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Addressing Clay Mineralogy Effects on Performance of

Chemically Stabilized Expansive Soils Subjected to


Seasonal Wetting and Drying
Bhaskar C. S. Chittoori, Ph.D., P.E., M.ASCE 1; Anand J. Puppala, Ph.D., P.E., F.ASCE 2;
and Aravind Pedarla, Ph.D., P.E., M.ASCE 3
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Abstract: Premature failures in chemically stabilized expansive soils cost millions of dollars in maintenance and repair. One reason for these
failures is the inability of existing stabilization design guidelines to take into account the complex interactions between the clay minerals and the
stabilizers. It is vital to understand these complex interactions, as they are responsible for the improved strength and reduction of swelling/shrinking
in these soils, which in turn affects the overall health of the infrastructure. This research study examined the longevity of chemically stabilized
expansive soils subjected to wetting/drying conditions, with a major focus on clay mineralogy. Eight different natural soils with varying clay
mineralogy were subjected to wetting/drying durability studies after they were stabilized with chemical additives including quicklime and cement.
Performance indicators such as volumetric strain and unconfined compressive strength trends were monitored at regular intervals during the
wetting/drying process. It was observed that clayey soils dominant in the mineral montmorillonite were susceptible to premature failures. It
was also noted that soils dominant in other clay minerals exhibited early failures at lower additive contents. For the first time, an attempt
was made to address the field implications of the laboratory studies by developing a correlation that predicts service life in the field based
on clay mineralogy and stabilizer dosage. DOI: 10.1061/(ASCE)GT.1943-5606.0001796. © 2017 American Society of Civil Engineers.
Author keywords: Soil stabilization; Durability; Seasonal changes; Clay mineralogy; Expansive soils; Volumetric strain.

Introduction design guides, several agencies have reported premature failures,


especially in the case of pavement infrastructure. These early fail-
Problematic expansive clays are often stabilized with chemical ad- ures are typically attributed to the loss of stabilizer, caused by sea-
ditives such as lime and cement to subdue the ill effects of swelling sonal changes. However, in some instances they could be due to the
and shrinking (Nelson and Miller 1992; Puppala et al. 2005; Rogers ineffectiveness of a stabilizer in some soils even though other soils
and Wright 1986; Sherwood 1993; Little and Nair 2009). This tech- with the same index properties respond well to that stabilizer. This
nique is widely used in the construction of roads, airports, embank- situation indicates that the current stabilizer design procedures are
ments, and canal linings built on or using expansive clays. In these not entirely equipped to stabilize all types of expansive soils, be-
cases, chemicals are mixed with the soil to improve workability, cause these guidelines recommend the selection of the type and
strength, stiffness, swelling characteristics, and bearing capacity amount of the stabilizer on the basis of the plasticity index (PI)
(Puppala et al. 2006, 2009; Pedarla et al. 2011; Yi et al. 2016). and the gradation characteristics of the soil.
In chemical treatment, soil property enhancements usually occur The long-term behavior of chemically treated soil is dependent
through chemical gel formation and bonding among soil particles, on the complex interactions between the mineralogy of the soil
along with a reduction in soil water affinity characteristics (Jones and the chemical additive, along with the environmental impacts
and Holtz 1973; Petry and Armstrong 1989; Al-Rawas et al. 2005; (Allam and Sridharan 1981; Pile and McInnes 1984; Day 1994;
Chittoori 2008). Lin and Benson 2000; Chittoori 2008; Pedarla et al. 2011). The
Chemical stabilization design guidelines for stabilizing expan- current stabilization design guidelines do not consider these miner-
sive soils (AF-JMAN/TM 1994; InDOT 2008; Little and Nair alogical characteristics and therefore cannot capture the difference
2009; TxDOT 2005) typically recommend that a minimum strength in performance (Chittoori 2008; Pedarla et al. 2011). This study at-
requirement be met after stabilization and that the durability of the tempted to understand the long-term behavior of chemically stabi-
stabilization be checked. Even after following these stabilization lized expansive soils by focusing on the clay minerals and their
interactions with chemical additives. This paper presents the details
1
Assistant Professor, Dept. of Civil Engineering, Boise State Univ., of the various durability tests conducted in this research study and
1910 University Dr., Boise, ID 83704 (corresponding author). E-mail: the results obtained from these tests. An analysis of these results is
bhaskarchittoori@boisestate.edu presented, highlighting the importance of clay mineralogy and the
2
Distinguished Teaching Professor and Associate Dean, Dept. of Civil shortcomings of the existing stabilization guidelines, along with a
Engineering, Univ. of Texas at Arlington, Arlington, TX 76019. E-mail: discussion on the development of a correlation to predict the field
anand@uta.edu
3 implications of the laboratory studies conducted in this research.
Postdoctoral Fellow, Dept. of Civil Engineering, Univ. of Texas at
Arlington, Arlington, TX 76019. E-mail: pedarla@uta.edu
Note. This manuscript was submitted on November 24, 2016; approved
on June 12, 2017; published online on October 24, 2017. Discussion period Documented Durability Studies
open until March 24, 2018; separate discussions must be submitted for in-
dividual papers. This paper is part of the Journal of Geotechnical and Several studies were performed to understand the effect of seasonal
Geoenvironmental Engineering, © ASCE, ISSN 1090-0241. moisture fluctuations and their relative volumetric changes on the

