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Article history: The paper presents an approach toward an enhancement of the measuring range of high-speed sensors
Received 22 January 2014 for the measurement of liquid film thickness distributions based on electrical conductance. This type of
Received in revised form sensors consists of electrodes mounted flush to the wall. The sampling of the current generated between
2 September 2014
a pair of neighboring electrode is used as a measure of the film thickness. Such sensors have a limited
Accepted 7 September 2014
Available online 17 September 2014
measuring range, which is proportional to the lateral distance between the electrodes. The range is
therefore coupled to the spatial resolution. The proposed new design allows an extension of the film
Keywords: thickness range by combining electrode matrices of different resolution in one and the same sensor. In
Gas–liquid flow this way, a high spatial resolution is reached with a small thickness range, whereas a film thickness that
Film Flow
exceeds the range of the high resolution measurement can still be acquired even though on the costs of a
Annular flow
lower spatial resolution. A simultaneous signal acquisition with a sampling frequency of 3.2 kHz
Liquid film thickness measurement
combines three measuring ranges for the characterization of a two-dimensional film thickness
distribution: (1) thickness range 0–600 mm, lateral resolution 2 2 mm2, (2) thickness range 400–
1300 mm, lateral resolution 4 4 mm2, and (3) thickness range 1000–3500 mm, lateral resolution
12 12 mm2. The functionality of this concept sensor is demonstrated by tests in a horizontal wavy
stratified air–water flow at ambient conditions. Using flexible printed circuit board technology to
manufacture the sensor makes it possible to place the sensor at the inner surface of a circular pipe.
& 2014 Elsevier Ltd. All rights reserved.
1. Introduction annular pipe flow. They are mostly based on the relationship
between conductance and liquid film thickness between a pair of
Liquid films that are wetting surfaces are prominent in many electrodes. To apply this technique, the liquid must be electrically
technical applications, for instance on fuel rods of boiling water conductive. As a second option, capacitance can be used as
reactors, were the presence of the film is a necessary condition for primary measuring quantity in case of nonconductive liquids [14].
a sufficient heat removal. They are found on cooled surfaces The electrical liquid film sensor used for the current work is
furthermore due to condensation or in numerous other fields of based on the principles of the signal acquisition of wire-mesh
chemical and mechanical process engineering. The measurement sensors [15]. The first application of this signal acquisition method
of the liquid film thickness is therefore of interest in experiments for the measurement of a liquid film thickness was presented by
aiming at an optimization of the related industrial processes, or, in Belt et al. [16,17]. Electrodes are mounted flush to the wall of a
certain cases, for their direct monitoring. flow channel. The sensor represents therefore essentially a non-
There are different methods which can be used for liquid film intrusive technique. The receiver electrodes are circular conduct-
thickness measurements. The principles are based on extraction of ing surfaces. The circumferential pitch between two receiver
the film by suction [1–3], on photons [4–6], on ultrasound [7] or electrodes is 4.9 mm. The transmitter electrodes are ring shaped
on electrical impedance [8–13]. Most of these methods are used and placed in an axial distance from the receivers. A total of 10
for the research on two-phase annular flow. Electrical methods rings of 32 measuring positions follow each other in axial direc-
have been widely applied for many years in the area of air–water tion. A second ring-shaped electrode separates the transmitter
ring from the subsequent ring of receiver electrodes. The separa-
tion of measuring positions in axial direction is 19.5 mm. The
n
Corresponding author.
spatial resolution of a sensor delivering a spatial distribution of the
E-mail address: hprasser@ethz.ch (H.-M. Prasser). measured quantity is given by the dimensions of the smallest
1
info.itfe.technik@fhnw.ch. structure which is resolved. Since the conductance is averaged
http://dx.doi.org/10.1016/j.flowmeasinst.2014.09.002
0955-5986/& 2014 Elsevier Ltd. All rights reserved.
R. Tiwari et al. / Flow Measurement and Instrumentation 40 (2014) 124–132 125
over the area of 4.9 19.5 mm2 given by the electrode spacing, the good compromise of resolution, penetration depth, signal quality
sensor averaged over smaller structures of the film thickness and easy manufacturing is described in [23]. This sensor geometry
distribution, which defines the spatial resolution. The measuring was taken as the basis for the multi-range sensor described below.
frequency was set to 5 kHz.
