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APPENDIX- I

Proposed Course Structure for Chemical Engg.


(IInd Semester Onwards)

B. Tech. 2nd Year (Chemical Engineering Branch) 3rd Semester

Sl. Course Subject Credits Teaching Evaluation


No. Code Load (Hrs.) Scheme
Lect. Tut. Prac. Sesl. End Total
Theory Courses Sem.
1 THU301 Engineering Economics & Costing 2 2 0 0 25 50 75
2 TCH301 Fluid Flow Operations 4 3 1 0 50 100 150
3 TCY301 Engineering Chemistry 4 3 1 0 50 100 150
4 TCH302 Process Calculations 4 3 1 0 50 100 150
5 TCS302 CBNST 2 2 0 0 25 50 75
6 TME 303 Solid Mechanics 4 3 1 0 50 100 150
Practical Courses
7 PCH301 Fluid Mechanics Lab 3 0 0 3 25 50 75
8 PCS302 CBNST Lab 2 0 0 2 25 25 50
9 PCY301 Chemistry Lab 3 0 0 3 25 50 75
10 PD 301 Personality development Lab - 0 0 2 0 0 50
Total 28 1000

B. Tech. 2nd Year (Chemical Engineering Branch) 4th Semester

Sl. Course Credits Teaching Evaluation


No. Code Subject Load (Hrs.) Scheme
Lect. Tut. Prac. Sesl. End Total
Theory Courses Sem.
1 TMA401 Chemical Engineering Mathematics 4 3 1 0 50 100 150
2 TCH401 Mechanical Operations 2 2 0 0 25 50 75
3 TCH402 Engineering Materials 2 2 0 0 25 50 75
4 TCH403 Chemical Engineering 4 3 1 0 50 100 150
Thermodynamics
5 TCH404 Mass Transfer Operations-I 4 3 1 0 50 100 150
6 TCH405 Heat Transfer Operations 4 3 1 0 50 100 150
Practical Courses
7 PCH404 Mass Transfer Operations Lab-I 3 0 0 3 25 50 75
8 PCH401 Mechanical Operations Lab 2 0 0 2 25 25 50
9 PCH405 Heat Transfer Operations Lab 3 0 0 3 25 50 75
10 PD 401 Personality development Lab - 0 0 2 0 0 50
Total 28 1000
B. Tech. 3rd Year (Chemical Engineering Branch) 5th Semester

Sl. Course Subject Units Teaching Evaluation


No. Code Load (Hrs.) Scheme
Lect. Tut. Prac. Sesl. End Total
Theory Courses Sem.
1 THU501 Principles of Management 2 2 0 0 25 50 75
2 TCH501 Mass Transfer Operations - II 4 3 1 0 50 100 150
3 TCH502 Chemical Technology-I 2 2 0 0 25 50 75
4 TCH503 Energy Resources & Utilization 4 3 1 0 50 100 150
5 TCH504 Chemical Reaction Engineering -I 4 3 1 0 50 100 150
6 TCH505 Industrial Pollution & Control 4 3 1 0 50 100 150
Practical Courses
7 PCH501 Mass Transfer Operations Lab-II 3 0 0 3 50 50 100
8 PCH505 Industrial Pollution & Control Lab 3 0 0 3 50 50 100
9 PCH503 Energy Resources Lab 2 0 0 2 25 25 50
Total 28 1000

B. Tech. 3rd Year (Chemical Engineering Branch) 6th Semester

Sl. Course Subject Credits Teaching Load Evaluation


No. Code (Hrs.) Scheme
Lect. Tut. Prac. Sesl. End Total
Theory Courses Sem.
1 TCH601 Transport Phenomena 4 3 1 0 50 100 150
2 TCH602 Chemical Technology-II 2 2 0 0 25 50 75
3 TCH603 Process Dynamics & Control 4 3 1 0 50 100 150
4 TCH604 Chemical Reaction Engineering-II 4 3 1 0 50 100 150
5 TCH605 Process Modeling & Simulation 4 3 1 0 50 100 150
6 TCH606 Process Instrumentation 2 2 0 0 25 50 75
Practical Courses
7 PCH602 Chemical Technology Lab 2 0 0 2 25 25 50
8 PCH604 Chemical Reaction Engineering Lab 3 0 0 3 50 50 100
9 PCH603 Process Dynamics & 3 0 0 3 50 50 100
Instrumentation Lab
Total 28 1000
B. Tech. 4th Year (Chemical Engineering Branch) 7th Semester

Sl. Course Subject Units Teaching Evaluation


No. Code Load (Hrs.) Scheme
Lect. Tut. Prac. Sesl. End Total
Theory Courses Sem.
1 TCH701 Process Equipment Design 4 3 1 0 50 100 150
2 TCH71 Professional Elective – I* 4 3 1 0 50 100 150
3 TCH 72 Professional Elective – II* 4 3 1 0 50 100 150
4 TCH 73 Professional Elective – III* 4 3 1 0 50 100 150
5 TOE01 Open Elective** 4 3 1 0 50 100 150
Practical Courses
6 PCH701 Minor Project 6 0 0 6 10 100 200
0
7 PCH702 Summer Training & Colloquium 2 0 2 0 50 0 50
Total 28 1000

Professional Electives
TCH 71: Professional Elective – I*
TCH 711 : Non Conventional Energy Resources TCH 712: Polymer Science & Technology
TCH 713: Fertilizer Technology
TCH 72: Professional Elective – II*
TCH 721: Safety & Hazard Analysis TCH 722: Food Technology
TCH 723: Hazardous Waste Management
TPE73: Professional Elective – III*
TCH 731: Advanced Separation Processes TCH 732: Intellectual Property Rights
TCH 733: Fluidization Engineering

**Open Elective
TOE011: Process Utilities & Safety TOE012: Intellectual Property Rights
TOE013: Non Conventional Energy Resources TOE014: Bioinformatics

** Open Elective course: Offered for other departments.


B. Tech. 4th Year (Chemical Engineering Branch) 8th Semester

Sl. Course Subject Units Teaching Evaluation


No. Code Load (Hrs.) Scheme
Lect. Tut. Prac. Sesl. End Total
Theory Courses Sem.
1 TCH80 Pilot Plants & Scale-Up Methods In 4 3 1 0 50 100 150
1 Chemical Engineering
2 TCH81 Professional Elective – IV* 4 3 1 0 50 100 150
3 TCH82 Professional Elective – V* 4 3 1 0 50 100 150
5 TCH83 Professional Elective - VI* 4 3 1 0 25 50 150
Practical Courses
7 PCH801 Major Project 10 0 0 10 100 250 350
8 PCH802 CAD Lab 2 0 0 2 25 25 50
Total 28 1000

Professional Electives
TCH81: Professional Elective – I*
TCH811 : Fundamentals of Biochemical TCH812: Petroleum Refining Technology
Engineering
TCH813: Oil and Fat Technology
TCH82: Professional Elective – II*
TCH821: Fermentation Technology TCH822: Plant Design & Economics

TCH823: Catalysis

TCH83: Professional Elective – III*


TCH831: Corrosion Engineering TCH832: Finite Elements Methods

TCH833: Process Utility & Piping Design


THU-301: ENGINEERING ECONOMICS AND COSTING
L T P 2 0 0

Unit I: Time value of money : Simple and compound interest, Time value equivalence,
Compound interest factors, Cash flow diagrams, Calculation, Calculation of time –
value equivalences. Present worth comparisons, Comparisons of assets with equal,
unequal and infinite lives, comparison of deferred investments, Future worth
comparison, payback period comparison.

Unit II: Use and situations for equivalent annual worth comparison, Comparison of assets
of equal and unequal life. Rate of return, Internal rate of return, comparison of IIR
with other methods, IRR misconceptions.

Unit III: Analysis of public Projects: Benefit/ Cost analysis, quantification of project, cost
and benefits, benefit/ cost applications, Cost –effectiveness analysis.

Unit IV: Depreciation, computing depreciation charges, after tax economic comparison,
Break-even analysis; linear and non-linear models.
Product and Process Costing, Standard Costing, cost estimation, Relevant Cost for
decision making, Cost control and Cost reduction techniques.

Text Book :
1. Horn green, C.T., Cost Accounting, Prentice Hall of India
2. Riggs, J.L., Dedworth, Bedworth, D.B, Randhawa, S.U. Engineering Economics,
McGraw Hill
International Edition, 1996

TCH 301: FLUID FLOW OPERATIONS

L T P 3 1 0

Unit I: Units and dimensions; Fluid, Properties of fluids; Classification of fluids; Fluid
statics, Absolute, Gauge, Atmospheric and Vacuum pressures, Pressure head,
Hydrostatic Law and Pressure Measurement.

Unit II: Kinematics of Flow: Types of fluid flow ( Laminar flow, Turbulent flow etc.),
Stream function, Rate of flow or Discharge, Continuity equation, Conservation of
mass and energy; Energy balance, Bernoulli's theorem, Bernoulli's equation and its
applications, Minor losses in pipe flow, Loss of energy due to friction, friction factor.

Unit III: Dimensional Analysis: Dimensionless numbers and their physical significance,
Methods of Dimensional Analysis, Dimensional Homogeneity; Free and Hindered
Settling; Equivalent Pipe, Flow through Parallel Pipe, Pipe fittings and valves.

Unit IV: Flow Measurements: Importance of Flow Measurements, Venturi meter, Orifice meter,
Rota meter, and Pitot tube.
Unit V: Transport of Fluids: Pumps, Classification, Construction and working of pumps,
Centrifugal Pump, Multistage Centrifugal Pumps, Cavitation, Effects of cavitation,
Priming; Reciprocating Pump, Single acting and Double acting Reciprocating
Pumps, Air vessels; Fans, Blowers and Compressors.

Text Book
1. McCabe, W.L., Smith J.C., and Harriot, P., “Unit Operations in Chemical Engineering”,
McGraw-Hill, Inc, 5th Ed., 2001.

References:
1. Coulson, J.M. and Richardson, J.F., “Chemical Engineering, Volume I”, Pergamon Press.
3rd Ed., 1981.
2. Shames, I.H., “Mechanics of Fluids”, McGraw-Hill, Inc. 3rd Ed. 1992.

TCY 301: ENGINEERING CHEMISTRY


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Unit I: Organic Chemistry: Organic reactions of Industrial Significance.


(i) Alcohols, phenols & ethers: Reactions of alcohols with alkaline earth metals ,
Iodoform reaction, Oxidation, conversion of alcohols into Mesylates &Tosylates ;
Crown ethers & epoxides; Reimer-Tiemann reaction , Kolbes-Schimidt reaction
mechanisms
(ii) Aldehydes & Ketones : Oxidation & reduction , Perkin reaction ,Claison-
Schmidt reaction, Benzoin condensation, Knovenagel reaction, reformatsky
reaction,Wittig reaction.
(iii) Carboxylic acids and their derivatives: Hell-Volhartd Zelinsky reaction ,
Hoffmann bromide reaction, Curtius and Lorsen Reaction
(iv) Nitrocompounds: Reduction of nitrobenzene under different conditions
(v) Amines: Reactions with nitrous acids, Diazotization and reactions of
arenedizonium salts
Unit II: (i) Concept of aromaticity in benzoid and non-benzoid compounds, aromatic and
non-aromatic compounds
(ii) Organomettalic compounds: Applications of Grignard Reagent and Lithium
aluminum hydride
(iii) Stereochemistry: Conformational analysis: various terms, conformational
analysis of cyclohexane and 1,2 –disubstituted cyclopean. Stereoisomerism of
cyclic compounds (cyclohexane), chiral drugs (ibuprofen), the relative and
absolute configuration, stereoselective and stereospecific reactions.
Unit III: Surface Chemistry (i) Catalysis : Acid base catalyzed reaction, enzyme catalyzed
reaction and heterogeneous catalyzed reaction
(ii) Surface tension determination and Applications
(iii) Adsorption Isotherms- Freundlich and Langmuir
(iv) Colloids: General methods of preparation and properties, hydrophilic and
hydrophobic sols, Electrical Properties of colloids
(v) Colligative Properties: Lowering of Vapor Pressure, Elevation in boiling point,
lowering in melting point, Osmotic Pressure and their relation with molecular
weight
Unit IV: Natural Organic Molecules: Biomolecules: Definition, types of biomolecules-
nucleosides & nucleotides (DNA and RNA), saccharides (glucose, fructose,
maltose and cellulose), lignin, lipids and amino acids (protein structure of
apoenzymes, isoenzymes and vitamins) and their industrial applications.