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J. Geotech. Geoenviron. Eng., 2018, 144(1): 04017097


long-term performance of chemically stabilized expansive clays Experimental Program
(Dif and Bluemel 1991; Lin and Benson 2000; Rao et al. 2001;
Guney et al. 2007; Khattab et al. 2007; Cui et al. 2011; Pedarla et al. The experimental program consisted of testing eight different soils
2011). The following sections present a brief overview of some of with varying clay mineralogies. Stabilization design was performed
these studies, followed by the shortcomings of these studies. on these soils as per the current procedures detailed in the manual
Rao et al. (2001) conducted a study to assess the long-term Modification and Stabilization of Soils and Base for Use in Pavement
performance of stabilized black cotton soils. Those black cotton Structures (TxDOT 2005). Initially, a quicklime additive was used as a
soils were stabilized with waste materials such as wood ash and stabilizer for all eight soils, and the additive dosage for soil was es-
organic matter (known as ash-modified soils) and also with a lime tablished using the current stabilization design guides. Durability
stabilizer. This study was conducted primarily to understand the studies were performed in the laboratory in accordance with ASTM
relative effectiveness of ash-modified soils and lime-treated black D559 (ASTM 2015a). The following sections detail the experimental
cotton soils. They observed that the ash-modified soil became more testing procedure followed to evaluate the stabilized clayey specimens
for long-term performance. Subsequently, four of the soils that
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porous due to cyclic wetting/drying and consequently collapsed


significantly. They also found that due to cyclic wetting/drying, showed premature failures under the durability studies were selected,
the beneficial strength effects attributed to the lime treatment were and additional mix designs were performed on these soils by increas-
partially lost. Hoyos et al. (2006) performed a series of wet and dry ing the lime dosage to arrive at a durable mix design that satisfied the
cyclic tests on different types of chemically-treated sulfate soils to durability criterion. Durability studies were also conducted on these
evaluate the strength, stiffness, and volume change property var- four soils by using cement as an additive to establish the dosage levels
iations with these cycles. It was observed that higher dosages of at which the cement would be adequate for these soils. The details of
stabilizer improved the unconfined compressive strength (UCS), the experimental program are presented in the following sections.
stiffness, and durability of the specimens.
Guney et al. (2007) performed cyclic wetting/drying (W/D) ex- Materials and Methods
periments to observe the effect of lime stabilization on the swelling A total of eight soils with soluble sulfate contents less than 50 ppm
potential of the soil. In this study, both swelling potential and swell- and varying plasticity characteristics were selected from different
ing pressure tests were performed on untreated and lime-treated soil parts of Texas, with the assistance of the Texas Department of Trans-
specimens subjected to cyclic W/D. They observed that the primary portation (TxDOT) districts. The soils were named after the region
benefits of lime stabilization were lost after the first W/D cycle, and from which they were obtained, as shown in Table 1. Physical or
the swelling potential increased for subsequent cycles. Khattab et al. index and chemical properties of all the eight soils were determined
(2007) conducted both W/D and leaching studies on bentonite using standard test procedures. Physical or index properties obtained
(a highly expansive clay mineral) stabilized with a 4% lime addi- for these soils included the Atterberg limits [ASTM D4318 (ASTM
tive. They observed that during the W/D process, the samples that 2017c)] and the gradation curve [ASTM D6913 (ASTM 2017d)—
were initiated with the wetting stage had lower swell potentials than Sieve analysis; ASTM D7928 (ASTM 2017b)—Hydrometer analy-
the samples that were started with the drying stage. sis]; the results are presented in Table 1. The chemical properties
Cui et al. (2011) conducted a study to understand the effect of consisted of the cation exchange capacity, the specific surface area,
the soil aggregate size and W/D on the stiffness of lime-stabilized and the total potassium, as suggested by Chittoori and Puppala
expansive soils. In that study, they observed that soils with finer (2011), to obtain the clay mineralogy information on the soils.
aggregate sizes had higher soil stiffness after the lime treatment. The dominant clay mineral and the approximate clay mineral per-
It was also found that W/D increased the soil stiffness of lime- centages of the minerals kaolinite, illite, and montmorillonite were
treated soils while it reduced the stiffness of untreated soils. It obtained by following the method outlined by Chittoori and Puppala
should be noted that Cui et al. (2011) conducted only five cycles (2011). Table 2 presents these results. Two types of additives/
of W/D, and during the drying process the samples were air dried to stabilizers, lime and cement, were studied in this research. The
their initial gravimetric moisture content and were not oven dried to cement used in this study was Portland cement, as per ASTM
constant weight. C150 (ASTM 2017a) type I, and the lime used was quicklime.
From these studies, it can be understood that W/D, due to
seasonal moisture fluctuations, leads to poor performance of the
stabilization, thereby causing failures to the structures built on Mix Design
those soils. However, very limited information is available on the The mix design was performed as per the highway agency test pro-
mechanisms causing these failures, and most of the research stud- tocols, namely, the TEX-121E (TxDOT 2017b) method for the soils
ies have not examined the effects of the clay minerals in the test
soils on the process of W/D. It is crucial to understand the role
Table 1. Soil Classification and Plasticity Index for Soils under Study
of the clay minerals on the durability of a chemical stabilization,
as these clay minerals participate in the chemical reactions that Atterberg
form pozzolanic compounds to strengthen the soil. The design Gradation (%) Classification limits
Serial
methods need to be examined by incorporating clay mineralogy number Soil name Gravel Sand Silt Clay USCS LL PL PI
and durability into the treatment studies. For this purpose, eight 1 Austin 0 5 38 57 CH 41 17 34
different soils with varying clay mineralogies were selected for this 2 Bryan 0 13 40 47 CL 45 14 31
study, to address their long-term performance when subjected to 3 El Paso 0 37 42 21 CL 30 14 16
W/D cycles. Durability tests revealed the ineffectiveness of the 4 Fort Worth 0 11 37 52 CH 61 32 29
stabilizer, as many soils failed after certain W/D cycles. This study 5 Keller 0 18 45 37 CL 25 14 11
addresses the inefficiency in stabilization and the factors that con- 6 Paris 0 9 45 46 CH 60 24 36
tribute to it. To predict the field design life, a parameter called field 7 Pharr-A 0 2 39 59 CH 67 22 45
survival years is determined on the basis of the montmorillonite- 8 Pharr-B 0 3 55 42 CH 56 19 37
lime ratio, which is obtained from the systematic durability evalu- Note: LL = liquid limit; PI = plasticity index; PL = plastic limit; USCS =
ation of clays. unified soil classification system.

