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Composite Structures 69 (2005) 396–406

www.elsevier.com/locate/compstruct

Low velocity impact of combination Kevlar/carbon fiber


sandwich composites
Jeremy Gustin, Aaran Joneson, Mohammad Mahinfalah *, James Stone
Department of Mechanical Engineering and Applied Mechanics, North Dakota State University Fargo, ND 58105, USA

Available online 24 August 2004

Abstract

Impact, compression after impact, and tensile stiffness properties of carbon fiber and Kevlar combination sandwich composites
were investigated in this study. The different samples consisted of impact-side facesheets having different combinations of carbon
fiber/Kevlar and carbon fiber/hybrid. The bottom facesheets remained entirely carbon fiber to maintain the high overall flexural stiff-
ness of the sandwich composite. The focus of this research was to determine if any improvement in impact properties existed as a
result of replacing the impact-side facesheet layers of carbon fiber with Kevlar or hybrid. Impact tests were conducted on different
sample types to obtain information about absorbed energy and maximum impact force. Also, compression after impact tests were
conducted to determine the reduction in compressive strength when comparing impacted to non-impacted samples. The elastic mod-
uli of carbon fiber, Kevlar, and hybrid were determined from tensile testing. This data was used to characterize the reduction in
stiffness from replacing carbon fiber layers with the Kevlar or hybrid layers. The experimental data in its entirety helps define
the benefits and disadvantages of replacing carbon fiber layers with Kevlar or hybrid.
 2004 Elsevier Ltd. All rights reserved.

Keywords: Sandwich composite; Hybrid; Carbon fiber; Kevlar; Low velocity impact

1. Introduction pact loading [5–10]. This is an important concern since


a reduction in stiffness and residual strength occurs after
Sandwich composites have become increasingly pop- impact.
ular for applications including aerospace, marine/off- Carbon fiber reinforced, epoxy matrix composites
shore industries, and ground transportation [1,2]. They have emerged as a very promising class of structural
are favored for their high specific strength and stiffness, materials with high static strength and stiffness proper-
corrosion resistance, tailorability, and stability [3]. ties [11]. The core, which is typically a low strength,
Sandwich composites are very suitable for lightweight lightweight material, is responsible for transmitting
structures requiring high in-plane and flexural stiffness shear forces between the facesheets [12]. A vital element
[4]. However, applications prone to impact are limited of the sandwich construction is the effective bond be-
because of a relatively poor resistance to localized im- tween the facesheets and the core material. The joint
must be stiff and strong, as well as tough in order to
allow the sandwich structure to sustain high loads over
a long service life [13].
*
Kevlar was added to the impact-side facesheet in an
Corresponding author. Tel.: +1 701 231 8839; fax: +1 701 231 attempt to improve upon the impact properties. Kevlar
8913.
E-mail addresses: jeremy.gustin@ndsu.nodak.edu (J. Gustin),
composites have been extensively utilized as lightweight
aaran.joneson@ndsu.nodak.edu (A. Joneson), m.mahinfalah@ndsu. armor structures in applications ranging from military
nodak.edu (M. Mahinfalah), james.stone@ndsu.nodak.edu (J. Stone). helmets to large scale vehicle systems such as aircraft,

0263-8223/$ - see front matter  2004 Elsevier Ltd. All rights reserved.
doi:10.1016/j.compstruct.2004.07.020
J. Gustin et al. / Composite Structures 69 (2005) 396–406 397

