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02. Design shell and tube horizontal condensor for condensation of 39000 kg/hr npropanol at 0.3 kgf/cm 2g by
cooling water at 32oCto 45oC. The condensing temp. at this pressure is
85.2oC. The dirt factors of both shell & tube side is 2200 kcal/hrm2oC. Assume that allowable pressure drop
on both the side is within limit. Assume the tube o.d. of 19.05 mm and 23.81 mm triangular pitch. Tube
wall thickness to be taken as 1.65 mm. Assume isothermal condensation. Properties for n-propanol:
Latent heat of condensation: 158 kcal/kg Thermal conductivity: 0.14 kcal/hrmoC Liquid density: 800 kg/m3
Liquid viscosity: 0.62 cP Vapor viscosity: 0.008 cP Thermal conductivity of tube metal = 39 kcal/hrm oC.
Condensation coefficient is to be calculated as:
03. Gas oil at 200 °C is to be cooled to 40 °C. The oil flow rate is 22500 kg/h. Cooling water is available at 30 °C
and the temperature rise is to be limited to 20 °C. The pressure drop allowance for each stream is 100
kN/m2 . Design a suitable heat exchanger. Physical properties of the fluid:
TUTORIAL: 04
01. Design shell and tube heat condenser for condensation of 46000 kg/hr n- propanol at 0.25 kgf/cm2 g by
cooling water at 320C. The dirt factor of both shell and tube side is 2000 kcal/hrm2oC. Assume that
allowable pressure drop on both the side is within limit. Assume the tube o.d. of 19.5 mm and 23.81 mm
triangular pitch. Tube wall thickness to be taken as 1.65 mm. assumes isothermal condensation. Properties
of n-propanol. Latent heat of condensation : 158 kcal/kg Thermal conductivity : 0.14 kcal/hrm oC Liquid
density : 800 kg/m3 Liquid viscosity : 0.62 cP Vapor viscosity : 0.01 cP Condensation co efficient is to be
calculated as:
02. 10900 kg/h of nearly pure saturated methyl ethyl ketone (MEK) vapor at 13.73 kPa g is to be condensed
and cooled to 60 ᵒC by cooling water which is available in plant at 32 ᵒC. Assume Uc = 800 W/m2ᵒC and
Usub = 200 W/m2 ᵒC. Calculate the % excess heat transfer area for the given condenser.
03. A horizontal shell & tube condenser is to be designed to condense 3.2 kg/s of isobutane at 8.3 kg/cm 2 .
Water available at 25oC is to be used in another process unit at 37oC. Tubes of 15 mm inside diameter & 2
mm wall thickness are available. Maximum lengths of the tubes are 4 m. The tubes are to be arranged on
25 mm square pitch. Fouling resistance on each side = 0.0004 m2 k/W. Condensation temperature of
isobutane = 640C. Latent heat of condensation of isobutene = 275 KJ/kg. Overall heat transfer for
condensing isobutene vapor ranges from 390 to 500 W/m2 K. Water velocity should not exceed 3m/s and
not to below 0.5 m/s. Thermal conductivity of material = 16 W/m 2 k. Assume isothermal condensation.
Physical Properties of isobutane:- K = 0.26 W/m K , ρ = 1080 kg/m3 , μ = 0.00477 kg/m s Physical Properties
of Water:- K = 0.62 W/m K , ρ = 1000 kg/m3 , μ = 0.00072 kg/m s, Cp = 4.1868 kJ/kg ˚C Friction factor f =
0.046 Re -0.2 Data for bundle diameter calculation: for Square pitch arrangement.
TUTORIAL: 05
01. Define schedule number, Equivalent length of pipe and NPSH
02. For the specified location of the pump calculated value of (NPSH)A is coming less than (NSPH)R. Suggest all
possible solutions to make(NPSH)A greater than (NPSH)R.
03. Write a brief note on NPSH for centrifugal pumps.
04. Discuss the Process Design of Fans and compressor.
TUTORIAL: 06
01. Crude dichlorobenzene is pumped from a storage tank to a distillation column. The tank is blanketed with
nitrogen and the pressure above the liquid surface is held constant at 0.1 bar g. The minimum depth of
liquid in the tank is 1 m. The distillation column operates at a pressure of 500 mm hg (absolute). The feed
point to the column is 12 m above the base of tank. The tank and column are connected by a 50 mm
internal diameter commercial steel pipe, 200 m long. The pipe running from the tank to the column
contains the valves and fittings: 20 no. of standard radius 90˚ elbows, two gate valves (fully open), an
orifice plate and a flow control valve. Neglect the friction loss in suction line. If the maximum flow rate
required is 20000 kg/hr, calculate the power required by pump. Pump efficiency is 70%. Pressure drop
across the control valve is 0.5 bar. Density of the dichlorobenzene is 1300 kg/m3 and viscosity is 1.4 cP.
