267 7.43307 3.43600 0.1154
14 2.676 BV 0.0503 18.16299 4.38873 0.2819
15 2.858 VB 0.0700 176.50706 30.96616 2.7398
16 3.770 VV 0.0286 6.78079 3.02599 0.1053
Totals : 6442.44769 1747.49601
=====================================================================

Sample Name: Zeledon_Caffeine
=====================================================================
(Sequence Method)

1.382
mAU
300
250
200
150
1.227
100
1.885
50
0
1 2 3 4 5 6 min
1.382
mAU
250
200
150
1.224
1.883
100
1.524
2.424
2.849
6.217
6.100
1.032
0.988
0.969
50
0
-50
-100
1 2 3 4 5 6 min
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000

----|-------|----|-------|----------|----------|--------|
1 1.227 BV 0.0413 158.54936 56.43439 13.6323
2 1.382 VB 0.0446 990.00281 329.12521 85.1217
3 1.885 BB 0.0541 14.49120 3.88202 1.2460
Totals : 1163.04337 389.44163

Sample Name: Zeledon_Caffeine

----|-------|----|-------|----------|----------|--------|
1 0.969 BV 0.0230 33.42023 18.17411 1.1854
2 0.988 VV 0.0224 54.04163 30.22685 1.9169
3 1.032 VB 0.0452 204.93929 56.04400 7.2693
4 1.224 BV 0.1014 945.87830 112.71323 33.5506
5 1.382 VV 0.0530 1354.42932 359.27292 48.0421
6 1.524 VB 0.0281 33.38754 14.36275 1.1843
7 1.883 VB 0.0496 162.78708 39.89810 5.7741
8 2.424 VV 0.0452 12.26410 3.27728 0.4350
9 2.849 VV 0.0291 7.01627 3.07725 0.2489
10 6.100 BV 0.0385 5.03646 1.56517 0.1786
11 6.217 VV 0.0380 6.05562 1.90903 0.2148
Totals : 2819.25583 640.52069
=====================================================================

DAD1 A, Sig 254,4 Ref Off (CHEM112 - 211 - 7S - A7.D)

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DAD1 A, Sig 254,4 Ref Off (CHEM112 - 211 - 7S - A7.D)

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Data File C:\CHEM32\1\DATA\CHEM112A_09_21_16 2016-09-21 13-10-19\CHEM112_211_7S_A7.

DAD1 A, Sig=254,4 Ref=off (CHEM112_211_7S_A7.D)

Signal 1: DAD1 A, Sig=254,4 Ref=off

Peak RetTime Type Width Area Height Area

Totals : 111.65780 29.25596

HPLC #3 9/21/2016 5:56:23 PM SYSTEM Page 1 of 2

Signal 2: DAD1 C, Sig=230,4 Ref=off

Peak RetTime Type Width Area Height Area

Totals : 2389.31568 558.95480

HPLC #3 9/21/2016 5:56:23 PM SYSTEM Page 2 of 2

DAD1 A, Sig=254,4 Ref=off (CHEM112_211_7S_A8.D)

Signal 1: DAD1 A, Sig=254,4 Ref=off

Peak RetTime Type Width Area Height Area

Totals : 1554.03563 562.91001

HPLC #3 9/21/2016 6:04:25 PM SYSTEM Page 1 of 2

Signal 2: DAD1 C, Sig=230,4 Ref=off

Peak RetTime Type Width Area Height Area

Totals : 2715.35898 660.66669

HPLC #3 9/21/2016 6:04:25 PM SYSTEM Page 2 of 2

DAD1 A, Sig=254,4 Ref=off (CHEM112_211_7S_A9.D)

Signal 1: DAD1 A, Sig=254,4 Ref=off

Peak RetTime Type Width Area Height Area

Totals : 4137.56138 1349.78697

HPLC #3 9/21/2016 6:12:20 PM SYSTEM Page 1 of 2

Signal 2: DAD1 C, Sig=230,4 Ref=off

Peak RetTime Type Width Area Height Area

Totals : 6435.37628 1660.28079

HPLC #3 9/21/2016 6:12:20 PM SYSTEM Page 2 of 2

DAD1 A, Sig=254,4 Ref=off (CHEM112_211_29S_B3.D)

Signal 1: DAD1 A, Sig=254,4 Ref=off

Peak RetTime Type Width Area Height Area

Totals : 274.89745 69.48838

HPLC #3 9/21/2016 6:44:10 PM SYSTEM Page 1 of 2

Signal 2: DAD1 C, Sig=230,4 Ref=off

Peak RetTime Type Width Area Height Area

Totals : 3403.79920 827.52344

HPLC #3 9/21/2016 6:44:10 PM SYSTEM Page 2 of 2

DAD1 A, Sig=254,4 Ref=off (CHEM112_211_29S_B4.D)

Signal 1: DAD1 A, Sig=254,4 Ref=off

Peak RetTime Type Width Area Height Area

Totals : 8102.40663 2818.69773

HPLC #3 9/21/2016 6:52:08 PM SYSTEM Page 1 of 2

Signal 2: DAD1 C, Sig=230,4 Ref=off

Peak RetTime Type Width Area Height Area

Totals : 6639.83475 1673.07786

HPLC #3 9/21/2016 6:52:08 PM SYSTEM Page 2 of 2

DAD1 A, Sig=254,4 Ref=off (CHEM112_211_29S_B5.D)

Signal 1: DAD1 A, Sig=254,4 Ref=off

Peak RetTime Type Width Area Height Area

Totals : 171.51293 57.04472

HPLC #3 9/21/2016 7:00:05 PM SYSTEM Page 1 of 2

Signal 2: DAD1 C, Sig=230,4 Ref=off

Peak RetTime Type Width Area Height Area

Totals : 1373.68118 247.26169

HPLC #3 9/21/2016 7:00:05 PM SYSTEM Page 2 of 2

DAD1 A, Sig=254,4 Ref=off (CHEM112_211_31S_A1.D)

Signal 1: DAD1 A, Sig=254,4 Ref=off

Peak RetTime Type Width Area Height Area

Totals : 1669.88721 556.70886

HPLC #3 9/21/2016 5:08:33 PM SYSTEM Page 1 of 2

Signal 2: DAD1 C, Sig=230,4 Ref=off

Peak RetTime Type Width Area Height Area

Totals : 3559.54535 951.43789