spacecraft, land vehicles, and naval vessels [14,15]. Rein- 2. Sample construction
forcement of composites with Kevlar fibers can signifi-
cantly improve the impact damage tolerance if used in A hand-layup method shown in Fig. 1 was used to
place of or in conjunction with graphite fibers [16–18]. construct the samples. The major components required
Bunsell and Harris [19] suggested that once the failure for this method are a vacuum pump, vacuum bagging,
strain of the brittle layers (carbon fiber) is reached in spiral tubing, and sealant tape. The spiral tubing en-
an interlaminar hybrid, the load can be transferred to sured a uniform vacuum across the sample and pre-
the ductile layers (Kevlar) if bonding between the lami- vented epoxy from pooling on the sample side with
nates is sufficient. less vacuum. This would have occurred on the side with-
In this study, sandwich composite plates with differ- out spiral tubing. If epoxy pooling occurs, the facesheet
ent combinations of Kevlar/carbon fiber and hybrid/car- thickness is not uniform. The facesheet would be the
bon fiber impact-side facesheets were subjected to low thickest on the sample side without the spiral tubing.
velocity impacts at energies ranging from 5 J to those The core of the sandwich composite consisted of poly-
that caused complete sample penetration. On the im- urethane foam filled honeycomb. The honeycomb struc-
pact-side facesheet, the very top 1, 2, 3, or 4 layers of ture was constructed out of kraft paper. The foam filled
carbon fiber were replaced with Kevlar or hybrid. Low honeycomb sheets, purchased from MGI, had the prop-
energy impacts were considered since even in the ab- erties indicated in Table 1. The carbon fiber, Kevlar, and
sence of fiber breakage, the laminate mechanical per- hybrid fabric properties are listed in Table 2. The epoxy
formance can be drastically affected [6,20]. These consisted of F-82 resin and TP-41 hardener, which was
experimental impact tests are necessary to determine im- allowed to cure under a 600 mm Hg vacuum for a min-
pact force and energy performance. Current sandwich imum of 9 h. The cured properties of the epoxy, pur-
composite impact theory does not consider impact ener- chased from Eastpointe Fiberglass, are listed in Table 3.
gies that result in facesheet cracking, which is very com- The hand-layup method provided high quality sam-
mon. For impacts without facesheet cracking, Hoo Fatt ples with minimal defects. To create the foam filled core
and Parks [3,21] used equivalent single and multi degree- samples, a layer of epoxy was applied before each layer
of-freedom systems to predict low velocity impact re- of fabric was placed. Special care was taken to insure the
sponse and damage initiation impact forces. correct amount of epoxy was used in addition to being
Compression tests were conducted to determine the evenly spread out. After the four layers were placed,
remaining compressive strength after impact. In-plane the vacuum bagging was carefully spread over the sam-
compression is the critical load for impact-damaged ple ensuring no wrinkles would form when the vacuum
specimens, since strength reductions are the largest was applied. Any wrinkles that form on the vacuum
under this type of loading [22]. The type of compression bagging will affect the surface finish of the sample. A
after impact failure depends on the impact damage. Da-
vies et al. [23] discussed the correlation between three
types of impact damage and the resulting compression
after impact failure. For an impact resulting in a perma-
nent indent to the facesheet, compressive loads can in-
crease local bending and push the skin further into the
core causing failure. For impacts that cause internal
delamination, compressive loads may cause localized
buckling where the skin is not supported by the foam.
For impacts where the top facesheet and core are pene-
trated, the bottom facesheet may experience massive
debonding. The combination of the bottom facesheet
debonding and penetration of the top facesheet would
Fig. 1. Sample construction setup.
significantly limit the compressive strength. Compressive
failure would likely occur as a result of top facesheet
cracking from stress concentrations and/or bottom face-
sheet buckling.
Table 1
Tensile tests were performed to characterize how the
Properties of MGI Canada MIKOR honeycomb sheets
addition of Kevlar or hybrid to the impact-side face-
Density 112 kg/m3
sheet would decrease the stiffness compared to face-
Compressive strength 2.02 MPa
sheets with only carbon fiber. Understanding how the Cell size 12.7 mm
stiffness is affected is necessary in determining potential Shear strength ? to ribbon 1.65 MPa
applications for sandwich composites incorporating car- Cell thickness 0.3175 mm
bon fiber with Kevlar or hybrid. Honeycomb thickness 25.4 mm
398 J. Gustin et al. / Composite Structures 69 (2005) 396–406

Table 2
Fabric properties
Carbon fiber Kevlar 49 Hybrid (3K carbon fiber/1500 Denier Kevlar)
Yarn type 3K
Weave type Plain 4 HS 2 · 2 Twill
Area density 193 g/m2 169 g/m2 183 g/m2
Thickness 0.3048 mm 0.254 mm 0.305 mm
Count (rows/tows per inch) 12.5 · 12.5 17 · 17 12.5 · 12.5