Text Books
1. Finar, I.L. “Organic Chemistry : Vol. I & II”.
2. Morrison & Boyd “Organic Chemistry”.
3. March, J. “Organic Chemistry”.
4. Soloman, T. “Organic Chemistry”.
5- Glasstone, S. “Physical Chemistry”
6- Atkin, P. W. “Physical Chemistry”
7- Banwell, C. N. “Fundamentals of Molecular Spectroscopy”
8- Willard Merit & Dean “Instrumental Methods of Chemical Analysis”
9- Skoog & West “Instrumental Methods of Chemical Analysis”

TCH 302: Process Calculations


L T P 3 1 0

Unit I: Unit and dimensions; Conservation of mass and energy; Problem solving
techniques; Computer based tools, Sources of data, Ideal gas law, Real gas
relationships, Vapour pressure; Vapour-liquid equilibria for binary and
multicomponent systems, Saturation, Partial saturation and humidity.
Unit II: Overall and component material balances; Material balance with chemical
reactions, Material balance without chemical reactions.

Unit III: Material balance involving multiple subsystems; Recycle, bypass, purge and
phase change; Material and energy balance calculations of some selected process
plants such as sulfuric acid, ammonia, urea, caustic soda etc.
Unit IV: Enthalpy changes; Energy balance with and without chemical reactions;
Reversible process and mechanical energy balance; Heats of solution and
mixing; Humidity charts and their use in solving humidification,
dehumidification and water cooling problems.
Unit V: Fuels and Combustion; Adiabatic flame temperature. Degrees of freedom in
steady-state processes; Simultaneous material and energy balance problems using
flow sheeting codes; Unsteady state material and energy balances.

Text Book:
1. Hougen, O.A., Watson. K.M. and Ragatz, R.A.,” Chemical Process Principles Part-I”,
John Wiley & Sons.
References:
1. Bhatt, B.L. and Vora, S.M., “Stoichiometry”, Tata McGraw-Hill Publishing Co., New
Delhi. 3rd Ed, 1996.
2. Himmelblau, D.M., “Basic Principles and Calculation in Chemical Engineering”,
Prentice Hall, Inc.7th Ed. 2004.

TCS 302: COMPUTER BASED NUMERICAL AND STATISTICAL TECHNIQUES


L T P 2 0 0

Unit I: Introduction: Numbers and their accuracy, Computer Arithmetic,Mathematical


preliminaries, Errors and their Computation, General error formula, Error in a
series approximation.
Solution of Algebraic and Transcendental Equation:
Bisection Method, Iteration method, Method of false position, Newton-Raphson
method, Methods of finding complex roots, Muller’s method, Rate of convergence
of Iterative methods, Polynomial Equations.

Unit II
Interpolation: Finite Differences, Difference tables Polynomial Interpolation:
Newton’s forward and backward formula Central Difference Formulae: Gauss forward and
backward formula, Stirling’s, Bessel’s, Everett’s formula.
Interpolation with unequal intervals: Langrange’s Interpolation, Newton Divided difference
formula, Hermite’s Interpolation

Unit-III
Numerical Integration and Differentiation: Introduction, Numerical differentiation
Numerical Integration: Trapezoidal rule, Simpson’s 1/3 and 3/8 rule, Boole’s rule, Waddle’s
rule.

Solution of differential Equations: Picard’s Method, Euler’s Method, Taylor’s Method,


Runge-Kutta Methods, Predictor Corrector Methods, Automatic Error Monitoring and
Stability of solution.
Unit-IV
Statistical Computation: Frequency chart, Curve fitting by method of least squares, fitting of
straight lines, polynomials, exponential curves etc, Data fitting with Cubic splines,
Regression Analysis, Linear and Non linear Regression, Multiple regression, Statistical
Quality Control methods.

Text Books:
1. Rajaraman V, “Computer Oriented Numerical Methods”, Pearson Education
2. Pradip Niyogi, “Numerical Analysis and Algorithms”, TMH
3. Jain, Iyengar and Jain, “Numerical Methods for Scientific and Engineering
Computations”, New Age Int.
References:
1. Gerald & Whealey, “Applied Numerical Analyses”, AW
2. Goyal, M, “Computer Based Numerical and Statistical Techniques”, Firewall Media,
New Delhi.
3. Grewal B S, “Numerical methods in Engineering and Science”, Khanna Publishers,
Delhi.
4. Numerical Method Principles, analysis and algorithms ,Srimamta Pal (Oxford
Higher ed)
5. Francis Scheld, ” Numerical Analysis”, TMH
6. Sastry S. S, “Introductory Methods of Numerical Analysis”, Pearson Education.
7. Gupta C.B., Vijay Gupta, “Introduction to Statistical Methods”, Vikas Publishing.
TME- 303: Solid Mechanics
L T P 3 1 0

Unit-I
Introduction. Stress and strain: stress at point, Cauchy stress tensor, equilibrium equations,
analysis of deformation and definition of strain components, compatibility relations, 8
principal stresses and strains, stress and strain invariants, Mohr's circle representation. 3

Unit-II
Constitutive relations: true and engineering stress-strain curves, Material properties for
isotropic materials and their relations. Theories of failures for isotropic materials.
7

Unit-III
Shear Force and Bending Moment diagrams. Axially loaded members. Torsion of circular
shafts
Stresses due to bending: pure bending theory, combined stresses. 7

Unit-IV
Deflections due to bending: moment-curvature relation, load-defection differential equation,
area moment method, and superposition theorem. Stresses and deflections due to transverse
shears. 8

Unit-V
Torsion of circular shaft. Energy methods: Strain energy due to axial, torsion, bending and
transverse shear. Castigliano's theorem, reciprocity theorem etc.
7

Text Books:
1. S. C. Crandall, N. C. Dahl, and T. J. Lardner, An Introduction to the Mechanics of Solids,
2e, McGraw Hill,1978.
References:
1. E. P. Popov, Engineering Mechanics of Solids, Prentice Hall, 1990
2. I. H. Shames, Introduction to Solid Mechanics, 2e, Prentice Hall, 1989
3. S. P. Timoshenko, Strength of Materials, vols. 1 & 2, CBS publ., 1986
4. Mechanics of Materials by Bear Jhonson

PCH 301: FLUID MECHANICS LAB


L T P 0 0 3

1. To calibrate the venturimeter and to find out its discharge coefficient. Also, to plot a
graph between Reynolds number and discharge coefficient.
2. To calibrate the orifice meter and to find out its discharge coefficient. Also, to plot a
graph between Reynolds number and discharge coefficient.
3. To calibrate the V-notch and to determine its discharge coefficient.
4. To find out the equivalent length of various pipe fittings (i) Gate valve, fully open
(ii) Globe valve, fully open (iii) Elbow (iv) Reducer (v) Socket and (vi) Bend.
5. To verify Bernoulli’s theorem.
6. To study the characteristics of a centrifugal pump (UPSH / NPSH) / compressor
7. To calibrate the Rotameter..
8. To study the flow characteristics using Reynolds’ apparatus.
9. To study the flow curves of fluid’s for Newtonian and Non-Newtonian fluids flow
conditions.
10. To calibrate and tofind out discharge coefficient using Nozzle flow meter.
11. To find out the viscosity of a given Liquid sample using Falling Ball Viscometer.
12. To calculate the power requirement of mixing.

PCS- 302: Computer Based Numerical Techniques Lab


L T P 0 0 2

Write Programs in ‘C’ Language:


1. To deduce error involved in polynomial equation.
2. To Find out the root of the Algebraic and Transcendental equations using
3. To implement Newton’s Forward and Backward Interpolation formula.
4. To implement Gauss Forward and Backward, Bessel’s, Sterling’s and Evertt’s
Interpolation formula.
5. To implement Newton’s Divided Difference and Langranges Interpolation formula.
6. To implement Numerical Differentiations.
7. To implement Numerical Integration using Trapezoidal, Simpson 1/3 and Simpson 3/8
rule.
8. To implement Least Square Method for curve fitting.
9. To draw frequency chart like histogram, frequency curve and pie-chart etc.
10. To estimate regression equation from sampled data and evaluate values of standard
deviation, t-statistics, regression coefficient, value of R2 for atleast two independent
variables.

PCY 301: Chemistry Lab


L T P 0 0 3
1. Identification of Organic Compounds in the mixture.
2. Estimation of Glucose, phenol, aniline.
3. Applications of TLC in the organic chemistry.
4. Determination of percentage composition of mixture with the help of viscosity
measurements.
5. Freundlich adsorption isotherm verification.
6. Distribution of solute between two immiscible solvents ( I2 / water + organic solvent),
Distribution law.
7. Conductivity: (i) Conductivity titration strength of strong acid vs. strong base, (ii)
Dissociation constant of a weak acid (CH3COOH).
8. Determination of molecular weight of a non volatile substance by (i) elevation in
boiling point (ii) depression in freezing point.
9. Determination of Iron by Specrophotometric method.
10. Potentiometric titration.
TMA 401:Chemical Engineering Mathematics
L T P 3 1 0

Unit I: Design of Engineering Experiments: Application of mathematical methods to


solve chemical engineering problems. Treatment of experimental data and
interpretation of results. Use of .different types of graph paper. Curve fitting
methods and empirical laws
Unit II: Formulation of Physical Problems: The mathematical statement of the problem,
Introduction. Representation of problem, Simple problems formulation on
solvent extraction in single and multistage. Radial heat transfer through a
cylindrical conductor. Salt accumulation in stirred tank .Summary of the method
of formulation.
Unit III: Linear and non-linear Algebraic Equations: Numerical solutions of linear and
non -linear algebraic equations in Chemical engineering, Interpolation and
extrapolation.
Unit IV: Numerical solution of Ordinary Differential Equations: Numerical solution of
initial value and boundary value, ordinary different equation problems in
chemical engineering.
Unit V: Numerical Solutions of Partial Differential Equations: Finite differences,
Orthogonal Collocation technique, Finite Element Method, Numerical solution of
partial differential equations in chemical engineering- elliptic, parabolic and
hyperbolic equations.

Text Book:
1.H.S. Mickley, T. K. Sherwood rod C.E. Reid, "Applied Mathematic in Chemical
Engineering", 2nd Ed., Tata McGraw Hill, New Delhi, 1978
References:
1. S.K.Gupta, "Numerical Techniques for Engineers", Wiley Eastern Ltd.,NewYork,1995.
2. O.F.Hanna and O.C. Sandall, "Computational Methods in Chemical Engineering",
Prentice-Hall, 1995.
3. W.F.Ramirez, "Computational Methods for process Simulation", Butterwortlia, 1989.
4. V. Q. Jenson and G. V. Jeffreys, "Mathematical Methods in Chemical Engineering"
2nd. Edn., 1977.

TCH 401: MECHANICAL OPERATIONS


L T P 2 0 0

Unit I: Introduction to unit operations and their role in Chemical Engineering industries.
Types of Mechanical Operations, Characteristics of particulate solids: sampling
techniques, specification and screen analysis, particle size distribution, particle
size measurement, Surface area measurements, statistical mean diameters,
relevant equations and problems.
Unit II: Principles of size reduction: Specific properties of solids for size reduction.
Energy required for size reduction. Crushing and grinding efficiency. Laws of
crushing, Pulverization and Ultra fine grinding. Classification of crushing and
grinding equipments. Construction and working principle of mostly used
equipments, viz., Jaw crushers, Gyratory crushers, Hammer mill, Crushing rolls,
Ball mills, and Fluid energy mills. Mixing of solids, blending, kneading, etc.
Unit III: Conveying of bulk solids, classification of conveyors, selection of conveyors.
Storage of solids in bulk protected and unprotected piles, bins, silos, hoppers,
mass flow and funnel flow Bins, Flow assisting devices, feeders. Weighing of
bulk solids, batch and continuous weighing techniques.
Unit IV: Classification of separation methods for different types of mixtures like solid-
solid, solid-gas, solid-liquid. Screening, classification of screening equipments.
Mechanical classification and classifiers. Rare and dense medium separation,
magnetic separation, electrostatic separation. Floatation and elutriation.
Unit V: Continuous thickeners, decantation, Phase separation: Centrifugal separation,
Electrostatic precipitators. Impingement separators, Gas-solid separation: Gravity
settling, Impingement separators, Cyclone separators, bag filters, scrubbers
Filtration: classification of filters, theory of filtration, cake resistance

Text Book
1. Narayanan C.M.& Bhattacharya B.C. “Mechanical operations for chemical engineers”,
Khanna Publishers. 3 rd Ed.1999
References
1. Coulson and Richardson: “Chemical Engineering, Vol. 2.” Butterworth Heinemann Pub.
3rd Ed.., 1999
2. Welty,Wicks,Wilson & Rorrer, “Fundamentals of Momentum, Heat and Mass Transfer”,
Wiley. 5th Ed., (2008)

TCH 402: ENGINEERING MATERIALS


L T P 2 0 0

Unit I: Structure and properties, relationship of Engineering Materials, Structure of


Crystalline Solids: Crystal structures and Systems, Unit Cells, Metallic Crystal
Structures, Crystallographic directions and Planes, Density Computations.
Characterization of Materials: Crystallography, Reciprocal Lattice, Stereographic
projections,
Unit II: Diffraction methods, Electron microscopy, Metallography, Thermal analysis.
Imperfections in Crystals: Point defects, Dislocations, Interfacial Defects, Bulk
defects. Diffusion: Mechanisms, steady state and non steady state Diffusion,
factors influencing diffusion.
Unit III: Multiphase Structures, Phase Transformations: Unary, Binary, Equilibrium Phase
Diagrams, Eutectic, Eutectoid Peritectic and Peritectoid Reactions, Iron Carbon
Diagram. Mechanical Behavior of Materials: Elastic and Plastic properties,
Creep, Fracture, Heat treatment of steels. Ceramic Materials: Ceramic Structures,
Properties.
Unit IV: Electric and Electronic materials: Electrical Conduction, Classification of
semiconductor materials, Materials and Technology for integrated circuits,
Photonic materials, super conductivity and special super-conducting materials,
Ferrites. Quartz crystal, Dielectric materials. Piezoelectric and Ferro-electric
materials, Electromechanical materials, Mechanism of polarization, Its
measurements.
Unit V: Magnetic Properties for Applications; ‘Diamagnetism, Paramagnetism,
ferromagnetism, Antiferromagnetism, Ferrimagnetism, Soft and hard magnetic
materials magnetic storage. Optical properties: Optical properties of Metals and
Nonmetals, Luminescence, photoconductivity, Optical Fibers in
communications.