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Table 2. Chemical Properties of the Soils along with Their Clay compaction method instead of the dynamic compaction method.
Mineralogies The dynamic compaction method was avoided because that ap-
Serial proach requires the soil to be compacted in layers, which hinders
number Soil PI CEC SSA TP %I %K %M the process of saturation during the moisture conditioning because
1 Austin 34 101 288 1.74 29 18 53
of the loss of pore connectivity due to the layering. The static
2 Bryan 31 77 205 1.36 23 40 37 method of sample preparation was done according to the procedure
3 El Paso 16 57 161 3.75 63 14 23 outlined in AASHTO (2004). The prepared samples were wrapped
4 Fort Worth 29 117 314 0.98 16 23 60 in plastic wrap to avoid moisture digress or ingress and cured in a
5 Keller 11 71 133 1.1 18 62 20 100% humidity room for seven days at a temperature of 25°C. A
6 Paris 36 133 431 0.79 13 17 70 higher temperature curing would reduce the time required for the
7 Pharr-A 45 104 306 1.55 26 26 48 pozzolanic compound formation (Zhang et al. 2014). Following the
8 Pharr-B 37 76.1 132 1.65 28 54 18 seventh day of curing, the samples were taken out of the moisture
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Note: CEC = cation exchange capacity; PI = plasticity index; SSA = room, the plastic wrap was removed, and durability tests were
specific surface area; TP = total potassium; %I = illite percent in performed.
clay fraction; %K = kaolinite percentage in clay fraction; %M =
montmorillonite percentage in clay fraction.
Durability Testing
The procedure outlined by the ASTM D559 method was closely
stabilized with lime and the TEX-120E (TxDOT 2017a) method followed; it simulates both wet and dry cycle conditions close to
for the soils stabilized with cement. For the soils stabilized with the field conditions in a reasonably short period. According to the
lime, an initial estimate of the amount of lime was made via a pH ASTM D559 method, the soil specimens should be prepared and
test or the Eades and Grim test (Eades and Grim 1966). Once an cured and then submerged in water for 5 h for the wetting cycle, and
initial estimate was made, the optimum moisture contents (OMC) then oven-dried at 71°C (160°F) for 42 h for the drying cycle. A
and maximum dry unit weights (MDUW) were obtained for vary- schematic of the test setup used in this research is presented in
ing soil-lime combinations with an additive content higher than Fig. 1. After removal from the oven, the specimen was subjected
that determined by the pH test. The OMC and MDUW for each to volume-change and moisture-content measurements. The pro-
soil-additive combination were determined by conducting the cedure was repeated for a total of 21 wet-dry cycles or until the
standard Proctor’s compaction test, as per ASTM D698 (ASTM sample failed. The soil specimens were allowed to swell and shrink
2012). unconfined compressive strength (UCS) tests, as per ASTM in both lateral and vertical directions during the wetting and the
D2166 (ASTM 2016), were performed on samples prepared at the drying cycles, as prior studies by Punthutaecha et al. (2006) noted
OMC and MDUW to determine the appropriateness of the stabi- that the volumetric swell/shrink strains measured in the laboratory
lizer and its content on the basis of the strength requirements per with no lateral or vertical restraints were in closer agreement with
TEX-121E, which recommends a UCS value of more than 345 kPa the field-measured values than those obtained by restraining the
(50 psi). A similar procedure was followed for the soils stabilized lateral movement. The vertical movement was measured with the
with cement, except that no pH testing was performed and the pro- help of a dial gauge, whereas the radial movements were measured
cedure outlined in TEX-120E was followed. Table 3 presents the using a pi tape.
type and the amount of stabilizer selected for each of the eight soils A sample is deemed to have failed when (1) the UCS of the sam-
used in this research, along with their dominant clay minerals, ple tested is close to zero; (2) the sample crumbles under its own
MDUW, and OMC. weight, and hence no further testing can be performed; and (3) the
sample becomes so sensitive that it can be crumbled/crushed during
sample-handling activities, including moving the sample from the
Sample Preparation oven to the water bath and/or making volumetric measurements.
The specimens of each soil/additive combination to be tested for the In this study, a mix design or soil/additive combination was
durability studies were prepared at the optimum moisture content considered to be effective if the soil samples prepared using a par-
and maximum dry unit weight condition, obtained during the ticular mix design lasted all 21 cycles and retained at least 50% of
mix design process. The samples were prepared using the static their initial strength at the beginning of wetting/drying. Unconfined
compressive strengths were performed on control and stabilized
soil samples as per ASTM D2166. Because the UCS tests were
destructive tests, a total of five soil samples were prepared so that
Table 3. Type and Amount of Stabilizer Selected for Each Soil along with each sample could be tested at 0, 3, 7, 14, and 21 W/D cycles for
Their Dominant Clay Mineral each soil-additive combination. Duplicate specimens were used
Amount of for obtaining each data point; thus, a total of 10 samples were cast
additive, for each of the soil/additive combinations. Each data point in the
Serial Dominating Type of (% by MDUW OMC plots is an average of two test results. The UCS tests were per-
number Soil clay mineral additive weight) (kN=m3 ) (%) formed after the corresponding wetting cycle, and because the sam-
1 Austin Montmorillonite Lime 6 17.1 20.4 ples were saturated after this cycle, the control sample at 0 cycles
2 Bryan Kaolinite Lime 8 15.3 22.7 was also tested after saturating the sample.
3 El Paso Illite Lime 8 18.2 15.1
4 Fort Montmorillonite Lime 6 14.6 23.1 Additional Durability Studies
Worth The soils that did not perform well after stabilization using the cur-
5 Keller Kaolinite Lime 6 19.1 13.4 rent design procedures were further analyzed with different additive
6 Paris Montmorillonite Lime 8 13.7 24.3 types in varying dosages to determine which stabilizer dosage
7 Pharr-A Montmorillonite Lime 4 13.4 31.0 combination would be effective for these soils. On the basis of
8 Pharr-B Kaolinite Lime 3 15.1 24.7
these observations, an alternative procedure was developed for