Table 3 sample types. The abbreviations for the sample types


Properties of Eastpointe Fiberglass epoxy shown in this table are used throughout the paper.
Density 1084 kg/m3
Compressive strength 131 MPa
Tensile strength 63.6 MPa 3. Test method
Cure time 9–12 h
Cure temperature 23.9 C
An Instron Dynatup drop tower, Model 9250HV,
was used for impact testing. This machine is capable
of impacting samples at energies of up to 826 J utilizing
Table 4
Properties of hybrid carbon fiber/Kevlar a spring-assist. For this study, all samples were impacted
with a 7.25 kg drop weight. Since the drop weight was
Abb. Sample type Weight (g)
not changed, the different impact energies were achieved
CF 4 carbon fiber layers 60.8
by adjusting the drop height. A pneumatic clamping fix-
1K 1 Kevlar–3 carbon fiber layers 59.7
2K 2 Kevlar–2 carbon fiber layers 60.5 ture, with a 76.2 mm (3 in) diameter opening, secured
3K 3 Kevlar–1 carbon fiber layers 59.8 each sample during impact. The air pressure was set to
4K 4 Kevlar layers 58.4 0.4 MPa, which was well below the 2.02 MPa compres-
1H 1 hybrid–3 carbon fiber layers 59.4 sive strength of the foam filled honeycomb core. The
2H 2 hybrid–2 carbon fiber layers 60.1
samples were impacted with a 12.7 mm (0.5 in) diameter
3H 3 hybrid–1 carbon fiber layers 59.7
4H 4 hybrid layers 59.3 striker with a hemispherical tip, constructed out of high
strength steel. Impulse software was used to display and
store the impact data.
rubber squeegee was used to remove the extra epoxy and The compression and tensile tests were conducted
trapped air. using a 50 kip MTS fatigue test system. The compres-
As shown in Table 2, the addition of Kevlar and hy- sion testing fixture was designed similar to a Boeing
brid to the facesheets actually reduced the overall weight Model CU-CI fixture [24]. This fixture is specifically de-
of the sandwich composite compared to the entirely car- signed with side supports to prevent buckling during
bon fiber samples. The Kevlar and hybrid fabrics had a compression testing. For this study, the side supports
lower areal densities compared to the carbon fiber. The were used for all compression tests.
different combinations of 100 mm · 100 mm samples
used in this study are listed in Table 4 with their corre-
sponding weights. The sample type abbreviations corre- 4. Low velocity impact results
spond to the impact-side facesheet information. The
very top layers of the impact-side facesheet were re- For the entire set of samples tested, partial/total face-
placed with either Kevlar (1K–4K) or hybrid (1H–4H). sheet penetration occurred for the 5–10 J impacts, total
Fig. 2 illustrates how Kevlar was added to the impact- facesheet and partial core penetration for the 15 J im-
side facesheet for the 2K sample type. The bottom face- pacts, and partial/total bottom facesheet penetration
sheets remained four layers of carbon fiber for all the for the 20–45 J impacts. In general, the initial force–time

Fig. 2. Illustration of facesheets and core for the 2K sample type.


J. Gustin et al. / Composite Structures 69 (2005) 396–406 399

Fig. 3. 25 J Impact damage of CF sample (a) rear damage-honeycomb structure not impacted, (b) rear damage-honeycomb structure impacted and
(c) front impact damage.