Text Book:
1.Raghavan V., “Material Science and Engineering”, Prentice- Hall of India Private
Limited, New Delhi, 5th ed., 2004
References:
1. Callister W. D., Jr., “Material Science and Engineering An Introduction”, John
Wiley & Sons, Inc., 6th Ed., 2003.

TCH403: CHEMICAL ENGINEERING THERMODYNAMICS


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Unit I: Basic Concepts and Definitions: System, Surroundings, Property, Macroscopic


and Microscopic Viewpoints, Thermodynamic Equilibrium, Heat and Work
interactions; First Law of Thermodynamics, Conservation of energy, Perpetual
Motion Machine of the First Kind, First Law analysis of Elementary Processes,
Steady and unsteady flow, SFEE; Applications to engineering problems.

Unit II: Second Law of Thermodynamics: Limitations of First Law of Thermodynamics,


Heat Engine, Heat Pump, Refrigerator, Statements of Second Law of
Thermodynamics, PMMSK, Thermodynamic Temperature Scale, Simultaneous
working of Heat Engine, Heat Pump and Refrigerator; Reversible Process,
Irreversible Process, Carnot Engine, Carnot Cycle, Carnot Theorems, Types of
Irreversibility, Available Energy, Dead State and Availability, Applications to
systems of engineering interest.

Unit III: Properties of Pure Substances: Concept of Phase, P-V and P-T Diagrams of a
pure substance, Changes in thermodynamic properties and their inter-
relationships, Maxwell’s Relations, Specific Heat Relations, Dryness Fraction,
Throttling Calorimeter, Steam Tables, Measurement of Steam Quality, Liquid-
Vapour mixtures, Equations of State; Applications to systems of engineering
interest.
Unit IV: Psychrometry: Properties of Ideal Gas Mixtures, Ideal Gas-Vapor Mixtures, Dew
point temperature, Specific humidity, Relative humidity, Adiabatic Saturation
Process, Psychrometer, Dry-bulb and Wet-bulb temperatures, Psychrometric
chart, Air-conditioning systems; Applications to engineering problems.

Unit V: Reactive Systems: Stoichiometric coefficients, Degree of Reaction, Law of mass


action, Heat of Reaction, Temperature Dependence of the Heat of Reaction,
Phase Rule and Duhem’s Theorem for Reacting Systems, Chemical Exergy;
Applications to engineering problems.

Text Book:
1. Smith, J.M., Van Ness, H.C. & Abbot, M.M. “Introduction to Chemical Engineering
Thermodynamics “, 5th edition. New York: Mc-Graw Hill 1996.

Reference Books
1. Narayanan K. V. “A Textbook of Chemical Engineering Thermodynamics”; Prentice-hall
of India Pvt Ltd. 2004
2. Daubert T.E., "Chemical Engineering Thermodynamics" McGraw Hill, 1986.

TCH 404: MASS TRANSFER OPERATIONS - I


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Unit I: Diffusion: Molecular and turbulent diffusion, diffusion coefficient, Fick’s Law of
diffusion, Dependence of diffusion coefficient on temperature, pressure and
composition; measurement and estimation of diffusivity. Diffusion in multi-
component gas mixtures. Diffusion in Solids: Molecular, Knudsen & surface
diffusion; Inter- phase mass transfer: Mass transfer coefficients, Diffusion
between phases, Equilibrium solubility of gases in liquids, Mass transfer theories,
Mass transfer in fluidized beds, Flow past solids and boundary layers,
Simultaneous heat and mass transfer.
Unit II: Absorption and Stripping: Equipments, Gas-liquid equilibria, Henry’s law,
Selection of solvent, Absorption in tray column, Graphical and analytical
methods, Absorption in packed columns, HTU, NTU &HETP concepts, Design
equations for packed column, Absorption with chemical reaction and mass
transfer.
Unit III: Humidification and Dehumidification: Vapour liquid equilibrium and enthalpy
for a pure substance, vapour pressure temperature curve, Vapour gas mixtures,
Definition and derivations of relationships related with humidity Fundamental
concept of humidification, Dehumidification and water cooling, Wet bulb
temperature, Adiabatic and non-adiabatic operations, Evaporative cooling,
Classification and design of cooling towers.
Unit IV: Drying: Solid-gas equilibria, Different modes of drying operations, Definitions
of moisture contents, Types of batch and continuous dryers, Rate of batch drying,
Time of drying, Mechanism of batch drying, Continuous drying, Design of
continuous dryers.
Unit V: Crystallisation: Equilibrium yield of crystallization, Heat and mass transfer rates
in crystallization, Theories of crystallization, Factors governing nucleation and
crystal growth rates, Controlled growth of crystal, Classification and design of
crystallizers.
Text Book
1. Treybal, R “Mass Transfer Operations”, 3rd Ed., McGraw-Hill New York, 1980.

Reference
1. Sherwood T. K., Pigford R. L. and _ilke P. “Mass Transfer” McGraw Hill, 1975.
2 Foust A. S. et.al., “Principles of Unit Operations” John Wiley, 1980.
3 Geankoplis, C.J.. “Transport Processes and Unit Operations”, 3rd Ed. Prentice Hall.
1993.

TCH405: HEAT TRANSFER OPERATIONS


L T P 3 1 0

Unit I: Conduction: Introduction to heat transfer and general concepts, Thermal


conductivity, Basic concepts of conduction in solids, liquids and gases, Steady
state temperature fields and one dimensional conduction without heat generation,
e.g., through plane walls, cylindrical and spherical surfaces, Conduction through
solids in series. Insulation materials, critical and optimum insulation thickness.
Introduction to unsteady state heat transfer.
Unit II: Convection: Fundamentals of convection, Basic concepts and definitions, natural
and forced convection, hydrodynamic and thermal boundary layers, laminar and
turbulent heat transfer inside and outside tubes, Determination of individual and
overall heat transfer coefficients and their temperature dependence, heat transfer
in molten metals.
Unit III: Radiation: Basic laws of heat transfer by radiation, black body and gray body
concepts, Opaque body, White body, Emissivity, Absorptivity, Reflectivity, and
Transmissivity, view factors, Kirchoff’s law, Stefan–Boltzmann law, Solar
radiations, Radiation to a small object from surroundings, Effect of radiation on
temperature measurement, Combined heat transfer coefficients by convection
and radiation.
Unit IV: Heat Transfer with Phase Change: Condensation of pure and mixed vapors, film
wise and drop wise condensation, loading in condensers and basic calculation on
condensers, heat transfer in boiling liquids, boiling heat transfer coefficients.
Evaporation: Elementary principles, types of evaporators. Single and multiple
effect evaporators and their calculations.
Unit V: Heat Transfer Equipment: Classification, principles and design criteria, Types of
heat exchangers, viz., Double Pipe, Shell and Tube, Plate Type, Scraped surface
heat exchanger, Furnaces, their classification and applications.

Text Book:
1. McCabe, W.L., Smith J.C., and Harriot, P., “Unit Operations in Chemical Engineering”,
McGraw-Hill, Inc. 5th Ed., 2001.

References
1. Holman, J. P., “Heat transfer” 9th Ed McGraw Hill, 1989.
2 Coulson, J.M. & Richardson, J.F. “Chemical Engineering :Vol-1”, 6th ed. Butterworth-
Heinemann,1999.
3 McAdams W.H. “Heat Transmission”, 3rd ed., McGraw-Hill, 1954.
4 Kern D.Q. “Process Heat Transfer” McGraw Hill Book, 1950.
5 Badger W.L. & Bancharo J.T. ,”Introduction to chemical engineering” Tata McGraw Hill,
5th Ed. 1996.

PCH 401:MECHANICAL OPERATIONS LAB


L T P 0 0 2

1. To study the performance of Ball Mill and find out it’s crushing efficiency.
2. To study the performance of Jaw Crusher and find out it’s crushing efficiency.
3. To study the performance of Crushing Rolls and find out it’s crushing efficiency.
4. To study the settling characteristics.(Free & Hindered settling) of a given suspension of
particles.
5. To study the filtration characteristics of rotary vacuum filter.
6. To study the filtration characteristics of Plate and frame filter press.
7. To study the filtration characteristics of Leaf and sparkle filter.
8. To carry out differential and cumulative screen analysis of given sample of solid particles.
9. To study the pressure drop characteristics through packed beds.
10. To study the pressure drop and porosity in Air fluidized bed.
11. To study the pressure drop and porosity in Liquid fluidized bed

PCH 404: MASS TRANSFER OPERATIONS LAB-I


L T P 0 0 3

1. Study the performance and determination of Equilibrium relationships


2. Mass transfer coefficients,
3. Diffusion coefficients,
4. Separation factors of the experiments with differential distillation,
5. Flash vaporization, vapour liquid equilibrium,
6. Liquid – liquid extraction,
7. Solid –liquid extraction,
8. Ion exchange and membrane separation.

PCH 405: HEAT TRANSFER OPERATIONS LAB


L T P 0 0 3

1. To find the thermal conductivity of metallic rod at different temperature and draw the
temperature profile for steady and unsteady state conduction.
2. To find out the thermal conductivity of insulating powder.
3. To find the thermal conductivity of liquid / gases.
4. To find the emissivity of grey plate with respect to black plate
5. To study the critical heat flux behaviour of a liquid
6. To find the heat transfer coefficient for parallel and counter current flow condition for a
Double pipe heat exchanger
7. To study the shell & Tube heat exchanger and find the heat duty and Over all heat transfer
coefficient for parallel flow condition.
8. To study the shell & Tube heat exchanger and find the heat duty and Over all heat transfer
coefficient for counter flow condition.