Pressure drop for turbulent flow of fluid through commercial steel pipe in KPa/m
02. A three stage reciprocating compressor is used to compress 306 Sm3 /h of methane from 0.95 atm a to 61.3
atm a. The inlet temperature is 26.7 °C. Specific heat ratio of methane is 1.31. Calculate (1) Power required
for compression, if mechanical efficiency is 80% and (2) discharge temperature of gas after 1st stage.
03. Benzene at 38°C is pumped through the system at a rate 9.09 m3/hr with the help of a centrifugal pump.
The reservoir is at atmospheric pressure. Pressure at the end of discharge line is 345 kPa g. The discharge
head is 3.05 meter and the 07 1 pump suction head is 1.22 meter above the level of liquid in reservoir. The
friction loss in suction line is 3.45 kPa and that in discharge line is 37.9 kPa. The mechanical efficiency of the
pump is 0.6. The density of benzene is 865 kg/m3 and its vapor pressure at 38°C is 26.2 kPa. Calculate (1)
NPSH and (2) Power required by pump. Power required by pump is given by,
P= (H×qv ×ρ) / (3.67×105 ×η)
Where P= power required in kW, H= Total dynamic head in meter, qv= volumetric flow rate,
m3/hr, ρ= density of fluid, kg/m3 , η= mech. efficiency of pump.
TUTORIAL: 07
01. Find out the power required for a turbo blower for the following duty. Fluid- Atmospheric Air, Capacity-
1000 Nm3/hr Discharge pressure - 2 atm a, Inlet temperature of Air- 500oC
For air k=1.395. Power requirement for blower is given by,
P = 2.78 × 10-4 k/(k-1) × qv1 × p1[(p2/p1)(k-1)/k -1]
Where P= Power required in kW, p1= inlet pressure in kPa, p2= discharge pressure,
qv1= volumetric flow rate of air based on inlet condition in m3/hr.
Also find the discharge temperature of air.
02. A centrifugal pump is drawing water from an overhead tank, exposed to atmosphere. Vertical distance
between free surface of liquid in the tank and centre line of the pump is 10 m. Capacity of centrifugal pump
is 10000 kg/h. Maximum operating temperature is 50 °C. Vapor pressure of water at 50 °C is 92.51 torr.
Total length of suction pipe 10.5 m, having two 90 ° elbows. Material of pipe is carbon steel. Density of
water = 1000 kg/m3 , Viscosity of water = 0.558 cP, K-Value for 90º elbow is 0.75. Surface roughness of
carbon steel and friction factor are 0.0457 mm & 0.005 respectively. For the velocity of water in suction
line 1 m/s, Determine (i) the size of suction pipe (ii) total frictional pressure drop in suction line (iii) (NPSH)
of centrifugal pump.
03. Estimate the optimum pipe diameter for a flow of dry chlorine gas of 20000 kg/hr at 3 atm a and 25 0C
through carbon steel pipe.
04. Estimate the optimum pipe diameter for a flow of dry chlorine gas of 10000 kg/hr at 6 atm a and at 200c
through carbon steel pipe. Also give the importance of Schedule no. in pipe design.
TUTORIAL: 08
01. Discuss the various factors considered for the selection of different types of trays for distillation column.
02. What is jet flooding and downcomer flooding? Explain the design steps for the determination of total
pressure drop in sieve tray distillation column.
03. State the advantages and disadvantages of vacuum distillation.
04. What is the function of downcomer? Discuss the different types of downcomer used in distillation column.
05. Explain FUG method for multi component distillation.
06. Explain McCabe-Thiele method for binary distillation.
TUTORIAL: 09
01. Explain the method of selection of operating pressure in distillation column.
02. Give merits and demerits of vacuum distillation over conventional distillation.
03. Write short note on selection of key components in multi component distillation.
04. Discuss about the Determination of Optimum Reflux Ratio.
05. Explain and write all equations involved in following condition for sieve tray tower. (a) Pressure drop across
tray tower (b) Checking of weeping condition (c) Checking of Down comer flooding (d) Checking of liquid
entrainment
06. Write a short note on flooding in tray type distillation column.
TUTORIAL: 10
01. Determine the minimum reflux ratio for the binary distillation at standard atmospheric pressure based on
the following data:
Feed = 100 kmol/hr has mole fraction of benzene= 0.4 and rest toluene. Feed is saturated liquid and mole
fraction of benzene in distillate = 0.99 Mole fraction of benzene in residue required = 0.02, αav = 2.25.
02. Determine minimum reflux ratio, minimum number of theoretical stages required, optimum reflux ratio
and theoretical stages required for desired separation for following system by FUG method. Feed flow rate
is 70 kmol/hr and feed is saturated liquid. Composition of distillation column streams and average relative
volatilities of all components of feed are as follows.