spike resulted from the top facesheet impact response, lar or hybrid were added to the facesheet. For each
the following drop and slow increase resulted from the sample type, the force–time curves were split into two
foam core crushing, and the final force–time spike re- impact energy groupings: those that did not penetrate
sulted from the bottom facesheet impact response. the bottom facesheet (5–15 J) and those that did (20–
Some deviation in the force–time results occurred be- 45 J). As shown in Table 5, the average maximum forces
cause of the non-homogeneous nature of the foam filled for the Kevlar samples (1K–4K) showed significant
honeycomb core. For some samples, the striker directly improvement over the CF samples. The hybrid samples
impacted the honeycomb structure after penetration of (2H–4H) showed an even more dramatic improvement.
the top facesheet. The additional support for the top The 1H samples were comparable to the CF samples.
facesheet resulted in higher forces and more absorbed The maximum forces developed for the top facesheet
energy compared to when the striker missed the honey- varied when considering the carbon fiber, Kevlar, and
comb structure. In addition, the bottom facesheet dam- hybrid sample types. The difference in maximum forces
age varied depending on whether the honeycomb was likely a result of the different failure modes. Each
structure was impacted, as can be seen by comparing sample type had different tensile and shear properties.
the two 25 J impacts shown in Fig. 3a and b. When The CF samples had high tensile strength, but lacked
the honeycomb structure was impacted, the loading the shear strength needed to achieve the impact per-
was more distributed over the bottom facesheet and formance of the Kevlar and hybrid samples. The hybrid
higher forces were required to create delamination and samples experienced the highest maximum forces, which
a larger cracking diameter. The low density of the core was likely a result of the combination of high tensile and
was the main reason that the honeycomb structure had shear properties. The facesheet penetration damage,
such a significant effect on impact response. Lower shown in Fig. 4, illustrates the shear and tensile failure
forces were required to shear the facesheet when there modes for the different sample types. The carbon fiber
was little support from the honeycomb structure. A samples clearly experienced shear failure, which resulted
higher density core would have likely reduced these ef- in cracking that corresponded to the diameter of the stri-
fects. The top facesheet cracking diameter (Fig. 3c) did ker. The Kevlar sample had a tensile failure mode,
not show any significant change regarding the amount which is shown by the bending at the striker perimeter
of honeycomb structure impacted. and tearing at the center of impact. The impact damage
The force–time curves shown in the Appendix Achar- to the top facesheet of the hybrid showed the failure
acterized how the maximum forces changed when Kev- characteristics of both the CF and 4K samples. The

Table 5
Average maximum force data
Sample type Average maximum force (kN)/ Average maximum force (kN)/percentage
percentage increase over CF (5–15 J) increase over CF (20–45 J)
CF 1.26 1.33
1K 1.41 11.9% 1.48 11.3%
2K 1.37 8.7% 1.45 9.0%
3K 1.35 7.1% 1.44 8.3%
4K 1.35 7.1% 1.43 7.5%
1H 1.27 0.9% 1.32 0.8%
2H 1.49 18.2% 1.63 22.5%
3H 1.44 14.3% 1.46 9.7%
4H 1.72 36.5% 1.67 25.6%
400 J. Gustin et al. / Composite Structures 69 (2005) 396–406

Fig. 4. 15 J impact damage to (a) CF, (b) 4K, and (c) 4H.

carbon fiber filaments experienced shear failure/cracking Table 6


and the Kevlar filaments tensile failure/tearing. Average absorbed energy of 35–45 J impact energies
Sample type Average absorbed energy (J)
CF 31
5. Absorbed––impact energy 1K 34.9
2K 33.2
3K 34.5
The addition of Kevlar and hybrid to layers 1, 2, 3, 4K 33.5
and 4 of the top facesheet resulted in higher absorbed 1H 32.4
energies compared to the CF samples as can be seen in 2H 31.9
Figs. 5 and 6. All of the sample types were able to ab- 3H 33.1
4H 32.8

sorb impact energies up to 30 J. However, after 30 J


the impact performance for the different sample types
varied. This performance can be seen in Table 6, which
lists the average absorbed energies of the 35–45 J
impacts. These impacts resulted in complete sample
penetration.
No significant difference in impact performance was
seen when considering the entire set of Kevlar samples,
which consist of replacing layers 1–4 of the top face-
sheet as shown in Table 6. The additional layers of
Kevlar were not required to achieve the improved im-
pact performance. In fact, the 1K samples had the
Fig. 5. Absorbed vs. impact energy for CF all Kevlar sample types. highest overall absorbed energy, reaching 36 J. This
represents a 14% increase over the 31.5 J reached by
the CF samples.
Just like the Kevlar samples, only minor improve-
ments were seen after adding the first layer of hybrid.
This impact data validates the benefits of replacing only
one layer of CF with Kevlar or hybrid. The Kevlar or
hybrid layer provides additional protection against im-
pact, while the remaining CF layers maintain the high
stiffness of the sandwich composite.