TCH 501:MASS TRANSFER OPERATIONS – II


L T P 3 1 0

Unit I: Distillation: Pressure-composition, Temperature-concentration, Enthalpy-


concentration diagrams for ideal and non-ideal solutions, Raoults law and its
application, Maximum and minimum boiling mixtures, concept of relative
volatility, Single Stage Distillation Differential distillation, Flash vaporization,
Vacuum, molecular and steam distillation.
Unit II: Continuous Distillation of Binary Mixtures: Multistage contact operations,
Characteristics of multistage tower, McCabe Thiele method, Ponchon Savarit
method, Reflux, maximum, minimum and optimum reflux, Use of open steam,
Tray efficiency, Determination of height and column diameter, Multistage batch
distillation; Principles of azeotropic and extractive distillation, Introduction to
multicomponent distillation system.
Unit III: Liquid-Liquid Extraction: Ternary liquid equilibria, Triangular graphical
representation concept of theoretical or ideal stage, Equipment used for single
stage and multistage continuous operation; Analytical and graphical solution of
single and multistage operation Super critical fluid extraction.
Unit IV: Solid /Liquid Extraction: Leaching, Solid liquid equilibrium, Equipment used in
solid-liquid extraction, Single and multistage cross current contact and counter
current operations. Concept of an ideal stage, Overall stage efficiency,
Determination of number of stages.
Unit V: Adsorption: Description of adsorption processes and their application, Types of
adsorption, Nature of adsorbents adsorption equilibria and adsorption hysterises,
Stage wise and continuous contact adsorption operations, Determination of
number of stages, Equipments;
Ion exchange, Equilibrium relationship, Principle of ion-exchange, techniques
and applications, Principles and application of dialysis, osmosis reverse osmosis,
thermal diffusion, sweep diffusion.
Text Book:
1. Treybal, R “Mass Transfer Operations”, 3rd Ed., McGraw-Hill, New York, 1980.
References:
1. Sherwood T. K., Pigford R. L. and Wilke P. “Mass Transfer” McGraw Hill, 1975.
2. Foust A. S. et.al., “Principles of Unit Operations” John Wiley, 1980.
TCH 502: CHEMICAL TECHNOLOGY -I (ORGANIC)
L T P 2 0 0

Unit I: Importance and Overview of Chemical Process Industries. Unit operations and
Unit process concept. Sugar, Glucose, Starch, Fermentation products such as
Alcohol, Acetic acid, Citric acid and antibiotics.
Unit II: Soap and Surfactants, Glycerin, Fatty acids, Hydrogenation of edible oils, paper
and pulp
Unit III: Synthetic and natural fibers: Nylon, Dacron, Terylyne, Polyester and other new
products, Viscose rayon, acetate rayon , synthetic rubber with special reference
to manufacture, vulcanization and reclaiming of rubber, SBR, Plastics,
Thermosetting and Thermo Plastics(PVC, Polyethylene, Polyurethane, Teflon )
Unit IV: Crude oil distillation, Thermal conversion processes (visbreaking, coking),
Catalytic conversion processes (fluid catalytic cracking, catalytic reforming,
hydro cracking, alkylation, isomerisation, polymerization) Finishing processes,
sulphur removal process, lub oil manufacture; Petrochemicals(ethylene,
propylene, formaldehyde, methanol, ethylene oxide , ethanolamine, cumene,
ethylene glycol, ethyl benzene)

Text Book:
1. Dryden, C. E. “Outlines of Chemical Technology” (Edited and Revised by M.Gopal Rao
and Sittig .M) East West Press.Pvt Ltd,New Delhi,3rd Ed., 1997.
References
2. Austin G. T, “Shreve’s Chemical Process Industries”, McGraw Hill, 5th Ed., 1984.

TCH 503: ENERGY RESOURCES AND UTILIZATION


L T P 3 1 0

Unit I: Energy Scenario: Indian and global, energy crisis, Classification of various
energy sources, Renewable and non-renewable energy sources, Remedial
measures to some energy crisis.
Energy Conservation: Energy: Biogas plants and their operation, Biomass and its
conversion routes to gaseous and liquid fuels. Wind energy, its potential and
generation by wind mills,
Unit II: Alternative Sources of Energy: Fuel cell, Solar Energy: Photo thermal and
photovoltaic conversion and utilization methods, solar water heating, cooking,
drying and its use for other industrial processes, solar cells their material and
mode of operation. direct and indirect methods of solar energy storage , sensible
heat and latent heat storage materials Solar ponds .
Bio energy, biogas plants and their operation, biomass and its conversion roots to
gaseous and liquid fuels, wind energy, its potential and generation by wind mills
Unit III: Hydroelectric potential, its utilization & production, Geothermal energy its
potential status and production, Nuclear energy: Status, nuclear raw materials,
nuclear reactors and other classification, Generation of Nuclear power, Nuclear
installations in India and their capacity of generation, Limitations of nuclear
energy, Reprocessing of spent nuclear fuel, Cogeneration of fuel and power,
Energy from tidal and ocean thermal sources, MHD systems.
Unit IV: Fossil and Processed Fuel: Coal its origin and formation, Coal analysis, Coal
classification, Coal preparation, Coal washing and coal blending, Coal
carbonization, Treatment of coal gas and recovery of chemical from coal tar,
Coal gasification, liquid fuel synthesis from coal, CBM.
Unit V: Petroleum crude, Types of crude, emergence of petroleum products as energy,
Gaseous Fuels: Natural gas, Water gas, producer gas, L.P.G., bio- gas, coke oven
gas, blast furnace gas, LNG ,CNG, Gas hydrates ,GTL Technology (gas to
liquid), Biodiesel.

Text Book:
1. Brame J.S.S. and King J.G., Edward Arnold “Fuel Solid, Liquid and Gases” Edward
Arnold, 1967.
References
1. Sukhatme S.P, "Solar Energy - Principles of Thermal Collection and Storage",2nd Ed.,
Tata McGraw- Hill, 1996.

TCH 504: CHEMICAL REACTION ENGINEERING - I


L T P 3 1 0

Unit I : Rate of reaction, Elementary and non-elementary homogeneous reactions,


Molecularity and order of reaction, Thermodynamic formulations of rates,
Mechanism of reaction, Temperature dependency from thermodynamics,
Arrhenius collision and activated complex theories.
Unit II: Integral and differential methods for analyzing kinetic data, Interpretation of
constant volume batch reactor, data for zero, first, second and third order
reactions, Half life period, Irreversible reaction in parallel and series, Auto
catalytic reaction.
Unit III: Interpretation of variable volume batch reactions data for zero, first and second
order reactions, Design equations for batch, plug flow, back mix flow and semi
batch reactors for isothermal, adiabatic homogeneous reaction.
Unit IV: Holding time and space-time for flow system, Design of batch, plug flow and
mixed flow reactors for first and second order single reactions, Optimum reactor
size, Plug flow reactors in series/parallel. Equal and different size of mixed
reactors in series and finding the best system for the given conversion, Recycle
reactor, Design of reactors for multiple reactions, parallel and series reaction,
series-parallel reactions.
Unit V: Temperature and pressure effects for single reaction, Optimal temperature
progression for first order reactions. Residence time distribution of fluid in
vessels, E, F and C curve, Dispersion models, Tanks in series model

Text Book:
1.Levenspiel, O. “Chemical Reaction Engineering”, 3rd Ed. New York John Wiley, 1998
References
1. Fogler, H.S. “Elements of Chemical Reaction Engineering”, 4th Ed. Prentice Hall, 1997.
2. Smith, J. “Chemical Engineering Kinetics “, 3rd Ed. McGraw-Hill. 1990.
TCH 505: INDUSTRIAL POLLUTION AND CONTROL
L T P 3 1 0

Unit I: Introduction: Environment and environmental pollution from chemical process


industries, characterization of emission and effluents, environmental laws and
rules, standards for ambient air, noise emission and effluents
Unit II: Pollution Prevention: Process modification, alternative raw material, recovery of
by co-product from industrial emission effluents, recycle and reuse of waste,
energy recovery and waste utilization. Material and energy balance for pollution
minimization. Water use minimization, Fugitive emission/effluents and leakages
and their control-housekeeping and maintenance.
Unit III: Air Pollution: Sources; Types of air pollutants; Classification of industries and
area. Atmospheric dispersion: Micrometeorology; Lapse rate; Atmospheric
classes; Plume and type of plume; Dispersion models; Ground and elevated
sources with and without reflection; Calculation for plume rise and stack gas
flow rates. Gaseous pollutants: Sources; Emission factors and control technology.
Particulate pollutants: Major sources; Effects; Emission factor and emission
limits; Combustion generated pollutants and control; Particulate emission control
equipment- Design and efficiency of centrifugal collectors, electrostatic
precipitators, bag filters and scrubbers; Vehicular emission control.
Unit IV: Water Pollution: Sources; Pollution laws and limits; Water quality modeling for
streams; Characterization and classification of effluents; Effluent standards;
Pretreatment and primary treatment methods; Physico-chemical methods of
water pollution control; Biological wastewater treatment processes; Advanced
treatment methods; Disinfections; Typical industrial and municipal applications.
Unit V: Noise Pollution: Measurements; Effects; Control methods. Solid waste:
Collection, treatment and disposal. Waste recovery system.

Text Book:
1. Peavy, H.S., Rowe D.R. and Tchobanoglous, G., “Environmental Engineering”, McGraw-
Hill Book Co., New Delhi, 5th Ed., 2003.

References:
1. Metcalf &Eddy, Inc., “Waste Water Engineering-Treatment, Disposal, Reuse”, Mcgraw-
Hill, Inc., 4th Ed., 2003.
2. Nevers, Noel de, “Air Pollution Control Engineering”, McGraw-Hill, Inc.
3. “Pollution Control Acts, Rules and Notifications”, CPCB, Delhi. 1995.
4. Conway R.A. & Ross R.D., “Handbook of Industrial Waste Disposal”, Van-Nostrand
Reinhold, 1980.
4. Kreith F. and Tchobanoglous G., “Handbook of Solid Waste Management”, Mc
Graw Hill, 2nd Ed., 2002.
PCH 501: MASS TRANSFER OPERATIONS LAB-II
L T P 0 0 3

Study of the performance and determination of equilibrium relationships, mass transfer


coefficient, Separation factors of the experiments with gas diffusion, packed bed absorption,
bubble gas absorption, humidification and dehumidification, cooling tower, tray dryers,
crystallization and adsorption.

PBE 505: INDUSTRIAL POLLUTION & CONTROL LABORATORY


L T P 0 0 3
Selected laboratory experiments based on sampling and analysis of air and water samples,
particulate pollutants and control, physico-chemical and biological methods of waste water
treatment

PCH 503: ENERGY RESOURCES LAB


L T P 0 0 3

1. Estimation of net & gross calorific value of coal sample using Bomb Calorimeter
2. Estimation of net calorific value of petroleum sample using Bomb Calorimeter
3. Derivation of kinematic viscosity by Saybolt Viscometer (Universal and Furol)
4. Determination of flash and fire points by Penskey Marten apparatus
5. Estimation of carbon residue
6. Efficiency of solar cell
7. Proximate analysis of Coal
8. Performance of solar water pump
9. Performance of solar regenerator

TCH 601: TRANSPORT PHENOMENA


L T P 3 1 0

Unit I: Introduction to Transport Phenomena, Similarity between momentum, heat and


mass transfer, The continuum hypothesis, Basic laws of fluid motion, Newton’s
second law of motion, principle of balance between momentum, heat and mass
transfer, Principles of conservation of momentum, mass and energy.
Unit II: Momentum Transport Phenomena: Momentum transport in laminar flow:
Newton’s law of viscosity, Science of rheology, Prediction of viscosity and its
dependence on temperature, pressure and composition, Boundary conditions,
Shell balance approach for stress distribution and velocity profiles. Introduction
to time derivatives and vector analysis, Equation of continuity and equation of
motion and their applications in fluid flow problems.
Unit III: Unsteady state momentum transport, Flow near a wall suddenly set in motion,
Momentum transport phenomena in turbulent flow. Definitions of friction
factors, friction factor for flow in tubes, for flow around spheres, for packed bed
column.
Unit IV: Energy Transport Phenomena: Energy transport in laminar flow: Fourier’s law of
heat conduction, Prediction of thermal conductivities and its dependence on
temperature, pressure and composition, Boundary conditions, shell balance
approach. Types of heat sources, Principle of extended surfaces, types of cooling
fans, free and forced convection. Unsteady state heat transport, Unsteady state
heat conduction in solids, heating of semi-infinite slab, heating of finite slab.
Unit V: Mass Transport Phenomena: Definitions of concentration, velocities and mass
fluxes, Fick’s law of diffusion, Prediction of diffusivity and its dependence on
temperature, pressure and composition, Boundary conditions, Shell balance
approach for mass transfer problems, Problems of diffusion with homogeneous
and heterogeneous chemical reaction, Diffusion and chemical reaction in porous
catalyst – the effectiveness factor. The equation of continuity for multicomponent
mixtures.

Text Books
1. Bird, R. B., Stewart, W. E. and Lightfoot, E. N., “Transport Phenomena”, John Wiley, 2nd
Ed,1960.
2. Bannet, C. O. and Myers J. E., “Momentum Heat and Mass Transfer” Tata McGraw Hill,
1973.
3. RS Broadkey and HC Hersey, "Transport Phenomena: A Unified approach", McGraw-
Hill Book, 1988.

Reference Books
1. Beck, W. J. and Muttzall, K.M.K., “Transport Phenomena”, John Wiley, 1975.
2. Loddha, G. S. and Degaleesan T. E. “Transport Phenomena in Liquid Extraction”, Tata
McGraw Hill, 1975.
3. Slattery, J. “Momentum, Energy and Mass Transfer in Continua”, McGraw Hill, 1972.
4. Scissom, L. E. and Pitts, D. R., “Elements of Transport Phenomena”, McGraw Hill, 1972.
5. Theodere, L. “Transport Phenomena for Engineers”, International Textbook Co. 1971.

TCH 602: CHEMICAL TECHNOLOGY – II (INORGANIC)


L T P 2 0 0

Unit I: Chlor-alkali industry: Common salt, Caustic soda and Chlorine, Soda Ash,
Hydrochloric acid.
Unit II: Sulfur Industry: Sulfur and sulfuric acid, Oleum Phosphorus Industry:
Phosphorus, Phosphoric acid and super phosphates
Unit III: Nitrogen Industry: Ammonia, Nitric acid, Urea and other nitrogen fertilizers,
Mixed fertilizers (SSP, TSP, NPK, KAP, DAP, Nitrophosphate) Bio fertilizers.
Unit IV: Industrial Gases: Oxygen, Nitrogen, Hydrogen Inert gases, Syngas, Cement.

