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by V. Cromwell, D.J. Kortum, and D.J. Bradley, Montana C. of Miners/ Science& Technology
SPE Members
This paper was presented at the 59th Annual Technical Conference and Exhibition held in Houston, Texas, September 16-19, 1964. The material is aub
ject to correction by the author. Permission to copy is restricted to an abstract of not more than 300 words. Write SPE, 6200 North Central Expressway,
Drawer 64706, Dallas, Texas 75206 USA Telex 730969 SPEDAL.
The average properties of the core specimens fol graph. ..—.______ I-11=u==
I-Klwevtx, Au- ...- “.
-.r .3 .=.L..-...-.I
--1 .++**al .7 ~=~~Q-
the experiments are presented in Table 2. Both the opaque iodine solution facilitated these contrast
chalk and the sandstone were water-wet. changes without damaging the cores or “altering
+1...
mwAmaw+<~. of +_hefluid=
~,= ~L”p=...=”
The apparatus used to hold the core was con-
structed of CPVC pipe with the core held in a wax The medical software available with this
sleeve in the pipe. Care was taken to file all system precluded magnification greater than 4x,
corners of fittings, pipe and core to reduce edge multiple image summation or subtraction, or quanti-
artifacts. fiable density measurements of the core.
A water and organically beund iodine solution The system was suitable to produce qualitative
was used for the purpose of displacement in the images showing rock heterogeneities, fluid satura-
experiments. This solution has about the same tions, and displacement. As such, the concept of
viscosity as water and was used to increase contrast CT analysis of cores was proved to a limited degree
in the CT image. v~ry inexpensively.
The image in Figure 1 and 2 demonstrate the use To allow for complete core analysis, a CT sys-
of the CT scan to display Berea rock matrix and ..-
cat shwdld hav= = I=rge zrr=y storage CaPaCitY for
fluid saturation variations, with the high-density the digital signal coming from the detector. The
(high effective atomic number) regions plainly use of a suite of X-ray sources of higher energy and
visible as the lighter sections of the photograph. signal strength than a medical CT would allow for
In Figure 1, variations in fluid saturations can be the imaging of larger diameter, higher density cores
seen, while in Figure 2, heterogeneities in the sand- with good interior resolution.
. . ~~~ ~~~krast in the
StOi@ ZOR d?.a~l.~ ‘V’LSIH=.
figures are a sum of X-ray counts per CRT pixel and Currently available CT technology limits the
are calibrated by a graduated bar at the side of the thickness of the slice to approximately 0.5 nun. To
image. A cursor, which can be seen in the photograph observe pores of smaller diameter than the slice,
can be placed on the image and an X-ray attenuation the core may be advanced by some fraction of the
value will be given by the CT in Hounsfield units. slice thickness and the first image subtracted from
the second. Also, two images from the same location
An attempt was made to observe differences in made as the fluid front is passing may be subtracted
water, oil, and air saturations in separate cores. to show only the differences in fluid density in the
The visual contrasts resulting from these satura- pores and not the rock matrix. It may be possible
tions were difficult to differentiate. However, to alter software from existing Scanning Electron
the computer software easily identified the various Microscope (SEM)3 libraries for subtraction, summa-
fluid “densities.” tion and quantitative X-ray microanalysis for use
with CT equipment.
A series of displacement experiments were per-
formed using a dilute iodine solution to displace Much of this work has begun, however the bulk
mineral oil. The iodine solution was then displaced of the software necessary for quality core analysis
by air. The images for this displacement were taken is still unavailable. As this software is developed,
as radial cross-sections and are seen in Figure 3 some conventional core analysis techniques may be
a, b, and c. Firstr in Figure 3a the cross-section replaced by CT analysis. The areas the CT may prove
with mineral oil is seen. In 3b, the high density to be of exceptional value include secondary and
iodine solution is moving through the slice. tertiary recovery studies of displacement mechanisms,
Finally, in 3c, the iodine solution is displaced by sweep efficiencies and other processes occurring
air and the subsequent “density” is much lower. within the core. We hope to carry out some of this
work in the future.
A low permeability Danian chalk core was used
to investigate a different rock lithology and to NOMENCLATURE
slow the movement of the fluid front. A low perm-
eability rock was necessary in these experiments Y = dimensionless X-ray attenuation factor
due to a lack of control over injection pressures.
Axial cross-sections were made as the iodine solu- W = water
tion was pushed through the core. Figures 4a, b,
and c show the passage of a well-defined front
H.U. = Hounsfield Units
through the chalk.
AC~OWLEDGEMENTS
DISCUSSION OF RESULTS
We would like to give special thanks to the
By design, a medical CT necessitates the use
Sisters of Charity of Leavenworth and St. James
of a low beam strength to avoid injury to the
Community Hospital of Butte, Montana for the gener-
patient. To image the interior of the rock, small
ous use of their CT equipment and Joyce Hettick, R.T.
core diameters were needed to enhance resolution.
for her help with the scanning. We would also like
to thank Phillips Petroleum company for supplying
The phase ‘*densities”had to vary considerably
.~=- tya<t . on the photo-
the chalk cores used in these experiments.
t= Z=2~iS@Z S .... ..E VISIJ21cop..__.
SPE 13098 Vern Cromwell, David J. Kortum, and Daniel J. Bradley 3
REFERENCES
TABLE 1
M~D 1A ATTENUATION
—
Water o
----
Air -lUUU
Fiberglass 870
Bone 860
I)anianChalk* 1280
Fig. 4b-Chalk with front ptogreaeing. Fig.4c-The fronthas moved approximately half WY thtwgh the
mre — air 1281 H.U. and iodne 1766 H.U.
SP E13098