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Dial Gauge

Water Bath Drying Oven


Porous Stone

Soil Sample

Porous Stone
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WETTING DRYING

Pi-tape

Fig. 1. Schematic and photographs of the wet/dry setup

determining the stabilizer type and dosage according to the miner- Summary of W/D Test Results
alogy and other index properties of a particular soil.
For example, the Austin soil, which has a PI of 34, was not sta- Volumetric strain changes were measured at the beginning and
bilized effectively when 6% lime was used as a stabilizer, due to the the end of each wetting and drying cycle. Percentage changes in
high montmorillonite content (40%) in its clay fraction. This soil volume after the corresponding cycle of W/D were calculated for
was retested with an increased dosage of lime (8%) and two dos- each sample on the basis of its initial dimensions before the W/D
ages of cement (3 and 6%). After different cycles of durability, the cycles started. Strength tests were performed after 3, 7, 14, and 21
soil specimens were tested for the retained strength. Similar tests cycles of W/D. The percentage of retained strength after a corre-
were conducted on the Pharr-A, Pharr-B, and Fort Worth soil spec- sponding W/D cycle was calculated by dividing the current UCS
imens; Table 4 summarizes the various mix designs performed on strength by the 0 cycle UCS strength before the first W/D cycle and
these soils. Following the procedures described previously, these after seven days of curing.
soil specimens were subjected to alternate wetting and drying For conciseness, the volumetric strain results are presented
studies. in three groups, based on their mineral dominance in their clay