References
1. Dryden, C. E. “Outlines of Chemical Technology” (Edited and Revised by M.Gopal
Rao and Sittig .M) East West Press, New Delhi,3rd Ed. 1997.
2. Austin G. T, “Shreve’s Chemical Process Industries”, McGraw Hill, 5th Ed.,1984.
3. Faith, W. L., Keyes, D. B. and Clark, R. L., “Industrial Chemicals” John Wiley, 1975.
4. Kirk and Othmer, "Encyclopaedia of Chemical Technology" Wiley, 2004.
5. Pandey G.N & Shukla.S.D, “Chemical Technology Vol - I” Mc-Graw Hill, 5th Ed.
1996”.

TCH 603: PROCESS DYNAMICS & CONTROL


L T P 3 1 0

Unit I : Introduction to Process control systems, Regulator & Servo control, Feed Forward
& Feed backward control, Negative & Positive Feed back Control, variables &
Physical Elements of a Control system, Physical, Block & Signal Flow Diagram.
Use of Laplace & Inverse Laplace Transformation is study of Process Dynamics.
Unit II: Dynamic Modeling of a Process, Dynamic behavior of First order systems and First
order systems in series. Dynamic behavior of second & higher order system for
various kind of inputs, Linearization of nonlinear system, Transportation &
Transfer Lag.
Unit III: Modes of control action, Controllers & Final control Elements, Reduction of Block
& Signal Flow Diagrams, Closed loop transfer function and response of closed
loop control system for various type of control actions.
Unit IV: Stability analysis, Rouths criterion, Root locus Analysis, Frequency Response
Analysis & Design of Controllers for optimum Performance.
Unit V: Advanced control strategies, cascade control, Feed forward control, Tuning Rules
for Feed Forward & Feed backward control, Ratio control, optimum controller
Tuning, Ziegler Nichol & Cohen Coon settings.
Text Book:
1 D.R. Coughanoowr, “Process system Analysis & Control”, Mc-Graw Hill, New York, 5th
Ed., 1996.

Reference
1. Peter Harriot, “Process Control”. Tata McGraw Hill, 8th Ed., 2000.

TCH 604: CHEMICAL REACTION ENGINEERING - II


L T P 3 1 0

Unit I: Reactor Models : Design equations for batch, continuous and semi batch reactors,
Selectivity and yield. Non-catalytic heterogeneous reactions ; Rate equations for
heterogeneous reactions.
Unit II: Heterogeneous Catalysis: Adsorption isotherms, Mechanism of catalytic
reactions, Physical properties of solid catalysts. Preparation testing and
characterization of catalysts, Catalyst selection, Catalyst poisoning.
Unit III: External Transport Process: Reaction and diffusion within porous catalysts,
Effective diffusivity, Thermal conductivity and effectiveness factor. Reactor
choice for single and multiple reactor system and recycle reactor. Stability of
Reactors: Non - isothermal design of ideal reactor, Hot spot in tubular reactor,
Steady state multiplicity and effect of operating variables on the stability of
C.S.T.R.
Unit IV: Reactor Design: Progressive conversion and un-reacted core model,
Determination of rate controlling step, application to design, fluidized bed
reactions Design of solid catalytic reactor, batch, CSTR and tubular reactor.
Design of fixed bed and fluidized bed reactors.
Unit V: Non elementary reactions and reactor design, biochemical reaction system,
Reactors for Enzyme fermentation, Microbial fermentation, polymerization.

Text Book:
1.Levenspiel, O., “Chemical Reaction Engineering”, John Wiley, New York, 3rd Ed., 1998.
References
1. Fogler, H.S. “Elements of Chemical Reaction Engineering”, Prentice Hall, 4th Ed. 1997.
2. Smith, J. “Chemical Engineering Kinetics “, McGraw-Hill, 3rd Ed., 1990.

TCH 605: PROCESS MODELING & SIMULATION


L T P 3 1 0

Unit I: Introduction to mathematical modeling; Advantages and limitations of models


and applications of process models of stand-alone unit operations and unit
processes; Classification of models – Simple vs. rigorous, Lumped parameter vs.
distributed parameter; Steady state vs. dynamic, Transport phenomena based vs.
Statistical; Concept of degree of freedom analysis.
Unit II: Simple examples of process models; Models giving rise to nonlinear algebraic
equation (NAE) systems, - steady state models of flash vessels, equilibrium
staged processes distillation columns, absorbers, strippers, CSTR, heat
exchangers, etc.; Review of solution procedures and available numerical software
libraries.
Unit III: Steady state models giving rise to differential algebraic equation (DAE) systems;
Rate based approaches for staged processes; Modeling of differential contactors
– distributed parameter models of packed beds; Packed bed reactors; Modeling of
reactive separation processes; Review of solution strategies for Differential
Algebraic Equations (DAEs), Partial Differential Equations (PDEs), and
available numerical software libraries.
Unit IV: Unsteady state (time dependent) models and their applications; Simple dynamic
models of Batch reactors, Adsorption columns, Multistage separation systems;
Model reduction through orthogonal collocation; Review of solution techniques
and available numerical software libraries.
Unit V: Introduction to flow sheet simulation; Sequential modular approach; Equation
oriented approach; artitioning and tearing; Recycle convergence methods;
Review of thermodynamic procedures and physical property data banks.

Text Book:
1. Luyben W.L., “Process Modeling, Simulation, and Control for Chemical Engineering”,
Wiley.
Reference
1. Denn, M.M., “Process Modelling”, Wiley, New York, 1990.
2. Hussain Asghar, “Chemical Process Simulation”, Wiley Eastern Ltd., New Delhi, 1986.
3. Holland, C.D. and Liapis, A.I. , “Computer Methods for Solving Dynamic Separation
Problems”, McGraw Hill, 1983.
4. Holland, C.D., “Fundamentals of Modelling Separation Processes”, Prentice Hall, 1975.
5. Walas, S.M. “Modelling with Differential Equations in Chemical Engineering”,
Butterworth, 1991.
6. Davis, M.E. “Numerical Methods and Modelling for Chemical Engineers”, Wiley, New
York, 1984.

TCH 606: PROCESS INSTRUMENTATION

L T P 2 0 0

Unit I: Importance of measuring of Instruments in Process Control, Classification of


Instruments, Elements of an Instruments, Static & Dynamic Characterization of
Instruments, Errors in measurements & Error Analysis, Selection of instrument
for a particular Measurement, transducers.
Unit II: Measurement of Temperature: Thermocouples, Resistance Thermometer,
Expansion Thermometers, Pyrometers.
Unit III: Measurement of Pressure & Vacuum, Hydrostatic type, Elastic Element type,
Electrical Type and other type of instruments like MacLeod Gauge,
Thermocouple gauge, Knudson Gauge, Ionization Gauge.
Unit IV: Instruments for Measurement of Flow rate, level & Viscosity, Variable Area &
variable head flow meters, Volumetric and Mass flow rate meters, Linear
velocity measurement systems, Anemometers, Pressure type, Resistance &
Capacitance type, Sonic & Ultrasonic, Thermal type Level meters. Viscometers:
Redwood, Saybolt, Engler, Cup & Cone type, Rheo & other types of
viscometers,

Text Book:
1. Eckman, D.P., “Industrial Instrumentation”, Wiley Eastern Ltd., New York 1990.

References
1. Jain, R.K., “Mechanical and Industrial Measurements”, Khanna Publishers, Delhi, 1st
Ed., 2000.

PCH 602: CHEMICAL TECHNOLOGY LAB


L T P 0 0 2

Preparation and Quality evaluation of following items:-


1. Cement Paint..
2. Dry Distemper.
3. Oil bound Distemper.
4. Plastic Emulsion Paint.
5. Polystyrene by Bulk Polymerization Technique.
6. PMMA by Bulk Polymerization Technique.
7. Transparent Soaps
8. Powdered Detergent.
9. Liquid Detergent
10. Washing Soap
PCH604: CHEMICAL REACTION ENGINEERING LAB
L T P 0 0 3

1. To determine the relative rates of reaction of iodide ion with hydrogen peroxide at room
temperature using different concentrations of the iodide ion.
2. To separate Organic Compounds by Paper Chromatography.
3. To study the effect of temperature, concentration of the reactants and a catalyst on the rate
of chemical reaction
4. To study the activity results or oxidation-reduction replacement reaction.
5. To purify water by ion -exchange.
6. To determine the order and rate constant of esterification reaction at room temperature.
7. To determine the order and rate constant of saponification reaction at room temperature.
8. To study the residence time distribution (R.T.D.) in a stirred tank reactor.
9. To study the residence time distribution (R.T.D.) in a plug flow reactor.
10. To study the decomposition of calcium carbonate
11. To determine the energy of activation of a given chemical reaction.

PCH 603: PROCESS DYNAMICS AND INSTRUMENTATION LAB


L T P 0 0 3

1. To study the response, time constant of thermocouple/ Bimetallic thermometer.


2. To study the response of a liquid level tank system
3. To study the response of a two tank non-interacting system
4. To study the response of a two tank interacting system.
5. To study the response of a stirred tank heater system
6. To study the characteristics of an on-off controller.
7. To study the characteristics of a PI/PID pneumatic / electronic controller.
8. To study the performance of a closed loop control system containing controller,
final control element, measuring element.
9. Calibration of temperature and pressure measuring instruments
10. Analysis of solution by UV/VIS spectrophotometer
11. Calibration of thermocouple/Bimetallic thermocouple/Resistance thermocouple.
12. Calibration of Pressure gauge/ Pnuematic pressure recorder/ Differential pressure
recorder.
13. Calibration of Orificemeter/ Venturimeter / Rotameter/ Gas flow meter.
14. Estimation of viscosity by Redwood/ Saybolt/ Ostwald viscometer.
15. Calibration of pH meter.
16. Calibration of Conductivity meter.

TCH 701: PROCESS EQUIPMENT DESIGN


L T P 3 1 0

Unit I: Introduction to various mechanical properties of materials to be used as material


of construction, resistance of metals to corrosion under varying conditions of
temperature and pressure etc. Application and use of various codes and standards
in design.
Unit II: Design of non-pressure storage vessel, tall vertical vessels, unfired pressure
vessels with internal pressure ,Design of unfired pressure vessels with external
pressures, end closures, flat plates, domed ends, torispherical, ellipsoidal,
hemispherical and conical ends. Design of nozzles, openings and
reinforcements, Bolts, flanges, gaskets .
Unit III: Bolted flanges, pipe line design and process design of a few equipments like heat
exchangers, Evaporators, Distillation columns, Absorbers, Reactors and Dryers .
Unit IV: Mechanical design of selected process equipments such as heat exchangers,
Evaporators, Distillation columns, Absorbers, Reactors and Dryers and
Crystallizers; Use of softwares (Chem CAD and Pro Sim) for design of
equipments.
Unit V: Liquid storage tanks: Storage tank codes; Classification; Design of shell, bottom
plates, self supported, and column supported roofs.

Text Book:
1. Coulson, J. M. and Richardson J. F. “Chemical Engineering, Vol. 6” Pargamon Press.
1989.
Reference
1. Peters Max. S., Timmerhaus Klaus D.and Ronald E West “Plant Design and Economics
for Chemical Engineers”, 5th Ed. McGraw Hill, 2003.
2. Brownel and Young, “Process Equipment Design ”, Wiley, 1968.
3. Indian and American Codes Used in Designing of equipments (TEMA and IS Codes)
4. Evans, F. L., “Equipment Design Handbook”, Gulf Publishing Company, 1979.