6. Compression test results

The maximum compressive stress resulting in failure


for the different sample types is shown in Figs. 7 and
Fig. 6. Absorbed vs. impact energy for CF and all hybrid sample 8. The compression data is the average of two tests con-
types. ducted at each impact energy. The non-impacted CF
J. Gustin et al. / Composite Structures 69 (2005) 396–406 401

Fig. 9. (a) Facesheet crushing during compression testing damage of


2H non-impacted sample and (b) Facesheet cracking from buckling
during compression testing of 2H 30 J sample.

Fig. 7. Maximum compressive stress vs. impact energy.


ing, the delamination that occurred during the impact
quickly spread and caused the bottom facesheet to
buckle. If a higher density, stronger core were used,
the facesheet buckling would have likely occurred at
much higher compressive loads.
The impact damage consisted of either facesheet
crushing, cracking, or delamination. As can be seen,
the samples followed a trend of decreasing compressive
strength as impact energy increased. The facesheet
crushing occurred on samples with minimal or no initial
impact damage shown in Fig. 9a. The facesheet cracking
occurred from the impact hole across the sample, per-
pendicular to the compressive load, as can be seen in
Fig. 9b. A combination of facesheet cracking and face-
sheet delamination occurred on some of samples im-
pacted at high energies. This likely occurred as a result
Fig. 8. Maximum compressive stress vs. impact energy.
of the striker partially or totally penetrating the bottom
facesheet. During these impacts, the bottom facesheet
sample had the highest compressive strength at 15.1 experienced both cracking and delamination, which in-
MPa. This was approximately 11.5% and 8.6% higher creased once the compressive load was applied.
than the average of the non-impacted Kevlar and hybrid The non-impacted compressive strength, the average
samples, respectively. Although the general trend was compressive strength for 35–45 J impacts, and the per-
decreased compressive strength with increased impact cent decrease in compressive strength when comparing
energy, some variation was observed. When delamina- impacted to non-impacted samples can be seen in Table
tion occurred to the bottom facesheet, the maximum 7. Some deviation occurred when considering the non-
compressive strength was greatly reduced. During test- impacted samples. The deviation between the different

Table 7
Compression testing data
Sample type Impacted
Non-impacted Compression strength (MPa) % Decrease
Compression strength (MPa) 35–45 J (Average) Non-impacted-impacted
CF 15.1 6.5 57
1K 13.2 6.0 55
2K 13.7 6.3 54
3K 12.4 7.0 44
4K 14.8 7.7 48
1H 13.1 8.3 37
2H 13.9 8.0 42
3H 13.6 7.9 42
4H 15.0 6.7 55
402 J. Gustin et al. / Composite Structures 69 (2005) 396–406