The electrical current flowing between electrodes mounted
flush to the wall reaches saturation at a certain liquid film 2. Sensor design
thickness. This is a fundamental property of the electrical potential
field. Since the field strength decreases with growing distance The sensor consists of a matrix of electrical conducting pads
from the electrodes, the sensibility to a change of the film arranged flush on an insulating surface which is representing the
thickness decreases when the film becomes thicker. The current wall of the flow duct in the same time. The conducting areas serve
converges toward a value characteristic for an infinite coverage as electrodes for establishing a contact with the fluid. There are
with the conducting liquid. The range at which the sensibility is three different types of electrodes, namely transmitter, receiver
still sufficient for a film thickness measurement is called “penetra- and ground electrodes. The basic idea for the fast acquisition of
tion depth”. It depends on the geometry of the electrodes and time sequences of two dimensional film thickness distributions is
scales with their size. This limits the measuring range. A similar the measurement of the electrical current flowing from a trans-
behavior was found by Hu et al. [18] for capacitance measure- mitter pad to a neighboring receiver pad due to potential differ-
ments with electrodes flush to the surface. In case of the sensor ence between both electrodes. The current depends on the
presented by Belt et al. [16,17], the penetration depth at which 95% thickness of the electrically conducting liquid film covering both
of the saturation is reached is 3.3 mm. electrodes. The two-dimensional array is arranged in such a way
Da Silva et al. [19] proposed a sensor with higher spatial that the transmitting electrodes are connected in one direction
resolution. Individual sensitive positions were designed as an (transmitter lines), while the receiver electrodes are coupled
interdigital structure of a pair of electrodes arranged in a two- perpendicular (receiver lines) to this direction (Fig. 1). The voltage
dimensional measuring matrix. The current generated between a pulses are supplied to the transmitter lines in successive order.
pair of interdigital electrode is sampled and used as a measure of During the excitation of each transmitter line, all currents arriving
the film thickness. The lateral period of measuring positions is at the receiver lines are sampled in parallel. After the excitation
7.8 mm in the first and 9.7 mm in the second direction; the of the last transmitter electrode, a complete matrix of primary
measuring frequency is 2500 Hz for a matrix with the dimensions measuring values is recorded. These values represent the con-
of 64 64. Transmitter electrodes have three fingers ranging into ductance distribution in the liquid film on the sensor surface,
gaps between the fingers of the opposite receiver electrode. The which is the measure of the film thickness.
interlaced structure has a spatial wavelength of 2.6 mm. The The signal acquisition method used for this sensor is equivalent
described structure leads to a penetration depth of 0.69 mm to the one of the wire-mesh sensors, which is described in detail in
given by the authors for 97% of saturation. This is a quite small [15]. A special feature of the wire-mesh electronic circuitry is the
measuring range compared to the lateral resolution given by the low impedance of transmitter driver and receiver pre-amplifier
spatial period of electrode pairs of about 8–9 mm. The small cascades, which guarantees that the potential at all non-activated
relative penetration depth which corresponds to only about 10% transmitter electrodes and all receiver electrodes remains very
of the lateral resolution is a clear disadvantage. The benefit of the close to ground potential. This is an important feature to suppress
interdigital geometry lays in a higher signal strength and with it in cross-talk to far located receiver electrodes, as discussed in [15].
a better sensibility for very thin films of a liquid with low The low impedance guarantees that all receives and the not
conductivity. This was not important neither in the application activated transmitter electrodes stay on ground potential during
to gravity driven mixing processes in a pool [19] nor in the the activation of one set of transmitter electrodes. Consequently,
experiments in the hydraulic coupling [20]. Both cases would parasitic currents traveling from not activated transmitters to
have benefitted from a higher penetration depth providing more receivers as well as from a receiver electrode to a neighboring
information from beyond the boundary layer. one are not induced and cannot affect the measurement.