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Table 4. Selected Soils Treated with Additional Stabilizer Dosages fraction. Group I consisted of four soils: Austin, Fort Worth, Paris,
Soil Additive OMC (%) MDUW (kN=m3 ) and Pharr-A (high PI), in which the clay fraction was dominated by
the mineral montmorillonite. Group II consisted of three soils from
Pharr-B Control 24.7 14.8
Bryan, Keller, and Pharr-B (medium PI), in which the clay fraction
6% lime 28.0 14.0
8% lime 29.0 13.7
was dominated by the mineral kaolinite. Group III consisted of only
6% cement 28.5 14.0 one soil from El Paso, which was dominant in the mineral illite. The
volumetric strain and the UCS strength variation with the W/D
Austin Control 20.5 16.7 cycles are presented in the following sections.
6% lime 21.0 14.9
3% cement 21.5 15.6
6% cement 21.0 15.1 Volumetric Strain Data
Pharr-A Control 31.0 13.1 The volumetric strain results for Group I, Group II, and Group III soils
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6% lime 31.5 12.2 are presented in Figs. 2–4, respectively. These three figures show
8% lime 32.5 11.9 that the treated soils had lower volumetric strains than the untreated
3% cement 32.0 12.1
soils, which was expected. Soils that survived all 21 cycles with min-
6% cement 32.5 11.9
imal volumetric changes (<10%) were considered to have performed
Fort Worth Control 24.0 14.4 well under the wetting/drying durability conditions.
6% lime 25.5 14.1 Figs. 2(a and b) show that the Austin and Fort Worth soils
3% cement 24.5 14.1 survived for a total of 12 and 11 cycles of durability, respectively,
6% cement 25.0 14.0 when treated with 6% lime. Similarly, the Paris soil samples treated
Note: MDUW = maximum dry unit weight; OMC = optimum moisture with 8% lime survived for only seven durability cycles, and this
content. can be observed in Fig. 2(c). Fig. 2(d) shows that the Pharr-A soil

Fig. 2. Volumetric strain change with W/D cycles for Group I soils: (a) Austin soil; (b) Fort Worth soil; (c) Paris soil; (d) Pharr-A soil

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Fig. 3. Volumetric strain change with W/D cycles for Group II soils: (a) Bryan soil; (b) Keller soil; (c) Pharr-B soil

samples survived for four W/D cycles when they were treated with
4% lime. It is apparent that none of the Group I soils mentioned
survived the entire W/D testing. Premature failure in one soil
(Pharr-A) was attributed to the low initial dosage used. However,
all Group I soils experienced early failures as these soils are dom-
inant in the montmorillonite mineral.
The Keller and Bryan soils, which fell under Group II, survived
all 21 W/D cycles when they were treated with 6 and 8% lime,
respectively. However, the Pharr-B soil samples, which belonged
to the same group, survived only eight W/D cycles when they were
treated with 3% lime; this is clearly shown in Fig. 3(c). Finally, the
El Paso soil, which belonged to Group III, survived all 21 W/D
cycles when it was treated with 8% lime. Fig. 2 also shows that the
treated soils did not survive all 21 cycles, whereas Figs. 3 and 4
shows that all the soils survived the 21 W/D cycles, except for the
Pharr-B soil shown in Fig. 3(c).

Unconfined Compression Strength Results


The UCS data obtained for Group I, Group II, and Group III soils
Fig. 4. Volumetric strain change with W/D cycles for Group III soil
are presented in Figs. 5–7, respectively. Figs. 5(a and b) show that
(El Paso)
the Austin and Fort Worth soil specimens treated with a 6% lime

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Fig. 5. Unconfined compression strength variation with W/D cycles for Group I soils: (a) Austin soil; (b) Fort Worth soil; (c) Paris soil;
(d) Pharr-A soil

dosage did not retain any strength after 12 and 11 W/D cycles, re- Effect of Soil Type
spectively. The Paris soil treated with 8% lime lost all of its strength
Table 5 shows that the Austin, Fort Worth, Paris, and Pharr clays,
after eight W/D cycles, as shown in see Fig. 5(c), whereas the
which have high amounts of the montmorillonite mineral in their
Pharr-A soil specimens treated with 4% lime lost all their strength
clay fractions, did not survive all 21 W/D cycles. The clays from El
after four durability cycles, as shown in Fig. 5(d). Figs. 6(a and b)
Paso, Bryan, and Keller, which have other clay minerals (illite or
show that both the Bryan and Keller soil specimens treated with 8
kaolinite) as the dominant mineral in their clay fraction, survived
and 6% lime, respectively, lasted all 21 W/D cycles and retained over
all 21 cycles. This indicates that soils containing montmorillonite
85% of their initial strength. The Pharr-B soil specimen treated with
as a dominant mineral are more susceptible to premature strength
3% lime failed to retain any strength after eight durability cycles, as
failures after chemical stabilization when they are exposed to
shown in Fig. 6(c). Finally, Fig. 7 shows that the El Paso soil speci-
volume changes caused by moisture movements. It should be noted
men treated with 8% lime retained 85% of its initial strength after
that although the Pharr-B soil is dominant in the mineral kaolinite,
21 W/D cycles. Table 5 summarizes the retained strength measure-
ments, along with the maximum volumetric strain change at the end it lasted for only eight cycles, primarily because of the low addi-
of the number of W/D cycles survived, for all the eight soils. tive dosage (3% lime). To further represent the effect of the min-
eral montmorillonite on the durability of stabilization, the retained
strengths and volumetric strain changes after seven W/D cycles for
Analysis and Discussion all the soils treated with 8% lime were plotted, as shown in Fig. 8.
This figure shows that as the percentage of montmorillonite in-
As explained previously, on the basis of the results, the four soils creased in the clay fraction, the retained strength after seven W/D
that did not perform well under the W/D durability were further cycles decreased whereas the volumetric strain change increased.
tested; those results are summarized in Table 6. All the above re- This is an important finding, as it shows the influence of the clay
sults were analyzed for the effects of clay mineralogy, additive type, mineralogy on the durability of the chemical stabilizer in providing
and additive dosage in the following sections. sustained strength over a long period of time. A similar figure was

