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MEASUREMENT SYSTEM the flow direction measures the sum of the static and
- Traditionally used to measure physical and electrical dynamic pressure
quantities, such as mass, temperature, pressure, Dynamic pressure – directional component of pressure in a
capacitance and voltage. moving (dynamic) fluid
- Often made a part of a control system. - used to measure flow rates and airspeed
CALIBRATION-Process of configuring an instrument to - can be measured by taking the differential pressure
provide a result for a sample within an acceptable range. between instruments parallel and perpendicular to the flow
RECALIBRATION- performed by adjusting the instrument. Applications
MEASURAND – property that is being measured. Altimeter
TOLERANCE - is term that is closely related to accuracy and Barometer
defines the maximum error that is to be expected in some MAP sensor
value Pitot tube
ACCURACY – refer to the CLOSENESS of measured value. Sphygmomanometer
ISO – international organization for standardization
- Organisation Internationale de Normalisation Evangelista Torricelli – invented the oldest type of liquid
(French) column (a vertical tube filled with mercury) manometer in
- Truness. 1643
- Defines accuracy as describing a combination of both Christian Huygens – invented the U-Tube in 1661
of observation error Hydrostatic gauge - (such as the mercury column
INACCURACY OR MEASUREMENT UNCERTAINTY manometer) compare pressure to the hydrostatic force per
-is the extent to which reading might be wrong and unit area at the base of a column of fluid
is often quoted as percentage of the full- scale reading of - measurements are independent of the type of gas being
instrument. measured, and can be designed to have a very linear
calibration
PRECISION – is the description of random errors and a - they have poor dynamic response.
measure of statical variability. Piston-type gauges - counterbalance the pressure of a fluid
- It refers to closeness of two more measurement to with a solid weight or a spring
each other. - also called as deadweight tester
REPEATABILITY - closeness output reading when the same Liquid Column – gauges consists of a vertical column of liquid
input is applied repetitively over short period of time. in a tube whose ends are exposed to different pressures
REPRODUCIBILITY - described the closeness of output Types of Manometer
reading for the same input when there are changes in the Simple Manometer
method. Micrometer
ERROR IN MEASUREMENTS Differential manometer
1. The instrument is not calibrated, and has an offset Inverted differential manometer
2. Reading uncertainty due to the presence of random McLeod gauge – isolates sample of gas and compresses it in a
noise. modified mercury manometer until the pressure is a few
3. Reading the instrument before it has reached it has mmHg
reached its steady state. Aneroid – gauges are based on metallic pressure sensing
4. Mistakes in recording measured data and calculating a element which flexes elastically under the effect of a pressure
derived measurand. difference across the element
MEASUREMENT UNITS - “Aneroid” means “without liquid,” and the term originally
MAGNITUDES OF MAESUREMENTS – are typically given in distinguished these gauges from the hydrostatic gauges
terms of a specific unit. - aneroid gauges can be used to measure the pressure of a
liquid as well as a gas, and they are not the only type of gauge
CHAPTER II that can operate without fluid. For this reason, they are often
PRESSURE MEASUREMENT called mechanical gauges in modern language
Gauges that rely on a change in capacitance are often
Pressure gauges or Vacuum gauges – instruments used to referred to as Baratron gauges
measure pressure Bourdon - Bourdon pressure gauge uses the principle that a
Manometer – could also be referring to pressure measuring flattened tube tends to change a more circular cross-section
instrument, usually limited to measuring pressure near when pressurized
atmospheric Eugene Bourdon – patented his gauge in France in 1849, and
- is often used to refer specifically to liquid column it was widely adopted because of its superior sensitivity,
hydrostatic instruments linearity, and accuracy
Vacuum gauges - is used to measure the pressure in a Edward Ashcroft – purchased Bourdon’s American patent
vacuum, which is further divided into two subcategories: high rights in 1852 and became a major manufacturer of gauges
and low vacuum (and sometimes ultra-high vacuum) Bernard Schaeffer – patented a successful diaphragm
Absolute pressure - is zero-referenced against a perfect pressure gauge, which together with the Bourdon gauge,
vacuum, so it is equal to gauge pressure plus atmospheric revolutionized pressure measurement industry, in 1849, in
pressure Magdeburg, Germany
Gauge pressure - is zero-referenced against ambient air 1875 – after Bourdon’s patents expired, his company
pressure, so it is equal to absolute pressure minus Schaeffer and Budenberg also manufactured Bourdon tube
atmospheric pressure. Negative signs are usually omitted gauges
Differential pressure - is the difference in pressure between Diaphragm – a second type of aneroid gauge uses the
two points deflection of a flexible membrane that separates regions of
Static pressure - is uniform in all directions, so pressure different pressure
measurements are independent of direction in an immovable For absolute measurements, welded pressure capsule with
(static) fluid diaphragms on either side are often used.
