S & Sri Krishna CERTIFICATE OF ANALYSIS PHARMACEUTICALS: CERTIFICATE OF ANAS ac DEPARTMENT, _ DATE: 31072018 ROOST —— | PARACETAMOL PREUr(GradoDENBE FOWDER) eee BATCH WS. |0840148-t4 DATE OF ANALYSIS ra 60 BATCH TY. | 2000 Kg. 7 ‘DATE OF MANUFACTURE ~_SUNE, 2043. FPCIPRENOBT S14 DATE OF EXPIRY AY, 2078 "AVAWSHI oe tt 416.082013 ct _SIGNATURE OF CHE! Si | __resverenronmeD REsuLrs SPECIFIORTIONS Of. Cheraciers Pace ec ~ +] Apeerance “ie stave poder | Wie orion wis cpstaine : if ponder 7 | Sony capes Sparnaly slabs wwe, fey soluble in alcohol, very sigh ee Soluble in methylene chloride (02,__[ Wdentication = ‘| Meling Point —qeeTeT TOSS «(| TORE T72C [Specific Absorbance 260 nm | 804 60-860, jet asbestos FetesprPne E, | Test for Acelyt | complies Fest as per Phew 7 (B.| Related Substance (By HPLC) BoLtebomy | Nemes than 70H ~ SoU Gtierpmy | Net mor hen 89 pom ay rly F —— ft (one [Neto en 08 1a) | Any other impurity BORE (0.09%) | Tetarotatierimparties =| BDRL (<0.40%) 04. | Heawy Metals. ~~“[ Lass than 20 ppm 95, Less On Deng 0.10% ‘lot more tan O-50% 7 6) Sulphaed Ach Toe —Fotmere an 010% ‘G7__[Assay (On Dited Beis) ‘Additional tests( Tapped Density Ai “Tapped density(1250 taps) 0; Retention on 425 maa) Retention 67-260 jam (604) NLT- 0.56 Natinore than TO% Feniion on £60 pn (O08) or For information Retaniion on 63 pm (230) _——| 02.48% fet 30.0% 10 65.0% a BEWARRS: The above product COMPLIES to eT FET DOL. “Below Detection Lit 2 BORL. Bolow Disregard Lith He é PREPARED BY ac { CHECKED BY QA ppl AppRovED BY, EY 4s BATE Ven OATES oF se TASER OCIDESIGNATE : aoe eee _ eae és : {SSUES TO AP CONSUMER BRANDS ion 089 (R REPORT Ni se tisina Pharmacol Saree Pace ce Ista eee Uppal Fverbad-S00039 A Ia senpeqoara0 101 -€2/27200i0)-0¢/27294474-72 Flan 27204870 Fskg@srbrtrngharmsom carat ch ats beveopmae eo Uppal Wferaied- 500089 AF ind {0 904 088 Company) stengphare or ‘Q vy @ Gb Sri Krishna CERTIFICATE OF ANALYSIS Q.C DEPARTMENT, isi DATE 106.07.2013 PRODUCT PARACETAMOL Ph.Eur.(Grade:Crystals) ‘BATCH NO. —[oteuria-14 DATE OF ANALYSIS Twa aT BATCH QTY. [2000 Kg. DATE OF MANUFACTURE APRIL, 2013 ARNO. FPCIPRUOTBOS-1a DATE OF EXPIRY MARCH, 2018 ‘SAMPLED BY”: T.RAVIKUMAR Ee DATE :40082019 __ SIGNATURE OF CHEMIST S.|__Tesrs renroRMeD RESULTS SPECIFICATIONS 01 Characters + ee 7. | Appearance White crystalline powder White or almost white crystalline powder, i] Sovbity Cones Spaingy solubie i water, Feely soluble in alcohol, very slightly soluble in methylene chloride 02. _| Identification ‘A. | Melting Point 169.0°C - 170.5°C 168°C - 172°C 8. | Specific Absorbance at 249 nm 895 860 — 980. D. | Cotourteat Compiles Test as per PhEur | Test for Acetyl _| Complies _| Test as per Ph Eur. 03. | Related Substance (By HPLC ) | Impurity T [BOL (0.5 ppm) Not more than 10 ppm i) | impurity K | BOL (<1.15 ppm) Not more than 50 ppm ii) | Impurity F BOL (<0.0000%) Not more than 0.05% iv) | Any other impurty. 