Professional Electives

Professional Elective-1*
L T P 3 1 0

TCH 711: NON CONVENTIONAL ENERGY RESOURCES


L T P 3 1 0

Unit I: Introduction to Energy Sources: Renewable and non-renewable energy sources,


energy consumption as a measure of Nation's development; strategy for meeting
the future energy requirements Global and National scenarios, Prospects of
renewable energy sources.
Solar Energy : Solar radiation - beam and diffuse radiation, solar constant, earth
sun angles, attenuation and measurement of solar radiation, local solar time,
derived solar angles, sunrise, sunset and day length. flat plate
collectors, concentrating collectors, Solar air heaters-types, solar driers,
storage of solar energy-thermal storage, solar pond , solar water
heaters, solar distillation, solar still, solar cooker, solar heating & cooling
of buildings, photo voltaics - solar cells & its applications
Unit II: Wind Energy : Principle of wind energy conversion; Basic components of wind
energy conversion systems; wind mill components, various types and their
constructional features; design considerations of horizontal and vertical
axis wind machines: analysis of aerodynamic forces acting on wind mill
blades and estimation of power output; wind data and site selection
considerations.
Energy from Biomass: Biomass conversion technologies, Biogas generation
plants, classification, advantages and disadvantages, constructional details,
site selection, digester design consideration, filling a digester for
starting, maintaining biogas production, Fuel properties of bio gas,
utilization of biogas.
Unit III: Geothermal Energy: Estimation and nature of geothermal energy, geothermal
sources and resources like hydrothermal, geo-pressured hot dry rock, magma.
advantages, disadvantages and application of geothermal energy,
prospects of geothermal energy in India
Energy from the ocean: Ocean Thermal Electric Conversion (OTEC) systems
like open cycle, closed cycle, Hybrid cycle, prospects of OTEC in India.
Energy from tides, basic principle of tidal power, single basin and
double basin tidal power plants, advantages, limitation and scope of
tidal energy.
Unit IV: Nuclear Fusion Energy: Introduction, nuclear fission and nuclear fusion.
Requirements for nuclear fusion. Plasma confinement - magnetic confinement
and inertial confinement. Basic Tokamak reactor, laser fusion reactor.
Advantages of nuclear fusion. Fusion hybrid and cold fusion.
Fuel Cells: Introduction, Design principle and operation of fuel cell, Types of
fuel cells, conversion efficiency of fuel cell, application of fuel cells.
Unit V: Hydrogen Energy: Introduction, Hydrogen Production methods, Hydrogen
storage, hydrogen transportation, utilization of hydrogen gas, hydrogen as
alternative fuel for vehicles. Energy Management: Energy economics, energy
conservation, energy audit, general concept of total energy system, scope of
alternative energy system in India.
Reference Books:
1. Non-conventional energy sources by G.D. Rai, Khanna Publishers
2. Solar Energy: Fundamentals and Applications by H.P. Garg & Jai Prakash, Tata
McGraw Hill
3. Solar Energy: Principles of Thermal Collection and Storage by S,P Sukhatme,
Tata McGraw Hill
4. Alternative Energy Sources by B.L. Singhal Tech Max Publication
5. Non Conventional Energy Resources by S.Hasan Saeed and D.K.Sharma
6. Fuel Cells by Bockris and Srinivasan; McGraw Hill

TCH 712: POLYMER SCIENCE AND TECHNOLOGY

Unit I: Classification of polymers: Natural and synthetic polymers; Thermosets and


thermoplasts; Copolymers; Terpolymers; Degradable and non-degradable
polymers.
Addition polymerization; Condensation polymerization; Ring opening
polymerization; Copolymerization; Polymerization by coordination catalyst;
Molecular weight distribution of polymers.
Unit II: Manufacturing processes of important polymers: Plastics-polyethylene;
polypropylene, polyvinyl chloride and copolymers, polystyrene; phenol-
formaldehyde, epoxides; urethane; teflon; Rubbers and elastomers; Fibres -
cellulosic (rayon), polyamides (6;6 Nylon), polyesters (Dacron), acrylic;
Polymeric oils. Micro-structure of polymer chains: Configuration and
conformation; Simple and hindered rotation; End-to-end distances;
Unit III: Crystallinity and melting; Glass transition temperature; Physical states of
polymers and mode of motion of polymer chains; Measurement of viscosity;
Cohesive energy density; Compatibility and solubility parameters; Polymer
additives, blends and composites. Flow properties of polymers: Bulk
deformation, elongational and shear flow; Non-Newtonian flow.
Unit IV: Polymer fabrication techniques: Formation of flat sheets and films; Laminations;
Foam formation; Extrusion, injection molding, blow molding, compression and
transfer molding; Spinning of fibres
Unit V: Mechanical properties of polymers: Rheology of polymers; Rubber elasticity;
Visco-elasticity; Creep and stress relaxation; Dynamic behavior; Stress and
fracture of rubber and glassy polymers. Polymer degradation. Conducting
polymers; Smart polymers.
Ecology and environmental aspects of polymer industries.

Text Book:
1. Fried, J.R., “Polymer Science and Technology”, Prentice Hall, Inc, 2nd Ed., 2003.

References
1. McCrum, N.G., Buckley, C.P. and Bucknall, C.B., “Principles of Polymer Engineering”,
Oxford University Press, 2nd Ed., 2009.
2. Tadmore, , and Gogvs, C.G., “Principles of Polymer Processing” John Wily & Sons.
3. Billmeyer, F.W., “Text Book of Polymer Science”, John Wiley & Sons, 3rd Ed., 2002.

TCH 713: FERTILIZER TECHNOLOGY

Unit I: Introduction to chemical fertilizers: Chemical inorganic Fertilizers and Organic


manures. Types of fertilizer-, Mixed, complex and granulated, plant nutrients.
Unit II: Processes for raw materials: Processes for manufacture of ammonia, nitric acid,
phosphoric acid and
Unit III: Nitrogenous and potassic fertilizers: Processes for urea and di-ammonium
phosphite. Recovery of Potassium salts processes for ammonia chloride and
ammonium phosphate.
Unit IV: Complex fertilizers: Processes for nitro - Phosphorous and complex NPK
fertilizers, liquid fertilizers.
Unit V: Phosphatic fertilizers and indian fertilizer industry: Single and Triple super
phosphate, bio-fertilizer. Fertilizer Industry in India.

Text Books:
1. Strelizoff, "Technology and Manufacture of Ammonia", Wiley, 2nd Ed., 1981.
2. Carpentire, L. J., "New Developments in Phosphate Fertilizer Technology", Elsevier,
1971.
3. Pozin, M. E., "Fertilizer Manufacture", MIR Publishers, Moscow, 1986.
4. A. V. Slack, "Phosphoric Acid", Marcell Dekkar, 2nd Ed., 1968

References:
"Handbook on Fertilizer Technology", Fertilizer Association of India, near JNU, New Delhi
1992

Professional Elective-II*
L T P 3 1 0

TCH 721: SAFETY AND HAZARD ANALYSIS

Unit I: History of safety movement; Development of safety programmes in process


industry.
Accident causation: Heinrich-Domino theory; Human error model; Petersen’s
accident/ incident model; Epidemiological models; System models; Multiple
causation.
Unit II: Systems safety management: Management task; Managerial roles and skills;
Management by objective.
Unit III: Hazard: Identification; Occupational hazard; Preliminary hazard analysis; Hazard
and operability review (HAZOP) Hazard control: Engineering and management
controls; Fault tree analysis; Risk analysis and management.
Unit IV: Fire prevention and protection: Chemistry of fire; Production of fire; Fire
development; Severity and duration; Effect of enclosure and heat transfer.
Unit V: Industrial hygiene; Routes of entry of foreign substance; Long term medical
disorders and epidemiology; Stress and the workplace ; Industrial noise;
Hazardous waste. Case studies of safety and hazard assessment in different
industries; Disaster management planning; Insurance tariffs in hazardous
industries; Design for safety, maintenance and fault diagnosis

Text Book:
1. Crowl, D.A. and Louvar, J.F., “Chemical Process Safety: Fundamentals with
Applications”, Prentice Hall, Inc, 2nd Ed., 2010
References
1. Wills, G.L., “Safety in Process”,
2. Lees, F.P., “Loss Prevention in Process Industries, Volume I & II”, Butterworth
Heinemann. 2nd Ed., 1995.
3. Pandey, C.G., “Hazards in Chemical Units: A Study”, Oxford IBH Publishing Co., New
Delhi.

TCH 722: FOOD TECHNOLOGY

Unit I: Food process engineering fundamentals: Fundamentals of food process


engineering, application of quantitative methods of material and energy balance
in food engineering practice.
Unit II: Unit operations in food industries: Fluid flow, thermal process calculations,
refrigeration, evaporation and dehydration operations in food processing.
Unit III: Food canning technology: Fundamentals of food canning technology. Heat
sterilization of canned food, containers: metal, glass and flexible packaging.
Canning procedures for fruits, vegetables, meats, poultry marine products.
Unit IV: Mechanical operations in food processing: Conversion operations, Size reduction
and screening of solids, mixing and emulsification and membrane separation,
centrifugation, extraction.
Unit V: Food biotechnology: Food Biotechnology, Dairy and cereal products, Beverages
and food ingredients, High fructose corn syrup, Single Cell protein.

Text Books:
1. R.T. Toledo, "Fundamentals of Food Process Engineering", AVI publishing Co., 1980.
2. J. G. Bernan, J. R. Butters, N. D. Cowell and A.E.V.Lilley, "Food Engineering
Operations", Applied Science, 2nd Ed., 1976.
3. Angold, R., Beech, G. and Taggart, J." Food Biotechnology", Cambridge University
Press, 1989

REFERENCES:
1. Jackson, J. M. and Shinn, B. M., "Fundamentals of Food Canning Technology" AVI
Publishing Co.,1978.
2. Briggs and Galloway, "Nutrition and Physical Fitness", 11th Ed., Holt Rinehart
Winston, 1984.

TCH 723: HAZARDOUS WASTE MANAGEMENT

Unit1: Characterization: Introduction to Hazardous wastes, Definition of Hazardous


waste, The magnitude of the problem. Characterization of industrial wastes;
hazardous and non-hazardous wastes. Waste disposal and management laws and
guidelines.
Unit2: Non-hazardous Waste Management: Non-hazardous industrial wastes-treatment,
disposal, utilization and management. Thermal gasification, combustion and
landfill.
Unit3: Hazardous Waste Management: Hazardous wastes – handling, storage.
Treatment and disposal methods: Physico-chemical and biological, stabilization
and solidification, thermal methods, land disposal, Waste site remediation and
clean-up technologies. Wastes from electroplating, lead batteries/cells, soldering
and electro winning operations, wastes from refineries and petrochemical units.
Unit4: Risk assessment, Environmental legislation, Dose-response assessment, exposure
assement, Waste minimisation and Value-extraction from the wastes. Medical /
biomedical and infectious waste management; Transportation of hazardous
waste; Ground water contamination.
Unit5: Case Studies: Case studies of a few real scenarios of hazardous waste
management in industries.

Text Books:
1. Shah K. L., “Basics of Solid and Hazardous Waste Management Techniques”, Prentice
Hall.1999
2. Tedder D. W. & Pohland F. G. (Editors), “Emerging Technologies in Hazardous Waste
Management”, ACS.1990

References:
1. Conway R. A. & Ross R. D., “Handbook of Industrial Waste Disposal”, Van-Nostrand
Reinhold.1980
2. Side G. W., “Hazardous Materials and Hazardous Waste Management”, John
Wiley,1993
1. Pichtel J., “Waste Management Practices: Municipal, Hazardous and Industrial”,
CRC.2005

Professional Elective-III*
L T P 3 1 0

TCH 731: ADVANCED SEPARATION PROCESS

Unit I: Principle of membrane separations process; Classification, characterization and


preparation of membrane. Types and choice of membranes, their merits,
commercial, pilot plant and laboratory membrane permeators. Dialysis, Ultra
Filtration and Economics of Membrane operations
Unit II: Reverse osmosis, micro-filtration, nano-filtration and dialysis; Analysis and
modeling of membrane separation processes; Membrane modules and
application; Ion selective membranes and their application in electro-dialysis;
Pervaporation and gas separation using membranes; Electrophorosis; Liquid
membranes and its industrial applications.
Unit III: Foam and bubble separation: Principle; Classification; Separation techniques;
Column operations. Zone melting, zone refining and zone leveling. Pressure and
temperature swing adsorption.
Unit IV: Cryogenic separation; Super- critical extraction. Parametric pumping: Batch,
continuous and semi-continuous pumping; Thermal, pH and heatless parametric
pumping. Multicomponent separation.

Text Book:
1. Seader, J.D, and Henley E.J., “Separation Process Principles”, John Wiley & Sons, Inc.
Reference
2. King, C.J., “Separation Processes”, McGraw-Hill, Inc.
3. H. M. Schoen, " New Chemical Engineering Separation Techniques", Inter Science
Publications, New York, 1972.
4. C. Loeb and R. E. Lacey, "Industrial Processing with Membranes", Wiley Inter
Science, 1972.

TCH 732: INTELLECTUAL PROPERTY RIGHTS

Unit I: Introduction: Nature of Intellectual Property: Patents, Designs, Trademarks and


Copyright. Process of Patenting and Development: technological research,
innovation, patenting, development. History - General Agreement on Trade and
Tariff (GATT).
Indian Position Vs WTO and Strategies - Indian IPR legislations - commitments
to WTO-Patent Ordinance and the Bill - Draft of a national Intellectual Property
Policy - Present against unfair competition
Unit II: International Scenario: International cooperation on Intellectual Property.
Procedure for grants of patents, Patenting under PCT.
Unit III: Patent Rights: Scope of Patent Rights. Licensing and transfer of technology.
Patent information and databases. Geographical Indications.
Unit IV: New Developments in IPR: Administration of Patent System. New developments
in IPR; IPR of Biological Systems, Computer Softwares etc. Traditional
knowledge Case Studies, IPR and IITs.