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Fig. 6. Unconfined compression strength variation with W/D cycles for Group II soils: (a) Bryan soil; (b) Keller soil; (c) Pharr-B soil

Table 5. Volumetric Strain and Retained Strength at the End of Wetting/


Drying Cycles Survived for all Eight Soils Treated with Lime
Amount of Number
additive, of cycles Retained
Dominating clay (% by sample Volumetric strength
Soil mineral weight) survived strain (%) (%)
Austin Montmorillonite 6 12 15 0
Fort Worth Montmorillonite 6 10 15 0
Paris Montmorillonite 8 7 15 0
Pharr-A Montmorillonite 4 4 30 0
Bryan Kaolinite 8 21 6 93
Keller Kaolinite 6 21 5 80
Pharr-B Kaolinite 3 8 18 0
El Paso Illite 8 21 12 80

plotted against the plasticity index of these soils; it is presented


in Fig. 9. This figure clearly shows that the current approach of the
Fig. 7. Unconfined compression strength variation with W/D cycles
PI-based chemical stabilizer design does not provide any insights
for Group III soil (El Paso)
into the chemical stabilizer durability.

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Table 6. Summary of Test Results for Soils Treated with Additional
Stabilizer Dosages
Number
of cycles Retained
Dominating the sample Volumetric strength
Soil mineral Stabilizer survived strain (%) (%)
Pharr-B Kaolinite 3% lime 8 18 0
6% lime 14 12 0
8% lime 21a 6 47
3% cement 14 10 0
6% cement 21a 4 59
Austin Montmorillonite 6% lime 12 15 0
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8% lime 21a 6 67
3% cement 14 10 0
6% cement 21a 4 80
Pharr-A Montmorillonite 4% lime 4 30 0
6% lime 9 9 0
8% lime 14 7 0
3% cement 9 9 0
6% cement 21a 5 83
Fort Montmorillonite 6% lime 10 15 0
Worth 8% lime 14 8 57
3% cement 14 11 42
6% cement 21a 5 57
a
Sample still intact. Fig. 9. Effect of plasticity index on durability of lime stabilization

Fig. 10. Effect of additive type on the W/D performance of chemical


stabilization

is considered the upper limit for the purpose of stabilization, and


higher amounts may not be economical.

Effect of Additive Type


The four soils that were selected for further evaluation were treated
Fig. 8. Effect of montmorillonite mineral on durability of lime with both lime and cement, as the lime-treated soils after using as
stabilization much as 8% by dry weight of the soil did not perform well in the
long term. Hence, those samples were treated with cement to assess
the percentage of cement that would effectively treat those soils. On
the basis of those tests’ performance, a comparison the additive
It was observed in this study that the samples that retained at types was performed as follows.
least 80% of their initial strength after seven W/D cycles lasted Fig. 10 presents a comparison of the number of W/D cycles that
for all 21 W/D cycles, retaining at least 50% of the initial strength. the samples survived for both cement and lime additives. In this
On the basis of this observation, it can be deduced from Fig. 8 that figure, the amount of lime and cement used was 6% by dry weight
soils containing more than 40% of the montmorillonite mineral in of the soil. The figure shows that the cement stabilization outper-
their clay fraction may not be efficiently stabilized with lime, as formed the lime stabilization for all four soils studied. Although the
those soils could not be stabilized effectively using 8% lime, which state of practice is to use lime for highly plastic soils and cement for

© ASCE 04017097-9 J. Geotech. Geoenviron. Eng.