Toluene is light key and ethyl benzene is heavy key component. Gilliland co relation is given by:
03. A saturated liquid consisting of Chloro methanes is fractioned to give a top product of 99.94% (by mole)
methyl chloride. Methyl chloride is light key and methylene chloride is heavy key component. Total
condenser is used. The compositions of the top product and of the methyl chlorides in the residues are
given.
(a) Complete the material balance over the still for a feed rate of 100 kmol/hr. (b) Calculate the minimum
reflux ratio by Underwood’s method.
04. A saturated liquid, consisting of phenol and cresol with some xylenols, is fractioned to give a top product of
95.3 mole % phenol. Metacresol is heavy key and phenol is light key component. Total condenser is used.
The composition of the top product and of the phenol in the bottom is given. (i) Complete the material
balance over the still for a feed rate of 100 kmol/h and (ii) Calculate the minimum reflux ratio by
Underwood’s method.
TUTORIAL: 11
01. Aqueous solution of ethanol contains 6 % by mass ethanol. It is to be concentrated in the distillation
column to 30 % by mass. Open steam, saturated at 80 kPa gauge pressure will be used for the distillation
column. Feed flow rate is 5000 kg/h and it is saturated liquid at its bubble point. Residue should not contain
more than 0.02 mass percent ethanol. Sparging steam flow rate is 0.2 kg of feed. Calculate the number of
theoretical stages required for the desired separation. The equilibrium data for ethanol-water system at
101.3 kPa is as follows.
02. Acetic acid is to be separated from a process stream containing 80 % acetic acid and 20 % Water (by mass)
by continuous distillation column at atmospheric pressure. Concentration of water in bottom product (pure
acetic acid) should not be greater than 50 ppm. Top product (distillate) contains 80% water and 20% acetic
acid (by mass). The feed is liquid at 300 C. estimate the number of theoretical stages required both
graphically and empirically. Vapor liquid equilibrium data are as follows.
Based on 85% flooding condition, Calculate (1) Tower diameter required at top and bottom. (2) Check
weeping for enriching section. (top section) Consider down comer area is 12% of column cross section and
hole area is 10% of active area.
04. Isopropyl alcohol (IPA) forms a minimum boiling azeotrope with water at 80.4 o C and 101.325 kPa, having
a composition of 31.47 mole % water. A feed consisting of 50 mass % IPA under saturated liquid condition
is to be distilled to give 67.5 mole % IPA as distillate (near azeotrope) and 0.1 mole % (0.0033 mass %) IPA
in the bottom. Using McCabe-Thiele technique and for R = 3, find the number of theoretical stages,
required for the separation at 1 atmospheric and locate the feed introduction stage. To find the nonideal
behaviour of IPA-water system, use of van Laar equation can be used. Assume the vapour fugacity to be
unity at low pressure. The vapour pressure of IPA can be calculated using Antoine equation.
04. For the separation of dimethylformamide (DMF) from its dilute solution having a flow rate of 1000 kg/h and
containing 20 % DMF by mass is to be counter currently extracted with methylene chloride to reduce the
DMF concentration to 1 % in the final raffinate. Determine (i) the minimum amount of solvent which can be
used and (ii) the number of theoretical stages if actual amount of solvent is double than the minimum
required. Phase equilibrium equation is given by = 0.5555 at 25oC where, Y and X are mass fractions of
solute.
TUTORIAL: 15
01. Discuss the design procedure of Continuous Gravity Decanter.
02. Briefly explain the desired solvent properties required for choice of solvent in liquid-liquid extraction.
03. State the merits and demerits of mixer-settler. Discuss the design steps for the process design of horizontal
and vertical gravity settler.
04. Define partition coefficient, extract phase and raffinate phase for liquid-liquid extraction.
05. Discuss the steps for process design of counter current multistage extractor.
06. List important industrial application of liquid-liquid extraction.
07. Discuss the process design of rotameter.
08. Discuss the Process Design of Orifice meter. Also Explain various locations of pressure taps with neat sketch
in orifice meter
Project Work:
(Ref.: Analysis, Synthesis and Design of Chemical Processes by Richard Turton, Richard C.
Bailie, Wallace B. Whiting, Joseph A. Shaeiwits)
Refer Page No. 1027 of above ref. for details of process and collect flow rate, temperature and
pressure data from the given ref.
Find suitable physical and thermodynamic properties and Design following equipment based on
the data given in above reference:
1. Find all physical, chemical and thermodynamic properties of the fluids being processed
in equipment
2. Design condenser – E-1104
3. Design reboiler – E-1105
4. Design Distillation Column including tray hydraulic design – E-1102
5. Piping design for reflux – Steam No. 9 for Feed, Steam 10 for reflux to column, Stream
11 for distillate, Stream 12 bottom product.
6. Select suitable pump and find NPSH and Power requirement for selected pump for reflux
stream.