7 BORL (<0.01%) Not more than 0.05% Ea |_¥) | Total of other impurities BDRL (<0.10%) ‘Not more than 0.10% 04. | Heavy Metais Less than 20 ppm ‘Not more than 20 ppm. 05. Loss On Drying 0.16% ‘Not more than 0.50% 06. ‘Sulphated Ash ~ | 0.06% ‘Not more than 0.70% 07. | Assay (On Dried Basis) 99.8% H = 99.0% to 101.0% WIW of CeHsNOz ____| Additional tests( Tapped Density & Sieve Analysis ~ Cumulative retention) i. ‘Tapped density(1260 taps) 0.833g/ml For information ii__| Retention on 30# (600 pm) 13.72% ‘Not more than 20.0% Retoniion on 60250 uit) 76.29% ‘Not ess than 70% REWARKS! Tho above product COMPLIES to Specifications of Ph. Eur.7.0 BDL - Balow Detection Limit BORL- Below Disregard Limit wgake PREPARED BY ac (- CHECKED BY QA, APPROVED BY © 06 DATE: DATE: Si, MANAGER-QCIDESIGNATE 0.043 ol jor b> sem ir. MANAGER-QCIDESIGN/ ISSUED TO: Mis.SIYEZA FINE CHEM. a ae REPORT NO: 0180 (R) ISSUED ON:UB.07.2018 Sl Krishna Pharmaceuticals [CORPORATE OFFICE: Cé Industrial Ares Uppsl Hyderabad - 500.039 AP India 7991 402720 1101-02 /2720 0103 -04/2720.4471 -72 491. 40:2720 4470 E:seg@anrebnaparia com FACTORY: Unit-1 Cé Indusirial Development Area Uppal Myderabad-S00039 AP india (450 9003:2008 Company) stkrshnapharma.com PHARMACEUTICALSCERTIFICATE OF ANALYSIS sy Sri Krishna PHARMACEUTICALS. Q.c DEPARTMENT, ne i eee DATE : 14.03.2018 [PRODUGT — “PARACETAMOL Ph.Eur [BATCH NO. | 3isarte.15 : DATE OF ANALYSIS — BATCH GTY_| 2000 Kg =e VATE OF MANUFACTURE | WARGH, 2015 ‘ARNO. FPCIPRUSIS24048 [DATE OF EXPIRY FEBRUARY, 2020 | SAMPLED BY YV.RAO — Gy | DATE : __SIGNATURE OF CHEMIST_ FF RESULTS SPECIFICATIONS [01. | Characters Eee genet a [1c Apssarance— ~ | White Systane powder Whig or aoa WS estate oveder 7.) Sbiiy —— “| Comaiies Sparingly Soluble waler, freely | soluble in alcohol, very slighty soluble in methylene chiorde 02. | iaenticabon ie et [a a A [ eting Poi TTS Te O= TT [8 | Specie: Absorbance at 240 am] 699 __ | 860-960. a B- Goiourtest ‘complies ‘The vole coor developed inte eae ___| reaction should not change to red |_E [Test forAcetyi Complies _| Test as per Ph. Eur. w iy] impurity J” | BDL OS ppm) ‘Not more than 10 ppm A) [Impurity BDL (<1.15 ppm) "Not more than 60 ppm Ti) [Trapuriy F BDL (=0,0008%) Not more than 0.05% a [> | Any other impurity ~[BDRL 20.07%) Not more than 0.05% ‘| Wy [Total oF other mpurias [BORE =O io ‘Not mare than 0.10% al 04. | Heavy Metas | Tess than 26 pom ‘Not more than 20 ppm | 05. | Loss On Drying 076% Not more than 0.50% (08. | Suiphatea Ash 7 808% Ret more tan 010% — [7. | Assay (On Dried Basis) [sae% 99.0% to 191% WITT OHING, | AaitionaT Tost 77 | Baieral Endotoan | 255 Euing Not more tan 5 Came © [Tota Bactenai court 25 ciulg Not more than 700 efulg | (soe Not more than 10 org | Roseat ~ | Should be absent} “Absent Should be absent [Absent oe Should be absent oa 3} | Slaphyocecus aureus ‘Absent : Should be absent | REMARKS: The above Product COMI aa BOL - Below Detection Limit, low Disregard Limit, PREPARED BY QC. ~ CHECKED BY QA DATE: DATE: [ISSUED TO: Ws. PHARMACHEMICALS HANDLES GnibH, [REPORT NO: 3152 (A) Se sha Pharmacauteals s, {CORPORATE OFFICE: C4 Indus Avza Uppal Hyderabad -500029 AP indi 491403720 1101 02/2720 0103-08 /27204871-72 F981 407720 4470 €: tg@sritrshnapharma.com FACTORY: Unit Industri Development ea Upeal Hyderabod-500 029 AP Indi (150 9003:2008compaey|sreisnaghanna.com LIES to the Specifications of Ph.Eur8.0 2 pwemomee Ape | St MANAGER -QC/DESIGNATE DATE