J. Geotech. Geoenviron. Eng., 2018, 144(1): 04017097


granular soils, in this research, it was observed that for the long-term stabilizer is ineffective in some soils even though other soils with
durability of the stabilization, cement performed better than lime. the same index properties respond well to that stabilizer. In this
The authors attributed this to the enhanced strength of the treated study, a similar response was observed with the Bryan and Fort
soil mixture, which resisted the stresses generated during the wetting Worth soils, which had similar PIs (31 and 29, respectively), when
and drying cycles. This was the main reason that the cement-treated they were treated with the same amount of lime additive. As the PI
soils with 6% cement additive showed consistent and lower volu- values of these soils were similar, the existing stabilization guide-
metric strains during the present experimental program. lines recommended the same type and amount of additive. However,
the Bryan soil that was dominant in kaolinite survived all 21 cycles
of W/D, whereas the Fort Worth soil, with montmorillonite as a
Effect of Additive Dosage
dominant clay fraction, survived only ten cycles of W/D. Hence,
Table 7 summarizes the effect of the dosage amount on the long- the selection of the type and amount of stabilizer on the basis of
term performance of a stabilized subgrade under the seasonal mois- the PI of the clay alone, is not sufficient for an effective stabilizer
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ture variations and volumetric movements due to these moisture design. It is highly important to include the clay mineralogy infor-
fluctuations. Two soils were selected for this analysis: Pharr-A, mation in the stabilizer design process to achieve a durable and sus-
dominant in the mineral montmorillonite; and Pharr-B, dominant tainable subgrade stabilization.
in the mineral kaolinite. The Pharr-A was treated with 4, 6, and
8% of lime, whereas the Pharr-B was treated with 3, 6, and 8%
of lime. It is shown by the table that as the lime dosage increased, Field Service Life Implications
the stabilization effectiveness of the Pharr-B soil improved consid- On the basis of the results obtained in this study, an effort was
erably, making the samples last longer with the increase in dosage. made to understand the implications of these laboratory studies
In the case of the Pharr-A soil, the stabilization effect lasted longer in field service life assessments. For that purpose, the researchers
when the dosage was increased from 4 to 8%; however, even at 8% attempted to predict the service life of stabilization, defined as field
lime, the samples lasted only 14 W/D cycles. Hence, this exercise service years (FSY), using the ratio between the percentage of mont-
shows that for soils dominant in the kaolinite mineral (in this case, morillonite in the clay fraction of the soil and the amount of lime
the Pharr-B soil), the lower dosage levels can lead to premature used to stabilize the soil, defined as the montmorillonite-lime ratio
failures, while a higher dosage can assure long-term performance. (MLR). This analysis is approximate and is dependent on the clay
The same is not true for the montmorillonite-dominant soils (in mineralogy and the additive dosages. The test database used is not
this case, Pharr-A), where a higher dosage did not result in better comprehensive, and more W/D studies with detailed mineralogy in-
performance. formation will enhance the correlation developed in this research.
One important observation regarding the montmorillonite-rich In the laboratory, the samples were dried for 42 h at 60°C, and
soils is that if these soils are restrained in volume changes due to the samples were submerged under water for 5 h, during which the
higher confinements (with the assumption that treatments are car- samples reached a saturation of 85–95%. No studies have been con-
ried out at medium-range depths of 1–2 m), the durability perfor- ducted so far to assess how many of these wetting and drying sce-
mance will be improved (Pedarla 2009). If the treatments are narios occur in a year; this study used the assumption that in a given
carried out at shallow depths within the top 0.6 m of the subgrade, year there were two such wetting/drying scenarios, although there
it is recommended to replace the montmorillonite-rich soils with a might be several rainfall events followed by dry periods in a given
quality fill material. Other methods of amending the natural soils year. The basis for this conservative assumption is that the labora-
with sand or other inert materials may also provide better W/D per- tory conditions in the study were extreme, whereas in the field,
formance, but those studies are not considered in this research and the soil rarely becomes completely dry unless there are prolonged
therefore no recommendations on those amendments can be made. drought conditions. This kind of approximation is area-specific and
varies among regions. However, the analysis attempted here pro-
Limitations of Existing PI-Based Design Methodologies vides a simple method that correlates the laboratory W/D cycles
with the actual field performance data. Hence, in this research,
So far in this research study, the soils stabilized using the current
on the basis of these approximations, the study’s 21 W/D cycles
stabilization design procedures have not survived the seasonal mois-
correspond to approximately 10 years of the field conditions.
ture fluctuations studied by conducting the W/D durability tests.
Fig. 11 presents a plot of the ratio of the percentage of mont-
The current stabilizer selection criterion, followed by various state
morillonite and the percentage of lime used for stabilization, de-
and federal agencies including TxDOT, FHWA, and the United
fined as the montmorillonite-lime ratio (MLR), versus the field
States Army Corps of Engineers, are based on the plasticity index
survival years (FSY). The FSY can be equated to the number of
(PI) and the gradation characteristics of the soil. These organizations
W/D cycles survived, divided by 2 (assuming two cycles per year).
have reported problems with subgrade failures that occur when a
With the assumption that the montmorillonite percentages in the
soil range from 10 to 80 in the clay fraction and the lime percent-
Table 7. Comparison of Results between the Additive Dosages ages range from 1 to 10, the MLR values can range from 1 to 80.
An MLR value of 80 indicates a worst-case scenario in which the
Amount Percentage
of Number retained percentage of montmorillonite in the soil is 80% and is treated
Soil Mineral Additive additive of cycles strength after with only 1% lime, whereas an MLR value of 1 indicates a best-
type dominance type (%) survived 7 W/D cycles case scenario in which the percentage of montmorillonite in the soil
is only 10% and the soil was treated with 10% of lime. Other com-
Pharr-A Montmorillonite Lime 4 4 0
6 9 29 binations are possible, but for the discussion, not all scenarios are
8 14 24 considered. The typical MLR values for Texas soils range from 2 to
20, based on the soils tested in this research and on standard prac-
Pharr-B Kaolinite Lime 3 8 32 tices. From Fig. 11, it can be observed that for the lower MLR val-
6 14 58 ues, the FSY was higher (at least 10 years) whereas for the higher
8 21 63
MLR values, the FSY values decreased. On the basis of the soils

© ASCE 04017097-10 J. Geotech. Geoenviron. Eng.