Text Books:
1. Subbaram N.R. " Handbook of Indian Patent Law and Practice ", S. Viswanathan
(Printers and Publishers) Pvt. Ltd., 1998
2. T. Ramappa, “Intellectual Property Rights Under WTO”, S. Chand.
3. Halbert, “Resisting Intellectual Property”, Taylor & Francis Ltd, 2007

TCH 733: FLUIDIZATION ENGINEERING

Unit I: Introduction: Importance of fluidization in process industry, comparison of fluidized


beds with other modes of contacting, advantages and disadvantages, industrial applications.
Fluidization: Fixed bed of particles of one and mixed sizes, fluidization with and without
carryover of particles, minimum fluidization, terminal velocity of particles, pneumatic
transport of solids.
UnitII: Bubble Behavior and Bed Properties: Single rising bubble models, wake region and
solids within bubbles, interaction and coalescence of bubbles, bubble formation, slug flow.
Unit III: Bubbling Fluidized Beds: Emulsion phase, gas flow, bubble properties, physical
and flow models. Entrainment and Elutriation From Fluidized Beds: Free boards behavior,
gas outlet location, entertainment from tall and short vessels.
UnitIV: High Velocity Fluidization: Turbulent fluidized beds, fast fluidization, pressure
drop in turbulent and fast fluidization. Spouted Beds: Hydrodynamics and processing in
spouted beds.
UnitV: Circulation Systems: Circuits for the circulation of solids, pressure balance, flow of
gas-solid mixtures in down-comers, flow in pneumatic transport lines. Design for Physical
Operations: Design of single stage and multistage systems, heat and mass transfer, fluid bed
drier.

Text Books:
1.Kunii D. and Levenspiel O., “Fluidization Engineering”, 2nd Ed., Butterworth-
Heinemann,1991.
2.Davidson D. and Harrison J. F., “Fluidization Engineering”, 2nd Ed., Academic
Press,1992.
References:
1. Yang W. C., “Handbook of Fluidization and Fluid Particle Systems”, 3rd Ed.
Open Electives
Open Elective-III*
L T P 3 1 0

TOE 011: PROCESS UTILITIES AND SAFETY


Unit I: Various process utilities, their role and importance in chemical plants. Water
Sources: Sources of water and their characteristics; Treatment storage and
distribution of water; water for use in boilers, cooling purposes, drinking and
process; Reuse and conservation of water; Water resource management.
Unit II: Steam Generation and Utilization: Steam generation and its application in
chemical process plants, distribution and utilization; Design of efficient steam
heating systems; steam economy, Steam condensers and condensate utilization
Expansion joints, flash tank design, steam traps their characteristics, selection
and application, waste heat utilization; Lagging, selection and thickness.
Selection and sizing of boilers; waste heat boilers.
Unit III: Compressors, blowers and Vacuum Pumps: Compressors, blowers and vacuum
pumps and their performance characteristics; Methods of developing vacuum and
their limitations, material handling under vacuum, Piping systems; Lubrication
and oil removal in compressors and pumps. Air filters, Air and gas leakage. Inert
gas systems, compressed air for process, Instrument air.
Insulation: Importance of insulation for meeting the process requirement,
insulation materials and their effect on various material of equipment piping,
fitting and valves etc. insulation for high intermediate, low and sub zero
temperatures, including cryogenic insulation.
Unit IV: Elements of Safety: Elements of safety, safety and site selection; Plant layout and
unit plot planning; Definition of risk and hazard, Identification and assessment of
the hazards, distinction between hazards and risk, Hazard operability (HAZOP)
hazard analysis (HAZAN);
Assessment of the risk, fault tree, event tree, scope of risk assessment; Control of
hazards, controlling toxic chemicals and controlling flammable materials.
Prevention of losses: Prevention of losses, Pressure relief, Provision of fire
fighting equipments, Technology selection and transfer, Choosing the right
process.
Unit V: Control of Process: Control of process, Prevention of hazardous deviation in
process variables, e.g. pressure, temperature flow by provision of automatic
control systems- interlocks, alarms, trips together with good operating practices
and management.
Regulations: Regulations and legislation, Role of government role, risk
management routines and tackling disaster.

Text Books:
1. Nordell, Eskel, “Water Treatment for Industrial and Other Uses”, Reinhold Publishing
Corporation, New York, 1961.
2. Crowl, D.A. and Louvar, J.F. “Chemical Process Safety: Fundamentals with
Applications”. New Jersey: Prentice-Hall, 1989.
3. Goodall, P. M., “The Efficient Use Of Steam” IPC Science and Technology, 1980.
4. Lees, F. P., “Loss Prevention in Process Industries 3 volume set” Butterwort -
Heinemann, Oxford, 1996.
TOE 012: INTELLECTUAL PROPERTY RIGHTS

Unit I: Introduction: Nature of Intellectual Property: Patents, Designs, Trademarks and


Copyright. Process of Patenting and Development: technological research, innovation,
patenting, development. History - General Agreement on Trade and Tariff (GATT).
Indian Position Vs WTO and Strategies - Indian IPR legislations - commitments to WTO-
Patent Ordinance and the Bill - Draft of a national Intellectual Property Policy - Present
against unfair competition
Unit II: International Scenario: International cooperation on Intellectual Property.
Procedure for grants of patents, Patenting under PCT.
Unit III: Patent Rights: Scope of Patent Rights. Licensing and transfer of technology.
Patent information and databases. Geographical Indications.
Unit IV: New Developments in IPR: Administration of Patent System. New developments
in IPR; IPR of Biological Systems, Computer Softwares etc. Traditional knowledge Case
Studies, IPR and IITs.

Text Books:
1. Subbaram N.R. " Handbook of Indian Patent Law and Practice ", S. Viswanathan
(Printers and Publishers) Pvt. Ltd., 1998
2. T. Ramappa, “Intellectual Property Rights Under WTO”, S. Chand.
3. Halbert, “Resisting Intellectual Property”, Taylor & Francis Ltd, 2007

TOE 013: NON CONVENTIONAL ENERGY RESOURCES

TOE 014: BIOINFORMATICS

L T P 3 1 0
Unit I: Primary and secondary databases. Specialized sequence databases of EST, TFB Sites,
SNPs, gene expression. Pfam, PROSITE, BLOCK( Secondary databases). Data retrieval
with ENTREZ, SRS, DBGET
Unit II: Principles of DNA sequencing (chemical chain termination, Dideoxy chain termination
method, Automatic sequencer). RNA sequencing . Protein sequencing ( Edmand
degradation method)
Unit III: Sequence alignment (pairwise and multiple, global and local). Sequence alignment
algorithm (FASTA, BLAST, Needleman and Wunsch, Smith Waterman ). Database
similarity searches (BLAST, FASTA and PSI BLAST). Amino acid substitution matrices
(PAM, BLOSUM)
Unit IV: Protein structure prediction ( Chou Fasman method) : Secondary and tertiary structures.
Homology Modelling, ORF prediction, Gene prediction, Micro array data analysis.
Profiles and motifs.
Unit V: Structure visualization methods ( RASMOL, CHIME etc.) . Protein Structure alignment
and analysis. Application of Bioinformatics in drug discovery and drug designing.

Text books:
1. Ghosh and Mallick, “Bioinformatics : Principles and applications”, Oxford University
Press)
2. Andreas D Boxevanis, “Bioinformatics” Wiley Interscience
3. Dan e. Krane, “Fundamental concept of bioinformatics”
Reference books:
1. Attwood and Parry Smith, “Introduction to bioinformatics” Pierson education Publication.
2. Westhead, Parish and Tweman, “Instant notes in Bioinformatics” Bios scientific
publishers.

TCH 801: PILOT PLANTS AND SCALE-UP METHODS IN


CHEMICAL ENGINEERING
L T P 3 1 0
Unit I: Introduction to pilot plants and models: Introduction to pilot plants and Models,
Process Development, Process study, the principle of similarity and similarity
criteria, dimensional analysis and its application in scaling-up or scaling-down
the chemical process plant.
Unit II: Mathematical equations: Mathematical Equations representing the Mechanical,
Thermal, Diffusional and chemical processes and derivation of the
dimensionless groups from these differential equations. Rate of chemical
reaction of Homogeneous and Heterogeneous chemical reactions.
Unit III: The regime concept: The Regime Concept, Laupichleir's study of catalytic
water gas reaction, chemical dynamic and mixed regime, Effect of temperature
on physical and chemical reactions. Similarly criteria for the principle types of
regime and scale equations.
Unit IV: Scale up of heat transfer equipments: Scale-up methods for Heat- Transfer
equipment e.g.-Heat Exchangers, Steam or vapour Heaters, Evaporators,
Condensers and Coolers.
Unit V: Scale-up of miscellaneous equipment: Scale-up methods for mixing equipment
and other miscellaneous equipment used in chemical process industries.

Text Book:
1. R.E. Johnstone and M.W. Thring, "Pilot Plants, Models and Scale-up methods in
Chemical Engineering ",McGraw Hill Book Company, New York,1957.

References
1. Bisio & Kabel, "Scale-up in Chemical Industry".
2. D.G. Jordan, "Chemical Process Development", Vol. I & II, Interscience Publishers,
1988.

PROFESSIONAL ELECTIVES

Professional Elective IV*


L T P 3 1 0

TCH 811: FUNDAMENTALS OF BIOCHEMICAL ENGINEERING

Unit I: Introduction to microbiology and biochemistry; Classification and characteristics


of microorganism; Essential chemicals of life- lipids, sugars and polysaccharides,
RNA and DNA, amino acids and proteins; Cell metabolism; Regulation;
Stoichiometry; End products. Cell growth kinetics; Product formation kinetics.
Unit II: Transport phenomena in cellular systems; Oxygen transfer rates; Mass transfer
coefficient and interfacial area; Mechanical agitation and power requirement.
Unit III: Thermal death kinetics; Media and air sterilization. Enzymes and their
classification; Enzyme kinetics; Immobilization of enzymes and whole cells;
Immobilized enzyme kinetics.
Unit IV: Bioreactors: Type, design, operation and scale-up; Instrumentation and control.
Down-stream processing
Unit V: Industrial production of ethanol, anti-biotics, single cell protein. Bioleaching.

Text Book
1. Bailey, J.E. and Ollis, D.F., “Biochemical Engineering Fundamentals” by, McGraw Hill
Book Co., 2nd Ed., 1986.
References
1. Shuler and Kargi, F., “Bioprocess Engineering” Prentice Hall, 2nd Ed. 2002.
2. Lee, J.M., “Biochemical Engineering”, Prentice Hall, 2nd Ed., 1992.

TCH 812: PETROLEUM REFINING TECHNOLOGY

Unit I: Petroleum Exploration: Production and Refining of Crude oils; Crude oils:
Chemistry and composition (Characteristics and constituents of crude oils,
Classification of crude oils).
Unit II: Quality Control of Petroleum Products: Classification of laboratory tests,
distillation, vapour pressure, flash and fire points, octane number, performance
number, cetane number, aniline point, viscosity index, calorific value, smoke
point, char value, viscosity, viscosity index, penetration tests, cloud and pour
points, drop point of grease, melting and settling points of wax, softening point
of Bitumen, induction period of gasoline, thermal stability of jet fuels, gum
content, Total Sulphur, Acidity and Alkalinity, Copper Strip Corrosion Test,
Silver – Strip Corrosion Test for ATF, Ash, Carbon Residue (Conradson
method, Ramsbottom method) Colour, Density and Specific gravity, Refractive
index of hydrocarbon liquids, water separation index (modified) (WSIM),
ductility.
Unit III: Petroleum Products: Composition, Properties & Specification of LPG,
Naphthas, motor spirit, Kerosine, Aviation Turbine Fuels, Diesel Fuels, Fuel
Oils, Petroleum Hydrocarbon Solvents, Lubricating oils (automotive engine
oils, industrial lubricating oils electrical insulating oils, Jute Batching oils,
white oils, steam turbine oils, metal working oils, etc.) Petroleum Waxes
Bitumens, Petroleum coke. Crude Oil Distillation, Desalting of crude oils,
Atmospheric distillation of crude oil, Vacuum distillation of atmospheric
residue.
Thermal Conversion Process: Thermal Cracking Reactions, Thermal Cracking,
Visbreaking, (Conventional Visbreaking and Soaker Visbreaking) Coking
(Delayed Coking, Fluid Coking, Flexicoking), Calcination of Green Coke.
Unit IV: Catalytic Converson Process: Fluid catalytic cracking; Catalytic reforming;
Hydrocracking Catalytic Alkylation, Catalytic Isomerization; Catalytic
Polymerization. Finishing Process, Hydrogen sulphide removal processes;
Sulphur conversion processes; Sweetening processes (Caustic treatment,
Solutizer process; Doctor treating process; Copper chloride sweetening,;
Hypochlorite sweetening ;Air and inhibitor treating process; Merox processes;
Sulphuric acid treatment; Clay treatment); Solvent extraction processes
(Edeleanu process, Udex process, Sulfolane process), Hydrotreating processes.
Unit V: Lube Oil Manufacturing Process: Evaluation of crude oils for lube oil base
stocks, Vacuum distillation, Solvent deasphalting Solvent extraction of lube oil
fractions (Furfural, NMP and Phenol), Solvent dewaxing, Hydrofinshing,
Manufacture of petroleum waxes (Wax sweating, Solvent deoiling)
Manufacture of Bitumens: Selection of crude oil, Methods of manufacture of
bitumens, (Distillation, Solvent precipitation, Air blowing).