Shape: Mass spec + ionization
Flat Sound – disturbances propagate from source as longitudinal
Corrugated pressure variations along the path of propagation
Flatten tube Sound pressure – is the instantaneous local pressure
Capsule deviation from the average pressure caused by a sound wave
Bellows – bellows configuration is used in aneroid - can be measured using a microphone in air and hydrophone
barometers, altimeters, altitude recording barographs, and in water
the altitude telemetry instrument used in weather balloon - are normally small and are often expressed in units of
radiosondes microbar
Electronic pressure sensors Frequency response of pressure sensors
Piezoresistive strain gage - Uses resonance
the piezoresistive effect of bonded or formed strain Effective sound pressure – is the root mean square of the
gauges to detect strain due to applied pressure instantaneous sound pressure over a given interval of time.
Capacitive - Uses a diaphragm and pressure cavity to
create a variable capacitor to detect strain due to CHAPTER III
applied pressure MASS AND WEIGHT MEASUREMENT
Magnetic - Measures the displacement of a
diaphragm by means of changes •Mass is a quantitative measure of inertia of a body at rest.
in inductance (reluctance), LVDT, Hall effect, or • mass is the product of density and volume.
by eddy current principle •Weight or weight force is the force with which a body is
Piezoelectric - Uses the piezoelectric effect in certain attracted toward the Earth.
materials such as quartz to measure the strain upon •Weight force is determined by the product of the mass and
the sensing mechanism due to pressure the acceleration of gravity.
Optical – Uses the physical change of an optical fiber •weights-The embodiment of units of mass
to detect strain due to applied pressure • kilogram - unit of mass (SI)
Potentiometric – Uses the motion of a wiper along a • Newton - unit of weight ( SI)
resistive mechanism to detect the strain caused by • Slug- unit of mass ( English)
applied pressure • Pound - unit of weight ( English )
Resonant – Uses the changes in resonant frequency •1893 -the pound has been defined in terms of the kilogram
in a sensing mechanism to measure stress, or change WEIGHING INSTRUMENT
in gas density, caused by applied pressure
Thermal Conductivity - as a real gas increases in density - 1. Platform Beam Balance
which may indicate an increase in pressure- its ability to - this ohaus brand platform balance is a triple beam
conduct heat increases. - - In this type of gauge, a wire poise carriage balance.
filament is heated by running current through it -patented in 1932
Thermocouple or resistance thermometer (RTD) - can be -To determine the weight of the object placed in the
used to measure the temperature of the filament weighing pan, the weights, known as POISE, must be moved
Pirani gauge - uses a single platinum filament as both the along the beam for hundreds, tens and units (grams).
heated element and RTD -The position of POISE indicate the weight of the
Pirani (one wire) – Pirani gauge consist of a metal wire open object placed on the pan.
to the pressure being measured -This balance can weigh objects up to 610 grams.
- This type of gauge was invented by Marcello Pirani 2. Platform Dial Scale
Thermocouple gauges and thermistor gauges work in similar -Ohause balance introduced on the market in 1957
manner, except a thermocouple of thermistor is used to -Marked a milestone in the history of this company
measure the temperature of the wire by introducing a new way system of counterweights.
Ionization gauge – are the most sensitive gauges for very low -Ohaus introduced a dial system that was turned to
pressures (also reffered to as hard or high vacuum) stabilize the beam in a perfectly horizontal position. When
Hot cathode - hot-cathode ionization gauge is composed the arrow of the beam is stabilized, the position of the dial
mainly of three electrodes acting together as a triode, where indicator the weight of the object placed in the pan.
the cathode is the filament -Known as "Dial-O-Gram"
Most common ion gauge is the hot cathode Bayard-Alpert -Used to measure small quantities of powder
gauge, with a small ion collector inside the grid 3. Toledo Balance
A glass envelope with an opening to the vacuum can - manufactured in the USA in 1945
surround the electrodes, but usually the Nude gauge is - based on a system of counter weights: the object to be
inserted in the vacuum chamber directly, the pins being fed weighed is deposited on the pan and the counterweight
through a ceramic plate in the wall of the chamber equilibrates the two ends of the weighing arm.
Cold cathode – there are two subtypes of a cold cathode - NEEDLE indicates the correct reading.
ionization gauges: the Penning gauge (invented by Frans - can weigh object up to 2500 grams
Michel Penning) , and the Inverted magnetron, also called a 4. Analytic Balance
Redhead gauge -electric model of a sartorious analytic or precision balance
Hydrostatic and elastic gauges measure pressure are directly dates from the 1950.
influenced by force exerted on the surface by incident - used by researchers at the Institut de Microbiologie et
particle flux, and are called direct reading gauges d'Hygiene de I'Universite de Montreal in 1964
Thermal and ionization gauges read pressure indirectly by -can measure precisely very small masses of substances --
measuring a gas property that changes in a predictable in the order of the milligram-- is essential to laboratory
manner with gas density works.