The first step to increase relative penetration depth is the The sensor introduced in this work is a modification of the
abandonment of the interdigital structures, which is accompanied sensor presented in [23]. The diameter of receiver and transmitter
by a reduction of the signal strength. This can be compensated by a electrodes was set to 0.5 mm, whereas the ground electrodes had
higher amplification of the input cascades of the signal acquisition a diameter of 0.9 mm (Fig. 2). The distance between the centers of
system. A second step consists of an optimization of the electrode
geometry. Li et al. [21] have shown that the relative penetration
depth of a single permittivity sensor with electrodes flush to the
wall can be increased by grounded shield electrodes put between
the measuring electrodes. Since sensors for permittivity and for
conductivity behave essentially similar, this concept can be
applied to conductivity sensors as well. Damsohn and Prasser
[22] succeeded in applying the approach of using shield electrodes
to increase the penetration depth relative to the lateral electrode
pitch in two-dimensional sensor arrays. Also there, the lateral
resolution can be increased by arranging grounded surfaces
between transmitter and receiver electrodes. In [22] a number of
periodic electrode structures were identified that are compatible
with the concept of the two-dimensional measuring array of their
liquid film sensor. This is novel compared to the solution of Da
Silva at al. [19], which used grounded surfaces only to reduce
cross-talk by shielding the second neighbors of receiver lines from
the potential of the activated transmitters. A sensor based on
electrodes and ground pitches with a circular shape represents a Fig. 1. Connection of electrode pads forming the sensor matrix [23].
126 R. Tiwari et al. / Flow Measurement and Instrumentation 40 (2014) 124–132
beyond the capacity which was available for the presented work
and must stay reserved for the future.
The size of an individual measuring volume is determined by
the pitch of the electrodes. In the given sensor geometry, it is a
square surface of 2 2 mm2. The film thickness range that can be
achieved with the described geometry is about 800 μm. The sensor
presented here has electrode islands with the same basic geome-
try. The small electrodes are used as transmitters and receivers for
a high-resolution but low range film thickness measurement. This
is called “near field measurements”.
All large electrodes are connected to ground potential. In the
same time, all non-activated transmitter electrodes as well as all
receiver electrodes are kept on ground potential, too, by the low
impedance of input and output cascades of the signal acquisition
system (Fig. 1). As a matter of fact, all receiver rows in Fig. 2 are
sampled in parallel, while there is only one transmitter column
activated at a time. Ground potential at all electrodes except the
activated transmitters guarantees a maximum suppression of
cross-talk.
The concept of extending the range of the sensor consists in the
idea to sample the currents between large electrodes, too. If a large
electrode pad is connected to a low impedance receiver, the
Fig. 2. Sensor geometry [23] (G—ground electrode, G*—transmitter or receiver
electrode grounded by the low impedance of the connected signal acquisition
function as grounded surface is maintained when the near field
circuits in the non-activated case, T—transmitter electrode, R—receiver). is measured. Their potential is then actively kept on ground
potential by the input cascade. The same is true for any large
electrode that is used in a separate transmitter cycle. In instants of
active electrodes and the centers of the ground electrodes is 1 mm. activation of a column of small transmitter electrodes, the large
As shown in Fig. 2, the measuring volume is limited by four transmitter electrodes will be kept on ground potential by the low
symmetry boundaries between columns of transmitter electrodes impedance outputs of the driver cascades. In turn, when the large
and rows of receiver electrodes. Due to the symmetry of the electrodes are activated, all small electrodes are kept on ground
periodicity of the electrode matrix, the measurement is focused on potential. It is thus obvious that a subsequent sampling of the
the rectangular sensitive area shown in grey color in Fig. 2. In case matrix of small electrodes, followed by a sampling of any matrix of
of a liquid film of constant thickness, the symmetry causes the large electrodes do not interfere with each other.
electrical streamlines of the potential field to follow the horizontal This approach was used to build a second electrode matrix with
boundaries of the sensitive area in Fig. 2. In the first order a higher measuring range interlaced to the near field matrix.
approximation, the conductivities in the upper and lower neigh- A single cell of this “middle field” matrix is shown in Fig. 3.
boring sensitive areas do therefore not affect the current between The center of the control volume is identical with the one formed
transmitters and receivers forming this sensitive area. Contribu- by the “near field” matrix. Due to the higher distance between
tions to the measuring result by currents traveling from the transmitter and receiver electrodes and the large area covered by
transmitter to more distant receiver electrodes cannot be excluded grounded electrodes located in between, the measuring
by symmetry considerations. They represent uncertainties of the range is much larger, as it will be shown in detail in the
measurement since they contain information on the liquid film
thickness outside the grey square marking the sensible area. In
general, uncertainties arise
Fig. 6. Two interlaced far fields organized by modified receiver electrode design.