Text Book:
1. Nelson, W.L., “Petroleum Refining Engineering”, McGraw Hill, 4th Ed., 1958,
References
1. Mall, I D , “Petrochemical Process Technology”, McMillan India, 4th Ed., 1998.
2. Sarkar, G.N., “Advance Petroleum Refining”, Oscar Publication, 4th Ed., 1998.

TCH 813: OIL AND FAT TECHNOLOGY

Unit I: Industrial oils and fats: Raw material properties: Sources, composition,
properties, classification and analysis of oils and fats.
Unit II: Recovery and refining of oils from raw materials: Extraction of oils,
Mechanical and solvent extraction methods. Refining and hydrogenation
of oils, Edible oil processing.
Unit III: Manufacture of fatty acids, glycerin and soap: Fat splitting and hydrolysis.
Manufacture of glycerine and fatty acids. Soap manufacture.
Unit IV: Technology of oil based detergents: Oil based raw material for
detergents. Detergents manufacturing processes. Oleo-Chemicals for
other applications.
Unit V: Modern development in detergents: Indian oils, fats and detergents
industries. Alpha Olefin from natural oils and conversion to sulphonate.
Fatty alchohols and their sulphates form natural oils.

TEXT BOOKS:
1. D.Swern, "Baileys Industrial Oils and Fat Products",4th Edn., Vol. I & II, Wiley,
1982.
2. Edgar Woollatt, "The Manufacture of Soaps, Other Detergents and Glycerine", 1st
Edn., Ellis Horwood,1985.

Professional Elective V*
L T P 3 1 0

TCH 821: FERMENTATION TECHNOLOGY


Unit-I: Introduction and scope of microbial processes. Alcoholic fermentation.
Glycerol fermentation, Baker’s yeast production.
Unit-II: Beer production, wine production, vinegar production.
Unit-III: Microbial production of organic acids, biopolymers production.
Unit-IV: Antibiotics production: Penicillin, streptomycin, tetracycline,
Unit-V: Amino acids: Lysine and glutamic acid. Commercial enzymes, Vitamins:
B12, Riboflavin etc.

TCH 822: PLANT DESIGN AND ECONOMICS

Unit I: Process Development: Process selection, study of alternative processes, pilot


plant, Scale up methods, Flow sheet preparation, sketching techniques,
Equipment numbering, Stream designation, Material and energy balances.
Plant Design: Design basis, Process selection-Selection of equipment,
specification and design of equipment’s, material of construction, Plant location,
Plant layout and installation, Safety, Start up, Shutdown and Operating
guidelines.
Unit II: Cost Engineering: Time value of money and equivalence, Interest, cost
comparisons by present worth, Annual equivalent cost and capitalized cost
methods, Uniform gradient and series.
Depreciation, Taxes and Insurances Nature of depreciation, Methods of
determining depreciation, depreciation rates in current Indian situation, Types of
taxes and insurance’s, Procedure for cost comparison after taxes.
Unit III: Cost Estimation: Types of cost estimation, capital investment cost, fixed capital
cost, working capital cost, start-up costs, process equipment cost estimation, cost
index, Equipment costs due to inflation, Battery limit investments, estimation of
plant cost, Estimation of total product cost, Manufacturing cost, General
expenses.
Profitability: Criteria of profitability, Payout period, Return on investment,
Present value, Cash flow analysis, Alternative investment analysis, Sensitive
analysis in project profitability.
Unit IV: Economic Optimization and Optimum Design: Nature of optimisation, Uni-
variable and multivariable systems, Analytical, graphical and incremental
methods of solution, LaGrange multiplier method, Linear programming and
dynamic programming establishing optimum conditions, Break even chart for
production schedule, Optimum production rates in plant operation, Optimum
conditions in batch, cyclic and semicyclic operation, Sensitivity and response
analysis.
Unit V: Optimization of Different Process Equipment: Viz., transportation systems, heat
exchangers, evaporators, mass transfer equipments and reactors. Determination
of height and diameter of different process equipments at conditions of optimum
cost. Pinch Technology analysis. Preparation of techno-economic feasibility
report.

Text Book
1. Peters M., Timmerhaus K. & Ronald W., “Plant Design & Economics for Chemical
Engineers”, McGraw Hill, 5th Ed., 2003.
References
1. Couper, J. R., “Process Engg. Economics (Chemical Industries)” CRC Press, 4th Ed.
1998.
2. Aries & Newton, “Chemical Engg. Cost Estimation”, McGraw Hill, 4th Ed., 1998.

TCH 823: SURFACE COATING

Unit I: Survey of paint industry and its scope in India. Pigments and their classification;
Methods of manufacture for white, coloured, metallic and luminous pigments.
Unit II: Classification of paints; Oil, emulsion, and water soluble paints and their
manufacturing processes; Drying oils; Natural and synthetic resins; Solvents and
plasticizers.
Unit III: Definition and classification of varnish; Oleoresinious and spirit varnishes;
Manufacture of different types of varnishes.
Unit IV: Ceramic coating; Glazing and enamelling. Metallic coating; Electroplating;
Galvanizing; Tinning.
Unit V: Polymeric coating; Protective and decorative coatings. Powder Coating.

Text Books:
1. Noel, H., “Out of Paint Technology”, Charles Griffin and Co., Ltd.
2. Morgans, W.M., “Outlines of Paint Technology”, Vol.I, Charles Griffin and Co.
3. Bidlack, C. and Edgar W. P., “Paints and Varnish Production Manual”, Chapman & Hall
Ltd.
4. Turner, G.P.A., “Introduction to Paint Chemistry Principles of Paint Technology”, Oxford
University Press.

Professional Elective VI*


L T P 3 1 0

TCH 831: CORROSION ENGINEERING

Unit I: Basic aspects introduction, classification, economics and cost of corrosion. Emf
series, Galvanic series, corrosion theories derivation of potential- current
relationship of activation controlled and diffusion corrosion processes. Potential-
pH diagrams Fe-H2O system, application and limitations. Passivation definition,
anodic Passivation, theory of Passivation, oxidation laws, effects of oxygen and
alloying on oxidation rates.
Unit II: Forms of corrosion-definition, factors and control methods of various forms of
corrosion such as pitting, inter granular, crevice, stress corrosion, corrosion
fatigue, hydrogen embrittlement, corrosion processes and control methods in
fertilizers, petrochemical and petroleum refineries
Unit III: Environmental aspects: Atmospheric corrosion- classification, factors influencing
atmospheric corrosion, temporary corrosion preventive methods, corrosion in
immersed condition, effect of dissolved gases, salts, pH, temperature and flow
rates on corrosion, Underground corrosion- corrosion process in the soil, factors
influencing soil corrosion.
Unit IV: Corrosion control aspects: Electrochemical methods of protection-theory of
cathodic protection, design of cathodic protection, sacrificial anodes, anodic
protection. Corrosion inhibitors for acidic, neutral and alkaline media, cooling
water system-boiler water system. Organic coating-surface preparation, natural
synthetic resin, paint formulation and applications. Design aspects in corrosion
prevention, corrosion resistant materials.
Unit V: Corrosion Testing, monitoring and inspection, laboratory corrosion tests,
accelerated chemical tests for studying different forms of corrosion.
Electrochemical methods of corrosion rate measurements by DC and AC
methods, corrosions monitoring methods, chemical and electrochemical removal
of corrosion products,

Text Books:
3. Banerjee, S.N., “An Introduction to Corrosion and Corrosion Inhibition”, Oxonian Press
Ltd., New Delhi, 1985
4. Fontana, M.G. and Greene, N.D., “Corrosion Engineering”, McGraw Hill, New York 3rd
Ed., 1986.

References
1. Shrier, L. L., “Corrosion Vol. I & II” George NownonsLtd., London 2nd. Ed.
2. Uhlig, H.H., “Corrosion and Corrosion Control’’ Wiley- Inter Science, New York 3rd
Ed., 1985.
3. Munger, C.T., “Organic Coatings”
4. Jain & Jain, “Engineering Chemistry”, Dhanpat Rai & Sons, New Delhi, 4th Ed., 2001

TCH 832: FINITE ELEMENTS METHODS

TCH 831: PROCESS UTILITIES AND PIPING DESIGN

Unit I: Various process utilities, their role and importance in chemical plants. Sources of
water and their characteristics; Treatment storage and distribution of water; water
for use in boilers, cooling purposes, drinking and process; Reuse and
conservation of water; Water resource management.
Unit II: Steam Generation and Utilization: Steam generation and its application in
chemical process plants, distribution and utilization; Design of efficient steam
heating systems; steam economy, Steam condensers and condensate utilization
Expansion joints ,flash tank design, steam traps their characteristics, selection
and application, waste heat utilization; Lagging, selection and thickness
.Selection and sizing of boilers; waste heat boilers.
Unit III: Compressors, blowers and Vacuum Pumps: Compressors, blowers and vacuum
pumps and their performance characteristics; Methods of developing vacuum and
their limitations, material handling under vacuum, Piping systems; Lubrication
and oil removal in compressors and pumps.Air filters,Air and gas leakage. Inert
gas systems, compressed air for process, Instrument air.
Insulation: Importance of insulation for meeting the process requirement,
insulation materials and their effect on various material of equipment piping,
fitting and valves etc. insulation for high intermediate, low and sub zero
temperatures, including cryogenic insulation.
Unit 1V: Energy losses in pipe lines, concept of equivalent length and equivalent pipes,
problems in pipe flow, hydraulic power transmission through a pipe line.
Negative pressure in pipe lines, Siphon, Multiple pipe systems, working pressure,
design pressure, choice of pipe materials, hydraulic analysis of complex pipe
networks.
Unit V: Aids in selecting pipe valves and fittings, standards for piping design,
Dimensional and mechanical standards for pipe valves and fittings. Pipe
fabrication, vibration, its prevention and control in piping systems.

Text Books
1. Nordell, Eskel, “Water Treatment for Industrial and Other Uses”, Reinhold Publishing
Corporation, New York., 1961.
2. Crowl, D.A. & Louvar, J.F. “Chemical Process Safety: Fundamentals with Applications”.
New Jersey: Prentice-Hall. (1989).
3. Goodall, P. M., “The Efficient Use Of Steam” IPC Science and Technology, 1980.
4. King, R. C. and Croker, S., “Piping Handbook”, McGraw Hill.

Reference Books
1. Lees, F. P., “Loss Prevention in Process Industries 3 volume set” Butterwort -
Heinemann, Oxford, 1996.
2. Kellogg, M. W Company., “Design of Piping Systems”, Pullman Power Products, New
York, 1976.

PCH852: C.A.D LAB


Credits : 4 L T P 0 0 4

Recommended to be done using a commercial simulator


1. Design of a Flow network containing Pumps, fittings and Piping (horizontal, vertical,
inclined)
2. Process design of simple reactors (CSTR, Tubular) with or without heat transfer.
3. Process design & Rating of stand alone Multi-component Distillation columns.
4. Process design & Rating of TEMA Type Shell &Tube Heat exchangers.
5. Steady state flow sheeting of acyclic processes.
6. Steady state flow sheeting of Processes with recycles /Purge/Bypass etc. Recommended
to be done using a Simulation Language/Programming Environment
1. Study of dynamic behavior of simple systems such as tank in series, double effect
evaporators,etc.
2. Study of coupling of manipulated and controlled variables using relative gain
analysis (RTA).
Recommended to be done using a commercial simulator
1. Dynamic simulation of Simple process systems with controllers
2. Dynamic simulation & controllability analysis of Binary distillation column.
Recommended Software
1. Steady state/Dynamic simulator (such as Hysys. Plant or Aspen Plus/Aspen
Dynamic)
2. Simulation Language /Programming Environment (MATLAB).

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