Indirect measurements are susceptible to more errors that 5. Electronic Analytical Balance
direct measurements -Mettler electronic analytic balance was purchased in 1976
Dead weight tester by Armand- Frappier Institute researchers.
McLeod
- can measure with great precision very small quantities of 4. Glass Pipettes - rarely used in contemporary routine
solid or liquid material. laboratories; were replaced by semiautomatic dispensers.
- It is one of the first model of its category to integrate
electronics as a basis for functioning. - vary from 1 to 100 mL.
- the weight of the material in the pan can ne determined - non-scaled for measuring of a certain volume or
up to 4 decimal smaller than unity ( 0.0001 grams) scaled with grades by 1 mL and 10 mL.
6. Dial Torsion Balance
-the rectangular box is a precision balance know as a " 5. Mircosyringes - serve for dispensing small volumes of
torsion balance" because its functioning is based on the liquids.
torsion of a metal wire.
- this type of balance has several uses - consists of a needle attached to a scaled glass
- measured weak force cylinder with a piston.
- this instrument used at Institut de Microbiologie et - vary in the diameter of needles and pistons.
d'Hygiene in 1977
6. Piston dispenser - consists of a piston with a scale attached
7. Two-Pan Balance to a flask.
-it is often used to equilibrate, two by two, solutions
- intended for repetitive dispensing of the same
that will undergo centrifugation.
volume from stock container.
-By proceeding in this manner, the volume may be
different, but the weight will identical. Dispensers - designed for measuring aggressive liquids made
-This intrument must be installed om flat stable of borosilicate glass; plastic parts that are in contact with
surface. measured liquid are made of PTFE, other parts of PE or PP.
CHAPTER V
VOLUME 7. Pipettors - manual and electronic pipettors can be
distinguised.
Volume - is a quantity of three-dimensional space enclosed
Manual pipettors - piston is moved by a thumb using an
by a closed surface.
operation knob.
- quantified numeriacally using the SI derived unit, m3 .
Electronic Pipettors - piston is moved by a small electric
Volume of some simple shapes, such as regular, straight- motor.
edged, and circular shapes calculated using arithmetic
TWO BIG GROUPS:
formulas.
“Air displacement” pipettors - also called air cushion, can be
Volume with complicated shapes, calculated with integral
designed as a single channel or multi channel.
calculus.
Multi-channel pipettors - intended for simultaneous
Volume of a solid can be determined by fluid displacement.
pippeting of the same volume of liquid to several wells of a
Displacement of liquid - used to determine the volume of a microtitration plate.
gas.
Micropipettors - are constructed for one fixed volume or it is
Laboratory vessels and devices - used for preparation of possible to set the volume.
solution and manipulation with liquid.
“Positive diplacement” pipettors - liquid is aspired into the
Volumetric vessels - usually calibrated for 20 degree Celsius. tip without any air cushion the piston is in contact with
measured liquid.
Calibration temperature - written at every volumetric
vessels. - suitable for very viscous ar voilatile liquids and for repetitive
pipetting.
1. Beakers - approximate determination of the volume of
liquids and not necessarily classified as measuring tools. Steppers - liquid is then delivered at once or in several steps.
Consists of 2 wooden blocks placed around a pulley The frictional torque due to rope, must be equal to
fixed to the shaft of an engine whose power is required to be the torque being transmitted by the engine.Let,
measured.
W = weight at the end of the rope (N)
Blocks are clamped by means of bolts and nuts.
S = spring balance reading (N)
A helical spring is provided between the nut and the
N = engine speed (rpm)
upper block to adjust the pressure on the pulley to control its
speed. D = diameter of the brake wheel (m)
The upper block has a long lever attached to it and d = diameter of the rope (m)
carries a weight W at its outer end. A counter weight is
placed at the other end of the lever which balances the brake (D + d) = Effective diameter of the brake wheel
when unloaded.
Then,
In order to limit the motion of the lever, two stops
work/revolution = torque x angle turned per revolution
provided.
= (W- S) x ((D + d)/2) x 2π
Working:
= (W - S) x (D - d) x π Construction:
work done per minutes = (W – S)π(D + d)N It consists of a pulley A (called driving pulley) which
is rigidly fixed to the shaft of an engine whose power is
required to be measured.
work done/ sec = ((W - S) π (D - d) N)/60 Pulley B (called driven pulley) mounted on another
shaft to which the power from pulley A is transmitted.
Brake power = ((W - S) π DN)/(60 x 1000) (kW) or = ((T x Pulleys A and B are connected by means of a
2πN)/(60 x 1000)) (kW) continuous belt passing round the two loose pulleys C and D
which are mounted on a T-shaped frame.
Advantage:
The frame is pivoted at E and its movement is
Cheap and easy construction. controlled by two stops.
Limitations:
2P x a = W x L or P = W x L/2a
Torque transmitted, T = P x R
Working Principal