J. Geotech. Geoenviron. Eng., 2018, 144(1): 04017097


12
Hence, further research in this direction is warranted, to design a
Note: Circled data points do not
follow the established trend and versatile setup that can simultaneously perform the W/D cycles and
are considered outliers the leaching cycles on the same sample, to provide a superior sim-
ulation of the field conditions.
9
FSY = -0.8 * MLR + 12.2
FSY - Field Service Years

R-squared = 0.62 Summary and Conclusions


Premature failures were reported in the field for various
transportation-related infrastructures constructed on chemically
6
stabilized expansive soils in different regions. Even though the ex-
pansive soils were stabilized following the existing stabilization de-
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sign guidelines, some soils performed as expected but other soils


did not. The reasons for this erratic behavior in treated expansive
soils were unknown. Hence, a research study was undertaken to
3
understand the reasons for this behavior. For that purpose, a total
of eight soils, with varying plasticity and mineralogical character-
istics, were selected from various regions of Texas and subjected
Optimal MLR value for a minimum to wetting/drying durability studies. ASTM D559 was closely fol-
service life of 10 years
lowed for conducting the wetting/drying durability studies on each
0
of these soils. Both the volumetric strain and the unconfined com-
0 5 10 15
MLR - Montmorillonite Lime Ratio
pressive strength were measured at various numbers of W/D cycles.
The mix design was initially performed on all eight soils following
Fig. 11. MLR based FSY predictions for the tested soils the existing stabilization design guidelines, and the treated and con-
trol soil samples were subjected to W/D cycles, as previously ex-
plained. Four of the soils, which did not perform well, were further
tested in this research, it can be deduced that an MLR value higher treated with different dosages of lime and cement to arrive at a mix
than 5 can lead to poor stabilization performance. Eq. (1) presents a design that satisfied the durability criterion. Based on these test re-
correlation between FSY and MLR based on the soils tested here. sults, the following important conclusions can be made:
and this equation has an R-squared value of 0.62. Although this is • Soils with similar plasticity characteristics do not have similar
not a generalized equation, it is important to note that this gives a behaviors following the same chemical treatment. This is clearly
rough estimate of field performance of similar soils, given the per- demonstrated in the case of the Bryan and Fort Worth soils.
centage of lime used for treatment. It should be noted here that the Therefore, it is important to know the mineralogical and plas-
plot contains two data points that are considered outliers, circled in ticity characteristics of the soils.
Fig. 11. These two data points contradict the previously established • The montmorillonite mineral is an important influence on the
threshold value of the MLR as less than or equal to 5 to be an in- engineering behavior of stabilized expansive soils. Soils that
dicator of optimal long-term performance. The data point to the contain low amounts of the montmorillonite mineral survived all
right of the dotted line in Fig. 11 had a higher MLR and yet sur- 21 W/D cycles, whereas those with high amounts failed quickly
vived all 21 cycles of W/D, whereas the data point on the left after the W/D cycles started.
(circled in Fig. 11) of the dotted line had a lower MLR but survived • Soils containing more than 40% of the montmorillonite mineral
only 14 cycles of wetting-drying. Further research is required to in their clay fraction may not be efficiently stabilized with lime,
understand this phenomenon as 8% lime is considered the upper limit for the purpose of sta-
bilization and anything beyond that may not be economical.
FSY ¼ −0.8 × MLR þ 12.2 ð1Þ • The effect of the additive type on the long-term performance of
stabilized expansive soils was studied in this research. It was
where FSY = field service years; and MLR = montmorillonite-lime observed that the cement treatment survived a greater number
ratio. of cycles than the lime treatment at similar dosage levels for
all four soils that were retested to arrive at the durable perfor-
mance. This finding is new and does not fall in line with current
Future Research practice.
The current research was carried out with the assumption that • A new empirical model was developed to predict the field ser-
the clay fraction contained montmorillonite, illite, and kaolinite. vice life of a stabilization based on the soil type and the amount
However, the presence of other clay minerals, such as chlorites and of additive used for stabilization. On the basis of this model, an
commonly occurring nonclay minerals such as quartz, feldspar, and MLR value of 5 or lower is recommended for better field per-
mica, might have profound effects on the stabilization behavior. formance for similar types of soils.
This was not studied in this research.
Leaching of the stabilizer during heavy rainfall events is another
major aspect of the durability assessments. This aspect was studied Acknowledgments
in this research on a separate set of samples, and the results were
presented in Chittoori et al. (2013). However, the authors believe The authors would like to express their sincere appreciation to
that the wetting/drying and leaching are not mutually exclusive pro- the Texas Department of Transportation (TxDOT) for their support
cedures and occur simultaneously in the field. Therefore, it would of this research. The authors would like to acknowledge Mark
provide more insight to conduct those two studies on the same sam- McDaniel of the TxDOT and Dr. Soheil Nazarian of the University
ple, rather than on separate samples, and to observe the changes. of Texas at El Paso for their assistance with this research.

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J. Geotech. Geoenviron. Eng., 2018, 144(1): 04017097


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