Table 8 data helped characterize the loss in stiffness resulting


Elastic moduli for the different sample types from the addition of Kevlar or hybrid to the facesheet.
Facesheet E1 (GPa) E2 (GPa) The following conclusions were drawn from this study:
Carbon fiber 52 52
Kevlar 31 31 1. The addition of Kevlar to the facesheet improved the
Hybrid (Kevlar E2 direction) 45 26 maximum absorbed energy and average maximum
1K 47.4 47.4
2K 42.5 42.5
impact force of the 1K–4K samples by approximately
3K 37 37 10% compared to the CF samples.
4K 31 31 2. The addition of hybrid to the facesheet improved the
1H 50.25 45.5 maximum absorbed energy of the 1K–4K samples by
2H 48.5 39 approximately 5% and the average maximum impact
3H 46.75 32.5
4H 45 26
force by approximately 14% compared to the CF
samples.
3. The addition of Kevlar or hybrid minimized the
reduction in compression after impact strength when
sample types can likely be attributed to irregularities be-
considering non-impacted samples and those that
tween the facesheet/core bond and also the sporadic nat-
experienced complete striker penetration. However,
ure of facesheet crushing/cracking. In addition, when the
the compression strength of the non-impacted sam-
carbon fiber layers were replaced by 2–4 layers of the
ples was the highest for the CF samples.
Kevlar in the facesheet, loading eccentricities might have
4. The elastic moduli, E1 and E2, were reduced when
occurred. Considering the overall compressive strength
Kevlar or hybrid were added to the facesheet. How-
data, the addition of Kevlar or hybrid to the facesheet
ever, the reduction can be minimized to around 9%
did not seem to alter the compressive strength signifi-
by replacing only one layer of carbon fiber with Kev-
cantly. In fact, considering all the data, 1K–4K and
lar or hybrid.
1H–4H, the non-impacted compressive strength aver-
5. The advantages and disadvantages of using 1K sam-
aged less than a 9% drop compared to the CF samples.
ples over CF are:
A noticeable difference between the different sample
Advantage
types was the percent decrease in compressive strength
(a) 12.5% higher average absorbed energy (35–45 J),
when comparing impacted to non-impacted samples.
(b) 11.9% higher average maximum force.
The better impact performance of the Kevlar and hybrid
Disadvantage
samples seemed to lessen the decrease in compressive
(c) 12.7% lower non-impacted compressive strength,
strength when compared to the CF samples.
(d) reduction in stiffness (9% decrease in E1 and E2).
6. The advantages and disadvantages of using 1H sam-
7. Modulus of elasticity ples over CF are:
Advantage
The modulus of elasticity for the carbon fiber, Kev- (a) 4.5% higher average absorbed energy (35–45 J).
lar, and hybrid were determined to characterize how Disadvantage
the addition of Kevlar reduced the tensile stiffness. (b) 13% lower non-impacted compressive strength,
ASTM standard D3039 was followed for determining (c) properties are not orthotropic,
the elastic moduli [25]. Table 8 lists the E1 and E2 values (d) reduction in stiffness (3.3% decrease in E1 and
for the different sample types. The rule of mixtures was 12.5% decrease in E2).
applied to determine how E1 and E2 of the facesheet
changed when layers of carbon fiber were replaced with
Kevlar or hybrid [26]. Acknowledgements

The National Science Foundation, under Grant


8. Conclusion 0082832, and the NASA Space Grant Fellowship Pro-
gram provided funding for this research. Their support
Carbon fiber sandwich composites have relatively low is greatly appreciated.
impact properties. In an attempt to improve upon the im-
pact properties while maintaining the high stiffness, light-
weight nature of the carbon fiber, Kevlar or hybrid were Appendix A
added to the facesheet. The impact and compression after
impact data characterized how adding Kevlar or hybrid 4 layers carbon fiber (CF): Fig. A.1.
to the facesheet improved the sandwich composite per- 3 layers carbon fiber 1 layer Kevlar (1K): Fig. A.2.
formance during and after impact. The elastic moduli 2 layers carbon fiber 2 layers Kevlar (2K): Fig. A.3.
J. Gustin et al. / Composite Structures 69 (2005) 396–406 403

Fig. A.1. Force vs. time response for CF: (a) 5–15 J; (b) 20–45 J.

Fig. A.2. Force vs. time response for 1K: (a) 5–15 J; (b) 20–45 J.

Fig. A.3. Force vs. time response for 2K: (a) 5–15 J; (b) 20–45 J.

3 layers carbon fiber 1 layer Kevlar (3K): Fig. A.4. 2 layers carbon fiber 2 layers hybrid (2H): Fig. A.7.
4 layers Kevlar (4K): Fig. A.5. 1 layer carbon fiber 3 layers hybrid (3H): Fig. A.8.
3 layers carbon fiber 1 layer hybrid (1H): Fig. A.6. 4 layer hybrid (4H): Fig. A.9.
404 J. Gustin et al. / Composite Structures 69 (2005) 396–406

Fig. A.4. Force vs. time response for 3K: (a) 5–15 J; (b) 20–45 J.

Fig. A.5. Force vs. time response for 4K: (a) 5–15 J; (b) 20–45 J.

Fig. A.6. Force vs. time response for 1H: (a) 5–15 J; (b) 20–45 J.
J. Gustin et al. / Composite Structures 69 (2005) 396–406 405

Fig. A.7. Force vs. time response for 2H: (a) 5–15 J; (b) 20–45 J.

Fig. A.8. Force vs. time response for 3H: (a) 5–15 J; (b) 20–45 J.

Fig. A.9. Force vs. time response for 4H: (a) 5–15 J; (b) 20–45 J.

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