functionality of the sensor we decided to neglect the influence of sensitive area of the near field. All borders of the sensor ranging
the bending on the calibration. beyond the sensitive area are covered with a conductive layer
which is connected to ground potential in order to minimize
border effects. The length of the sensitive area of 192 mm occupies
an angular interval from 110 to þ 110 deg, 0 deg being at the
4. Test of the sensor in a wavy-stratified flow
lowest point of the pipe cross-section. The transmitters formed
lines running in circumferential direction, receiver lines run
For the test of the sensor, a two-phase flow was created by
parallel to the pipe axis. For transient measurements, the number
injecting water and air in an 8 m long horizontal pipe with a
of receivers was reduced to the capacity of the signal acquisition
diameter of 0.1 m (L/D¼ 80). The air was taken from the ambient
unit. In the result, the circumferential range was reduced to
and the water was stored in a vessel and was circulated in a closed
118 mm, which corresponds to an angular interval from 68 to
loop during the experiments (Fig. 9). The bendable sensor was
þ68 deg with 0 deg being at the lowest point.
mounted at the inside of the pipe wall (Fig. 10) downstream of the
All experiments were conducted at ambient temperature of
air–water inlet, where the flow is fully developed. The sensor was
297 K and atmospheric pressure. The tests were carried out under
mounted on the bottom of the circular pipe cross-section. In axial
steady-state conditions. The measuring frequency of the liquid
direction, it was 70 mm long, from which 52 mm is covered by the
film sensor was 3200 Hz.
Two-dimensional film thickness profiles shown in Fig. 11 were
obtained by time averaging of the instantaneous film thickness
measurements over a measuring sequence of 10 s. The superficial
velocities (air: 18 m/s, water 0.009 m/s ) for the demonstration of
the function of the sensor were chosen such that the variation of
the average film thickness covers all three measuring ranges. The
results are shown for all three measurement ranges individually in
Fig. 11. As expected for a steady-state stratified flow in a horizontal
pipe, the time average film thickness does not vary in flow
Fig. 9. Measurement set-up. direction. A significant profile exists only in the circumferential
direction. In the near-field the spatial resolution is the highest. The
measurement range is up to 600 mm. Close to the lowest point of
the pipe cross-section, the film thickness exceeds the measuring
range of the near field and the signal goes to a value near
saturation at 600 mm. In the middle field the measurement range
is from 400 mm to 1300 mm. The plot on the right side of in Fig. 11
shows the far-field.
Combining the results of all three measurement set leads to the
profile shown in Fig. 12. The curve on the right side shows the
azimuthal water film thickness distribution, i.e. along the peri-
meter of the pipe. Zero corresponds to the lowest point of the pipe
cross-section. Besides the averaging over the measuring time, the
film thickness is averaged over the extension of the sensor in flow
direction.
The generation of the composite film thickness shown in Fig. 12
is illustrated in Fig. 13. The upper limit of the near field measure-
Fig. 10. Flexible wall sensor mounted in the pipe. ment is shown as a red horizontal dashed line. Above this line, the
Fig. 11. Time averaged film thickness profiles measured by all three sets of electrodes individually (superficial velocity of air: 18 m/s, superficial velocity of water: 0.009 m/s,
liquid volume flow ratio: 5 10 4).
130 R. Tiwari et al. / Flow Measurement and Instrumentation 40 (2014) 124–132
Fig. 12. Measured time averaged film thickness as a composite of all three measurement sets shown in Fig. 11.
Fig. 14. Sequence of instantaneous two-dimensional film thickness profiles in an experiment with roll waves (flow from the right to the left, superficial velocity of air: 42 m/
s, superficial velocity of water: 0.0165 m/s).
on a grid with the size of 12 12 mm2. The sensor can be For a test under realistic flow conditions, a flexible sensor was
manufactured as a flat sensor but also in a bendable version using mounted in a horizontal pipe and film thickness measurements in
flexible PCB board technology. a wavy stratified flow of with water and air were conducted. They
A calibration of the sensor was performed in order to quantify confirm the functionality of the novel sensor. The measured film
the measuring ranges of the three interlaced electrode patterns. thickness values delivered by near, middle and far field electrode
132 R. Tiwari et al. / Flow Measurement and Instrumentation 40 (2014) 124–132
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